CN108865395A - A kind of microemulsified rust preventive cutting fluid and preparation method thereof - Google Patents

A kind of microemulsified rust preventive cutting fluid and preparation method thereof Download PDF

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Publication number
CN108865395A
CN108865395A CN201811075799.5A CN201811075799A CN108865395A CN 108865395 A CN108865395 A CN 108865395A CN 201811075799 A CN201811075799 A CN 201811075799A CN 108865395 A CN108865395 A CN 108865395A
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CN
China
Prior art keywords
parts
cutting fluid
microemulsified
rust preventive
preventive cutting
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Pending
Application number
CN201811075799.5A
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Chinese (zh)
Inventor
秦波
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Jiangsu Baoji Numerical Control Technology Co Ltd
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Jiangsu Baoji Numerical Control Technology Co Ltd
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Priority to CN201811075799.5A priority Critical patent/CN108865395A/en
Publication of CN108865395A publication Critical patent/CN108865395A/en
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C10M173/02—Lubricating compositions containing more than 10% water not containing mineral or fatty oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/12—Glass
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/026—Butene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/08—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
    • C10M2209/084—Acrylate; Methacrylate
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/106—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing four carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/108—Polyethers, i.e. containing di- or higher polyoxyalkylene groups etherified
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/086—Imides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/046—Overbasedsulfonic acid salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/24—Emulsion properties
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling

Abstract

A kind of microemulsified rust preventive cutting fluid and preparation method thereof, is related to technical field of mechanical processing, is grouped as by each group of following mass fraction：12-25 parts of polytetrahydrofuran diol, 5-12 parts of water soluble polymer lotion, 2-4 parts of triethanolamine, 1-2 parts of polyisobutene, 2-5 parts of mono alkenyl succimide, 1-3 parts of glass fibre, 45-85 parts of deionized water, 1-3 parts of detersive, 2-7 parts of emulsifier.Microemulsified rust preventive cutting fluid provided by the invention, manufacture craft is simple and fast, can be very convenient according to operation place active configuration；And the cutting fluid mobility is moderate, has excellent cooling and lubricating action, is a kind of ideal machining of metals liquid.

Description

A kind of microemulsified rust preventive cutting fluid and preparation method thereof
Technical field
The invention belongs to mechanical chemical industry field, in particular to micro-emulsion cutting fluid used in a kind of process of metal working.
Background technique
Cutting fluid is a kind of in metal cutting, mill process, for cooling down and lubricating the work of cutter and workpiece Industry liquid, cutting fluid from a variety of super strong functional auxiliary agents through science it is compound with form, be provided simultaneously with good cooling performance, profit Slip energy, rustless property, oil removing cleaning function, anti-corrosion function, easily dilutable feature.
Cutting fluid is different from traditional tradition soap base emulsion, and there is no easily smelly, the winter difficult dilutions, antirust of tradition soap base emulsion summer The problems such as effect is poor, thus save and utilize more convenient.
Intermetallic composite coating cutting fluid extremely takes a fancy to its cooling performance and greasy property, and antirust, anti-corrosion and oil removing are also very It is important, but cooling and lubrication is the basic of cutting fluid.Process of metal working, the mobility of cutting fluid exactly react cooling and profit The key of sliding effect.Existing cutting fluid can be divided into two classes：Aqueous cutting fluid and non-aqueous cutting fluid, aqueous cutting fluid Mobility is preferable, but viscosity is lower, is unfavorable for taking away the clast in process；And the non-aqueous cutting fluid in part, viscosity are suitable In, but poor fluidity, cooling and lubricant effect is bad, therefore, how to further provide for cooling in process of metal working and Lubricating action is the technical problem urgently to be resolved that cutting fluid faces.
Summary of the invention
Present invention solves the technical problem that：In view of the above deficiencies, it overcomes the deficiencies of existing technologies, the purpose of the present invention is mention For a kind of rust preventive cutting fluid and preparation method thereof with microemulsifiable energy.
Technical solution of the present invention：
A kind of microemulsified rust preventive cutting fluid is grouped as by each group of following mass fraction：
12-25 parts of polytetrahydrofuran diol, 5-12 parts of water soluble polymer lotion, 2-4 parts of triethanolamine, 1-2 parts of polyisobutene, 2-5 parts of mono alkenyl succimide, 1-3 parts of glass fibre, 45-85 parts of deionized water, 1-3 parts of detersive, 2-7 parts of emulsifier.
Preferably, the water soluble polymer lotion is acrylic emulsion or polyaminoester emulsion.
Preferably, the detersive is that middle base number calcium mahogany sulfonate, high base number calcium mahogany sulfonate or middle base number synthesize sulphur Sour calcium.
Preferably, the emulsifier is sulfonated oil, sorbitan monooleate or fatty alcohol polyoxyethylene ether.
More preferably, the emulsifier is sorbitan monooleate.
A kind of preparation method of microemulsified rust preventive cutting fluid, includes the following steps：
（1）It weighs：Each component is weighed according to the mass fraction of each component；
（2）Mixing：Each component is sequentially placed into blender and is stirred；
（3）Vacuum is stood：The mixed liquor being stirred is put into container, is placed under vacuum room temperature environment and stands 8-15h；
（4）Encapsulation:After vacuum is stood, packaging is carried out to get microemulsified rust preventive cutting fluid is arrived.
Beneficial effect：Microemulsified rust preventive cutting fluid provided by the invention, manufacture craft is simple and fast, can be according to operation place Active configuration, it is very convenient；And the cutting fluid mobility is moderate, has excellent cooling and lubricating action, be it is a kind of very Ideal machining of metals liquid.
Specific embodiment
For a further understanding of the present invention, the preferred embodiment of the invention is described below with reference to embodiment, still It should be appreciated that these descriptions are only further explanation the features and advantages of the present invention, rather than to the claims in the present invention Limitation.
Embodiment 1：
A kind of microemulsified rust preventive cutting fluid is grouped as by each group of following mass fraction：
25 parts of polytetrahydrofuran diol, 12 parts of acrylic emulsion, 4 parts of triethanolamine, 2 parts of polyisobutene, mono alkenyl succinyl are sub- 5 parts of amine, 3 parts of glass fibre, 85 parts of deionized water, 3 parts of middle base number calcium mahogany sulfonate, 2-7 parts of fatty alcohol polyoxyethylene ether.
A kind of preparation method of microemulsified rust preventive cutting fluid, includes the following steps：
（1）It weighs：Each component is weighed according to the mass fraction of each component；
（2）Mixing：Each component is sequentially placed into blender and is stirred；
（3）Vacuum is stood：The mixed liquor being stirred is put into container, is placed under vacuum room temperature environment and stands 15h；
（4）Encapsulation:After vacuum is stood, packaging is carried out to get above-mentioned microemulsified rust preventive cutting fluid is arrived.
The microemulsified rust preventive cutting fluid obtained according to method made above is homogeneous liquid, no layering and precipitating phenomenon, measurement Thermal coefficient be： 0.58 w/（m*k）.
Embodiment 2：
A kind of microemulsified rust preventive cutting fluid is grouped as by each group of following mass fraction：
12 parts of polytetrahydrofuran diol, 5 parts of acrylic emulsion, 2-4 parts of triethanolamine, 1-2 parts of polyisobutene, mono alkenyl succinyl 2 parts of imines, 1 part of glass fibre, 45 parts of deionized water, 1 part of high base number calcium mahogany sulfonate, 2 parts of fatty alcohol polyoxyethylene ether.
A kind of preparation method of microemulsified rust preventive cutting fluid, includes the following steps：
（1）It weighs：Each component is weighed according to the mass fraction of each component；
（2）Mixing：Each component is sequentially placed into blender and is stirred；
（3）Vacuum is stood：The mixed liquor being stirred is put into container, quiet 15h under vacuum room temperature environment is placed on；
（4）Encapsulation:After vacuum is stood, packaging is carried out to get above-mentioned microemulsified rust preventive cutting fluid is arrived
The microemulsified rust preventive cutting fluid obtained according to method made above, for homogeneous liquid, no layering and precipitating phenomenon, measurement is led Hot coefficient is： 0.57 w/（m*k）.
Embodiment 3：
A kind of microemulsified rust preventive cutting fluid is grouped as by each group of following mass fraction：
18 parts of polytetrahydrofuran diol, 11 parts of polyurethane, 3 parts of triethanolamine, 1 part of polyisobutene, mono alkenyl succimide 3 Part, 2 parts of glass fibre, 55 parts of deionized water, 3 parts of high base number calcium mahogany sulfonate, 4 parts of sorbitan monooleate.
A kind of preparation method of microemulsified rust preventive cutting fluid, includes the following steps：
（1）It weighs：Each component is weighed according to the mass fraction of each component；
（2）Mixing：Each component is sequentially placed into blender and is stirred；
（3）Vacuum is stood：The mixed liquor being stirred is put into container, is placed under vacuum room temperature environment and stands 15h；
（4）Encapsulation:After vacuum is stood, packaging is carried out to get above-mentioned microemulsified rust preventive cutting fluid is arrived.
The microemulsified rust preventive cutting fluid obtained according to method made above is homogeneous liquid, no layering and precipitating phenomenon, measurement Thermal coefficient be： 0.59 w/（m*k）.
The foregoing description of the disclosed embodiments enables those skilled in the art to implement or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, as defined herein General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, of the invention It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one The widest scope of cause.

Claims (6)

1. a kind of microemulsified rust preventive cutting fluid, which is characterized in that be grouped as by each group of following mass fraction：Polytetrahydrofuran Glycol, 12-25 parts；Water soluble polymer lotion, 5-12 parts；Triethanolamine, 2-4 parts；Polyisobutene, 1-2 parts；Mono alkenyl fourth two Acid imide, 2-5 parts；Glass fibre, 1-3 parts；Deionized water, 45-85 parts；Detersive, 1-3 parts；Emulsifier, 2-7 parts.
2. microemulsified rust preventive cutting fluid according to claim 1, it is characterised in that：The water soluble polymer lotion is third Olefin(e) acid lotion or polyaminoester emulsion.
3. microemulsified rust preventive cutting fluid according to claim 1, it is characterised in that：The detersive is middle base number petroleum sulphur Sour calcium, high base number calcium mahogany sulfonate or middle calcium alkylbenzensulfonates.
4. microemulsified rust preventive cutting fluid according to claim 1, it is characterised in that：The emulsifier is sulfonated oil, sorb Sugar alcohol acid anhydride monoleate or fatty alcohol polyoxyethylene ether.
5. microemulsified rust preventive cutting fluid according to claim 4, it is characterised in that：The emulsifier is sorbitan list Oleate.
6. a kind of method for preparing microemulsified rust preventive cutting fluid described in claim 1, which is characterized in that include the following steps：
（1）It weighs：Each component is weighed according to the mass fraction of each component；
（2）Mixing：Each component is sequentially placed into blender and is stirred；
（3）Vacuum is stood：The mixed liquor being stirred is put into container, is placed under vacuum room temperature environment and stands 8-15h；
（4）Encapsulation:After vacuum is stood, packaging is carried out to get microemulsified rust preventive cutting fluid is arrived.
CN201811075799.5A 2018-09-14 2018-09-14 A kind of microemulsified rust preventive cutting fluid and preparation method thereof Pending CN108865395A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811075799.5A CN108865395A (en) 2018-09-14 2018-09-14 A kind of microemulsified rust preventive cutting fluid and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811075799.5A CN108865395A (en) 2018-09-14 2018-09-14 A kind of microemulsified rust preventive cutting fluid and preparation method thereof

Publications (1)

Publication Number Publication Date
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Country Link
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114682998A (en) * 2022-03-18 2022-07-01 无锡中氏机械有限公司 Production process of flyer presser aluminum product

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114682998A (en) * 2022-03-18 2022-07-01 无锡中氏机械有限公司 Production process of flyer presser aluminum product
CN114682998B (en) * 2022-03-18 2024-04-05 无锡中氏机械有限公司 Production process of presser finger aluminum product

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