CN108823015B - Production method of wheat-flavor distilled liquor and wheat-flavor distilled liquor obtained by production method - Google Patents

Production method of wheat-flavor distilled liquor and wheat-flavor distilled liquor obtained by production method Download PDF

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Publication number
CN108823015B
CN108823015B CN201810629917.6A CN201810629917A CN108823015B CN 108823015 B CN108823015 B CN 108823015B CN 201810629917 A CN201810629917 A CN 201810629917A CN 108823015 B CN108823015 B CN 108823015B
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malt
liquor
distilled liquor
beer
vol
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CN108823015A (en
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董建军
尹花
邢磊
李华
常宗明
刘晓琳
钱中华
黄树丽
胡孝丛
陈华磊
王剑锋
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Tsingtao Brewery Co Ltd
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Tsingtao Brewery Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12CBEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C12/00Processes specially adapted for making special kinds of beer
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12CBEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C11/00Fermentation processes for beer
    • C12C11/11Post fermentation treatments, e.g. carbonation, or concentration

Abstract

The invention provides a production method of wheat-flavor distilled liquor and the obtained wheat-flavor distilled liquor, belongs to the technical field of brewing of alcoholic beverages, and can solve the current situation that no wheat-flavor distilled liquor exists in the market at present. The technical scheme comprises the steps of preparation of beer fermentation liquor, preparation of pretreated beer distilled liquor, ageing, dilution and blending, extraction of scorched and fragrant malt and the like. The wheat-flavor distilled liquor provided by the invention is different from the existing distilled liquor, not only retains the characteristics of the distilled liquor, but also has the wheat-flavor of scorched-flavor malt, and has the advantages of full mouthfeel, slight sweetness and good drinkability.

Description

Production method of wheat-flavor distilled liquor and wheat-flavor distilled liquor obtained by production method
Technical Field
The invention belongs to the technical field of alcoholic beverage brewing, and particularly relates to a production method of wheat-flavor distilled liquor and the wheat-flavor distilled liquor.
Background
The alcoholic beverage can be divided into fermented alcoholic beverage, distilled alcoholic beverage and blended alcoholic beverage, wherein the distilled alcoholic beverage is prepared from grain, potato, fruit and milk as main raw materials by fermenting, distilling and blending. Distilled liquor is the highest alcohol content in alcoholic beverages, and various distilled liquor products are created around the world due to different weathers, climates, physical and chemical properties, cultures, habits and hobbies, and mainly comprise white spirit, brandy, whisky, vodka, rum, gin, milk liquor (distilled type) and other distilled liquors.
The burnt malt is widely used in beer, especially in dark beer, and is mainly used for improving the fullness of the beer, strengthening the aroma of the malt and improving the chroma of the beer. The first world of China's beer production and sales and the first country of China's distilled liquor production and sales, how to combine distilled liquor with scorched fragrant malt, and research and development of novel distilled liquor with fragrant malt and wheat flavor has important significance for expanding the current product types of distilled liquor.
Disclosure of Invention
The invention provides a production method of wheat-flavor distilled liquor and the obtained wheat-flavor distilled liquor, which is different from the existing distilled liquor, not only keeps the characteristics of distilled liquor, but also has the characteristics of clearness and sweetness, has the characteristics of hops, has slightly bitter and fresh hop flavor, and has good drinkability.
In order to achieve the aim, the invention provides a production method of wheat-flavor distilled liquor, which comprises the following steps:
selecting malt and water as main raw materials, mixing the raw materials at a ratio of 1:3-1:4, carrying out protein resting on the malt at 50-55 ℃, and then saccharifying at 62-72 ℃;
after saccharification, filtering the saccharified mash at 73 +/-1 ℃ to obtain clear wort, boiling, adding hops or hop products in the boiling process, carrying out rotary precipitation after boiling, adding or not adding hops or hop products in the rotary precipitation process, then cooling to 8-10 ℃, simultaneously oxygenating and inoculating upper yeast or lower yeast for fermentation, and adding or not adding hops or hop products in the fermentation process to obtain beer fermentation liquor;
feeding beer fermentation liquor into a tower-type or kettle-type distiller to carry out primary atmospheric distillation at 78-95 ℃ to obtain a distilled crude product with the alcoholic strength of 20-40 vol%, then feeding the distilled crude product into the tower-type or kettle-type distiller to carry out secondary atmospheric distillation at 78-95 ℃, removing the head and tail of the distilled liquor, only collecting the body part, and obtaining the pretreated beer distilled liquor with the alcoholic strength of more than or equal to 60 vol%;
ageing the pretreated beer distilled liquor in a tank for more than 2 months, and then diluting and blending the pretreated beer distilled liquor by using purified water to obtain beer distilled liquor with different alcoholic contents;
soaking the burnt malt in beer distilled liquor with different alcoholic contents according to the addition amount of 1-5%, and filtering after 24-36 h to obtain the malt distilled liquor with different alcoholic contents.
Preferably, malt and water are selected as main raw materials, rice, corn or syrup is selected as auxiliary materials, and the raw materials and the water are mixed according to the material-water ratio of 1:3-1: 4; wherein, when rice or corn is used as adjuvant, the adjuvant is pulverized, mixed with slurry, gelatinized at 80-90 deg.C, and saccharified with malt after protein stop.
Preferably, inoculating the above yeast with oxygen to obtain Ale beer, fermenting at 16-20 deg.C for 15-25 days; inoculating oxygen to the yeast to obtain Lager beer, fermenting at 8-13 deg.C for 15-25 days.
Preferably, the Ale beer has a wort concentration of 10.9-14.5 ° P, an alcoholic strength of 4.5-7.0% vol, and a bitter taste of 6-60 EBC; the concentration of the original wort of the Lager beer is 10-21P degrees, the alcoholic strength is 4-10 vol percent, and the bitter taste quality is 10-30 EBC.
Preferably, the alcohol content of the pre-treated beer distilled liquor is more than or equal to 70% vol.
Preferably, the foreshot accounts for 1-10% of the total volume, the feints accounts for 5-10% of the total volume, and the wine body with the alcoholic strength of more than or equal to 60% vol accounts for 80-94% of the total volume.
Preferably, the hop or hop product used in boiling, whirlpool precipitation, fermentation, ageing is bitter, scented or combination bitter and scented, selected from one or more of Qingdao Dahua, Zaoyanghua, Hallertauer trade, Tettanger, Hersbrucker, Herkules, Cascade, Citra, Saaz, Herkules, Magnum, EK Golding, Perle, Tettnanger, Nugget, Spalter Select and Northern Brewer.
Preferably, the malt having burnt aroma is at least one selected from the group consisting of pilsner malt having burnt aroma, pale malt having burnt aroma and amber malt having burnt aroma.
The invention also provides the malt distilled liquor produced by the production method of the malt distilled liquor in any technical scheme.
Preferably, the alcohol content of the malt distilled liquor is 10-60% vol, preferably 20-50% vol, and more preferably 40-50% vol.
Compared with the prior art, the invention has the advantages and positive effects that:
the wheat-flavor distilled liquor product provided by the invention is different from the existing distilled liquor, the current situation that the wheat-flavor distilled liquor is not available at present is solved, the obtained wheat-flavor distilled liquor product not only keeps the characteristics of the distilled liquor, is fresh and cool, but also has the wheat-flavor of scorched-flavor malt, and is full and slightly sweet in taste.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The embodiment of the invention provides a production method of beer distilled liquor, which comprises the following steps:
s1: selecting malt and water as main raw materials, mixing the raw materials at a ratio of 1:3-1:4, carrying out protein resting on the malt at 50-55 ℃, and then saccharifying at 62-72 ℃.
In the step, main raw materials can be independently saccharified after being treated, and rice, corn or syrup can also be used as auxiliary materials for saccharification. Wherein, when rice or corn is used as adjuvant, the adjuvant is pulverized, and then mixed with syrup to gelatinize at 80-90 deg.C, and then saccharified with malt after protein resting. The saccharification process can be adjusted by a person skilled in the art according to the actual production situation.
S2: after saccharification, the saccharified mash is filtered at 73 +/-1 ℃ to obtain clear wort, the clear wort is boiled, hops or hop products are added in the boiling process, rotary precipitation is carried out after boiling, the hops or the hop products are added or not added in the rotary precipitation process, then the clear wort is cooled to 8-10 ℃, simultaneously, top yeast or bottom yeast is inoculated in an oxygenated state for fermentation, and the hops or the hop products are added or not added in the fermentation process to obtain beer fermentation liquor. In the above process, the boiling time is about 1 hour, and a small amount of syrup may be added after the boiling to adjust.
S3: the beer fermentation liquor is sent into a tower type or kettle type distiller to be distilled at normal pressure for the first time at 78-95 ℃ to obtain a distilled crude product with the alcoholic strength of 20-40 vol%, then the distilled crude product is sent into the tower type or kettle type distiller to be distilled at normal pressure for the second time at 78-95 ℃, the distilled foreshot and the distilled tail are removed, only the wine body part is collected, and the pretreated beer distilled wine with the alcoholic strength of more than or equal to 60 vol% is obtained.
In the step, on the basis of obtaining different types of beer fermentation liquids, different distillation equipment is used, so that the pretreated beer distilled liquor products with different flavors can be obtained. After the secondary atmospheric distillation process is optimized, the pretreated beer distilled liquor with high alcoholic strength can be obtained, the aim of effectively reducing the content of aldehydes and higher alcohol substances can be achieved, and the phenomenon of top-end after drinking is avoided. And compared with vacuum low-pressure distillation, atmospheric distillation can make the flavor substance content richer and the alcohol ester content higher.
S4: ageing the pre-treated beer distilled liquor in a tank for more than 2 months, adding or not adding hops or hops products in the ageing process, and then diluting and blending the pre-treated beer distilled liquor by using purified water to obtain the beer distilled liquor with different alcoholic contents.
In the step, the problem of pungency of the new beer of the distilled beer can be effectively solved through aging, and the beer of the distilled beer has a cool and tasty mouthfeel and good drinkability.
S5: soaking the burnt malt in beer distilled liquor with different alcoholic contents according to the addition amount of 1-5%, and filtering after 24-36 h to obtain the malt distilled liquor with different alcoholic contents.
In the step, the active ingredients in the burnt malt can be extracted by soaking the burnt malt, and finally the wheat-flavor distilled liquor product with the burnt malt and wheat flavor is obtained.
In a preferred embodiment, the above yeast is inoculated in oxygen to obtain Ale beer, the fermentation temperature is 16-20 ℃, and the fermentation time is 15-25 days; inoculating oxygen to the yeast to obtain Lager beer, fermenting at 8-13 deg.C for 15-25 days. In this example, the fermentation temperatures and times when different fermentation yeasts were added were listed, which was beneficial to the overall process control. It should be noted that the examples are given only for the fermentation temperature and time of the beer, and those skilled in the art can make appropriate adjustments within the above range according to actual conditions.
In a preferred embodiment, the Ale beer has a wort concentration of 10.9-14.5 ° P, an alcoholic strength of 4.5-7.0% vol, and a bittering quality of 6-60 EBC; the concentration of the original wort of the Lager beer is 10-21P degrees, the alcoholic strength is 4-10 vol percent, and the bitter taste quality is 10-30 EBC. In a further alternative embodiment, the 20 ° P Lager beer is preferably used because it is a high gravity beer, which is advantageous for increasing the alcohol content of the distilled base liquor and lowering the distillation boiling point, thereby reducing the content of high boiling point substances such as higher alcohols in the product and increasing the alcohol content of the product to 70% vol or more.
In a preferred embodiment, the pre-treated beer still has an alcohol content of 70% vol or more. When the alcoholic strength of the pretreated beer distilled liquor is improved to more than 70, the impurities in the liquor can be effectively reduced, and the liquor is cleaner.
In a preferred embodiment, the wine head accounts for 1% -10% of the total volume, the wine tail accounts for 5% -10% of the total volume, and the wine body with the alcoholic strength of more than or equal to 60% vol accounts for 80% -94% of the total volume. The distillation process adopted by the embodiment can keep the faint scent of the beer to the maximum extent, and simultaneously can keep the wine body with absolute advantage volume, thereby being beneficial to being used in large-scale industrial production.
In a preferred embodiment, the hop or hop preparation used in boiling, whirlpool, fermentation, ageing is bitter, scented or combination bitter and scented, selected from one or more of the group consisting of Qingdao, Zaoyanghua, Hallertauer trade, Tettanger, Hersbrucker, Herkules, Cascade, Citra, Saaz, Herkules, Magnum, EKGolding, Perle, Tettnanger, Nugget, Spalter Select and Northern Brewer. In a preferred embodiment, the burnt malt is selected from at least one of Pearson burnt malt (color number 3-5EBC), pale burnt malt (color number 25-30EBC) and amber burnt malt (color number 75-150 EBC). It is understood that the choice of the hop or hop product and the scorched and fragrant malt is not limited to those listed in the above examples, and may be other kinds that are reasonably and alternatively used and known to those skilled in the art, but it is proved by many experiments that the hop or hop product and the scorched and fragrant malt provided in the above examples are more favorable for producing the wheat-fragrant distilled liquor having both the characteristics of distilled liquor and the scorched and fragrant malt flavor, full mouthfeel and slightly sweet.
The embodiment of the invention also provides the wheat-flavor distilled liquor produced by the production method of the wheat-flavor distilled liquor. The wheat-flavor distilled liquor provided by the invention is different from the existing distilled liquor, not only keeps the characteristics of the distilled liquor, is cold and sweet, but also has the wheat-flavor of scorched-flavor malt, and has full mouthfeel, slight sweetness and good drinkability.
In a preferred embodiment, the alcohol content of the wheat-flavored distilled liquor is 10-60% vol, preferably 20-50% vol, and more preferably 40-50% vol. In the embodiment, a series of malt distilled liquors with different alcoholic strength can be obtained by diluting and blending the beer distilled liquor with purified water based on pretreatment and then immersing the beer distilled liquor into the burnt malt, and for example, the malt distilled liquor can comprise a plurality of types of malt distilled liquor such as 10% vol, 14% vol, 28% vol, 38% vol, 40% vol, 43% vol, 46% vol, 52% vol, 53% vol and 60% vol.
In order to more clearly and specifically describe the preparation method of the malt distilled liquor and the malt distilled liquor obtained by the preparation method, the following embodiments are provided.
Example 1
Taking barley malt and water as main raw materials, and crushing → saccharifying → filtering → boiling (hops or hop extract is required to be added) → rotary precipitation → cooling → oxygenating → adding subsurface yeast → fermenting → obtaining the 20 ℃ P Lager beer.
Distilling 11 ° P Ale beer twice with a tower distiller to obtain pretreated beer distilled liquor product with alcoholicity of 86% vol, aging for more than 2 months, diluting to 20% vol, soaking un-pulverized burnt malt (Carahil) in beer distilled liquor for 24 hr at an amount of 1%, and filtering to obtain malt distilled liquor product
Example 2
Distilling 11 ° P Ale beer twice with a tower distiller to obtain pretreated beer distilled liquor product with alcoholicity of 86% vol, aging for more than 2 months, diluting to 50% vol, soaking pulverized burnt malt (Carahil) in beer distilled liquor for 24 hr at 2%, and filtering to obtain malt distilled liquor product
Example 3
Distilling 20 ° P Lager beer twice with a tower distiller to obtain pretreated beer distilled liquor product with alcoholicity of 87% vol, aging for more than 2 months, diluting to 50% vol, soaking pulverized burnt malt (Carahil) in beer distilled liquor for 24 hr at 5%, and filtering to obtain malt-flavored distilled liquor product
Example 4
Distilling 20 ° P Lager beer twice with a tower distiller to obtain pretreated beer distilled liquor product with alcoholicity of 87% vol, aging for more than 2 months, diluting to 40% vol, soaking pulverized burnt malt (Caraamber) in beer distilled liquor for 24 hr at 5%, and filtering to obtain malt-flavored distilled liquor product
Detection of wheat-flavor substance in wheat-flavor distilled liquor
Table 1 examples 1-4 results of testing wheat-scented materials
Examples 2-AP(μg/L)
Example 1 2.04
Example 2 6.79
Example 3 7.78
Example 4 59.76
As is clear from the data in Table 1, the malt distilled liquor provided in the examples of the present invention contains typical malt substances.
Evaluation of flavor
The results of the flavor evaluation of the wheat-flavored distilled liquors obtained in examples 1 to 4 are shown in Table 2.
TABLE 2 evaluation results of flavor of the malt distilled liquor products obtained in examples 1 to 4
Figure BDA0001700232110000071
As can be seen from the results in Table 2, the malt-flavored distilled liquor provided by the invention is different from the existing distilled liquor, not only retains the characteristics of the distilled liquor, but also has the malt-flavored flavor of scorched malt, is full in taste, slightly sweet and good in drinkability, and effectively expands the selectable varieties of the existing distilled liquor.

Claims (10)

1. The production method of the wheat-flavor distilled liquor is characterized by comprising the following steps of:
selecting malt and water as main raw materials, mixing the raw materials at a ratio of 1:3-1:4, carrying out protein resting on the malt at 50-55 ℃, and then saccharifying at 62-72 ℃;
after saccharification, filtering the saccharified mash at 73 +/-1 ℃ to obtain clear wort, boiling, adding hops or hop products in the boiling process, carrying out rotary precipitation after boiling, adding or not adding hops or hop products in the rotary precipitation process, then cooling to 8-10 ℃, simultaneously inoculating subsurface yeast with oxygenation to obtain Lager beer, and adding or not adding hops or hop products in the fermentation process to obtain beer fermentation liquor, wherein the concentration of the original wort of the Lager beer is 10-21 DEG P, the alcoholic strength is 4-10 vol% and the bitter taste quality is 10-30 EBC;
feeding beer fermentation liquor into a tower-type or kettle-type distiller to carry out primary atmospheric distillation at 78-95 ℃ to obtain a distilled crude product with the alcoholic strength of 20-40 vol%, then feeding the distilled crude product into the tower-type or kettle-type distiller to carry out secondary atmospheric distillation at 78-95 ℃, removing the head and the tail of distilled liquor, and only collecting the body part to obtain the pretreated beer distilled liquor with the alcoholic strength of more than or equal to 60 vol%, wherein the head accounts for 1-10% of the total volume, the tail accounts for 5-10% of the total volume, and the body with the alcoholic strength of more than or equal to 60 vol accounts for 80-94% of the total volume;
ageing the pretreated beer distilled liquor in a tank for more than 2 months, and then diluting and blending the pretreated beer distilled liquor by using purified water to obtain beer distilled liquor with different alcoholic contents;
soaking the burnt malt in beer distilled liquor with different alcoholic contents according to the addition amount of 1-5%, and filtering after 24-36 h to obtain the malt distilled liquor with different alcoholic contents.
2. The production method according to claim 1, characterized in that malt and water are selected as main raw materials, rice, corn or syrup is selected as auxiliary materials, and the raw materials and the water are mixed according to a material-to-water ratio of 1:3-1: 4; wherein, when rice or corn is used as adjuvant, the adjuvant is pulverized, mixed with slurry, gelatinized at 80-90 deg.C, and saccharified with malt after protein stop.
3. The method according to claim 1, wherein the Lager beer is obtained by inoculating the subsurface yeast with oxygen at a fermentation temperature of 8-13 ℃ for 15-25 days.
4. The method of claim 1, wherein the alcohol content of the pre-treated beer distilled liquor is not less than 70% vol.
5. The method of claim 1, wherein the hop or hop preparation used in boiling, whirlpool precipitation, fermentation, aging is bitter, savoury or combination bitter and savoury, and is selected from one or more of the group consisting of Qingdao flower, Zanthoxylum, Hallertauer trade, Tettanger, Hersbrucker, Herkules, Cascade, Citra, Saaz, Herkules, Magnum, EK gold, Perle, Tettnanger, Nugget, Spalter Select and Northern Brewer.
6. The production method according to claim 1, wherein the malt having burnt aroma is selected from at least one of pilsner malt having burnt aroma, pale malt having burnt aroma, and amber malt having burnt aroma.
7. A malt liquor produced by the method of any one of claims 1 to 6.
8. The malt liquor according to claim 7, wherein the malt liquor has an alcohol content of 10 to 60 vol%.
9. The malt liquor according to claim 8, wherein the malt liquor has an alcohol content of 20 to 50% vol.
10. The malt liquor according to claim 9, wherein the malt liquor has an alcohol content of 40 to 50% vol.
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