CN108822578A - A kind of disperse brilliant blue dye mixture - Google Patents
A kind of disperse brilliant blue dye mixture Download PDFInfo
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- CN108822578A CN108822578A CN201810527800.7A CN201810527800A CN108822578A CN 108822578 A CN108822578 A CN 108822578A CN 201810527800 A CN201810527800 A CN 201810527800A CN 108822578 A CN108822578 A CN 108822578A
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- component
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- brilliant blue
- blue dye
- dye mixture
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0046—Mixtures of two or more azo dyes
- C09B67/0051—Mixtures of two or more azo dyes mixture of two or more monoazo dyes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0079—Azoic dyestuff preparations
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of disperse brilliant blue dye mixtures, and based on mass percentage, which mainly includes following component：The sodium lignin sulfonate of 10~65% component A, 1~20% component B, 0.1~60% component C, 0.5~35% component D, 0.5~40% component E, 0~13% component F, 0~16% component G, 20~75% Dispersant MF and/or dispersing agent NNO and 0~5%.A kind of disperse brilliant blue dye mixture of the present invention, bright in color light, equalization is good, has good water-fastness, friction, fast light and sublimation reliability, the dyeing demand suitable for various fabrics.
Description
Technical field
The present invention relates to technical field of disperse dyes, more particularly, to a kind of disperse brilliant blue dye mixture.
Background technique
As worldwide the increase of yield and kind increase synthetic fibers, the dosage of disperse dyes increases year by year
Greatly.In existing disclosed dyestuff data and production practices, blue dyes dosage is only second to black dyes dosage, wherein cobalt blue
Disperse dyes account for 40% or so of blue based dye again.The disperse brilliant blue dyestuff items application performance supplied currently on the market is inadequate
Ideal and higher cost, can't meet all kinds of dyeing demands well.Therefore, it is gorgeous to research and develop more excellent performance of dispersion
Blue dyes is an especially important project.
Summary of the invention
The present invention provides a kind of disperse brilliant blue dye mixture to solve the deficiencies in the prior art, bright in color light,
Metachromia is good, has good water-fastness, friction, fast light and sublimation reliability, the dyeing demand suitable for various fabrics.
To achieve the above object, the present invention uses following technical scheme：
A kind of disperse brilliant blue dye mixture, based on mass percentage, which mainly includes
Following component：Such as III institute of formula of 10~65% component A as shown in formula I, 1~20% component B as shown in formula II, 0.1~60%
Component C, 0.5~35% component D as shown in formula IV, 0.5~40% component E as shown in formula V, 0~13% such as formula VI shown
Shown in the component G as shown in formula VII of component F, 0~16%, 20~75% Dispersant MF and/or dispersing agent NNO and 0~5%
Sodium lignin sulfonate；
Based on mass percentage, the disperse brilliant blue dye mixture mainly includes following component：36% as shown in formula I
Component A, the 1.5% component B as shown in formula II, the 23% component C as shown in formula III, the 2.8% component D as shown in formula IV,
The 0.8% component E as shown in formula V, the 6.6% component F as shown in formula VI, 2.5% component G, 26.3% as shown in formula VII
Dispersant MF and 0.5% sodium lignin sulfonate.
The Dispersant MF, dispersing agent NNO and sodium lignin sulfonate are as auxiliary agent in disperse brilliant blue dye mixture
Effect is：It is when being sanded that dye crystal is evenly dispersed in water, so that aqueous dye solutions is become a kind of level dyeing body；In high-temperature dyeing
Dyestuff is prevented to agglomerate in application process.
Disperse brilliant blue dyestuff in the present invention can be used to lower section method preparation：Each dye composition and auxiliary agent are matched as defined
After preparing dye composite, it is ground in water and reaches dispersion requirement and then be filtered and dry, preferably done by spraying
It is dry.
The component A, component B, component C, component D, component E, component F, component G can be by well known to those skilled in the art
Mode synthesizes, as according to conventional diazotising, couling process preparation or according to method described in publication or similar side
Method preparation, can also be used commercial product, as component A is purchased from Jiangsu Zhijiang River Chemical Co., Ltd., the limited public affairs of the intercalation native share in Zhejiang
Department etc.；Component B is purchased from Zhejiang Province Runtu intercalated Co., Ltd, Zhejiang mountain valley Science and Technology Co., Ltd., Zhejiang Wan Feng chemical industry have
Limit company etc.；Component C is purchased from Wenzhou Yan Leng Chemical Co., Ltd.；Component D is purchased from Penglai Jiaxin Dye Chemical Co., Ltd.；
Component E is purchased from Penglai Jiaxin Dye Chemical Co., Ltd.；Component F can be for purchased from Zhejiang Province Changzheng Chemical Co., Ltd；Component G can
Purchased from Jiangsu Zhijiang River Chemical Co., Ltd..
Beneficial effects of the present invention：By the existing dispersed blue dye compound of rational proportion and auxiliary agent, a kind of dispersion is obtained
Brilliant blue dye mixture dyes demand in which can meet various fabrics, and fabric coloured light is gorgeous after dyeing, and enhancing is good, water-fastness, resistance to
Every fastness ability such as friction and resistance to distillation is excellent.
Specific embodiment
Below with reference to example, property feature and advantage is further described for the essence of the present invention, but the present invention does not limit to
In listed embodiment.
Embodiment 1~15：
According to data shown in table 1, each dye component and auxiliary agent are added water and stirred uniformly, with grinder grinding distribution, then
It is filtered and is spray-dried to get finished product is arrived.
The dosage of each component of 1 embodiment 1~15 of table
Admixture of disperse dyes made from Example 1~15 is test specimen respectively, carries out the survey of single sample color fastness
It has a try and tests, concrete mode is：0.5g test specimen is respectively taken respectively, is dispersed in 500ml water, is mixed after drawing 20ml with 60ml water
It closes；With acetic acid tune dye bath pH=5, it is warming up to 70 DEG C while 2g polyester cotton cloth is added and dyed, in temperature in 30min by 70 DEG C
130 DEG C are risen to, 30min is kept the temperature, starts to detect the cloth sampling after dyeing when being cooled to 90 DEG C.Using national standard GB/
T3921-1997, GB/T3920-1997, GB/T8427-1998, GB/T5718-1997 test its washing color fastness, resistance to respectively
Colorfastness to rubbing, color fastness to light and sub-limation fastness.
Testing result：As shown in table 2, the sample washing color fastness of embodiment 1~15, colour fastness to rubbing, resistance to photochromic
Fastness and sub-limation fastness accord with or surpass the standard requirements of woven dacron in the market.
2 single sample color fastness testing experiment result of table statistics
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all in spirit of the invention and
Within principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (2)
1. a kind of disperse brilliant blue dye mixture, it is characterised in that：Based on mass percentage, the disperse brilliant blue dye mixture
It mainly include following component：10~65% component A as shown in formula I, 1~20% component B, 0.1~60% as shown in formula II
The component D as shown in formula IV of the component C as shown in formula III, 0.5~35%, 0.5~40% component E as shown in formula V, 0~
The 13% component F as shown in formula VI, 0~16% component G as shown in formula VII, 20~75% Dispersant MF and/or dispersing agent
The sodium lignin sulfonate of NNO and 0~5%；
2. a kind of disperse brilliant blue dye mixture as described in claim 1, it is characterised in that：It is described based on mass percentage
Disperse brilliant blue dye mixture mainly includes following component：The 36% component A as shown in formula I, 1.5% component as shown in formula II
B, the 23% component C as shown in formula III, the 2.8% component D as shown in formula IV, 0.8% component E, 6.6% as shown in formula V is such as
Component F shown in formula VI, 2.5% component G, 26.3% Dispersant MF as shown in formula VII and 0.5% sodium lignin sulfonate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810527800.7A CN108822578B (en) | 2018-05-29 | 2018-05-29 | Disperse brilliant blue dye mixture |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810527800.7A CN108822578B (en) | 2018-05-29 | 2018-05-29 | Disperse brilliant blue dye mixture |
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| Publication Number | Publication Date |
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| CN108822578A true CN108822578A (en) | 2018-11-16 |
| CN108822578B CN108822578B (en) | 2020-01-03 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810527800.7A Active CN108822578B (en) | 2018-05-29 | 2018-05-29 | Disperse brilliant blue dye mixture |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0026596A1 (en) * | 1979-09-26 | 1981-04-08 | Imperial Chemical Industries Plc | Disperse monoazo dyestuffs, their preparation and use for dyeing synthetic textile materials |
| CN101629026A (en) * | 2009-08-27 | 2010-01-20 | 浙江闰土股份有限公司 | Black-blue disperse dye composition |
| CN101705020A (en) * | 2009-11-13 | 2010-05-12 | 烟台澳土复合材料有限公司 | Blue disperse dye mixture |
| CN102127315A (en) * | 2010-12-24 | 2011-07-20 | 上海宜连化工科技有限公司 | Blue disperse dye composition with high light fastness and application thereof |
-
2018
- 2018-05-29 CN CN201810527800.7A patent/CN108822578B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0026596A1 (en) * | 1979-09-26 | 1981-04-08 | Imperial Chemical Industries Plc | Disperse monoazo dyestuffs, their preparation and use for dyeing synthetic textile materials |
| CN101629026A (en) * | 2009-08-27 | 2010-01-20 | 浙江闰土股份有限公司 | Black-blue disperse dye composition |
| CN101705020A (en) * | 2009-11-13 | 2010-05-12 | 烟台澳土复合材料有限公司 | Blue disperse dye mixture |
| CN102127315A (en) * | 2010-12-24 | 2011-07-20 | 上海宜连化工科技有限公司 | Blue disperse dye composition with high light fastness and application thereof |
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| CN108822578B (en) | 2020-01-03 |
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