CN108818807A - A kind of preparation method of resistance to bubble health care wicker plaiting article pillow - Google Patents
A kind of preparation method of resistance to bubble health care wicker plaiting article pillow Download PDFInfo
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- CN108818807A CN108818807A CN201810384563.3A CN201810384563A CN108818807A CN 108818807 A CN108818807 A CN 108818807A CN 201810384563 A CN201810384563 A CN 201810384563A CN 108818807 A CN108818807 A CN 108818807A
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- pillow
- plaiting article
- wicker plaiting
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/02—Processes; Apparatus
-
- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47G—HOUSEHOLD OR TABLE EQUIPMENT
- A47G9/00—Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
- A47G9/10—Pillows
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/005—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process employing compositions comprising microparticles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/007—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process employing compositions comprising nanoparticles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/70—Hydrophobation treatment
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Otolaryngology (AREA)
- Pulmonology (AREA)
- Nanotechnology (AREA)
- Inorganic Chemistry (AREA)
- Bedding Items (AREA)
Abstract
The present invention discloses a kind of preparation method of resistance to bubble health care wicker plaiting article pillow, including following operating procedure：（1）After mixing by hydroxytyrosol, glycerine, succinic acid, aluminium isopropoxide, aluminium chloride, urea are then added thereto, after insulation reaction 16-19 hours, the liquid on the device of falling dereaction upper layer, then lower layer's sticky mass is centrifuged, and is precipitated, and nano-carrier is made；（2）Nano-carrier and negative ion powder are added into ball mill, and calcium stearate is added thereto, functional additive is made in ball-milling treatment；（3）It is lasting to stir after functional additive, sodium phytate, polyethylene glycol 200, water are mixed, wicker plaiting article pillow treatment fluid is made；（4）Wicker plaiting article pillow after knitting forming is added into wicker plaiting article pillow treatment fluid, immersion treatment, drying and processing, finished product.The effect of wicker plaiting article pillow produced by the present invention, water soak resistance can be excellent, and anion is discharged after cleaning will not disappear.
Description
Technical field
The invention belongs to wicker products preparation technical fields, and in particular to a kind of preparation side of resistance to bubble health care wicker plaiting article pillow
Method.
Background technique
Wicker plaiting article is one of folks of china traditional handicraft product, wicker plaiting article pillow because its comfort level is higher, moulding it is simple and unsophisticated and by
The liking of the majority of consumers.With the swift and violent growth of modern economy, the living standard of the mankind is increasingly improved, and is being enjoyed increasingly
While excellent material life, the living environment of the mankind but declines year by year, and anion concentration is also reduced year by year in air.Study table
Bright, anion can be with floating dust, bacterium etc. in air in conjunction with electropositive particle phase, reaching neutralization, and particle
Partial size is smaller, easier to be neutralized, it can be seen that, when the anion in air is more, floating dust and bacterium in air also can
It reduces therewith.In the prior art, have and anion powder is used for fibrous material clothes are made, be used for interior decoration and are used for wood
Material, but when anion powder is used on wood materials, there is the caducous phenomenons of anion powder, especially water resistance
It is poor, cause the health-care efficacy duration of anion product obtained shorter.
Summary of the invention
Anion is applied into the method on wicker products the object of the present invention is to provide a kind of, and then one kind is made to have
The wicker plaiting article pillow of healthcare function.
The present invention is achieved by the following technical solutions.
A kind of preparation method of resistance to bubble health care wicker plaiting article pillow, including following operating procedure：
（1）By weight, after mixing by 4-8 parts of hydroxytyrosols, 36-44 parts of glycerine, 65-70 is then added thereto
Succinic acid, the 29-32 parts of aluminium isopropoxides, 11-15 parts of aluminium chloride, 39-41 parts of urea of part, after being mixed evenly, by mixture
Temperature rise to 210-220 DEG C, insulation reaction 16-19 hours after, be cooled to room temperature, the liquid on the device of falling dereaction upper layer, so
Lower layer's sticky mass is centrifuged afterwards, is precipitated, and after washing of precipitate, drying process, nano-carrier is made；
（2）By nano-carrier and negative ion powder according to 1:The mass ratio of 1.2-1.4 is added into ball mill, and is added receives thereto
After ball-milling treatment 3-4 hours, functional additive is made in the calcium stearate of rice carrier quality 10-15%；
（3）By weight, by 28-33 parts of functional additives, 5-9 parts of sodium phytates, 1-5 parts of polyethylene glycol 200s, 160-200 parts
After water mixing, 30-40min is persistently stirred using the revolving speed of 400-450r/min, wicker plaiting article pillow treatment fluid is made；
（4）Wicker plaiting article pillow after knitting forming is added into wicker plaiting article pillow treatment fluid, after immersion treatment 4-5 hours, takes out, puts
Enter in baking oven, drying and processing, finished product.
Specifically, above-mentioned steps（1）In, after the method for washing of precipitate is cleans twice using deionized water, then use nothing
Water-ethanol cleaning is primary.
Specifically, above-mentioned steps（1）In, the temperature of drying process is 75-80 DEG C.
Specifically, above-mentioned steps（4）In, the temperature of drying and processing is 45-50 DEG C, and the time of drying and processing is 3-4 hours.
From the above technical scheme, it can be seen that the beneficial effects of the invention are as follows：
A kind of preparation method of resistance to bubble health care wicker plaiting article pillow provided by the invention can effectively promote anion product obtained
Water soak resistance energy, anion powder is strong in interiors of products binding force, is not susceptible to the phenomenon that falling off, and can effectively discharge for a long time
Anion, far infrared and anti-microbial property effectively improve the health-care effect of wicker plaiting article pillow, wicker plaiting article especially produced by the present invention
The effect of pillow, water soak resistance can be excellent, and anion is discharged after cleaning will not disappear.Wherein, step（1）Nanometer obtained carries
Body, it is strong to the absorption of anion powder, improve the stability of anion powder, infiltration of the nano-carrier inside wicker products
Property it is stronger, it is strong with the lignin binding force in wicker plaiting article, at the same its can and anion powder generate synergistic effect, increase anion
The quantity of release；Step（3）In, sodium phytate can further promote binding force of the anion powder inside wicker products,
And then effectively improve the water soak resistance energy of wicker plaiting article pillow.
Specific embodiment
Below by specific embodiment, the present invention is described in detail, but the purposes of these illustrative embodiments and
Purpose is only used to enumerate the present invention, not constitutes any type of any restriction to real protection scope of the invention, more non-to incite somebody to action
Protection scope of the present invention is confined to this.
Embodiment 1
A kind of preparation method of resistance to bubble health care wicker plaiting article pillow, including following operating procedure：
（1）By weight, after mixing by 4 parts of hydroxytyrosols, 36 parts of glycerine, 65 parts of amber is then added thereto
The temperature of mixture after being mixed evenly, is risen to 210 DEG C, protected by acid, 29 parts of aluminium isopropoxides, 11 parts of aluminium chloride, 39 parts of urea
After temperature reaction 16 hours, it is cooled to room temperature, the liquid on the device of falling dereaction upper layer, then lower layer's sticky mass is centrifuged,
It is precipitated, after washing of precipitate, drying process, nano-carrier is made；
（2）By nano-carrier and negative ion powder according to 1:1.2 mass ratio is added into ball mill, and nanometer is added thereto and carries
After ball-milling treatment 3 hours, functional additive is made in the calcium stearate of weight 10%；
（3）By weight, it after 28 parts of functional additives, 5 parts of sodium phytates, 1 part of polyethylene glycol 200,160 parts of water being mixed, adopts
30min is persistently stirred with the revolving speed of 400r/min, wicker plaiting article pillow treatment fluid is made；
（4）Wicker plaiting article pillow after knitting forming is added into wicker plaiting article pillow treatment fluid, after immersion treatment 4 hours, takes out, is put into
In baking oven, drying and processing, finished product.
Specifically, above-mentioned steps（1）In, after the method for washing of precipitate is cleans twice using deionized water, then use nothing
Water-ethanol cleaning is primary.
Specifically, above-mentioned steps（1）In, the temperature of drying process is 75 DEG C.
Specifically, above-mentioned steps（4）In, the temperature of drying and processing is 45 DEG C, and the time of drying and processing is 3 hours.
Embodiment 2
A kind of preparation method of resistance to bubble health care wicker plaiting article pillow, including following operating procedure：
（1）By weight, after mixing by 6 parts of hydroxytyrosols, 40 parts of glycerine, 68 parts of amber is then added thereto
The temperature of mixture after being mixed evenly, is risen to 215 DEG C, protected by acid, 31 parts of aluminium isopropoxides, 13 parts of aluminium chloride, 40 parts of urea
After temperature reaction 18 hours, it is cooled to room temperature, the liquid on the device of falling dereaction upper layer, then lower layer's sticky mass is centrifuged,
It is precipitated, after washing of precipitate, drying process, nano-carrier is made；
（2）By nano-carrier and negative ion powder according to 1:1.3 mass ratio is added into ball mill, and nanometer is added thereto and carries
After ball-milling treatment 3.5 hours, functional additive is made in the calcium stearate of weight 13%；
（3）By weight, it after 30 parts of functional additives, 7 parts of sodium phytates, 3 parts of polyethylene glycol 200s, 180 parts of water being mixed, adopts
35min is persistently stirred with the revolving speed of 430r/min, wicker plaiting article pillow treatment fluid is made；
（4）Wicker plaiting article pillow after knitting forming is added into wicker plaiting article pillow treatment fluid, after immersion treatment 4.5 hours, takes out, puts
Enter in baking oven, drying and processing, finished product.
Specifically, above-mentioned steps（1）In, after the method for washing of precipitate is cleans twice using deionized water, then use nothing
Water-ethanol cleaning is primary.
Specifically, above-mentioned steps（1）In, the temperature of drying process is 78 DEG C.
Specifically, above-mentioned steps（4）In, the temperature of drying and processing is 48 DEG C, and the time of drying and processing is 3.5 hours.
Embodiment 3
A kind of preparation method of resistance to bubble health care wicker plaiting article pillow, including following operating procedure：
（1）By weight, after mixing by 8 parts of hydroxytyrosols, 44 parts of glycerine, 70 parts of amber is then added thereto
The temperature of mixture after being mixed evenly, is risen to 220 DEG C, protected by acid, 32 parts of aluminium isopropoxides, 15 parts of aluminium chloride, 41 parts of urea
After temperature reaction 19 hours, it is cooled to room temperature, the liquid on the device of falling dereaction upper layer, then lower layer's sticky mass is centrifuged,
It is precipitated, after washing of precipitate, drying process, nano-carrier is made；
（2）By nano-carrier and negative ion powder according to 1:1.4 mass ratio is added into ball mill, and nanometer is added thereto and carries
After ball-milling treatment 4 hours, functional additive is made in the calcium stearate of weight 15%；
（3）By weight, it after 33 parts of functional additives, 9 parts of sodium phytates, 5 parts of polyethylene glycol 200s, 200 parts of water being mixed, adopts
40min is persistently stirred with the revolving speed of 450r/min, wicker plaiting article pillow treatment fluid is made；
（4）Wicker plaiting article pillow after knitting forming is added into wicker plaiting article pillow treatment fluid, after immersion treatment 5 hours, takes out, is put into
In baking oven, drying and processing, finished product.
Specifically, above-mentioned steps（1）In, after the method for washing of precipitate is cleans twice using deionized water, then use nothing
Water-ethanol cleaning is primary.
Specifically, above-mentioned steps（1）In, the temperature of drying process is 80 DEG C.
Specifically, above-mentioned steps（4）In, the temperature of drying and processing is 50 DEG C, and the time of drying and processing is 4 hours.
Comparative example 1
By step（3）In functional additive be substituted for the negative ion powder of its half weight, remaining operating procedure and embodiment 1
It is identical.
Comparative example 2
Step（3）In do not add sodium phytate, remaining operating procedure is identical with embodiment 2.
Health care wicker plaiting article pillow is made with the method for each embodiment and comparative example respectively, then uses II air of COM-3200PRO
Ion detection instrument tests its Negative ion disengagement, then by after health care wicker plaiting article pillow into the water immersion treatment 24 hours, tests
Its Negative ion disengagement, wherein the size of health-care pillow is 30cm × 20cm × 10cm, and test box is that insulation is closed
Test box (size：100cm × 100cm × 50cm) in, sample is opened after air ion tester 5cm, the static 900s of sample
Begin to test, need to take a breath to test box before test every time, air ion tester returns to zero, and test result is as shown in table 1：
1 health care wicker plaiting article pillow Negative ion disengagement of table
As shown in Table 1, health care wicker plaiting article pillow produced by the present invention still has excellent anion release property after bubble
Energy.
It should be understood that the application of the present invention is not limited to the above for those of ordinary skills can
With improvement or transformation based on the above description, all these modifications and variations all should belong to the guarantor of appended claims of the present invention
Protect range.
Claims (4)
1. a kind of preparation method of resistance to bubble health care wicker plaiting article pillow, which is characterized in that including following operating procedure：
（1）By weight, after mixing by 4-8 parts of hydroxytyrosols, 36-44 parts of glycerine, 65-70 is then added thereto
Succinic acid, the 29-32 parts of aluminium isopropoxides, 11-15 parts of aluminium chloride, 39-41 parts of urea of part, after being mixed evenly, by mixture
Temperature rise to 210-220 DEG C, insulation reaction 16-19 hours after, be cooled to room temperature, the liquid on the device of falling dereaction upper layer, so
Lower layer's sticky mass is centrifuged afterwards, is precipitated, and after washing of precipitate, drying process, nano-carrier is made；
（2）By nano-carrier and negative ion powder according to 1:The mass ratio of 1.2-1.4 is added into ball mill, and is added receives thereto
After ball-milling treatment 3-4 hours, functional additive is made in the calcium stearate of rice carrier quality 10-15%；
（3）By weight, by 28-33 parts of functional additives, 5-9 parts of sodium phytates, 1-5 parts of polyethylene glycol 200s, 160-200 parts
After water mixing, 30-40min is persistently stirred using the revolving speed of 400-450r/min, wicker plaiting article pillow treatment fluid is made；
（4）Wicker plaiting article pillow after knitting forming is added into wicker plaiting article pillow treatment fluid, after immersion treatment 4-5 hours, takes out, puts
Enter in baking oven, drying and processing, finished product.
2. a kind of preparation method of resistance to bubble health care wicker plaiting article pillow according to claim 1, which is characterized in that above-mentioned steps
（1）In, after the method for washing of precipitate is cleans twice using deionized water, then it is primary using washes of absolute alcohol.
3. a kind of preparation method of resistance to bubble health care wicker plaiting article pillow according to claim 1, which is characterized in that above-mentioned steps
（1）In, the temperature of drying process is 75-80 DEG C.
4. a kind of preparation method of resistance to bubble health care wicker plaiting article pillow according to claim 1, which is characterized in that above-mentioned steps
（4）In, the temperature of drying and processing is 45-50 DEG C, and the time of drying and processing is 3-4 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810384563.3A CN108818807A (en) | 2018-04-26 | 2018-04-26 | A kind of preparation method of resistance to bubble health care wicker plaiting article pillow |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810384563.3A CN108818807A (en) | 2018-04-26 | 2018-04-26 | A kind of preparation method of resistance to bubble health care wicker plaiting article pillow |
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| Publication Number | Publication Date |
|---|---|
| CN108818807A true CN108818807A (en) | 2018-11-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810384563.3A Pending CN108818807A (en) | 2018-04-26 | 2018-04-26 | A kind of preparation method of resistance to bubble health care wicker plaiting article pillow |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109093816A (en) * | 2018-08-17 | 2018-12-28 | 阜阳大可新材料股份有限公司 | A kind of production method of heel dedicated fiber plate |
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| JP2004156169A (en) * | 2002-11-06 | 2004-06-03 | Hidekazu Itaka | Material consisting of wool, cotton, textile fiber, nonwoven fabric, membrane, wood, plywood or particle board using structurized concentrated deep layer water |
| CN105563590A (en) * | 2015-12-24 | 2016-05-11 | 阜南县金地柳木工艺品有限公司 | Enhancing pretreating agent for anion healthcare effect of wicker for wickerwork and preparing method of enhancing pretreating agent |
| CN105729602A (en) * | 2016-03-16 | 2016-07-06 | 王璐 | Novel wood softening agent |
| CN106431418A (en) * | 2016-09-26 | 2017-02-22 | 中国科学院福建物质结构研究所 | Method for preparing nanometer AlN powder through hydrothermal method and intermediate and product produced through method |
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2018
- 2018-04-26 CN CN201810384563.3A patent/CN108818807A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004156169A (en) * | 2002-11-06 | 2004-06-03 | Hidekazu Itaka | Material consisting of wool, cotton, textile fiber, nonwoven fabric, membrane, wood, plywood or particle board using structurized concentrated deep layer water |
| CN105563590A (en) * | 2015-12-24 | 2016-05-11 | 阜南县金地柳木工艺品有限公司 | Enhancing pretreating agent for anion healthcare effect of wicker for wickerwork and preparing method of enhancing pretreating agent |
| CN105729602A (en) * | 2016-03-16 | 2016-07-06 | 王璐 | Novel wood softening agent |
| CN106431418A (en) * | 2016-09-26 | 2017-02-22 | 中国科学院福建物质结构研究所 | Method for preparing nanometer AlN powder through hydrothermal method and intermediate and product produced through method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109093816A (en) * | 2018-08-17 | 2018-12-28 | 阜阳大可新材料股份有限公司 | A kind of production method of heel dedicated fiber plate |
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Application publication date: 20181116 |