CN108815392A - A kind of processing method of HERBA DENDROBII - Google Patents

A kind of processing method of HERBA DENDROBII Download PDF

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Publication number
CN108815392A
CN108815392A CN201811103556.8A CN201811103556A CN108815392A CN 108815392 A CN108815392 A CN 108815392A CN 201811103556 A CN201811103556 A CN 201811103556A CN 108815392 A CN108815392 A CN 108815392A
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China
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herba dendrobii
quick
frozen
processing method
cleaning
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CN201811103556.8A
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不公告发明人
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An Zhiming
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An Zhiming
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/898Orchidaceae (Orchid family)
    • A61K36/8984Dendrobium
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/13Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/17Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Medical Informatics (AREA)
  • Medicinal Chemistry (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention belongs to Chinese medicine processing technique fields, are the fresh HERBA DENDROBII medicinal material of picking first more particularly to a kind of processing method of HERBA DENDROBII, go to cut weeds, fibrous root and leaf;Followed by the HERBA DENDROBII after cleaning is cleaned with clear water;Be again by cleaning after HERBA DENDROBII be placed on it is quick-frozen in refrigerator-freezer;Be finally will be quick-frozen after HERBA DENDROBII be placed in microwave field it is dry.The present invention is by combining quick-frozen and microwave drying; first with the quick-frozen cell for protecting HERBA DENDROBII not by the destruction of mechanism; reduce the moisture and solute migration osmosis inside and outside HERBA DENDROBII; original structure is kept to make to carry out dendrobium nobile; avoid the loss of benefit materials in HERBA DENDROBII; then surface is shifted to the state of water vapour with microwave-driven HERBA DENDROBII internal moisture, reaches quick-drying purpose, substantially reduce the loss late of benefit materials in HERBA DENDROBII in drying process.

Description

A kind of processing method of HERBA DENDROBII
Technical field
The present invention relates to Chinese medicine processing technique fields, it particularly relates to a kind of processing method of HERBA DENDROBII.
Background technique
HERBA DENDROBII is the traditional rare Chinese medicine in China, is classified as top grade in " Sheng Nong's herbal classic ".Modern medicine and Chinese medicine It is apparent that pharmacological research shows that dendrobium nobile has in terms of improving human immunological competence, anti-aging, inhibiting tumour, tonifying five zang organs Effect.The function of dendrobium nobile is mainly reinforcing stomach reg fluid, nourishing yin and clearing heat.It is clinically used for that consumption of body fluid caused by febrile disease, thirsty tongue be dry, abnormal heat, stomach after being ill Disease is retched, tongue light less fur.Immune with enhancing, strong negative strengthening the essence promoting fluid production and nourishing stomach, moistening lung to arrest cough, nourishing Yin and clearing heat, promotes the production of body fluid to quench thirst, uses In consumption of body fluid caused by febrile disease, thirsty tongue is dry, abnormal heat, anticancer, reinforcing stomach reg fluid, nourishing Yin and clearing heat, improving eyesight, adjust blood lipid, are hypoglycemic clearing liver after being ill Deng.There is special efficacy to cardiovascular and cerebrovascular, digestive system and respiratory system, ophthalmology etc..Crack In Guizhou Chishui HERBA DENDROBII belongs to orchid family for many years Raw herbaceous plant, is grown between overhanging cliff, and cloud and mist rain and dew of satisfying throughout the year are to be moistened, by the essence of life yin-yang.It is used as medicine with base, Have the function of to promote the production of body fluid throat soothing, heat clearing and inflammation relieving, voiceless sound improving eyesight, cancer-resisting, is the rare rare traditional Chinese medicine both domestic and external that is renown far and wide.
HERBA DENDROBII is dry mainly using drying, dry in the shade (air-dried) and the techniques such as tradition hot-air seasoning at present.Although Traditional dry technology has accumulated many invaluable experiences, but the four natures and five flavors of drug of HERBA DENDROBII often cannot be good in drying Protection leads to problems such as HERBA DENDROBII deterioration, institutional framework destroy, pharmacological property changes, loss of effective components.In addition traditional hot air drying The dry time is long, and energy consumption is high, and drying efficiency is low.
Summary of the invention
In view of this, the object of the present invention is to provide a kind of processing method of HERBA DENDROBII, to solve existing HERBA DENDROBII In drying process generate deterioration, institutional framework destroy, pharmacological property change, loss of effective components and.
The present invention solves above-mentioned technical problem by the following technical programs:
A kind of processing method of HERBA DENDROBII, includes the following steps:
(1)It cleans:Fresh HERBA DENDROBII medicinal material is picked, goes to cut weeds, fibrous root and leaf;
(2)Cleaning:HERBA DENDROBII after cleaning is cleaned with clear water;
(3)It is quick-frozen:HERBA DENDROBII after cleaning is placed on quick-frozen in refrigerator-freezer;
(4)It is dry:HERBA DENDROBII after will be quick-frozen be placed in microwave field dry to get.
The step(2)In, by HERBA DENDROBII put 2 ~ 3 times amount clear water clean 1 ~ 3 time, every time 5 ~ 10 minutes to get.
The step(3)In, it is quick-frozen, the time in -30 DEG C ~ -24 DEG C refrigerator-freezers that the HERBA DENDROBII after cleaning, which is placed on temperature, For 3 ~ 5h.
The step(3)In, it is quick-frozen, time 4h in -27 DEG C of refrigerator-freezers that the HERBA DENDROBII after cleaning, which is placed on temperature,.
The step(4)In, will be quick-frozen after HERBA DENDROBII place in the microwave field of 1600 ~ 1800w and dry to golden hairpin stone Dry measure used in former times moisture content be 6 ~ 10% to get.
The step(4)In, will be quick-frozen after HERBA DENDROBII place in the microwave field of 1700w and dry to HERBA DENDROBII moisture Content be 8% to get.
The beneficial effects of the present invention are:Microwave drying is the processing method of a kind of water translocation and evaporation while progress, Microwave heating generates heat from inside, and the steam being quickly generated inside material forms huge driving force, generates a kind of " pumping Effect " drives moisture to shift to surface from the state of water vapour, even generates very big total pressure gradient sometimes, makes partial moisture also It has not enough time to be vaporized and has just been discharged to surface of material, therefore rate of drying is very fast.And due to evaporation surface temperature ratio It is internal low, surface of material overheat will not be generated, burn into the phenomenon that inside and outside uneven drying.Microwave can also be selectively directed to Ice cube heating, and drying nest has seldom absorbed microwave energy, so that rate of drying greatly increases.Quick-frozen purpose is exactly to make Jin Chai Moisture and solute migration osmosis inside and outside dendrobium nobile reduce, and portion and space between cells ice crystal generated are tiny in the cell, make It obtains mechanism to reduce the destruction of cell, so that HERBA DENDROBII is able to maintain original structure.The present invention pass through will it is quick-frozen with Microwave drying combines, and is first reduced inside and outside HERBA DENDROBII with the quick-frozen cell for protecting HERBA DENDROBII not by the destruction of mechanism Moisture and solute migration osmosis, thus make carry out dendrobium nobile keep original structure, avoid benefit materials in HERBA DENDROBII Loss, then shifts to surface with microwave-driven HERBA DENDROBII internal moisture with the state of water vapour, reaches quick-drying purpose, Substantially reduce the loss late of benefit materials in HERBA DENDROBII in drying process.
Specific embodiment
In order to facilitate the understanding of those skilled in the art, below in conjunction with embodiment, the present invention will be further described. Embodiment is only to the invention for example, not being limitation of the invention, the step of not illustrating in embodiment It is prior art, is not described in detail herein.
Embodiment one
A kind of processing method of HERBA DENDROBII picks the fresh HERBA DENDROBII medicinal material in Crack In Guizhou Chishui Region, goes to cut weeds, fibrous root and leaf Son;The clear water that HERBA DENDROBII after cleaning puts 2 times of amounts is cleaned 1 time, every time 5 minutes;HERBA DENDROBII after cleaning is placed on temperature Degree is quick-frozen, time 3h in -30 DEG C of refrigerator-freezers;HERBA DENDROBII after will be quick-frozen, which is placed in the microwave field of 1600w, to be dried to Jin Chai Dendrobium nobile moisture content be 6% to get.
Embodiment two
A kind of processing method of HERBA DENDROBII picks the fresh HERBA DENDROBII medicinal material in Crack In Guizhou Chishui Region, goes to cut weeds, fibrous root and leaf Son;The clear water that HERBA DENDROBII after cleaning puts 3 times of amounts is cleaned 3 times, every time 10 minutes;HERBA DENDROBII after cleaning is placed on temperature Degree is quick-frozen, time 5h in -24 DEG C of refrigerator-freezers;HERBA DENDROBII after will be quick-frozen, which is placed in the microwave field of 1800w, to be dried to Jin Chai Dendrobium nobile moisture content be 10% to get.
Embodiment three
A kind of processing method of HERBA DENDROBII picks the fresh HERBA DENDROBII medicinal material in Crack In Guizhou Chishui Region, goes to cut weeds, fibrous root and leaf Son;The clear water that HERBA DENDROBII after cleaning puts 3 times of amounts is cleaned 2 times, every time 8 minutes;HERBA DENDROBII after cleaning is placed on temperature Degree is quick-frozen, time 4h in -27 DEG C of refrigerator-freezers;HERBA DENDROBII after will be quick-frozen, which is placed in the microwave field of 1700w, to be dried to Jin Chai Dendrobium nobile moisture content be 8% to get.
Comparative example one
A kind of processing method of HERBA DENDROBII picks the fresh HERBA DENDROBII medicinal material in Crack In Guizhou Chishui Region, goes to cut weeds, fibrous root and leaf Son;The clear water that HERBA DENDROBII after cleaning puts 3 times of amounts is cleaned 2 times, every time 8 minutes;HERBA DENDROBII after cleaning is placed on temperature Degree is quick-frozen, time 4h in -20 DEG C of refrigerator-freezers;HERBA DENDROBII after will be quick-frozen, which is placed in the microwave field of 1700w, to be dried to Jin Chai Dendrobium nobile moisture content be 8% to get.
Comparative example two
A kind of processing method of HERBA DENDROBII picks the fresh HERBA DENDROBII medicinal material in Crack In Guizhou Chishui Region, goes to cut weeds, fibrous root and leaf Son;The clear water that HERBA DENDROBII after cleaning puts 3 times of amounts is cleaned 2 times, every time 8 minutes;HERBA DENDROBII after cleaning is placed on temperature Degree is quick-frozen, time 4h in -27 DEG C of refrigerator-freezers;HERBA DENDROBII after will be quick-frozen in 75 DEG C of baking ovens forced air drying to HERBA DENDROBII Moisture content be 8% to get.
Comparative example three
A kind of processing method of HERBA DENDROBII picks the fresh HERBA DENDROBII medicinal material in Crack In Guizhou Chishui Region, goes to cut weeds, fibrous root and leaf Son;The clear water that HERBA DENDROBII after cleaning puts 3 times of amounts is cleaned 2 times, every time 8 minutes;HERBA DENDROBII after cleaning is placed In the microwave field of 1700w dry to HERBA DENDROBII moisture content be 8% to get.
By the separately sampled of dry HERBA DENDROBII obtained by above-mentioned six kinds of processing methods, through containing for Phenol sulfuric acid procedure measurement polysaccharide Amount, efficient liquid phase(HPLC)Method measurement dendrobium nobile alkaloid, the content of aluminum nitrate determination of color HERBA DENDROBII flavones, as a result It is shown in Table 1.
1 HERBA DENDROBII composition measurement result of table
Key is the rate of control freezing during quick-frozen, and freezing rate is faster, the moisture and solute of HERBA DENDROBII intraor extracellular Migration osmosis is smaller, and cell interior and space between cells ice crystal generated are thinner, acts on also just the mechanical failure of cell It is smaller, be more conducive to keep the original structure of HERBA DENDROBII, protect the benefit materials inside HERBA DENDROBII.From comparative example one and in fact The comparison of example is applied as can be seen that the quick-frozen control for freezing rate in the process(Select quick-frozen temperature)For protecting Jin Chai The benefit materials of dendrobium nobile such as dendrobium polysaccharide and dendrobium nobile alkaloid etc. are most important.The present invention passes through the stringent control to quick freezing temperature System, it is a greater degree of to keep the original structure of HERBA DENDROBII, avoid the loss of the benefit materials inside HERBA DENDROBII.
From the testing result of comparative example two and embodiment three can be seen that by HERBA DENDROBII it is quick-frozen after, if unhappy rapid-curing cutback It is dry, it will to lead to the loss of benefit materials inside HERBA DENDROBII, the present invention by quick-frozen with microwave drying by combining, more great Cheng The original structure of holding HERBA DENDROBII of degree, avoids the loss of the benefit materials inside HERBA DENDROBII.
It can be seen that from the testing result of comparative example three and embodiment three only with microwave drying HERBA DENDROBII, can make At the loss of a large amount of benefit materials, the beneficiating ingredients such as dendrobium polysaccharide and dendrobine is caused to reduce.The present invention pass through will it is quick-frozen and Microwave drying combines, a greater degree of to keep the original structure of HERBA DENDROBII, avoids the benefit materials inside HERBA DENDROBII Loss.

Claims (6)

1. a kind of processing method of HERBA DENDROBII, it is characterised in that include the following steps:
(1)It cleans:Fresh HERBA DENDROBII medicinal material is picked, goes to cut weeds, fibrous root and leaf;
(2)Cleaning:HERBA DENDROBII after cleaning is cleaned with clear water;
(3)It is quick-frozen:HERBA DENDROBII after cleaning is placed on quick-frozen in refrigerator-freezer;
(4)It is dry:HERBA DENDROBII after will be quick-frozen be placed in microwave field dry to get.
2. the processing method of HERBA DENDROBII according to claim 1, it is characterised in that:The step(2)In, by golden hairpin stone Dry measure used in former times put 2 ~ 3 times amount clear water clean 1 ~ 3 time, every time 5 ~ 10 minutes to get.
3. the processing method of HERBA DENDROBII according to claim 1, it is characterised in that:The step(3)In, after cleaning HERBA DENDROBII be placed on temperature be it is quick-frozen in -30 DEG C ~ -24 DEG C refrigerator-freezers, the time is 3 ~ 5h.
4. the processing method of HERBA DENDROBII according to claim 1 or 3, it is characterised in that:The step(3)In, it will be clear It is quick-frozen, time 4h in -27 DEG C of refrigerator-freezers that HERBA DENDROBII after washing, which is placed on temperature,.
5. the processing method of HERBA DENDROBII according to claim 1, it is characterised in that:The step(4)In, after quick-frozen HERBA DENDROBII place 1600 ~ 1800w microwave field in dry to HERBA DENDROBII moisture content be 6 ~ 10% to get.
6. the processing method of HERBA DENDROBII according to claim 1 or 5, it is characterised in that:The step(4)In, it will be fast HERBA DENDROBII after jelly place dried in the microwave field of 1700w to HERBA DENDROBII moisture content be 8% to get.
CN201811103556.8A 2018-09-20 2018-09-20 A kind of processing method of HERBA DENDROBII Pending CN108815392A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR860001812B1 (en) * 1981-04-13 1986-10-24 메이지 세이카주식회사 Method for manufacturing dry ginseng
CN101352525A (en) * 2008-03-24 2009-01-28 阳瑞鸿 Lyophilized dendrobium
CN103417848A (en) * 2013-07-25 2013-12-04 张更海 Dendrobe freeze drying and processing method
CN105674687A (en) * 2016-01-21 2016-06-15 广西大学 Microwave vacuum freeze-drying method for Dendrobium officinale
CN106237106A (en) * 2016-08-05 2016-12-21 安徽淮仁堂药业有限公司 A kind of processing method of lyophilized dendrobium
CN106546070A (en) * 2015-09-16 2017-03-29 广西巴马兰长寿科技有限公司 A kind of Herba Dendrobii microwave freeze-drying method

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR860001812B1 (en) * 1981-04-13 1986-10-24 메이지 세이카주식회사 Method for manufacturing dry ginseng
CN101352525A (en) * 2008-03-24 2009-01-28 阳瑞鸿 Lyophilized dendrobium
CN103417848A (en) * 2013-07-25 2013-12-04 张更海 Dendrobe freeze drying and processing method
CN106546070A (en) * 2015-09-16 2017-03-29 广西巴马兰长寿科技有限公司 A kind of Herba Dendrobii microwave freeze-drying method
CN105674687A (en) * 2016-01-21 2016-06-15 广西大学 Microwave vacuum freeze-drying method for Dendrobium officinale
CN106237106A (en) * 2016-08-05 2016-12-21 安徽淮仁堂药业有限公司 A kind of processing method of lyophilized dendrobium

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
张璧光: "《木材科学与技术研究进展》", 30 January 2004, 中国环境科学出版社 *

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Application publication date: 20181116