CN108774583A - The preparation method of a kind of potpourri and its for purposes in tobacco product - Google Patents
The preparation method of a kind of potpourri and its for purposes in tobacco product Download PDFInfo
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- CN108774583A CN108774583A CN201810554377.XA CN201810554377A CN108774583A CN 108774583 A CN108774583 A CN 108774583A CN 201810554377 A CN201810554377 A CN 201810554377A CN 108774583 A CN108774583 A CN 108774583A
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- Prior art keywords
- insoluble matter
- potpourri
- preparation
- cigarette
- tobacco
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Health & Medical Sciences (AREA)
- Botany (AREA)
- General Chemical & Material Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Paper (AREA)
Abstract
The invention discloses a kind of preparation method of potpourri, step is：(1) starting material with water is extracted, detaches leaching liquor and insoluble matter；(2) substrate is made in the insoluble matter that step (1) obtains；(3) by the leaching liquor substrate that dip-coating is obtained to step (2) after cryogenic vacuum concentrates that step (1) obtains to get to the potpourri.The invention also discloses potpourris made from the preparation method for the purposes in tobacco product.
Description
Technical field
The invention belongs to technical field of tobacco, it is specifically related to a kind of preparation method of potpourri and its is used for tobacco system
Purposes in product.
Background technology
It is the reconstruction that is process with paper technology using offal and offal as raw material with paper process production reconstituted tobacco
Tobacco leaf, production method are to be soaked in water, extract after mixing offal and offal, detach insoluble matter and soluble matter extract liquor, no
Molten object is used for slurrying, and manufactures paper with pulp into substrate, after the concentration modulation of soluble matter extract liquor, immerses in substrate or is coated on substrate, or
It is the extraction and separation by offal and offal respectively with after corresponding solvent soaking, the insoluble matter mixed pulp of gained respectively, upper paper machine
Substrate is manufactured paper with pulp into, the soluble matter extract liquor concentration adjustment of gained is made coating fluid, is applied on substrate.The production technology is letter
Tobacco material is regulated and controled and is recombinated by single ground, is had no other special functions or is inhaled taste.Due to the particularity of raw material, lead to this
Body flue gas is thin, single, not strong with the compatibility of tobacco leaf in use, modifies the effect unobvious along making up.In the past
Mainly improved by manually adding fragrance.With the emergence of new cigarette material, according to different trade mark cigarette
Style and the difference for inhaling taste, targetedly select suitable raw material to be combined collocation, it has also become papermaking-method reconstituted tobaccos are given birth to
Conventional technical means in production.
Invention content
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide the preparation of the potpourri in a tobacco articles
The purposes of method and the potpourri in tobacco product, with increase cigarette fragrance and it is jealous, reduce xylon gas and pungent
Sense, to promote the integrated sensory quality of cigarette.
The purpose of the present invention is achieved by the following technical programs.
Unless otherwise indicated, percentage of the present invention is mass percent.
First aspect present invention discloses a kind of preparation method of potpourri, and step is：
(1) starting material with water is extracted, detaches leaching liquor and insoluble matter；
(2) substrate is made in the insoluble matter that step (1) obtains；
(3) by the leaching liquor substrate that dip-coating is obtained to step (2) after cryogenic vacuum concentrates that step (1) obtains, i.e.,
Obtain the potpourri.
Preferably, the raw material is the composition of vegetables and herbal plant, and mass ratio is vegetables dry product 5 in the composition
~20 parts, 5~20 parts of herbal plant dry product.
Preferably, the vegetables be celery, carrot, radish, Chinese yam, taro, tomato, ginger, cucumber, green onion, garlic, pumpkin,
One or more compositions in cabbage, balsam pear, fennel；
The herbal plant is the stem of noble dendrobium, ganoderma lucidum, green tea, black tea, Pu'er tea, mate, pueraria lobata, Radix Glycyrrhizae, Siraitia grosvenorii, chicken
Egg flower, honeysuckle, the sterculia seed, dandelion, rose, iris, sensitive plant, asia peppermint, strawflower, Jasmine, lemongrass, ladanum,
Valerian, rosemary, stays orchid, raspberry, fish pelargonium, faenum graecum, witloof, malt, Radix Ophiopogonis, violet leaf, ylang-ylang at vanilla
In one or more compositions；
Preferably, the mass ratio of the raw material dry product and water of step (1) is 1:8~1:15, ultrasound extraction, the time is 20~40
Minute.
Preferably, the step of substrate is made in insoluble matter by step (2) be：
1. the mixture of insoluble matter or insoluble matter and waste/hypo-tobacco leaf is added 5~10 times of water rettings of its quality, and pectin is added
Enzyme, amylase and cellulase carry out catalytic degradation；
2. again 1. 1~10% wood fibre of insoluble matter or insoluble matter and waste/hypo-tobacco leaf gross mass is added to step
Mixed pulp is carried out in obtained mixture, is manufactured paper with pulp using conventional paper process and substrate is made.
Preferably, the dosage of the pectase, amylase and cellulase accounts for the insoluble matter or insoluble matter and gives up respectively
The percentage of the mixture gross mass of hypo-tobacco leaf is：Pectase 0.03%~0.1%, amylase 0.1%~0.6%, cellulose
Enzyme 0.5%~1%；Hydrolysis temperature is 30 DEG C~60 DEG C；1~4 hour catalytic degradation time.
Second aspect of the present invention discloses potpourri made from above-mentioned preparation method for the purposes in tobacco product.
Preferably, the potpourri is used separately as pipe tobacco or is used in mixed way with common pipe tobacco.
Preferably, when potpourri is used in mixed way with common pipe tobacco, the ratio of the potpourri is 1~55wt%.
Compared with the existing technology, the present invention has the following advantages：
1, the present invention takes full advantage of the active ingredient and fragrance matter of extract, and is handled to insoluble by catalytic degradation
Pectin and protein etc. carry out fully degraded in object, produce a large amount of Maillard reaction precursor.Improve the potpourri
Adaptability in cigarette composition and compatibility can fully promote the suction quality of cigarette made of the potpourri, reach portion
Point or replacing whole tobacco leaf purpose.
2, vegetables herbal plant potpourri of the invention is used for cigarette products, and the style that can enhance tobacco product is special
Sign keeps fragrance more abundant, enhances fresh and sweet note and sense of promoting the production of body fluid, flue gas is finer and smoother, soft, preferably improves the synthesis of cigarette
Organoleptic quality.It has been surprisingly found that, which can reduce the content of harmful substance for cigarette products, special
It is not tar content to reduce obviously；Water content obviously increases simultaneously.
3, the vegetables herbal plant and waste/hypo-tobacco leaf used in the present invention, can reduce the demand to wood fibre, therefore
Compared with the suction of cigarette reconstituted tobacco, can the bad breath such as substantially reduced woody odor, while also solving and cigarette enterprise
The problem of fighting for raw material.
4, vegetables herbal plant potpourri of the invention extends the use scope of vegetables herbal plant, enriches cigarette
Fragrance type, can preferably meet the needs of cigarette product specializes.
5, the shortage problem that material is inevitably encountered in cigarette product, causes product quality to fluctuate.The present invention
Production of cigarettes raw material is enriched, alleviates the problem of raw tobacco material shortage to a certain extent, and then stable prod can be reached and matched
The purpose of side.
Specific implementation mode
With reference to specific embodiment, the present invention is described in further detail, but embodiment is not to skill of the present invention
The restriction of art scheme.
Embodiment 1
Choose mass parts：1 portion of spinach, 2 portions of Chinese yams, 3 parts of mates, 2 portions of Radix Glycyrrhizaes are chosen, ultra micro is carried out after being baked to
It crushes, then using water as solvent, solid-to-liquid ratio 1:8, through ultrasound extraction 20 minutes, isolated leaching liquor and not after extraction
Molten object.Leaching liquor is spare after cryogenic vacuum concentration, distinguishes by insoluble matter plus 5 times of water rettings, then by insoluble matter gross mass
Be added 0.03% pectase, 0.6% amylase, 0.5% the catalyzing enzymes such as cellulase, catalytic degradation temperature is 30 DEG C,
Stirring 2 hours.Then wood fibre progress slurrying is added in 2% mass ratio for pressing insoluble matter gross mass again, then manufactures paper with pulp into base
Piece.By in leaching liquor uniform dip-coating to above-mentioned substrate, after roll paper, cutting, drying, potpourri is made.It can independent chopping
And the tobacco products such as cigarette are made, also it can be mixed and made into tobacco product with pipe tobacco.
The cigarette process of potpourri obtained routinely rolls into cigarette through flavoring, volume job contract skill.Through sensory evaluating smoking,
Overall process can obviously experience suck cigarette custom continuity and satisfaction, flue gas it is soft it is smooth, fragrance is elegant, sweet sense
Well, overall comfort is good, and the ash rate tobacco ash content to burn is white.Potpourri obtained is mixed with pipe tobacco in varing proportions
Tobacco product is prepared, can embody above-mentioned sensory effects in various degree.
Potpourri obtained is mixed with 8wt% ratios with pipe tobacco, cigarette is rolled into through flavoring, volume job contract skill, names
For No. 1 cigarette.On same production line, control cigarette is rolled by identical cigarette process, control sample is that obtained mix is not added
The normal cigarette of blending material.Then national standard is pressed《The tobaccos of GB/T16447~1996 and tobacco product adjust the big compression ring with test
Border》Adjust cigarette sample moisture content be 12%, by smoke panel test panel of expert by《The requirement of the cigarette sense organ technologies of GB5606.4~1996》
Regulation carry out cigarette sensory evaluating smoking.Smoking result is shown in Table 1.Specific sense organ marking is shown in Table 2 and table 3.According to GB 5606.5-
2005 pairs of cigarette carry out flue gas conventional detection, and testing result is shown in Table 4.
Embodiment 2
Choose mass parts：3 portions of balsam pears, 2 parts of faenum graecums, 3 parts of Pu'er teas, 2 parts of pueraria lobatas are chosen, ultra micro is carried out after being baked to
It crushes, then using water as solvent, solid-to-liquid ratio 1:10, through ultrasound extraction 40 minutes.After extraction isolated leaching liquor and
Insoluble matter.Leaching liquor is spare after cryogenic vacuum concentration, by insoluble matter and the waste/hypo-tobacco leaf (matter of insoluble matter and waste/hypo-tobacco leaf
Amount is than being 1:1) plus 7 times of water impregnate again, then by insoluble matter and waste/hypo-tobacco leaf gross mass be separately added into 0.15% pectase,
The catalyzing enzymes such as 0.3% amylase, 0.8% cellulase, catalytic degradation temperature are 50 DEG C, are stirred 3 hours.Then it presses again not
8% mass ratio of molten object gross mass is added wood fibre and carries out slurrying, then manufactures paper with pulp into substrate.The uniform dip-coating of leaching liquor is arrived
On above-mentioned substrate, after roll paper, cutting, drying, potpourri is made.Individually chopping and the tobacco products such as cigarette can be made,
Also tobacco product can be mixed and made into pipe tobacco.
The cigarette process of potpourri obtained routinely rolls into cigarette through flavoring, volume job contract skill.Through sensory evaluating smoking,
Overall process can obviously experience suck cigarette custom continuity and satisfaction, flue gas it is soft it is smooth, fragrance is elegant, sweet sense
Well, overall comfort is good, and the ash rate tobacco ash content to burn is white.Potpourri obtained mixes system with pipe tobacco in varing proportions
Standby tobacco product, can embody above-mentioned sensory effects in various degree.
Potpourri obtained is mixed with 6wt% ratios with pipe tobacco, cigarette is rolled into through flavoring, volume job contract skill, names
For No. 2 cigarettes.On same production line, control cigarette is rolled by identical cigarette process, control sample is that obtained mix is not added
The normal cigarette of blending material.Then national standard is pressed《The tobaccos of GB/T16447~1996 and tobacco product adjust the big compression ring with test
Border》Adjust cigarette sample moisture content be 12%, by smoke panel test panel of expert by《The requirement of the cigarette sense organ technologies of GB5606.4~1996》
Regulation carry out cigarette sensory evaluating smoking.Smoking result is shown in Table 1.Specific sense organ marking is shown in Table 2 and table 3.According to GB 5606.5-
2005 pairs of cigarette carry out flue gas conventional detection, and testing result is shown in Table 4.
Embodiment 3
Choose mass parts：3 portions of carrots, 1 portion of ginger, 2 portions of valerians, 1 part of asia peppermint, ultramicro grinding is carried out after being baked to,
Again using water as solvent, solid-to-liquid ratio 1:15, through ultrasound extraction 30 minutes, isolated leaching liquor and insoluble after extraction
Object.Leaching liquor is spare after cryogenic vacuum concentration, by insoluble matter and the waste/hypo-tobacco leaf (mass ratio of insoluble matter and waste/hypo-tobacco leaf
It is 2:1) plus 10 times of water impregnate again, then by insoluble matter and waste/hypo-tobacco leaf gross mass be separately added into 0.1% pectase, 0.3%
Amylase, 1% the catalyzing enzymes such as cellulase, catalytic degradation temperature is 60 DEG C, is stirred 4 hours.It is pressed again not after mixed pulp
Molten object and the mass ratio of waste/hypo-tobacco leaf gross mass 10% are added wood fibre and carry out slurrying, then manufacture paper with pulp into substrate.By leaching liquor
In uniform dip-coating to above-mentioned substrate, after roll paper, cutting, drying, potpourri is made.Individually chopping and cigarette can be made etc.
Tobacco product also can be mixed and made into tobacco product with pipe tobacco.
By the cigarette process of obtained potpourri routinely, cigarette is rolled into through flavoring, volume job contract skill.Through sensory evaluating smoking,
Overall process can obviously experience suck cigarette custom continuity and satisfaction, flue gas it is soft it is smooth, fragrance is elegant, sweet sense
Well, overall comfort is good, and the ash rate tobacco ash content to burn is white.Obtained potpourri is mixed into system with pipe tobacco in varing proportions
Standby tobacco product, can embody above-mentioned sensory effects in various degree.
Obtained potpourri is mixed with 4wt% ratios with pipe tobacco, cigarette is rolled into through flavoring, volume job contract skill, is named as 3
Number cigarette.On same production line, control cigarette is rolled by identical cigarette process, control sample is that cigarette formula mixing is not added
The normal cigarette of fragrance.Then national standard is pressed《The tobaccos of GB/T16447~1996 and tobacco product adjust the atmospheric environment with test》
Adjust cigarette sample moisture content be 12%, by smoke panel test panel of expert by《The requirement of the cigarette sense organ technologies of GB5606.4~1996》Rule
Surely cigarette sensory evaluating smoking is carried out.Smoking result is shown in Table 1.Specific sense organ marking is shown in Table 2, table 3.According to GB 5606.5-2005 to volume
Cigarette carries out flue gas conventional detection, and testing result is shown in Table 4.
1 cigarette sensory evaluating smoking's result of table
2 sensory evaluation of table marking table
3 sense organ evaluating meter of table
4 flue gas conventional analysis result of table
Show that the potpourri of preparation is added in cigarette by the smoking result in table 1- tables 3, cigarette obtained is smoked panel test
Divide 0.55 point higher than control sample or so.Compared with control sample, the comfort mean height 0.5 of cigarette obtained divides or so, flue gas
Feature mean height 0.4 divides or so, more than sweet taste mean height 0.5 divides in taste style, tart flavour mean height 0.2 or so.Therefore this hair
Bright potpourri, which is added in cigarette, can be obviously improved cigarette perfume, coordinate flue gas, increase the sweet sense of flue gas, reduce cigarette smoke thorn
The effect for swashing property, improving user throat comfort, can increase the richness and sophistication of cigarette perfume, there is preferable cigarette application effect
Fruit.As shown in Table 4, it compared with control sample, adds total in the cigarette mainstream flue gas of the cigarette herbal plant potpourri of the present invention
Granule phase substance, smoking nicotine and CO decrease, and especially tar content is substantially reduced, averagely have dropped 0.80mg/ branch with
On；Flue gas moisture obviously increases simultaneously, averagely increases 0.45mg/ branch or so.
Claims (9)
1. a kind of preparation method of potpourri, which is characterized in that step is：
(1) starting material with water is extracted, detaches leaching liquor and insoluble matter；
(2) substrate is made in the insoluble matter that step (1) obtains；
(3) by the leaching liquor substrate that dip-coating is obtained to step (2) after cryogenic vacuum concentrates that step (1) obtains to get to
The potpourri.
2. preparation method according to claim 1, which is characterized in that the raw material is the combination of vegetables and herbal plant
Object, mass ratio is 5~20 parts of vegetables dry product, 5~20 parts of herbal plant dry product in the composition.
3. the preparation method described in claim 2, which is characterized in that the vegetables be celery, carrot, radish, Chinese yam, taro,
One or more compositions in tomato, ginger, cucumber, green onion, garlic, pumpkin, cabbage, balsam pear, fennel；
The herbal plant is the stem of noble dendrobium, ganoderma lucidum, green tea, black tea, Pu'er tea, mate, pueraria lobata, Radix Glycyrrhizae, Siraitia grosvenorii, egg
Flower, honeysuckle, the sterculia seed, dandelion, rose, iris, sensitive plant, asia peppermint, strawflower, Jasmine, lemongrass, ladanum, figured silk fabrics
Grass, rosemary, stays in orchid, raspberry, fish pelargonium, faenum graecum, witloof, malt, Radix Ophiopogonis, violet leaf, ylang-ylang vanilla
One or more compositions.
4. preparation method according to claim 1, which is characterized in that the raw material dry product of step (1) and the mass ratio of water are
1:8~1:15, ultrasound extraction, the time is 20~40 minutes.
5. preparation method according to claim 1, which is characterized in that the step of substrate is made in insoluble matter by step (2) be：
1. the mixture of insoluble matter or insoluble matter and waste/hypo-tobacco leaf is added into 5~10 times of water rettings of its quality, and be added pectase,
Amylase and cellulase carry out catalytic degradation；
2. 1~10% wood fibre of insoluble matter or insoluble matter and waste/hypo-tobacco leaf gross mass is added to step again 1. to obtain
Mixture in carry out mixed pulp, manufactured paper with pulp using conventional paper process and substrate be made.
6. preparation method according to claim 5, which is characterized in that the pectase, amylase and cellulase use
Measuring the percentage of mixture gross mass for accounting for the insoluble matter or insoluble matter and waste/hypo-tobacco leaf respectively is：Pectase 0.03%~
0.1%, amylase 0.1%~0.6%, cellulase 0.5%~1%；Hydrolysis temperature is 30 DEG C~60 DEG C；The catalytic degradation time
1~4 hour.
7. a kind of being used for the use in tobacco product according to potpourri made from any preparation methods of claim 1-6
On the way.
8. purposes according to claim 7, which is characterized in that the potpourri separately as pipe tobacco use or with it is general
Logical pipe tobacco is used in mixed way.
9. purposes according to claim 8, which is characterized in that described mixed when potpourri is used in mixed way with common pipe tobacco
The ratio of blending material is 1~55wt%.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810554377.XA CN108774583A (en) | 2018-06-01 | 2018-06-01 | The preparation method of a kind of potpourri and its for purposes in tobacco product |
| CN201910181089.9A CN109691684A (en) | 2018-06-01 | 2019-03-11 | The preparation method and its purposes in tobacco product of a kind of fragrance |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810554377.XA CN108774583A (en) | 2018-06-01 | 2018-06-01 | The preparation method of a kind of potpourri and its for purposes in tobacco product |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108774583A true CN108774583A (en) | 2018-11-09 |
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ID=64026485
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810554377.XA Pending CN108774583A (en) | 2018-06-01 | 2018-06-01 | The preparation method of a kind of potpourri and its for purposes in tobacco product |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110638086A (en) * | 2019-09-12 | 2020-01-03 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
-
2018
- 2018-06-01 CN CN201810554377.XA patent/CN108774583A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110638086A (en) * | 2019-09-12 | 2020-01-03 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
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Application publication date: 20181109 |