CN108741218A - A kind of preparation method and purposes of cigarette vegetable solids fragrance - Google Patents
A kind of preparation method and purposes of cigarette vegetable solids fragrance Download PDFInfo
- Publication number
- CN108741218A CN108741218A CN201810554380.1A CN201810554380A CN108741218A CN 108741218 A CN108741218 A CN 108741218A CN 201810554380 A CN201810554380 A CN 201810554380A CN 108741218 A CN108741218 A CN 108741218A
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- Prior art keywords
- cigarette
- fragrance
- insoluble matter
- vegetable solids
- preparation
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a kind of cigarette preparation method of vegetable solids fragrance, step is：(1) by vegetables flooding, leaching liquor and insoluble matter are detached；(2) substrate is made in the insoluble matter that step (1) obtains；(3) by the leaching liquor substrate that dip-coating is obtained to step (2) after cryogenic vacuum concentrates that step (1) obtains to get to cigarette vegetable solids fragrance.The invention also discloses cigarette made from the preparation method with vegetable solids fragrance for the purposes in tobacco product.
Description
Technical field
The invention belongs to cigarette solid spice technical fields, are specifically related to a kind of preparation of cigarette vegetable solids fragrance
Method and purposes.
Background technology
Traditional papermaking-method reconstituted tobaccos are the methods for using for reference papermaking, and the tobacco wastes such as offal, offal and tobacco cut are passed through
After crossing the processing of recombination reproduction process, a kind of raw material of cigarette produced is one of module important in production of cigarettes.In cigarette original
Material formula designs and has preferable application value in product reformation.A certain amount of reconstituted tobacco is added in cigarette can not only drop
Low cigarette cost saves raw material, the filling capacity and flammability of cigarette is improved, and can change flue gas composition, in certain journey
The physical property and chemical composition that cigarette may be implemented on degree are adjusted and improve as required, reduce and improve tobacco it is bad at
Point, so improve cigarette in quality.But that there are irritations on sense organ is larger for papermaking-method reconstituted tobaccos, xylon gas' weight, fragrant
The shortcomings of makings is poor, perfume quantity is poor, and there are problems that fighting for raw material with Cigarette Industrial Enterprise, in addition, traditional paper process is again
The production for making tobacco leaf needs more log resource.Therefore, seek the external source for being more advantageous to papermaking-method reconstituted tobaccos quality-improving
Property addition raw material, just become the important topic constantly exploring and study in production of cigarettes field.
Invention content
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of cigarette vegetable solids fragrance and its preparation
Methods and applications, with increase cigarette fragrance and it is jealous, reduce xylon gas and pungent sense, to promote integrated sensory's product of cigarette
Matter.
The purpose of the present invention is achieved by the following technical programs.
Unless otherwise indicated, percentage of the present invention is mass percent.
The first aspect of the present invention discloses a kind of preparation method of cigarette vegetable solids fragrance, and step is：
(1) by vegetables flooding, leaching liquor and insoluble matter are detached；
(2) substrate is made in the insoluble matter that step (1) obtains；
(3) by the leaching liquor substrate that dip-coating is obtained to step (2) after cryogenic vacuum concentrates that step (1) obtains, i.e.,
Obtain the cigarette vegetable solids fragrance.
Preferably, the vegetables be celery, spinach, Chinese cabbage, carrot, radish, Chinese yam, taro, tomato, ginger, cucumber,
One or more compositions in green onion, garlic, pumpkin, cabbage, balsam pear, fennel, cordate houttuynia.
Preferably, the mass ratio of the vegetables of step (1) and water is 1:8~1:15, ultrasound extraction, the time is 20~60 points
Clock.
Preferably, the step of substrate is made in insoluble matter by step (2) be：
1. the mixture of the insoluble matter or insoluble matter and waste/hypo-tobacco leaf is added 5~10 times of water rettings of its quality, and it is added
Pectase, amylase and cellulase carry out catalytic degradation；The mass ratio of the insoluble matter and waste/hypo-tobacco leaf is 10:90-90:
10。
2. 1~10% wood fibre of the mixture gross mass of the insoluble matter or insoluble matter and waste/hypo-tobacco leaf is added
Enter and carry out mixed pulp in the mixture 1. obtained to step, is manufactured paper with pulp using conventional paper process and substrate is made.By roll paper, divide
After cutting, drying, cigarette vegetable solids fragrance is made.
Preferably, the dosage of the pectase, amylase and cellulase accounts for the insoluble matter or insoluble matter and gives up respectively
The percentage of the mixture gross mass of hypo-tobacco leaf is：Pectase 0.03%~0.1%, amylase 0.1%~0.6%, cellulose
Enzyme 0.5%~1%；Hydrolysis temperature is 30 DEG C~60 DEG C；1~4 hour catalytic degradation time.
Second aspect of the present invention discloses cigarette made from any of the above-described preparation method and is used for vegetable solids fragrance
Purposes in tobacco product.
Preferably, the cigarette is used separately as pipe tobacco with vegetable solids fragrance or is used in mixed way with common pipe tobacco.
Preferably, when cigarette vegetable solids fragrance is used in mixed way with common pipe tobacco, the adding proportion of vegetable solids fragrance is 1
~55wt%.
Compared with the existing technology, the present invention has the following advantages：
1, the present invention takes full advantage of the active ingredient and fragrance matter of vegetable solids extract, and by catalytic degradation at
Reason carries out fully degraded to pectin in insoluble matter and protein etc., produces a large amount of Maillard reaction precursor.Improve this
Adaptability and compatibility of the solid spice in cigarette composition can fully promote cigarette made of the cigarette vegetable solids fragrance
Suction quality achievees the purpose that partly or entirely to substitute tobacco leaf.
2, cigarette of the invention is used for cigarette products with vegetable solids fragrance, can enhance the style and features of tobacco product, make
Fragrance is more abundant, enhances fresh and sweet note and sense of promoting the production of body fluid, flue gas is finer and smoother, soft, preferably improves the integrated sensory of cigarette
Quality.It has been surprisingly found that, which can reduce the content of harmful substance, especially tar for cigarette products
Content reduces apparent；Water content obviously increases simultaneously.
3, the vegetable solids and waste/hypo-tobacco leaf used in the present invention, can reduce the demand to wood fibre, therefore and cigarette
The suction of reconstituted tobacco compares, can the bad breath such as substantially reduced woody odor, while also solving and cigarette enterprise contention is former
The problem of material.
4, cigarette of the invention extends the use scope of vegetables with vegetable solids fragrance, enriches the fragrance type of cigarette,
Can preferably meet the needs of cigarette product specializes.
5, the shortage problem that material is inevitably encountered in cigarette product, causes product quality to fluctuate.The present invention
Production of cigarettes raw material is enriched, alleviates the problem of raw tobacco material shortage to a certain extent, and then stable prod can be reached and matched
The purpose of side.
Specific implementation mode
With reference to specific embodiment, the present invention is described in further detail, but embodiment is not to skill of the present invention
The restriction of art scheme.Unless otherwise indicated, percentage of the present invention is mass percent.
Embodiment 1
Choose mass parts：3 portions of fennels, 1 portion of spinach, 2 portions of Chinese yams soak raw material by leaching liquor ultrasound of water after mixing
It carries 30 minutes, solid-to-liquid ratio 1:10.Isolated leaching liquor and insoluble matter after extraction.Leaching liquor is concentrated through cryogenic vacuum
It is spare after processing, by insoluble matter be added 5 times of water rettings, then by insoluble matter gross mass be separately added into 0.03% pectase, 0.6%
Amylase, 0.5% the catalyzing enzymes such as cellulase, catalytic degradation temperature is 30 DEG C, is stirred 2 hours.Then insoluble matter is pressed again
2% mass ratio is added wood fibre and carries out slurrying, then manufactures paper with pulp into substrate.By in leaching liquor uniform dip-coating to above-mentioned substrate,
After roll paper, cutting, drying, cigarette vegetable solids fragrance is made.Individually chopping and the tobacco products such as cigarette can be made, also may be used
It is mixed and made into tobacco product with pipe tobacco.
Cigarette process of the cigarette with vegetable solids fragrance routinely rolls into cigarette through flavoring, volume job contract skill.It is commented through sense organ
Inhale, overall process can obviously experience suck cigarette custom continuity and satisfaction, flue gas it is soft it is smooth, fragrance is elegant, sweet tea
Moisture feeling is good, overall comfort is good, and the ash rate tobacco ash content to burn is white.By cigarette with vegetable solids fragrance in varing proportions with cigarette
Silk is mixed with tobacco product, can embody above-mentioned sensory effects in various degree.
Cigarette is mixed with 8wt% ratios with pipe tobacco with vegetable solids fragrance, cigarette is rolled into through flavoring, volume job contract skill, orders
Entitled No. 1 cigarette.On same production line, control cigarette is rolled by identical cigarette process, control sample is that cigarette is not added to use vegetable
The normal cigarette of dish solid spice.Then national standard is pressed《The tobaccos of GB/T16447~1996 and tobacco product adjust the air with test
Environment》Adjust cigarette sample moisture content be 12%, by smoke panel test panel of expert by《The cigarette sense organ technologies of GB5606.4~1996 are wanted
It asks》Regulation carry out cigarette sensory evaluating smoking.Smoking result is shown in Table 1；Specific sense organ marking is shown in Table 2, table 3；According to GB 5606.5-
2005 pairs of cigarette carry out flue gas conventional detection, and testing result is shown in Table 4.
Embodiment 2
Choose mass parts：3 portions of balsam pears, 1 portion of Chinese cabbage, 2 portions of carrots, by raw material after mixing using water as leaching liquor ultrasound
Extraction 20 minutes, solid-to-liquid ratio 1:8.Isolated leaching liquor and insoluble matter after extraction.Leaching liquor is dense through cryogenic vacuum
Spare after contracting processing, by insoluble matter and waste/hypo-tobacco leaf, (mass ratio of insoluble matter and waste/hypo-tobacco leaf is 1:1) 7 times of water are added to soak again
Stain, then by insoluble matter and waste/hypo-tobacco leaf gross mass be separately added into 0.15% pectase, 0.3% amylase, 0.8% fiber
The catalyzing enzymes such as plain enzyme, catalytic degradation temperature are 50 DEG C, are stirred 3 hours.Insoluble matter and the total matter of waste/hypo-tobacco leaf are pressed after mixed pulp again
The mass ratio of amount 4% is added wood fibre and carries out slurrying, then manufactures paper with pulp into substrate.By the uniform dip-coating of leaching liquor to above-mentioned substrate
On, after roll paper, cutting, drying, cigarette vegetable solids fragrance is made.Individually chopping and the tobacco products such as cigarette can be made,
Also tobacco product can be mixed and made into pipe tobacco.
Cigarette process of the cigarette with vegetable solids fragrance routinely rolls into cigarette through flavoring, volume job contract skill.It is commented through sense organ
Inhale, overall process can obviously experience suck cigarette custom continuity and satisfaction, flue gas it is soft it is smooth, fragrance is elegant, sweet tea
Moisture feeling is good, overall comfort is good, and the ash rate tobacco ash content to burn is white.By cigarette with vegetable solids fragrance in varing proportions with cigarette
Silk is mixed with tobacco product, can embody above-mentioned sensory effects in various degree.
Cigarette is mixed with 6wt% ratios with pipe tobacco with vegetable solids fragrance, cigarette is rolled into through flavoring, volume job contract skill, orders
Entitled No. 2 cigarettes.On same production line, control cigarette is rolled by identical cigarette process, control sample is that cigarette is not added to use vegetable
The normal cigarette of dish solid spice.Then national standard is pressed《The tobaccos of GB/T16447~1996 and tobacco product adjust the air with test
Environment》Adjust cigarette sample moisture content be 12%, by smoke panel test panel of expert by《The cigarette sense organ technologies of GB5606.4~1996 are wanted
It asks》Regulation carry out cigarette sensory evaluating smoking.Smoking result is shown in Table 1；Specific sense organ marking is shown in Table 2, table 3；According to GB 5606.5-
2005 pairs of cigarette carry out flue gas conventional detection, and testing result is shown in Table 4.
Embodiment 3
Choose mass parts：Raw material is extracted 40 points by 3 portions of green onions, 1 portion of ginger, 2 portions of garlics by leaching liquor ultrasound of water after mixing
Clock, solid-to-liquid ratio 1:15, isolated leaching liquor and insoluble matter after extraction.Leaching liquor is after cryogenic vacuum concentration
Spare, by insoluble matter and waste/hypo-tobacco leaf, (mass ratio of insoluble matter and waste/hypo-tobacco leaf is 2:1) 10 times of water are added to impregnate again, then press
Insoluble matter and waste/hypo-tobacco leaf gross mass be separately added into 0.1% pectase, 0.3% amylase, 1% the catalysis such as cellulase
Enzyme, catalytic degradation temperature are 60 DEG C, are stirred 4 hours.The quality of insoluble matter and waste/hypo-tobacco leaf gross mass 6% is pressed after mixed pulp again
Slurrying is carried out than wood fibre is added, then manufactures paper with pulp into substrate.By in leaching liquor uniform dip-coating to above-mentioned substrate, by roll paper,
After cutting, drying, cigarette vegetable solids fragrance is made.Individually chopping and the tobacco products such as cigarette can be made, it also can be mixed with pipe tobacco
Tobacco product is made in conjunction.
Cigarette process of the cigarette with vegetable solids fragrance routinely rolls into cigarette through flavoring, volume job contract skill.It is commented through sense organ
Inhale, overall process can obviously experience suck cigarette custom continuity and satisfaction, flue gas it is soft it is smooth, fragrance is elegant, sweet tea
Moisture feeling is good, overall comfort is good, and the ash rate tobacco ash content to burn is white.By cigarette with vegetable solids fragrance in varing proportions with cigarette
Silk is mixed with tobacco product, can embody above-mentioned sensory effects in various degree.
Cigarette is mixed with 8wt% ratios with pipe tobacco with vegetable solids fragrance, cigarette is rolled into through flavoring, volume job contract skill, orders
Entitled No. 3 cigarettes.On same production line, control cigarette is rolled by identical cigarette process, control sample is that cigarette is not added to use vegetable
The normal cigarette of dish solid spice.Then national standard is pressed《The tobaccos of GB/T16447~1996 and tobacco product adjust the air with test
Environment》Adjust cigarette sample moisture content be 12%, by smoke panel test panel of expert by《The cigarette sense organ technologies of GB5606.4~1996 are wanted
It asks》Regulation carry out cigarette sensory evaluating smoking.Smoking result is shown in Table 1；Specific sense organ marking is shown in Table 2, table 3；According to GB 5606.5-
2005 pairs of cigarette carry out flue gas conventional detection, and testing result is shown in Table 4.
1 cigarette sensory evaluating smoking's result of table
2 sensory evaluation of table marking table
Table 3 aspirates evaluation table
4 flue gas conventional analysis result of table
Show that the cigarette of preparation is added to vegetable solids fragrance in cigarette by the smoking result in table 1- tables 3, sample cigarette
Smoke panel test point higher than control sample 0.4 point or more.Compared with control sample, the comfort mean height 0.6 of sample cigarette divides or so, cigarette
Gas feature mean height 0.4 divides or so, and sweet taste mean height 0.6 divides or so in taste style, 0.2 or more tart flavour mean height.Therefore originally
The cigarette of invention, which is added to vegetable solids fragrance in cigarette, can be obviously improved cigarette perfume, coordinate flue gas, increase the sweet sense of flue gas, reduce
Cigarette smoke irritation, the effect for improving user throat comfort, can increase the richness and sophistication of cigarette perfume, have preferable
Cigarette application effect.As shown in Table 4, compared with control sample, the cigarette main flue of the cigarette vegetable solids fragrance of the present invention is added
Total granules, smoking nicotine and CO decrease in gas, and especially tar content is substantially reduced, and averagely have dropped
0.80mg/ branch or so.Flue gas moisture obviously increases simultaneously, averagely increases 0.3mg/ branch or so.
Claims (8)
1. a kind of cigarette preparation method of vegetable solids fragrance, which is characterized in that step is：
(1) by vegetables flooding, leaching liquor and insoluble matter are detached；
(2) substrate is made in the insoluble matter that step (1) obtains；
(3) by the leaching liquor substrate that dip-coating is obtained to step (2) after cryogenic vacuum concentrates that step (1) obtains to get to
Cigarette vegetable solids fragrance.
2. preparation method according to claim 1, which is characterized in that the vegetables be celery, spinach, Chinese cabbage, carrot,
It is one or more in radish, Chinese yam, taro, tomato, ginger, cucumber, green onion, garlic, pumpkin, cabbage, balsam pear, fennel, cordate houttuynia
Composition.
3. preparation method according to claim 1, which is characterized in that the vegetables of step (1) and the mass ratio of water are 1:8~
1:15, ultrasound extraction, the time is 20~40 minutes.
4. preparation method according to claim 1, which is characterized in that the step of substrate is made in insoluble matter by step (2) be：
1. the mixture of the insoluble matter or insoluble matter and waste/hypo-tobacco leaf is added 5~10 times of water rettings of its quality, and pectin is added
Enzyme, amylase and cellulase carry out catalytic degradation；
2. 1~10% wood fibre of the mixture gross mass of the insoluble matter or insoluble matter and waste/hypo-tobacco leaf is added to
Mixed pulp is carried out in 1. mixture that step obtains, is manufactured paper with pulp using conventional paper process and substrate is made.
5. preparation method according to claim 4, which is characterized in that the pectase, amylase and cellulase use
Measuring the percentage of mixture gross mass for accounting for the insoluble matter or insoluble matter and waste/hypo-tobacco leaf respectively is：Pectase 0.03%~
0.1%, amylase 0.1%~0.6%, cellulase 0.5%~1%；Hydrolysis temperature is 30 DEG C~60 DEG C；The catalytic degradation time
1~4 hour.
6. a kind of being used for tobacco product according to cigarette vegetable solids fragrance made from any preparation methods of claim 1-5
In purposes.
7. purposes according to claim 6, which is characterized in that the cigarette vegetable solids fragrance makes separately as pipe tobacco
It is used in mixed way with or with common pipe tobacco.
8. purposes according to claim 7, which is characterized in that when cigarette is used in mixed way with vegetable solids fragrance and common pipe tobacco
When, the ratio of vegetable solids fragrance is 1~55wt%.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810554380.1A CN108741218A (en) | 2018-06-01 | 2018-06-01 | A kind of preparation method and purposes of cigarette vegetable solids fragrance |
| CN201910181089.9A CN109691684A (en) | 2018-06-01 | 2019-03-11 | The preparation method and its purposes in tobacco product of a kind of fragrance |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810554380.1A CN108741218A (en) | 2018-06-01 | 2018-06-01 | A kind of preparation method and purposes of cigarette vegetable solids fragrance |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108741218A true CN108741218A (en) | 2018-11-06 |
Family
ID=64001729
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810554380.1A Pending CN108741218A (en) | 2018-06-01 | 2018-06-01 | A kind of preparation method and purposes of cigarette vegetable solids fragrance |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108741218A (en) |
-
2018
- 2018-06-01 CN CN201810554380.1A patent/CN108741218A/en active Pending
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| PB01 | Publication | ||
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Application publication date: 20181106 |