CN108728582A - A kind of equipment efficiently preparing functional low polyxylose - Google Patents
A kind of equipment efficiently preparing functional low polyxylose Download PDFInfo
- Publication number
- CN108728582A CN108728582A CN201810914794.0A CN201810914794A CN108728582A CN 108728582 A CN108728582 A CN 108728582A CN 201810914794 A CN201810914794 A CN 201810914794A CN 108728582 A CN108728582 A CN 108728582A
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- efficiently preparing
- pipeline
- functional low
- preparing functional
- equipment efficiently
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- 230000001105 regulatory effect Effects 0.000 claims abstract description 30
- 238000000227 grinding Methods 0.000 claims abstract description 27
- 239000002253 acid Substances 0.000 claims abstract description 19
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 7
- 238000007789 sealing Methods 0.000 claims description 10
- 238000005119 centrifugation Methods 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 2
- 238000007599 discharging Methods 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- HEBKCHPVOIAQTA-NGQZWQHPSA-N d-xylitol Chemical compound OC[C@H](O)C(O)[C@H](O)CO HEBKCHPVOIAQTA-NGQZWQHPSA-N 0.000 abstract description 7
- 239000000463 material Substances 0.000 description 18
- 239000000843 powder Substances 0.000 description 8
- 238000010669 acid-base reaction Methods 0.000 description 6
- 238000000605 extraction Methods 0.000 description 5
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 description 4
- 238000005520 cutting process Methods 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229920001542 oligosaccharide Polymers 0.000 description 2
- 150000002482 oligosaccharides Chemical class 0.000 description 2
- FGRBYDKOBBBPOI-UHFFFAOYSA-N 10,10-dioxo-2-[4-(N-phenylanilino)phenyl]thioxanthen-9-one Chemical compound O=C1c2ccccc2S(=O)(=O)c2ccc(cc12)-c1ccc(cc1)N(c1ccccc1)c1ccccc1 FGRBYDKOBBBPOI-UHFFFAOYSA-N 0.000 description 1
- 241000186000 Bifidobacterium Species 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- -1 corncob Chemical compound 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000009700 powder processing Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 230000002459 sustained effect Effects 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C18/00—Disintegrating by knives or other cutting or tearing members which chop material into fragments
- B02C18/06—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
- B02C18/08—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives within vertical containers
- B02C18/12—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives within vertical containers with drive arranged below container
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B1/00—Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/007—Separation of sugars provided for in subclass C13K
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Sustainable Development (AREA)
- Molecular Biology (AREA)
- General Health & Medical Sciences (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Centrifugal Separators (AREA)
- Extraction Or Liquid Replacement (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The present invention provides a kind of equipment efficiently preparing functional low polyxylose, it is related to xylo-oligosaccharide preparing technical field, a kind of equipment efficiently preparing functional low polyxylose, including rotary shaft and the grinding device and centrifugal device that are set in rotary shaft, grinding device is set to centrifugal device top, regulating device is provided between grinding device and centrifugal device, grinding device includes feeding mouth, discharge port and the cutter being fixedly installed in rotary shaft, regulating device includes that acid solution enters pipe, lye enters pipe and soda acid inductor, centrifugal device includes entering pipeline, separate pipeline and for connect enter pipeline and separate pipeline connecting pipe, it is connected with collection conduit below separate pipeline, effuser is provided in collection conduit.A kind of equipment high efficiency efficiently preparing functional low polyxylose of the present invention is stablized, and extracting solution purity is high, a running body, and controllability is high, simple in structure, easy to use.
Description
Technical field
The present invention relates to xylo-oligosaccharide preparing technical field,
Especially, the present invention relates to a kind of equipment efficiently preparing functional low polyxylose.
Background technology
Xylo-oligosaccharide has the function of that Bifidobacterium is promoted to increase and improve function of intestinal canal.Compared with other oligosaccharide,
Xylo-oligosaccharide have the characteristics that dosage it is small, it is acidproof, heat-resisting, reduce and moisture and prevent from freezing, in addition its raw materials for production be it is inexpensive easily
The agricultural byproduct obtained, such as corncob, cotton seed hull etc., therefore be a kind of oligosaccharide with development prospect.Currently, domestic is oligomeric
Xylose extraction research is still in the starting stage, and the conversion ratio of xylo-oligosaccharide is relatively low, and used equipment includes pulverizer, impregnates dress
It sets, the individual equipments such as autoclave, vortex mixer, PH meter, constant-temperature shaking incubator, production efficiency is very low, then needs
Consume a large amount of cost of labor and machine cost.
Invention content
The purpose of the present invention is to provide a kind of efficient stables, and extracting solution purity is high, a running body, and controllability is high, structure
Simply, the equipment for efficiently preparing functional low polyxylose easy to use.
To solve the above problems, the present invention is adopted the following technical scheme that and is achieved：
It is a kind of efficiently prepare functional low polyxylose equipment, including rotary shaft and be set in the rotary shaft crushing dress
Set and centrifugal device, the grinding device is set to the centrifugal device top, the grinding device and the centrifugal device it
Between be provided with regulating device, the grinding device includes feeding mouth, discharge port and the cutting being fixedly installed in the rotary shaft
Knife, the regulating device include that acid solution enters pipe, lye enters pipe and soda acid inductor, and the centrifugal device includes entering to manage
Road, separate pipeline and for connecting the connecting pipe into pipeline and separate pipeline, connection below the separate pipeline
There is collection conduit, effuser is provided in the collection conduit.
Preferably, the quantity at least two of the separate pipeline.
It is further preferred that it is arc that the collection conduit is at least part of.
It is further preferred that being provided with filter screen in the connecting pipe.
It is further preferred that the discharge port and the junction of the regulating device are provided with the first sealing ring, the tune
The junction of regulating device and the centrifugal device is provided with the second sealing ring.
It is further preferred that the regulating device and the junction of the centrifugal device are provided with sliding groove.
It is further preferred that it is arc that the sliding groove is at least part of.
It is further preferred that functional protrusion is arranged in the rotary shaft, the function protrusion is at least part of to be located at
In the regulating device.
It is further preferred that the rotary shaft lower end is provided with driving motor, the driving motor passes through fixing bolt
It is fixed in fixed platform.
It is further preferred that being provided in the fixed platform for the fixed supporting beam for supporting the regulating device.
A kind of equipment advantageous effect efficiently preparing functional low polyxylose of the present invention is：Efficient stable, extracting solution are pure
Degree is high, a running body, and controllability is high, simple in structure, easy to use.
Description of the drawings
Fig. 1 is the structural schematic diagram of one embodiment of the invention；
Fig. 2 is the main structure diagram of one embodiment of the invention；
Fig. 3 is the structural schematic diagram of the centrifugal device of one embodiment of the invention；
In figure：1, grinding device, 11, feeding mouth, 12, discharge port, 13, cutter, the 14, first sealing ring, 2, centrifugal device,
21, into pipeline, 22, separate pipeline, 23, connecting pipe, 24, collection conduit, 25, effuser, 3, regulating device, 31, acid solution
Into pipe, 32, lye enter pipe, 33, soda acid inductor, the 34, second sealing ring, 35, sliding groove, 9, rotary shaft, 91, driving electricity
Machine, 92, fixed platform, 93, supporting beam, 94, function protrusion.
Specific implementation mode
The present invention is described further with reference to the accompanying drawings and examples.
Embodiment one：As shown in Figures 1 to 3, only one of present invention embodiment, a kind of efficiently preparation are functional oligomeric
The equipment of xylose, including rotary shaft 9 and the grinding device 1 and centrifugal device 2 that are set in the rotary shaft 9, the crushing
Device 1 is set to 2 top of the centrifugal device, and regulating device 3 is provided between the grinding device 1 and the centrifugal device 2,
The grinding device 1 includes feeding mouth 11, discharge port 12 and the cutter 13 being fixedly installed in the rotary shaft 9, the tune
Regulating device 3 enters pipe 31 including acid solution, lye enters pipe 32 and soda acid inductor 33, and the centrifugal device 2 includes entering pipeline
21, separate pipeline 22 and for connecting the connecting pipe 23 into pipeline 21 and separate pipeline 22, the separate pipeline
22 lower sections are connected with collection conduit 24, and effuser 25 is provided in the collection conduit 24.
Grinding device 1, functional device 3 and centrifugal device 2 are set in the rotary shaft 9 from top to bottom successively, but by
Rotary shaft 9 drive be only grinding device 1 and centrifugal device 2, and in grinding device 1 also only have cutter 13 and rotary shaft
9 are fixedly connected, and since rotary shaft 9 is rotation, centrifugal device 2 and cutter 13 are driven to be rotated.
Then it is exactly the operation principle of grinding device 1, functional device 3 and centrifugal device 2.
Grinding device 1 first, cutter 13 rotate under the drive of rotary shaft 9,1 shell of grinding device be it is motionless,
Make the material of xylo-oligosaccharide（Such as corncob, cotton seed hull etc., hereinafter referred to as material）By the feeding mouth 11 of grinding device 1 into
Enter, crushed under the cutting of cutter 13, the material powders then formed are flowed out from discharge port 12.
Followed by functional device 3, the material powders that grinding device 1 is formed are flow to from discharge port 12 in functional device 3,
Functional device 3 is also associated with that acid solution enters pipe 31 and lye enters pipe 32, each serves as the effect for flowing into acid solution and lye, material
The powder processing Jing Guo acid solution and lye successively forms fluid after being sufficiently mixed, continues to flow downward out.
In the process, it should be noted that acid solution enters pipe 31 and lye to enter pipe 32 be isolated operation, and material
In powder mixed process, the acid-base value that the soda acid inductor 33 of 3 lower part of functional device can in real time in reading device facilitates work
Personnel carry out the addition of acid solution or lye.
It is also to be noted that the rotation of rotary shaft 9 will not drive the functional device 3 to be rotated.
It is finally centrifugal device 2, material powders mixed liquor flows into after centrifugal device 2, can stay in into pipeline 21,
Since entire centrifugal device 2 follows rotary shaft 9 to be rotated, the power of generation is rotated as the centrifugal force of centrifugal device 2
There is provided, centrifugal device 2 into the fluid in pipeline 21 into cross high speed centrifugal movement, separating pipe is flowed by connecting pipe 23
Road 22, the liquid in separate pipeline 22 have been the separation liquid products by being sufficiently separated acquisition, and separating liquid is from separating pipe
Road 22 converges to collection conduit 24 and is collected, and is finally flowed out from effuser 25, just obtains final xylo-oligosaccharide extracting solution.
In the present invention, power source only only has rotary shaft 9 one, in the case where its rotation drives, completes cutting and grinding, soda acid
The work of reaction mixing and centrifugation extraction, it is simple in structure, while being conveniently operated, significantly improve existing multiple devices
The efficiency separately to work has extraction efficiency height, safety and stability, the high advantage of a running body controllability.
Embodiment two：Still as shown in Figures 1 to 3, only one of present invention embodiment, in order to ensure that the present invention's is steady
A qualitative more step improves, and a kind of equipment efficiently preparing functional low polyxylose of the present invention also has following design：
First at centrifugal device 2, the quantity at least two of the separate pipeline 22, the actually quantity one of separate pipeline 22
As at 6 or so, multiple separate pipelines 22 are uniformly distributed in into 21 surrounding of pipeline, and 22 quantity of separate pipeline is more, centrifugation
Effect is better.Since extracting solution will flow to separate pipeline 22 by connecting pipe 23 from into pipeline 21, then residual in order to prevent
The recycling of slag generates blocking, is provided with filter screen in the connecting pipe 23, prevents residue from passing through.
In centrifugal device 2, the separating liquid being finally separating in pipeline 22 converges in collecting pipe 24, collection conduit described herein
24 it is at least part of be arc, actually collection conduit 24 should be annular shape, be sequentially connected multiple separate pipelines 24.
Followed by functional device 3, since acid-base reaction needs the regular hour, then material powders are needed in function
It retains a period of time in device 3 to be reacted, then needing to be sealed in 3 top and the bottom of functional device, then the discharge port
12 are provided with the first sealing ring 14, the company of the regulating device 3 and the centrifugal device 2 with the junction of the regulating device 3
The place of connecing is provided with the second sealing ring 34, and the first sealing ring 14 is closed, and material powders stop being added to regulating device 3, can also prevent
Only air or other foreign matters, which enter to regulating device 3, influences acid-base reaction, and the second sealing ring 34 is closed, and mixed liquor then stays in tune
Sustained response is carried out in regulating device 3.
It is had an advantage that in the present invention, being exactly three devices such as grinding device 1, functional device 3 and centrifugal device 2 can divide
The work that goes into operation can also work at the same time, when the first batch materials are extracted by crushing and entering to centrifugal device 2 after acid-base reaction,
The second batch materials can be put into crush and acid-base reaction, it, can be with while even the second batch materials carry out acid-base reaction
Third batch materials are put into crush.
And in the process, can according to adjust rotary shaft 9 rotating speed come control material cutting speed, and control from
Heart extraction rate.Can play and save labour turnover, the acid-base reaction period is identical with centrifugation extracting cycle be then it is best, at this time two
A step is carried out at the same time, and when synchronous progress, can be carried out more batches of material while be processed extraction.
It is finally to ensure that the operation of the present invention is smooth, reduce loss.
Since regulating device 3 does not rotate, and centrifugal device 2 is rotated with rotation axis 9, generates rub between the two in order to prevent
It wipes, then the junction of the regulating device 3 and the centrifugal device 2 is provided with sliding groove 35, certain sliding groove 35
At least part of is arc, and the sliding groove 35 is circle.
Material powders need to ensure to be sufficiently mixed, are to be reacted with acid solution or lye in regulating device 3
Accelerate the speed of its mixing, then functional raised 94 are arranged in the rotary shaft 9, the function protrusion 94 at least one
Part is located in the regulating device 3, then carry out the agitation of ingredient in regulating device 3, accelerate material powders and acid solution or
Lye carries out hybrid reaction.
Since the upper end of rotary shaft 9 is grinding device 1, progress material is needed to devote oneself to work at grinding device 1, so rotation
The power output of shaft 9 preferably not in upper end, then, 9 lower end of the rotary shaft is provided with driving motor 91, the driving
Motor 91 is fixed to by fixing bolt in fixed platform 92.
Since regulating device 3 is not connect with rotary shaft 9, Gu it does not support, so being arranged in the fixed platform 92
It is useful for the fixed supporting beam 93 for supporting the regulating device 3.
A kind of equipment high efficiency efficiently preparing functional low polyxylose of the present invention is stablized, and extracting solution purity is high, a running body,
Controllability is high, simple in structure, easy to use.
The present invention is not limited to above-mentioned specific embodiment, and the invention may be variously modified and varied.Every foundation
The technical spirit of the present invention should be included in the present invention to embodiment of above any modification, equivalent replacement, improvement and so on
Protection domain.
Claims (10)
1. a kind of equipment efficiently preparing functional low polyxylose, it is characterised in that：Including rotary shaft（9）And it is set to described
Rotary shaft（9）On grinding device（1）And centrifugal device（2）, the grinding device（1）It is set to the centrifugal device（2）On
Portion, the grinding device（1）With the centrifugal device（2）Between be provided with regulating device（3）, the grinding device（1）Including
Feeding mouth（11）, discharge port（12）Be fixedly installed on the rotary shaft（9）On cutter（13）, the regulating device（3）
Enter pipe including acid solution（31）, lye enter pipe（32）With soda acid inductor（33）, the centrifugal device（2）Including entering pipeline
（21）, separate pipeline（22）And it is described into pipeline for connecting（21）And separate pipeline（22）Connecting pipe（23）, institute
State separate pipeline（22）Lower section is connected with collection conduit（24）, the collection conduit（24）On be provided with effuser（25）.
2. a kind of equipment efficiently preparing functional low polyxylose according to claim 1, it is characterised in that：The separation
Pipeline（22）Quantity at least two.
3. a kind of equipment efficiently preparing functional low polyxylose according to claim 1, it is characterised in that：The collection
Pipeline（24）At least part of is arc.
4. a kind of equipment efficiently preparing functional low polyxylose according to claim 1, it is characterised in that：The connection
Pipeline（23）In be provided with filter screen.
5. a kind of equipment efficiently preparing functional low polyxylose according to claim 1, it is characterised in that：The discharging
Mouthful（12）With the regulating device（3）Junction be provided with the first sealing ring（14）, the regulating device（3）With the centrifugation
Device（2）Junction be provided with the second sealing ring（34）.
6. a kind of equipment efficiently preparing functional low polyxylose according to claim 1, it is characterised in that：The adjusting
Device（3）With the centrifugal device（2）Junction be provided with sliding groove（35）.
7. a kind of equipment efficiently preparing functional low polyxylose according to claim 6, it is characterised in that：The sliding
Slot（35）At least part of is arc.
8. a kind of equipment efficiently preparing functional low polyxylose according to claim 1, it is characterised in that：The rotation
Axis（9）The upper functional protrusion of setting（94）, the function protrusion（94）It is at least part of to be located at the regulating device（3）It is interior.
9. a kind of equipment efficiently preparing functional low polyxylose according to claim 1, it is characterised in that：The rotation
Axis（9）Lower end is provided with driving motor（91）, the driving motor（91）It is fixed to fixed platform by fixing bolt（92）
On.
10. a kind of equipment efficiently preparing functional low polyxylose according to claim 9, it is characterised in that：It is described solid
Fixed platform（92）On be provided with and support the regulating device for fixed（3）Supporting beam（93）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810914794.0A CN108728582A (en) | 2018-08-13 | 2018-08-13 | A kind of equipment efficiently preparing functional low polyxylose |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810914794.0A CN108728582A (en) | 2018-08-13 | 2018-08-13 | A kind of equipment efficiently preparing functional low polyxylose |
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| Publication Number | Publication Date |
|---|---|
| CN108728582A true CN108728582A (en) | 2018-11-02 |
Family
ID=63942857
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810914794.0A Withdrawn CN108728582A (en) | 2018-08-13 | 2018-08-13 | A kind of equipment efficiently preparing functional low polyxylose |
Country Status (1)
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| CN (1) | CN108728582A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114392811A (en) * | 2022-01-17 | 2022-04-26 | 皖西卫生职业学院 | Visual centrifugal extraction device and extraction method for natural medicine |
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Application publication date: 20181102 |