CN108704770A - 一种氧化铝陶瓷花洒及其制备方法 - Google Patents
一种氧化铝陶瓷花洒及其制备方法 Download PDFInfo
- Publication number
- CN108704770A CN108704770A CN201810853424.0A CN201810853424A CN108704770A CN 108704770 A CN108704770 A CN 108704770A CN 201810853424 A CN201810853424 A CN 201810853424A CN 108704770 A CN108704770 A CN 108704770A
- Authority
- CN
- China
- Prior art keywords
- aluminium oxide
- shower
- oxide ceramics
- product
- count
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 title claims abstract description 138
- 239000000919 ceramic Substances 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- 229910052593 corundum Inorganic materials 0.000 claims abstract description 17
- 229910001845 yogo sapphire Inorganic materials 0.000 claims abstract description 17
- MCMNRKCIXSYSNV-UHFFFAOYSA-N ZrO2 Inorganic materials O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims abstract description 16
- AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Inorganic materials [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 claims abstract description 15
- 239000004615 ingredient Substances 0.000 claims abstract description 14
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 13
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 13
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000012222 talc Nutrition 0.000 claims abstract description 12
- 239000000454 talc Substances 0.000 claims abstract description 12
- 229910052623 talc Inorganic materials 0.000 claims abstract description 12
- 239000000463 material Substances 0.000 claims description 15
- 239000012188 paraffin wax Substances 0.000 claims description 15
- 239000002994 raw material Substances 0.000 claims description 14
- 239000001993 wax Substances 0.000 claims description 13
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 12
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 12
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 12
- 239000005642 Oleic acid Substances 0.000 claims description 12
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 12
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 12
- 239000012535 impurity Substances 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 10
- 238000005245 sintering Methods 0.000 claims description 10
- 235000015895 biscuits Nutrition 0.000 claims description 9
- 238000004140 cleaning Methods 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 6
- 238000001514 detection method Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000004018 waxing Methods 0.000 claims description 6
- 238000003860 storage Methods 0.000 claims description 5
- 238000010304 firing Methods 0.000 claims description 4
- 238000012797 qualification Methods 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 claims description 3
- 238000000498 ball milling Methods 0.000 claims description 3
- 230000008030 elimination Effects 0.000 claims description 3
- 238000003379 elimination reaction Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 238000002347 injection Methods 0.000 claims description 3
- 239000007924 injection Substances 0.000 claims description 3
- 238000007689 inspection Methods 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 238000000465 moulding Methods 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 238000007873 sieving Methods 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims 4
- 238000005516 engineering process Methods 0.000 abstract description 4
- 230000007797 corrosion Effects 0.000 abstract description 3
- 238000005260 corrosion Methods 0.000 abstract description 3
- 230000003670 easy-to-clean Effects 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- ZQPPMHVWECSIRJ-MDZDMXLPSA-N elaidic acid Chemical compound CCCCCCCC\C=C\CCCCCCCC(O)=O ZQPPMHVWECSIRJ-MDZDMXLPSA-N 0.000 description 8
- 238000004364 calculation method Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000004568 cement Substances 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B1/00—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means
- B05B1/14—Nozzles, spray heads or other outlets, with or without auxiliary devices such as valves, heating means with multiple outlet openings; with strainers in or outside the outlet opening
- B05B1/18—Roses; Shower heads
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3244—Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/349—Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/442—Carbonates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/612—Machining
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/77—Density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9669—Resistance against chemicals, e.g. against molten glass or molten salts
- C04B2235/9692—Acid, alkali or halogen resistance
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Nozzles (AREA)
Abstract
一种氧化铝陶瓷花洒及其制备方法，克服了现有技术陶瓷花洒结构复杂，不易于清洗和耐腐蚀性差的问题，特征是花洒主体呈喇叭状的筒体，在喇叭状筒体的底部设有出水板，在出水板上设有若干个出水孔，在花洒主体的上端设有圆柱形凸起，并在该圆柱形凸起的外缘设有外螺纹，所述氧化铝陶瓷花洒采用的主料配方（按重量百分比计算）为：Al2O3 92～96%，BaCO3 0.5～3%，Si02 1～4%，高岭土1～4%，滑石0.5～3%，ZrO2 0.3～2%，所述氧化铝陶瓷花洒制备方法采用热压成型工艺制作，有益效果是结构简单，花洒的整体结构均为氧化铝陶瓷，表面光滑平整，易于清洗，且提高了产品的耐腐蚀性能。
Description
技术领域
本发明属于花洒技术领域，特别是涉及一种氧化铝陶瓷花洒及其制备方法。
背景技术
花洒是淋浴时的出水喷头，现有技术中，常见的花洒多是金属的或塑胶的，这些喷头长期使用容易出现塑胶老化问题或者金属锈化问题，使花洒的使用寿命缩短。申请号为200910309295.X的发明公开了一种淋浴龙头，该发明包括工字形结构的龙头主体、冷水及热水进水口、冷热水混合阀芯、出水功能切换阀芯，在龙头主体内设有冷水与热水混合腔、热水及冷水通道、温水通道、顶淋大花洒及侧淋小花洒接口、与冷热水混合阀芯相配的阀座、与出水功能切换阀芯相配的阀座，该发明只是在出水功能的切换阀芯的四通阀芯的阀瓣材料为精磨氧化铝陶瓷片。申请号为201520135547.2的实用新型公开了一种陶瓷喷嘴花洒，包括依次连接的连接件、过滤器、花洒主体和喷头，喷头与花洒主体通过螺纹连接，喷头上设有多个均匀分布的陶瓷喷嘴，陶瓷喷嘴为氧化铝陶瓷构造的中空的锥体，过滤器内部依次固定有金属丝网层、海绵层以及活性炭层，过滤器分别通过螺纹与连接件和花洒主体连接。该实用新型所述陶瓷喷嘴花洒，也只是花洒主体和喷嘴为氧化铝陶陶瓷，且结构复杂。
发明内容
本发明所要解决的技术问题是，克服现有技术的不足之处，提供一种结构简单，花洒整体结构均为氧化铝陶瓷的一种氧化铝陶瓷花洒及其制备方法。
本发明所述一种氧化铝陶瓷花洒，包括花洒主体，所述花洒主体呈喇叭状的筒体，该呈喇叭状筒体的顶部开口形成进水口，在喇叭状筒体的底部设有出水板，进水口与出水板之间为中空腔，在出水板上设有若干个出水孔，在花洒主体的上端设有圆柱形凸起，并在该圆柱形凸起的外缘设有外螺纹，所述氧化铝陶瓷花洒采用的氧化铝陶瓷的主料配方（按重量百分比计算）为：Al2O3（92～96）% ，BaCO3(0.5～3)%，Si02（1～4）%，高岭土（1～4）% ，滑石（0.5～3）%，ZrO2（0.3～2）% ；辅料配方（按重量百分比计算）为：油酸1％～1.2%，石蜡15%～17%。
所述氧化铝陶瓷花洒采用的氧化铝陶瓷的主料配方（按重量百分比计算）为：Al2O3 94%，BaCO3 1.1% ，高岭土1.4%，Si02 2.4% ，滑石0.7%， ZrO2 1.4%，辅料配方（按重量百分比计算）为：油酸1％，石蜡 16%。
所述氧化铝陶瓷花洒采用的氧化铝陶瓷的主料配方（按重量百分比计算）为：Al2O3 94.7% ， BaCO3 0.5%，高岭土1.6%，Si02 1.2%，滑石1.0%，ZrO2 1.0%，辅料配方（按重量百分比计算）为：油酸1.2%，石蜡15%。
所述氧化铝陶瓷花洒采用的氧化铝陶瓷的主料配方（按重量百分比计算）为：Al2O3 92.5% ，BaCO3 1.1%，高岭土2.2%，Si023.2%，滑石0.7%，ZrO2 0.3%，辅料配方（按重量百分比计算）为： 油酸1％，石蜡17%。
本发明所述一种氧化铝陶瓷花洒制备方法，其特征在于，采用热压成型工艺并采用如下步骤：
第一步，去杂：首先将各种原料进行精加工处理，即进行除铁、过筛、去除杂质，改善其表面形状和大小，将Al2O3原料的密度控制在3.91～3.93g/cm³；
第二步，配料球磨：按配方比准确称取各种原料：将称好的各种原料投入球磨机中，研磨32小时，并用激光粒度分析仪检测粉料的细度，细度D50<5μm，将磨好的料放出后备用；
第三步，加蜡搅拌：取15%～17%石蜡化开，筛除杂质，放入合蜡桶中，保持恒温100℃，将磨好的料慢慢地加入合料桶中，边加边搅拌；
第四步，热压成型：搅拌好的料要进行真空，真空度≤-0.1MPa，保温70 ℃，将真空好的料浆加入成型机内，保持料温65℃注入模具中待稍冷，卸压后脱模取出产品；
第五步，排蜡：把压好的产品经过检查人员检查合格后转入排蜡工序，将产品埋入吸附粉中，产品之间要有一定的距离，缓慢升温让产品中的蜡通过吸附粉缓慢排除掉并使产品有一定的强度，便于后期清理和修坯；
第六步，修坯：将排完蜡的产品经过修坯人员修整，保证毛坯无磕碰、无坑、无裂纹等缺陷；
第七步，烧结：把产品按一定的高度放在推板上，按照合理升温曲线进行烧制，烧结温度为1600～1650℃；
第八步，清洗：烧结好的产品进行尺寸和外观检测，合格后转入下道工序；
第九步，施釉：将产品的表面喷釉，釉层厚度在0.2～0.3mm，然后进行釉烧，釉面烧结温度为1450～1470℃；
第十步，釉烧后的产品检验合格后打包入库。
与现有技术相比，本发明的有益效果是：
（1）本发明结构简单，花洒的整体结构均为氧化铝陶瓷，并在花洒主体、圆柱形凸起、外螺纹和出水板的外表面均设有釉层，表面光滑平整，易于清洗，使用时通过花洒主体上端圆柱形凸起的外缘设有的外螺纹与花洒手柄连接即可使用；
（2）本发明由于在原料配制之前将各种原料进行精加工处理，改善其表面形状，因此采用的Al2O3粉为高纯料，有机物少、杂质少、同时增加了ZrO2的含量，提高了产品的耐腐蚀性，可耐酸≤0.7mg/cm²，耐碱≤0.1mg/ cm²，产品的韧性和使用寿命也有所提高，产品硬度由原来的≥HRA65增加到≥HRA70，抗折强度大于320MPa，密度可达到>3.8g/cm3以上；
（3）本发明由于蜡比减少，降低了产品的变形量，提高了产品的合格率，相应地降低了产品的成本；
（4）本发明烧结温度降至1600～1650℃，由于烧结温度降低，可节能20～30%。
附图说明
图1是本发明的主视图；
图2是图1所示的俯视图；
图3是图1所示的仰视图；
图4是图1的A-A剖视图。
图中：1.花洒主体；2.圆柱形凸起；3.外螺纹；4.中空腔；5.出水板；6.出水孔。
具体实施方式
具体实施方式1
如图1～图4所示，本发明所述氧化铝陶瓷花洒采用的技术方案包括花洒主体1，所述花洒主体1是一个采用氧化铝陶瓷制作的呈喇叭状的筒体，该呈喇叭状筒体的顶部开口形成进水口，该呈喇叭状筒体的底部为出水板5，进水口与出水板5之间为中空腔4，该中空腔4既是储水腔也是出水腔，在出水板5上设有若干个出水孔6，在花洒主体1的上端设有圆柱形凸起2，并在该圆柱形凸起2的外缘设有与花洒手柄连接的外螺纹3，在花洒主体1、圆柱形凸起2、外螺纹3和出水板5的外表面均设有釉层。
所述氧化铝陶瓷花洒采用的氧化铝陶瓷的主料配方（按重量百分比计算）为Al2O3（92～96）% ，BaCO3(0.5～3)% ，Si02（1～4）%，高岭土（1～4）%，滑石（0.5～3）%，
ZrO2（0.3～2）% ；辅料为：油酸1％～1.2%，石蜡15%～17%。
具体实施方式2
与具体实施方式1相同，区别在于，主料配方为：Al2O3 94%，BaCO3 1.1% ， 高岭土1.4%，Si02 2.4% ，滑石0.7%， ZrO2 1.4%，辅料配方为：油酸1％，石蜡 16%。
具体实施方式3
与具体实施方式1相同，区别在于，主料配方为：Al2O3 94.7% ， BaCO3 0.5% ， 高岭土1.6% ， Si02 1.2% ，滑石1.0% ， ZrO2 1.0% ， 辅料配方为：油酸1.2% ，石蜡15%。
具体实施方式4
与具体实施方式1相同，区别在于，主料配方为：Al2O3 92.5%，BaCO3 1.1% 高岭土2.2%，Si02 3.2% ， 滑石0.7% ，ZrO2 0.3%，辅料配方为： 油酸1％，石蜡17%。
具体实施方式5
本发明所述氧化铝陶瓷花洒的制备方法为热压成型工艺，主料配方和辅料配方与具体实施方式1或具体实施方式2或具体实施方式3或具体实施方式4相同，制备方法为：
第一步，去杂：首先将各种原料进行精加工处理，即进行除铁、过筛、去除杂质，改善其表面形状和大小，将Al2O3原料的密度控制在3.91～3.93g/cm3（克/立方厘米）；
第二步，配料球磨：按配方比准确称取各种原料：将称好的各种原料投入球磨机中，研磨32小时，并用激光粒度分析仪检测粉料的细度，细度D50<5μm，将磨好的料放出后备用；
第三步，加蜡搅拌：取15%～17%的石蜡化开，筛除杂质，放入合蜡桶中，保持恒温100℃，将磨好的料慢慢地加入合料桶中，边加边搅拌；
第四步，热压成型：搅拌好的料要进行真空，真空度≤-0.1MPa，保温70 ℃，将真空好的料浆加入成型机内，保持料温65℃注入模具中待稍冷，卸压后脱模取出产品；
第五步，排蜡：把压好的产品经过检查人员检查合格后转入排蜡工序，将产品埋入吸附粉中，产品之间留有一定的距离，缓慢升温让产品中的蜡通过吸附粉缓慢排除掉并使产品有一定的强度，便于后期清理和修坯；
第六步，修坯：将排完蜡的产品经过修坯人员修整，保证毛坯无磕碰、无坑、无裂纹等缺陷；
第七步，烧结：把产品按一定的高度放在推板上，按照合理升温曲线进行烧制，烧结温度为1600～1650℃；
第八步，清洗：烧结好的产品进行尺寸和外观检测，合格后转入下道工序，初检后的产品如果不需磨削可以直接打包入库，如果需要磨削，需要按照图纸要求进行加工，然后进行清洗，清洗好后检查；
第九步，施釉：将产品的表面喷釉，釉层厚度在0.2～0.3mm，然后进行釉烧，釉烧温度在1450～1470℃，使产品表面光泽，易于清洗和增加产品的强度；
第十步，釉烧后的产品检验合格后打包入库。
Claims (5)
1.一种氧化铝陶瓷花洒，包括花洒主体（1），所述花洒主体（1）呈喇叭状的筒体，该呈喇叭状筒体的顶部开口形成进水口，其特征在于，在喇叭状筒体的底部设有出水板（5），进水口与出水板（5）之间为中空腔（4），在出水板（5）上设有若干个出水孔（6），在花洒主体（1）的上端设有圆柱形凸起（2），并在该圆柱形凸起（2）的外缘设有外螺纹（3），所述氧化铝陶瓷花洒采用的氧化铝陶瓷的主料配方（按重量百分比计算）为：Al2O3 92～96%，BaCO3 0.5～3%，Si02 1～4%，高岭土1～4%，滑石0.5～3%，ZrO2 0.3～2% ；辅料配方（按重量百分比计算）为：油酸1％～1.2%，石蜡15%～17%。
2.根据权利要求1所述的一种氧化铝陶瓷花洒，其特征在于，所述氧化铝陶瓷花洒采用的氧化铝陶瓷的主料配方（按重量百分比计算）为：Al2O3 94%，BaCO3 1.1% ， 高岭土1.4%，Si02 2.4% ，滑石0.7%， ZrO2 1.4%，辅料配方（按重量百分比计算）为：油酸1％，石蜡 16%。
3. 根据权利要求1所述的一种氧化铝陶瓷花洒，其特征在于，所述氧化铝陶瓷花洒采用的氧化铝陶瓷的主料配方（按重量百分比计算）为：Al2O3 94.7% ， BaCO3 0.5%，高岭土1.6%，Si02 1.2%，滑石1.0%，ZrO2 1.0%，辅料配方（按重量百分比计算）为：油酸1.2% ，石蜡15%。
4. 根据权利要求1所述的一种氧化铝陶瓷花洒，其特征在于，所述氧化铝陶瓷花洒采用的氧化铝陶瓷的主料配方（按重量百分比计算）为：Al2O3 92.5% ，BaCO3 1.1%，高岭土2.2%，Si02 3.2%，滑石0.7%，ZrO2 0.3%，辅料配方（按重量百分比计算）为：油酸1％，石蜡17%。
5.一种如权利要求2或3或4或5所述的氧化铝陶瓷花洒制备方法，其特征在于，采用热压成型工艺并采用如下步骤：
第一步，去杂：首先将各种原料进行精加工处理，即进行除铁、过筛、去除杂质，改善其表面形状和大小，将Al2O3原料的密度控制在3.91～3.93g/cm³（克/立方厘米）；
第二步，配料球磨：按配方比准确称取各种原料：将称好的各种原料投入到球磨机中，研磨32小时，并用激光粒度分析仪检测粉料的细度，细度D50<5μm，将磨好的料放出后备用；
第三步，加蜡搅拌：取15%～17%石蜡化开，筛除杂质，放入合蜡桶中，保持恒温100℃，将磨好的料慢慢地加入合料桶中，边加边搅拌；
第四步，热压成型：搅拌好的料要进行真空，真空度≤-0.1MPa，保温70 ℃，将真空好的料浆加入成型机内，保持料温65℃注入模具中待稍冷，卸压后脱模取出产品；
第五步，排蜡：把压好的产品经过检查人员检查合格后转入排蜡工序，将产品埋入吸附粉中，产品之间留有一定的距离，缓慢升温让产品中的蜡通过吸附粉缓慢排除掉并使产品有一定的强度，便于后期清理和修坯；
第六步，修坯：将排完蜡的产品经过修坯人员修整，保证毛坯无磕碰、无坑、无裂纹等缺陷；
第七步，烧结：把产品按一定的高度放在推板上，按照合理升温曲线进行烧制，烧结温度为1600～1650℃；
第八步，清洗：烧结好的产品进行尺寸和外观检测，合格后转入下道工序，
第九步，施釉：将产品的表面喷釉，釉层厚度在0.2～0.3mm，然后进行釉烧，釉面烧结温度为1450～1470℃；
第十步，釉烧后的产品检验合格后打包入库。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810853424.0A CN108704770A (zh) | 2018-07-30 | 2018-07-30 | 一种氧化铝陶瓷花洒及其制备方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810853424.0A CN108704770A (zh) | 2018-07-30 | 2018-07-30 | 一种氧化铝陶瓷花洒及其制备方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108704770A true CN108704770A (zh) | 2018-10-26 |
Family
ID=63874386
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810853424.0A Pending CN108704770A (zh) | 2018-07-30 | 2018-07-30 | 一种氧化铝陶瓷花洒及其制备方法 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108704770A (zh) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111266590A (zh) * | 2020-01-21 | 2020-06-12 | 中科英冠(厦门)陶瓷科技有限公司 | 陶瓷金属化原料、陶瓷金属化的方法及金属化陶瓷 |
| CN112317457A (zh) * | 2020-09-27 | 2021-02-05 | 山东国晶新材料有限公司 | 一种氧化铝陶瓷制品的清洗方法 |
| CN113277838A (zh) * | 2021-07-02 | 2021-08-20 | 深圳艾利佳材料科技有限公司 | 一种一次烧结氧化铝陶瓷上釉方法及制品 |
| US20220033315A1 (en) * | 2020-07-31 | 2022-02-03 | Xinxing Electronic Ceramics Co., Ltd | Preparation method of alumina ceramic valve core ceramic chip and product thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1390648A (zh) * | 2002-05-06 | 2003-01-15 | 蒋龙福 | 脱硫除尘用锥形螺旋喷头及制造方法和模具 |
| CN102070342A (zh) * | 2010-08-02 | 2011-05-25 | 湖南华联特种陶瓷有限公司 | 一种陶瓷饰品生产方法 |
| CN205550630U (zh) * | 2016-04-26 | 2016-09-07 | 傅文疆 | 一种带有增压装置的花洒 |
| CN106587943A (zh) * | 2015-10-16 | 2017-04-26 | 新化县顺达电子陶瓷有限公司 | 一种氧化铝和氧化锆复合陶瓷 |
| CN106747351A (zh) * | 2016-11-29 | 2017-05-31 | 伍志文 | 氧化铝增韧陶瓷水龙头主体及配件的制造工艺 |
-
2018
- 2018-07-30 CN CN201810853424.0A patent/CN108704770A/zh active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1390648A (zh) * | 2002-05-06 | 2003-01-15 | 蒋龙福 | 脱硫除尘用锥形螺旋喷头及制造方法和模具 |
| CN102070342A (zh) * | 2010-08-02 | 2011-05-25 | 湖南华联特种陶瓷有限公司 | 一种陶瓷饰品生产方法 |
| CN106587943A (zh) * | 2015-10-16 | 2017-04-26 | 新化县顺达电子陶瓷有限公司 | 一种氧化铝和氧化锆复合陶瓷 |
| CN205550630U (zh) * | 2016-04-26 | 2016-09-07 | 傅文疆 | 一种带有增压装置的花洒 |
| CN106747351A (zh) * | 2016-11-29 | 2017-05-31 | 伍志文 | 氧化铝增韧陶瓷水龙头主体及配件的制造工艺 |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111266590A (zh) * | 2020-01-21 | 2020-06-12 | 中科英冠(厦门)陶瓷科技有限公司 | 陶瓷金属化原料、陶瓷金属化的方法及金属化陶瓷 |
| US20220033315A1 (en) * | 2020-07-31 | 2022-02-03 | Xinxing Electronic Ceramics Co., Ltd | Preparation method of alumina ceramic valve core ceramic chip and product thereof |
| US11834380B2 (en) * | 2020-07-31 | 2023-12-05 | Xinxing Electronic Ceramics Co., Ltd | Preparation method of alumina ceramic valve core ceramic chip and product thereof |
| CN112317457A (zh) * | 2020-09-27 | 2021-02-05 | 山东国晶新材料有限公司 | 一种氧化铝陶瓷制品的清洗方法 |
| CN113277838A (zh) * | 2021-07-02 | 2021-08-20 | 深圳艾利佳材料科技有限公司 | 一种一次烧结氧化铝陶瓷上釉方法及制品 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108704770A (zh) | 一种氧化铝陶瓷花洒及其制备方法 | |
| CN106882961B (zh) | 一种易洁日用瓷器及其制备方法 | |
| CN101844910B (zh) | 一种薄壁轻量化卫生陶瓷坯体及其制造方法 | |
| CN107473708B (zh) | 一种慢导热、高强度陶瓷制品及其制造工艺 | |
| CN103531315B (zh) | ±1120kV特高压直流棒形瓷绝缘子制备方法 | |
| CN111056818B (zh) | 高透明抛光陶瓷厚板及其制备方法 | |
| CN110117184A (zh) | 一种耐磨损日用陶瓷及其制备方法 | |
| CN109851376B (zh) | 一种锡槽底砖及其制备方法、用于制备锡槽底砖的组合物 | |
| CN108706961B (zh) | 一种实验台环保型陶瓷面板及其制备方法 | |
| CN108547421B (zh) | 一次烧成发泡陶瓷装饰板材及其制备方法 | |
| CN101181798A (zh) | 一种陶瓷注浆成型用多层梯度多孔陶瓷模具及制作方法 | |
| CN109020481A (zh) | 一种高强度耐污瓷砖及其制备方法 | |
| CN102060542A (zh) | 熔融石英陶瓷坩埚的制备方法 | |
| CN113400442B (zh) | 采用实心粉料制作釉面砖的方法 | |
| CN101717274A (zh) | 一种陶瓷喷墨打印用棕色颜料及其制备方法 | |
| CN106518043A (zh) | 低成本铝钙硅质锡槽底砖的制备方法 | |
| CN107032771A (zh) | 一种石英陶瓷坩埚的制造方法 | |
| CN108439801B (zh) | 一次烧成发泡通体装饰板材及其制备方法 | |
| CN107540346B (zh) | 一种耐高温的陶瓷烘焙碗及其制作工艺 | |
| CN111039699B (zh) | 一种具有负离子功能的超大规格薄型瓷质板材及其生产方法 | |
| CN108484116A (zh) | 卫生陶瓷高压成型用浆料及其制备方法和高压成型方法 | |
| CN106542848B (zh) | 具有保温性能的日用多孔复合陶瓷及其制备方法 | |
| CN101328084B (zh) | 电真空器件用中温釉配方及制备工艺 | |
| CN108530035A (zh) | 一种高性能日用陶瓷及其制备方法 | |
| CN115073132A (zh) | 一种细腻面纯色超薄岩板 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information | ||
| CB02 | Change of applicant information |
Address after: 121213 No. 13E 104, Shanghai Road Section 5, Linghe District, Jinzhou City, Liaoning Province Applicant after: Mo Guangguang Address before: 121213 No. 13E 104, Shanghai Road Section 5, Linghe District, Panjin City, Liaoning Province Applicant before: Mo Guangguang |
|
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20181026 |