CN108703940A - A kind of water chestnut facial mask liquid and preparation method thereof, water chestnut facial mask - Google Patents
A kind of water chestnut facial mask liquid and preparation method thereof, water chestnut facial mask Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K2800/72—Hypo-allergenic
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
The present invention relates to a kind of water chestnut facial mask liquid and preparation method thereof, water chestnut facial masks, belong to cosmetic field.The raw material of facial mask liquid include the oligopeptides -1 of 1-4wt%, the Herba Saussureae Involueratae extract of 0.5-3wt%, the glycerine of 2-4wt%, the reed fragrant plant oil of 1-3wt%, the amino acid humectant of 1-4wt%, 0.05-0.5wt% bacillus/glutamic acid fermentation Product filtrate, the Sodium Hyaluronate of 0.1-0.3wt% and 3-10wt% water chestnut, surplus is purified water.The facial mask liquid is safe and non-toxic, is free of preservative substance, and smell is naturally pure, non-stimulated to skin, has preferable preserving moisture and protecting skin effect.Preparation method includes mixing above-mentioned each raw material according to the ratio.This method is simple and quick, and condition controllability is good, is suitable for large-scale production.Water chestnut facial mask containing above-mentioned water chestnut facial mask liquid, wide application of the crowd, skin effect are preferable.
Description
Technical field
The present invention relates to cosmetic fields, and more particularly to a kind of water chestnut facial mask liquid and preparation method thereof, water chestnut facial mask.
Background technology
In today of epoch fast development, the economic consumption level of people is higher and higher, and life is become better and better, but surrounding
Environment be but not equal to before, in addition the influence at people's unhealthy habit and age, the skin of human body face will appear
Many problems, such as skin aging, drying, pigmentation, long whelk, fat secretion exception.For above-mentioned problem, people
And develop various anti-acnes, anti-ageing, face cleaning, various skin care item such as moisturizing and whitening etc., the usage amount of wherein facial mask is
It is maximum.
The requirement of attention with people to Product Safety, natural skin care product is higher and higher, facial mask production at this stage
Product cannot meet the needs of people.And most of mask product all uses chemical preservative, and long-time service can be to human body
Skin causes certain injury.
Invention content
The purpose of the present invention is to provide the materials safety of a kind of water chestnut facial mask liquid, the water chestnut facial mask liquid is nontoxic, without anti-
Rotten substance, smell is naturally pure, non-stimulated to skin, has preferable preserving moisture and protecting skin effect.
The second object of the present invention is to provide a kind of preparation method of above-mentioned water chestnut facial mask liquid, and this method is simple and quick,
Condition controllability is good, is suitable for large-scale production.
The third object of the present invention is to provide a kind of water chestnut facial mask including above-mentioned water chestnut facial mask liquid, which is applicable in people
Group is wide, and skin effect is preferable.
The present invention solves its technical problem using following technical scheme to realize：
The present invention proposes a kind of water chestnut facial mask liquid, and raw material includes the lanatechead saussurea herb with flower of the oligopeptides -1 of 1-4wt%, 0.5-3wt%
The gemma of extract, the glycerine of 2-4wt%, the reed fragrant plant oil of 1-3wt%, the amino acid humectant of 1-4wt%, 0.05-0.5wt%
The water chestnut of bacillus/glutamic acid fermentation Product filtrate, the Sodium Hyaluronate of 0.1-0.3wt% and 3-10wt%, surplus are purifying
Water.
The present invention also proposes the preparation method of above-mentioned water chestnut facial mask liquid：Oligopeptides -1, Herba Saussureae Involueratae extract, sweet is mixed according to the ratio
Oil, reed fragrant plant oil, amino acid humectant, bacillus/glutamic acid fermentation Product filtrate, Sodium Hyaluronate, water chestnut and purified water.
The present invention also proposes a kind of water chestnut facial mask comprising above-mentioned water chestnut facial mask liquid.
Water chestnut facial mask liquid that present pre-ferred embodiments provide and preparation method thereof, the advantageous effect of water chestnut facial mask include：
The materials safety for the water chestnut facial mask liquid that present pre-ferred embodiments provide is nontoxic, is free of preservative substance, and smell is natural
It is pure, it is non-stimulated to skin, there is preferable preserving moisture and protecting skin effect.Preparation method is simple and quick, and condition controllability is good, is suitable for
Large-scale production.Water chestnut facial mask containing above-mentioned water chestnut facial mask liquid, wide application of the crowd, skin effect are preferable.
Specific implementation mode
It in order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below will be in the embodiment of the present invention
Technical solution be clearly and completely described.The person that is not specified actual conditions in embodiment, builds according to normal condition or manufacturer
The condition of view carries out.Reagents or instruments used without specified manufacturer is the conventional production that can be obtained by commercially available purchase
Product.
Water chestnut facial mask liquid of the embodiment of the present invention and preparation method thereof, water chestnut facial mask are specifically described below.
The present invention water chestnut facial mask liquid raw material include the oligopeptides -1 of 1-4wt%, 0.5-3wt% Herba Saussureae Involueratae extract,
Bacillus/paddy of the glycerine of 2-4wt%, the reed fragrant plant oil of 1-3wt%, the amino acid humectant of 1-4wt%, 0.05-0.5wt%
Propylhomoserin tunning filtrate, the Sodium Hyaluronate of 0.1-0.3wt% and 3-10wt% water chestnut, surplus is purified water.
In some specific embodiments, raw material includes the lanatechead saussurea herb with flower extraction of the oligopeptides -1 of 2-3wt%, 1-2.5wt%
Object, the glycerine of 2.5-3.5wt%, the reed fragrant plant oil of 1.5-2.5wt%, the amino acid humectant of 2-3wt%, 0.2-0.4wt%
The water chestnut of bacillus/glutamic acid fermentation Product filtrate, the Sodium Hyaluronate of 0.15-0.25wt% and 5-8wt%, surplus are
Purified water.
In other specific embodiments, raw material include the oligopeptides -1 of 2.5wt%, 2wt% Herba Saussureae Involueratae extract,
Bacillus/glutamic acid fermentation of the glycerine of 3wt%, the reed fragrant plant oil of 2wt%, the amino acid humectant of 2.5wt%, 0.3wt%
The water chestnut of Product filtrate, the Sodium Hyaluronate of 0.2wt% and 6.5wt%, surplus are purified water.
Wherein, oligopeptides -1 is also known as epidermal growth factor (EGF), is a kind of polypeptide being made of 53 amino acid residues.
In this application, oligopeptides -1 preferably uses the oligopeptides-that Guangzhou no added doctrine cosmetics Co., Ltd voluntarily produces
1.The oligopeptides -1 is fermented under conditions of 30-38 DEG C 24-28h by strain (saccharomycete), and Purification by filtration belongs to human body
A kind of interior existing growth factor, a kind of active material.The oligopeptides -1 can not only promote various kinds of cell in epidermal cell tissue
Growth division makes epidermal cell become full, restores younger state, but also with the ability for promoting collagen growth, repaiies
The collagen elastomer of multiple aging fracture, the cells of superficial layer of repairing and supplement skin.In addition, it also has senile-resistant efficacy, energy
Fine wrinkles are enough smoothed, skin elasticity is improved, improve dermatoglyph degree.
It is worth noting that the oligopeptides -1 involved by the application is not limited in above-mentioned oligopeptides -1, can also use other
Producer or commercially available oligopeptides -1.
Containing such as xuelianlactone in Herba Saussureae Involueratae extract, amino acid, vitamin, sugar, minerals, phytosterin compound with
And biological enzyme isoreactivity substance, it is lightly seasoned refined pleasant, it is ideal natural antidotal agent.
In the water chestnut facial mask liquid of the application, on the one hand Herba Saussureae Involueratae extract can inhibit Epidermophyton and star to exert card bacterium
Equal dermatophytes, on the other hand its have the effects that moist, sun-proof, softening, smoothly and only white to skin.In addition, lanatechead saussurea herb with flower carries
Take object that can also block ultraviolet light, antiphlogistic and bactericidal and treatment whelk etc..
As can refer to ground, above-mentioned Herba Saussureae Involueratae extract for example can be, but not limited to be purchased from Guangzhou profit alcohol chemical industry, can also
Using voluntarily prepare or be purchased from other producers.
Glycerine contains there are three hydroxyl, has good hydrophily, as one of the ingredient of water chestnut facial mask liquid, on the one hand
It can avoid the moisture on skin to distribute too soon, on the other hand can also suitably draw aqueous vapor from air, build good hydrone
Atmosphere is to keep the humidity of skin surface.
Oily (Lubrajel Oil) main component of reed fragrant plant is polyglycerolmethacrylate, with unique cage type knot
Hydrone is incorporated by hydrogen bond and Van der Waals force in the cage structure of polyglycerolmethacrylate formation by structure.When reed fragrant plant
When oil is contacted with human skin, since the presence of salt can cause the pH value of reed fragrant plant oil to change, strong electrolyte or skin temperature
Change causes the cage structure of polyglycerolmethacrylate slowly to be destroyed, and leads to water release, to provide skin with light
Pool and moistening effect.
Amino acid humectant is trimethylglycine, is a kind of natural structure substance amphoteric ion type moisturizing ingredient,
It can play the role of improving rapidly moisture holding capacity, the activated cell vigor of skin in the water chestnut facial mask liquid of the application, and have
Have and skin is kept to moisten, is smooth, prevents effect that is dry and shading.
Bacillus/glutamic acid fermentation Product filtrate in the application is to pass through natto gemma bar using glutamic acid as raw material
The fermentation of bacillus such as bacterium or bacillus subtilis, are then filtered, and obtain tunning filtered fluid.Specifically, above-mentioned fermentation
Temperature is 30-38 DEG C, fermentation time 20-48h.Through the bacillus obtained by above-mentioned fermentation/glutamic acid fermentation Product filtrate master
Containing polyglutamic acid, the molecular weight of the polyglutamic acid is no more than 10000Da.Polyglutamic acid under the molecular weight ranges is more conducive to
Skin absorbs, and can not only extend moistening effect, and can also assign the skin sense as skin silk cunning.In this application, have
Extremely strong moisture-retaining capacity can effectively increase the moisture-retaining capacity of skin as one of the ingredient of water chestnut facial mask liquid, promote skin
Skin health.
It is worth noting that bacillus/glutamic acid fermentation Product filtrate in the application can also be that molecular weight is more than
Other polyglutamic acids of 10000Da, but the preferably above-mentioned molecular weight voluntarily produced by our company is no more than 10000Da.
Sodium Hyaluronate itself is one of composition of human skin, belongs to acid glutinous sugar, using Sodium Hyaluronate as water chestnut
One of ingredient of facial mask liquid can keep moisture of skin, skin care, increase gloss, and can prevent chapped skin and wrinkle
It generates.
Water chestnut itself is the fruit of annual herb water plant water chestnut, and the crisp meat of Shui Lipi is beautiful, peels off after boiling edible, also may be used
It cooks gruel food, water chestnut contains abundant protein, unsaturated fatty acid and multivitamin and trace element.Taking orally can be with tonifying spleen benefit
Gas invigorating the spleen, strong stock knee, strong power QI invigorating, anticancer, weight-reducing.In the application, using water chestnut as raw material, water chestnut extracting solution is obtained after extracted
With external application, not only human skin can be made more moist, but also multiple dermatosis can be alleviated, energy is supplemented to skin,
Beauty care.
For above-mentioned each raw material in addition to each own effect, it includes following interaction also to have：In this application,
Glycerine, reed fragrant plant oil and amino acid humectant are compounded, skin can be allowed more to moisten, is pleasant；Again on the basis of this, with by
Strain fermentation and come high molecular polymer bacillus/glutamic acid fermentation Product filtrate and Sodium Hyaluronate further compound,
It can allow the permanent moisturizing of skin, and be free of preservative in the water chestnut facial mask liquid ingredient of the application, the stimulation components such as essence make production
Product safety, it is effectively, without side-effects.
It holds, the materials safety of water chestnut facial mask liquid provided herein is nontoxic, is free of preservative substance and essence, smell day
So pure, non-stimulated to skin, safety is without side-effects, has preferable preserving moisture and protecting skin effect.
In addition, the embodiment of the present invention additionally provides a kind of preparation method of above-mentioned water chestnut facial mask liquid, i.e., mixing is few according to the ratio
Peptide -1, Herba Saussureae Involueratae extract, glycerine, reed fragrant plant oil, amino acid humectant, bacillus/glutamic acid fermentation Product filtrate, hyalomitome
Sour sodium, water chestnut and purified water.
Preferably, in preparation process, the second component and third component can be first mixed, is then mixed again with the first component.
Wherein, the first component includes oligopeptides -1 and Herba Saussureae Involueratae extract；Second component includes glycerine, reed fragrant plant oil, amino acid humectant, bud
Spore bacillus/glutamic acid fermentation Product filtrate and Sodium Hyaluronate；Third component includes water chestnut and purified water.
Specifically, can refer to：Water chestnut (shell and meat that water chestnut can be included simultaneously) is first crushed, is then mixed with purified water, in
40-60min is extracted under conditions of 70-80 DEG C, filter centrifugation collects supernatant.Mixing supernatant and the second component, sterilizing, obtain
Sterilize mixed liquor, is then mixed with the first component.Then, sterile filling can be carried out to mixed facial mask liquid and is sealed, and obtained
Safe and non-stimulating water chestnut facial mask liquid.
In some embodiments, water chestnut preferably carries out under agitation with the mixed extraction process of purified water, stirs
Mix rotating speed can be 100-150r/min.
In some embodiments, before being mixed with the second component, water chestnut extracting solution can be cooled to 36-42 DEG C, so
Filter centrifugation (condition of centrifugation can be 7000-12000r/min) afterwards collects supernatant in sterilizing in autoclave.
Ground is can refer to, the sterilizing being previously mentioned in the application can carry out 35- under conditions of 110-125 DEG C and 0.1MPa
40min。
In some embodiments, sterilizing mixed liquor is mixed with the first component can also carry out under agitation, and stirring turns
Speed or 100-150r/min.
In some embodiments, the first component is mixed with sterilizing mixed liquor again after filtration sterilization.The mistake of first component
Filter out bacterium for example can pass through 0.22 μm of membrane filtration by the first component.
It holds, in above-mentioned preparation process, by each raw material component batch mixing, more meets each atman of raw material in each raw material group
Matter is conducive to avoid the active ingredient inactivation for being unable to high-temperature process as contained in raw material in sterilization process in high temperature.
In addition, present invention also provides a kind of water chestnut facial mask containing above-mentioned water chestnut facial mask liquid, face mask substrate material is unlimited, preferably
For inert solid support, such as can be non-woven fabrics, silk fabric, bacterial fibers film or chemically synthesized hydrogel etc..
Ground is can refer to, above-mentioned water chestnut facial mask can be by carrying out sterile filling to through spoke by water chestnut facial mask liquid provided by the present application
According in the face mask substrate material of processing and seal obtain.It is worth noting that form of ownership contains the faces Shui Li involved by the application
The facial mask of film liquid is within the scope of protection of this application.
The feature and performance of the present invention are described in further detail with reference to embodiments.
Embodiment 1
The raw material of water chestnut facial mask liquid provided in this embodiment contains the lanatechead saussurea herb with flower extraction of the oligopeptides -1 of 1wt%, 0.5wt%
Bacillus/glutamic acid hair of object, the glycerine of 2wt%, the reed fragrant plant oil of 1wt%, the amino acid humectant of 1wt%, 0.05wt%
The water chestnut of ferment Product filtrate, the Sodium Hyaluronate of 0.1wt% and 3wt%, surplus are purified water.Wherein, bacillus/paddy ammonia
The molecular weight of acid fermentation Product filtrate is 10000Da.
Preparation method：With reference to said ratio, the shell meat of wild water chestnut is crushed, is mixed with purified water, in 70 DEG C and turned
Speed extracts 60min under conditions of being 100r/min, is cooled to 36 DEG C, and the filter centrifugation under conditions of 7000r/min collects supernatant
Liquid in autoclave with glycerine, reed fragrant plant oil, amino acid humectant, bacillus/glutamic acid fermentation Product filtrate and hyalomitome
Sour sodium mixing obtains sterilizing mixed liquor in 110 DEG C and 0.1MPa of pieces sterilizing 40min.
The filter membrane that oligopeptides -1 and Herba Saussureae Involueratae extract are crossed to 0.22 μm respectively, then mixes with above-mentioned sterilizing mixed liquor,
It in last sterile filling to the face mask substrate material of irradiated processing and seals, obtains safe and non-stimulating water chestnut facial mask.
Embodiment 2
The present embodiment and embodiment 1 difference lies in：The raw material of water chestnut facial mask liquid contains the oligopeptides -1 of 4wt%, 3wt%
Herba Saussureae Involueratae extract, the glycerine of 4wt%, the reed fragrant plant oil of 3wt%, the amino acid humectant of 4wt%, 0.5wt% bacillus/
The water chestnut of glutamic acid fermentation Product filtrate, the Sodium Hyaluronate of 0.3wt% and 10wt%, surplus are purified water.
Embodiment 3
The present embodiment and embodiment 1 difference lies in：The raw material of water chestnut facial mask liquid contains the oligopeptides -1 of 2wt%, 1wt%
The gemma of Herba Saussureae Involueratae extract, the glycerine of 2.5wt%, the reed fragrant plant oil of 1.5wt%, the amino acid humectant of 2wt%, 0.2wt%
The water chestnut of bacillus/glutamic acid fermentation Product filtrate, the Sodium Hyaluronate of 0.15wt% and 5wt%, surplus are purified water.
Embodiment 4
The present embodiment and embodiment 1 difference lies in：The raw material of water chestnut facial mask liquid contains the oligopeptides -1 of 3wt%, 2.5wt%
Herba Saussureae Involueratae extract, the glycerine of 3.5wt%, the reed fragrant plant oil of 2.5wt%, the amino acid humectant of 3wt%, 0.4wt% bud
The water chestnut of spore bacillus/glutamic acid fermentation Product filtrate, the Sodium Hyaluronate of 0.25wt% and 8wt%, surplus are purified water.
Embodiment 5
The present embodiment and embodiment 1 difference lies in：The raw material of water chestnut facial mask liquid contains the oligopeptides -1 of 2.5wt%, 2wt%
Herba Saussureae Involueratae extract, the glycerine of 3wt%, the reed fragrant plant oil of 2wt%, the amino acid humectant of 2.5wt%, 0.3wt% gemma
The water chestnut of bacillus/glutamic acid fermentation Product filtrate, the Sodium Hyaluronate of 0.2wt% and 6.5wt%, surplus are purified water.
Wherein, the molecular weight of bacillus/glutamic acid fermentation Product filtrate is 10000Da.
Embodiment 6
The present embodiment and embodiment 5 difference lies in：Preparation method：With reference to proportioning, the shell meat of wild water chestnut is crushed, with
Purified water mixes, and extracts 40min under conditions of being 150r/min in 80 DEG C and rotating speed, 42 DEG C is cooled to, in 12000r/min
Under conditions of filter centrifugation, collect supernatant in autoclave with glycerine, reed fragrant plant oil, amino acid humectant, bacillus/paddy ammonia
Acid fermentation Product filtrate and Sodium Hyaluronate mixing, in 125 DEG C and 0.1MPa of conditions sterilizing 35min, must sterilize mixing
Liquid.
The filter membrane that oligopeptides -1 and Herba Saussureae Involueratae extract are crossed to 0.22 μm respectively, then mixes with above-mentioned sterilizing mixed liquor,
It in last sterile filling to the face mask substrate material of irradiated processing and seals, obtains safe and non-stimulating water chestnut facial mask.
Embodiment 7
The present embodiment and embodiment 5 difference lies in：Preparation method：With reference to proportioning, the shell meat of wild water chestnut is crushed, with
Purified water mixes, and extracts 50min under conditions of being 125r/min in 75 DEG C and rotating speed, 40 DEG C is cooled to, in 10000r/min
Under conditions of filter centrifugation, collect supernatant in autoclave with glycerine, reed fragrant plant oil, amino acid humectant, bacillus/paddy ammonia
Acid fermentation Product filtrate and Sodium Hyaluronate mixing must sterilize mixed in 118 DEG C and 0.1MPa of conditions sterilizing 37.5min
Close liquid.
The filter membrane that oligopeptides -1 and Herba Saussureae Involueratae extract are crossed to 0.22 μm respectively, then mixes with above-mentioned sterilizing mixed liquor,
It in last sterile filling to the face mask substrate material of irradiated processing and seals, obtains safe and non-stimulating water chestnut facial mask.
Embodiment 8
The present embodiment and embodiment 5 difference lies in：With reference to proportioning, the shell meat of wild water chestnut is crushed, is mixed with purified water,
60min is extracted under conditions of being 100r/min in 70 DEG C and rotating speed, 36 DEG C is cooled to, is filtered under conditions of 7000r/min
Centrifugation, collect supernatant in autoclave with 110 DEG C and 0.1MPa of condition sterilizing 40min for the first time.
Supernatant after sterilizing is filtered with glycerine, reed fragrant plant oil, amino acid humectant, bacillus/glutamic acid fermentation product
Liquid and Sodium Hyaluronate mixing must sterilize in being sterilized for the second time 40min with the condition of 110 DEG C and 0.1MPa in autoclave
Mixed liquor.
The filter membrane that oligopeptides -1 and Herba Saussureae Involueratae extract are crossed to 0.22 μm respectively, then mixes with above-mentioned sterilizing mixed liquor,
It in last sterile filling to the face mask substrate material of irradiated processing and seals, obtains safe and non-stimulating water chestnut facial mask.
Embodiment 9
The present embodiment and embodiment 5 difference lies in：Each raw material disposably mixes simultaneously.
Embodiment 10
The present embodiment provides a kind of water chestnut facial mask, the base material of the facial mask is non-woven fabrics, contains such as embodiment 1-9 on non-woven fabrics
The water chestnut facial mask liquid that any embodiment provides.
Embodiment 11
The present embodiment provides a kind of water chestnut facial mask, the base material of the facial mask is silk fabric, contains such as implementation on silk fabric
The water chestnut facial mask liquid that example 1-9 any embodiments provide.
Test example 1
It repeats to implement above-described embodiment 1-9, obtains enough water chestnut facial mask liquids.Sample to be tested 45 is set, and every 5 are
One group, amount to 9 groups, above-mentioned 9 groups correspond to by the water chestnut facial mask liquid obtained by embodiment 1-9 respectively.Used by 45 samples to be tested
Face mask substrate material is non-woven fabrics, and the water chestnut facial mask liquid hold-up that non-woven fabrics is coated with is equal, presses《QB/T-2872》Detection method pair
Above-mentioned 45 samples to be tested are tested, and the results are shown in Table 1, wherein alphabetical " P " representative " qualification ".
1 testing result of table
As can be seen from Table 1, the water chestnut facial mask provided herein containing water chestnut facial mask liquid refers in organoleptic indicator, physics and chemistry
It is marked with and sanitary index aspect meets《QB/T-2872》It is required that.
Test example 2
It repeats to implement above-described embodiment 1-9, obtains enough water chestnut facial mask liquids.Sample to be tested 64 is set, and every 8 are
One group, amount to 8 groups, above-mentioned 8 groups correspond to respectively by the water chestnut facial mask liquid of 9 gained of embodiment 1-7 and embodiment.64 are waited for test sample
Facial mask material used by product is non-woven fabrics, and the water chestnut facial mask liquid hold-up that non-woven fabrics is coated with is equal.
It randomly selects 60 users and distinguishes 60 water chestnut facial masks in the above-mentioned product to be tested of random application：60 users
Middle women 45, male 15；25 years old age or less 38,26-35 Sui 18,36-45 Sui 4,46 years old or more 0；Dryness
10, skin, neutral partially dry 6, skin, neutral partially oily 9, skin, 24, mixed type skin, oily skin 11.
Application method：After warm water cleaning cheek 15 minutes, under conditions of epidemic disaster is 75-85% in room, water chestnut is used
Facial mask applies face 20 minutes.
After use, 60 users are as follows to the evaluation of water chestnut facial mask：
(1) it scores, full marks are 10 points of meters：User's scoring of 18.3% (11) is 10 points, and 23.3% (14 s') makes
User's scoring is 9 points, and the user of 40% (24) scoring is 8 points, and user's scoring of 13.3% (8) is 7 points, 3.3%
User's scoring of (2) is 6 points, and user's scoring of 1.7% (1) is 5 points.
(2) mildness：The user of 80% (48) is evaluated as " very mild ", and the user of 20% (12) is evaluated as
" general ".
(3) smell：The user of 46.7% (28) is evaluated as " fine ", and the user of 38.3% (23) is evaluated as
The user of " can receive ", 5% (3) is evaluated as " smell is too heavy ", and the user of 6.7% (4) is evaluated as that " smell is too
It is light ", the user of 3.3% (2) is evaluated as " not liking ".
(4) moisturizing effect：The user of 86.6% (52) is evaluated as " fine ", user's evaluation of 13.4% (8)
For " general ".
(5) moisturizing effect：The user of 83.3% (50) is evaluated as " fine ", and the user of 16.7% (10) comments
Valence is " general ".
(6) moisturizing effect：The user of 85% (51) is evaluated as " fine ", and the user of 15% (9) is evaluated as
" general ".
(7) tightening effect：The user of 16.6% (10) is evaluated as " fine ", and the user of 78.3% (47) comments
Valence is " general ", and the user of 5.1% (3) is evaluated as " bad ".
(8) allergic phenomena：User's " no allergy " of 96.6% (58), user's " slight mistake of 3.4% (2)
It is quick ".
(9) phenomenon is stimulated：User's " non-stimulated " of 98.3% (59), user's " slight thorn of 1.7% (1)
Swash ".
The above results show that water chestnut facial mask provided by the embodiments of the present application has good moisturizing, moisturizing and moisturizing effect,
Various skin are applicable in, mild non-stimulated, smell is naturally pure.
In addition, evaluation result is also shown：User comments the water corresponding water chestnut facial mask of chestnut facial mask liquid obtained by embodiment 9
It is point worse compared with embodiment 1-7, illustrate in water chestnut facial mask liquid preparation process, obtained by each relatively disposable mixing of raw material substep mixing
Facial mask liquid quality more preferably.
Comparative example 1-5 shows that the corresponding water chestnut facial mask of water chestnut facial mask liquid of 5 gained of embodiment is compared with embodiment 1-4 institutes
The corresponding water chestnut facial mask scoring higher of water chestnut facial mask liquid obtained, and the corresponding faces Shui Li of water chestnut facial mask liquid obtained by embodiment 3-4
Film illustrates that the raw material proportioning of embodiment 5 is more sharp compared with the corresponding water chestnut facial mask scoring higher of water chestnut facial mask liquid obtained by embodiment 1-2
In obtaining quality more preferably facial mask liquid.
In addition, setting control group 1-4, control group 1 is commercially available imperial mud mill moisture saver mask, the area of control group 2 and embodiment 5
Be not that the molecular weight of bacillus/glutamic acid fermentation Product filtrate is 10000Da, control group 3 and embodiment 5 difference lies in
The molecular weight of bacillus/glutamic acid fermentation Product filtrate is 100000Da, and difference lies in gemma with embodiment 5 for control group 4
The molecular weight of bacillus/glutamic acid fermentation Product filtrate is 700000Da.
32 users separately are randomly selected, according to the method described above, average corresponding facial masks of application control group 1-4 respectively make
With rear, 32 users show the evaluation of facial mask：Control group 3-4 is being mended compared with embodiment 5 and 2 corresponding facial mask of control group
Water, moisturizing and moist aspect are clearly worse, but with control group 1 without significant difference.Illustrate bacillus/glutamic acid in facial mask liquid
The molecular weight of tunning filtrate is conducive to absorption of the skin to facial mask liquid really no more than 10000Da, improve moisturizing, moisturizing and
Moisturizing effect.
In conclusion the materials safety of water chestnut facial mask liquid provided in an embodiment of the present invention is nontoxic, preservative substance, smell are free of
It is natural pure, it is non-stimulated to skin, there is preferable preserving moisture and protecting skin effect.Preparation method is simple and quick, and condition controllability is good,
Suitable for large-scale production.Water chestnut facial mask containing above-mentioned water chestnut facial mask liquid, wide application of the crowd, skin effect are preferable.
Embodiments described above is a part of the embodiment of the present invention, instead of all the embodiments.The reality of the present invention
The detailed description for applying example is not intended to limit the range of claimed invention, but is merely representative of the selected implementation of the present invention
Example.Based on the embodiments of the present invention, those of ordinary skill in the art are obtained without creative efforts
Every other embodiment, shall fall within the protection scope of the present invention.
Claims (10)
1. a kind of water chestnut facial mask liquid, which is characterized in that its raw material include the oligopeptides -1 of 1-4wt%, 0.5-3wt% lanatechead saussurea herb with flower carry
Take the gemma bar of object, the glycerine of 2-4wt%, the reed fragrant plant oil of 1-3wt%, the amino acid humectant of 1-4wt%, 0.05-0.5wt%
The water chestnut of bacterium/glutamic acid fermentation Product filtrate, the Sodium Hyaluronate of 0.1-0.3wt% and 3-10wt%, surplus are purified water.
2. water chestnut facial mask liquid according to claim 1, which is characterized in that raw material includes the oligopeptides -1, the 1- of 2-3wt%
Reed fragrant plant oil, the 2- of the Herba Saussureae Involueratae extract of 2.5wt%, the glycerine of 2.5-3.5wt%, 1.5-2.5wt%
The amino acid humectant of 3wt%, the bacillus/glutamic acid fermentation Product filtrate, the 0.15- of 0.2-0.4wt%
The Sodium Hyaluronate of 0.25wt% and the water chestnut of 5-8wt%, surplus are the purified water.
3. water chestnut facial mask liquid according to claim 2, which is characterized in that raw material include 2.5wt% the oligopeptides -1,
The amino acid of the Herba Saussureae Involueratae extract of 2wt%, the glycerine of 3wt%, the reed fragrant plant oil of 2wt%, 2.5wt%
Moisturizer, the bacillus/glutamic acid fermentation Product filtrate of 0.3wt%, 0.2wt% the Sodium Hyaluronate and
The water chestnut of 6.5wt%, surplus are the purified water.
4. according to claim 1-3 any one of them water chestnut facial mask liquids, which is characterized in that the bacillus/glutamic acid hair
The molecular weight of ferment Product filtrate is no more than 10000Da.
5. the preparation method of water chestnut facial mask liquid according to any one of claims 1-4, which is characterized in that according to the ratio described in mixing
Oligopeptides -1, the Herba Saussureae Involueratae extract, the glycerine, reed fragrant plant oil, the amino acid humectant, the bacillus/paddy
Propylhomoserin tunning filtrate, the Sodium Hyaluronate, the water chestnut and the purified water.
6. preparation method according to claim 5, which is characterized in that first mix the second component and third component, then again
It is mixed with the first component；
First component includes the oligopeptides -1 and the Herba Saussureae Involueratae extract；
Second component includes the glycerine, reed fragrant plant oil, the amino acid humectant, the bacillus/glutamic acid
Tunning filtrate and the Sodium Hyaluronate；
The third component includes the water chestnut and the purified water.
7. preparation method according to claim 6, which is characterized in that first crush the water chestnut, then with the purified water
Mixing, extracts 40-60min under conditions of 70-80 DEG C, and filter centrifugation collects supernatant；Mix the supernatant and described
Two components, sterilizing, obtain sterilizing mixed liquor, are then mixed with first component.
8. preparation method according to claim 7, which is characterized in that sterilizing is in 110-125 DEG C and 0.1MPa of item
35-40min is carried out under part.
9. preparation method according to claim 7, which is characterized in that first component after filtration sterilization again with it is described
Sterilize mixed liquor mixing.
10. a kind of water chestnut facial mask, which is characterized in that the water chestnut facial mask contains water chestnut according to any one of claims 1-4
Facial mask liquid.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810951417.4A CN108703940A (en) | 2018-08-20 | 2018-08-20 | A kind of water chestnut facial mask liquid and preparation method thereof, water chestnut facial mask |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810951417.4A CN108703940A (en) | 2018-08-20 | 2018-08-20 | A kind of water chestnut facial mask liquid and preparation method thereof, water chestnut facial mask |
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| CN103800219A (en) * | 2012-11-08 | 2014-05-21 | 山东福瑞达生物科技有限公司 | Multifunctional high-efficiency moisturizing stock solution |
| CN107213107A (en) * | 2017-07-13 | 2017-09-29 | 北京健旭康技术有限公司 | Purposes of the Yangtze River Delta Area special product in cosmetics are prepared |
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| CN103800219A (en) * | 2012-11-08 | 2014-05-21 | 山东福瑞达生物科技有限公司 | Multifunctional high-efficiency moisturizing stock solution |
| CN107213107A (en) * | 2017-07-13 | 2017-09-29 | 北京健旭康技术有限公司 | Purposes of the Yangtze River Delta Area special product in cosmetics are prepared |
| CN107951756A (en) * | 2017-12-26 | 2018-04-24 | 广州莱蔓诗生物科技有限公司 | A kind of full effect whitening and moisturizing anti-wrinkle speckle removing, acne removing elite and preparation method thereof |
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Application publication date: 20181026 |