CN108703340A - A kind of eucommia ulmoides seed oil powder electuary and preparation method thereof - Google Patents

A kind of eucommia ulmoides seed oil powder electuary and preparation method thereof Download PDF

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Publication number
CN108703340A
CN108703340A CN201810282404.2A CN201810282404A CN108703340A CN 108703340 A CN108703340 A CN 108703340A CN 201810282404 A CN201810282404 A CN 201810282404A CN 108703340 A CN108703340 A CN 108703340A
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eucommia
powder
seed oil
rice
eucommia ulmoides
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李加兴
严友兵
朱式业
黄诚
杨建军
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XIANGXI LAODIE BIOLOGICAL CO Ltd
Jishou University
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XIANGXI LAODIE BIOLOGICAL CO Ltd
Jishou University
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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    • A23L25/00—Food consisting mainly of nutmeat or seeds; Preparation or treatment thereof
    • A23L25/30—Mashed or comminuted products, e.g. pulp, pastes, meal, powders; Products made therefrom, e.g. blocks, flakes, snacks; Liquid or semi-liquid products
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
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    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/15—Vitamins
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    • A23P10/35—Encapsulation of particles, e.g. foodstuff additives with oils, lipids, monoglycerides or diglycerides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07K—PEPTIDES
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    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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Abstract

The invention discloses a kind of eucommia ulmoides seed oil powder electuary and preparation method thereof, preparation method includes pretreatment of raw material, vacuum microwave humid heat treatment, supercritical extract carries oil, mechanical ball mill activates, super-high-pressure homogenization processing, is concentrated and dried, allotment drying.The method of the present invention first extracts eucommia ulmoides seed oil using Eucommia as raw material from Eucommia；Then it is raw material rationally to utilize the waste seed of bark of eucommia dregs of rice after carrying oil, using technologies such as mechanical ball mill activation, super-high-pressure homogenization processing, spray drying, it prepares rich in small molecular protein, starch and contains a small amount of gutta-percha, while there is the seed dregs of rice activity powder of preferably embedding effect and emulsifiability；Further, it is that wall material passes through micronization processing, vacuum spray drying using eucommia ulmoides seed oil as core material, seed dregs of rice activity powder, can prepare mobility, favorable dispersibility powdered oil, and has reducing blood lipid, blood pressure lowering, promote the development of nervous system, brain and retina, prevents senile dementia and allergy and other effects.

Description

A kind of eucommia ulmoides seed oil powder electuary and preparation method thereof
Technical field
The invention belongs to powdered oil processing technique fields, and in particular to a kind of eucommia ulmoides seed oil powder electuary and its preparation side Method.
Background technology
Cortex Eucommiae (EucommiaulmoidesOliv.) also known as kapok think celestial, the secondary, Si Jinshu of think of, and it is tall to belong to fallen leaves for branch list Wood is known as " living fossil plant ", is the distinctive rare tree in China.China's Cortex Eucommiae forest reserves are abundant, and total amount accounts for the whole world 95%, wild distribution center is planted extensively in central section of China area in Hunan, Hubei, Henan, Shanxi, Sichuan, expensive The provinces such as state, Yunnan, cultivated area is up to 4,000,000 mu.Cortex Eucommiae has more than 2000 years medicinal history in China.《Sheng Nong's herbal classic》With 《Compendium of Materia Medica》Cortex Eucommiae is classified as top grade, and records that " Cortex Eucommiae color is purple, sweet in flavor and pungent, and property is wet flat, and sweet temperature can mend, micro-pungent energy Profit, therefore liver can be entered and kidney tonifying；Cure mainly waist and knee, bowl spares strengthening the essence gas, hard muscles and bones, Qiang Zhi, except wet, dribbling urination of itching under the moon；Long term usage, It makes light of one's life by commiting suicide and endures hardships ".Modern research shows that Cortex Eucommiae contains lignanoids, iridoids, flavonoids, Phenylpropanoid Glycosides class, sterols and triterpene The various actives substance such as class, polysaccharide, antifungal protein and mineral element, wherein most have health-care efficacy and pharmacological activity, Such as lowering blood pressure and blood fat, hypoglycemic, antitumor, inhibitory anti-virus, anti-inflammatory, anti-oxidant.Root, stem, leaf, flower, the fruit of Cortex Eucommiae With in seed also contain natural polymer child resource-gutta-percha.Gutta-percha has high anti-tear, low-heat-generation, high temperature degree high-damping The performances such as property, can be used as the production material of high-end green tire, medical instrument, damping and silencing device etc., are Cortex Eucommiae industrial research With the emphasis and hot spot of exploitation, gutta-percha is expected to as China's the second natural rubber resource.
The discovery of medicinal health effect and gutta-percha based on Cortex Eucommiae, Cortex Eucommiae this unique " living fossil " is increasingly by weight Depending on people also deepen continuously to the research of Cortex Eucommiae.Wherein, eucommia ulmoides seed oil is because it rich in а-leukotrienes is that Cortex Eucommiae was again in recent years One exploitation hot spot.Eucommia ulmoides seed oil is primarily present in the samara of Cortex Eucommiae, rich in polyunsaturated fat such as leukotrienes, linoleic acid Acid, especially а-linolenic acid content are up to 60% or more, are a kind of good linolenic acid plant resources.Alpha-linolenic acid and linoleic acid It is essential fatty acid, wherein alpha-linolenic acid is that the structural material of each tissue biomembrane and synthesized human are a series of in vivo The precursor of prostaglandin.Normal person extends the effect of enzyme etc. through △ 6- dehydrogenases, carbochain after absorbing alpha-linolenic acid in food, A series of metabolites are generated, most important of which is that EPA and DHA.EPA is internal triolefin prostaglandin (such as PGI3, TXA3) Precursor, DHA are the main ingredient of the nervous systems phosphatide such as brain, retina.It is based on alpha-linolenic acid, linoleic effect, Make eucommia ulmoides seed oil that there is reducing blood lipid, blood pressure lowering to promote the development of nervous system, brain and retina, prevents senile dementia and mistake Quick disease and other effects.Powdered oil be it is a kind of core material is wrapped up with water-soluble wall material after the powder particle that obtains, there is preferable stream Dynamic property, emulsion stability and dispersibility, can facilitate the use, transport and storage of grease.It therefore, can be with Eucommia or Cortex Eucommiae Seed oil is raw material, eucommia ulmoides seed oil powdered oil or solid beverage product is developed, to give full play to the health-care efficacy valence of eucommia ulmoides seed oil It is worth, widens the purposes of eucommia ulmoides seed oil and improves its added value.
In general, powdered oil generally uses cyclodextrin, gelatin, Arabic gum etc. to be used as wall material, pass through spray drying technology It is prepared.Such as, fiber crops at gold it is equal (eucommia key fruit seed oil microencapsulation and antioxygenic property are studied, Food Science, 2005,26 (9):261~264) Microencapsulation Method for disclosing eucommia key fruit seed oil is wall by core material, beta-cyclodextrin of eucommia ulmoides seed oil Material, first heating are added eucommia key fruit seed oil after so that cyclodextrin is cooled down, certain time are stirred on magnetic stirring apparatus, is placed in ice About 48h in case refrigerating chamber, then filters and is dried in vacuo again.For another example, at gold etc., (spray drying process prepares microencapsulation seed of bark of eucommia to fiber crops The research of oil, Chinese grain and oil journal, 2008,23 (6):141~144) it discloses spray drying process and prepares microencapsulation seed of bark of eucommia The technique of oil, using eucommia ulmoides seed oil as core material, wall material has selected gelatin:Maltodextrin is 3:2, the pure glue of A types:Maltodextrin is l: L, Arabic gum:Maltodextrin 1:Seed of bark of eucommia is added after emulsifier, water and wall material mixed dissolution in 1.5 3 kinds of compound wall materials Oil, the homogenization under 30MPa pressure are spray-dried under the conditions of 190 DEG C of inlet air temperature, 80~90 DEG C of leaving air temp. Although above-mentioned two technical solution can prepare eucommia ulmoides seed oil powdered oil product, it is contemplated that more fully, reasonably Using seed of bark of eucommia samara, above-mentioned technical proposal still has improved space.
The wall material that grease uses when embedding mainly has protide, carbohydrate and hydrophilic colloid etc., such as soybean protein, breast Albumin, converted starch, Arabic gum etc..It has been found that being rich in egg in the Eucommia extraction remaining seed dregs of rice of peony seed oil White matter, starch, and meeting nubbin gutta-percha, therefore it is raw material that can utilize the seed dregs of rice, further processing processing is prepared into can The wall material for embedding peony seed oil, has been achieved the recycling of the residue seed dregs of rice after carrying oil, has made the oil in seed of bark of eucommia samara Fat, protein, starch, colloid etc. are by abundant, reasonable utilization.Moreover, having been disclosed in the prior art through aqueous enzymatic method technique Scheme of the soybean oil and soybean protein of preparation as the core material and wall material for producing powdered oil specifically opens the (response surfaces such as thunder Optimization aqueous enzymatic method prepares soybean powder oil, Chinese oil, 2017,42 (3):12-17) disclose the preparation of soybean powder oil Technique is crushed after being cleared up using fresh soybean, and alkali protease is added, digested, enzyme deactivation, after centrifugation, take from It is rich in the liquid phase of soybean oil and soybean protein after the heart, compound emulsifying agent and maltodextrin, casein sodium are further added, by liquid Mutually by constant temperature high-speed stirred, high-pressure homogeneous, spray drying, soybean powder oil is obtained.Although the technique realizes while profit Powdered oil is prepared respectively as core material, wall material, but core material can not be accurately controlled with soybean oil, the soybean protein in soybean The ratio of soybean oil, wall material soybean protein, the product quality finally prepared are simultaneously unstable.
Invention content
In view of the above-mentioned problems, the present invention provides a kind of eucommia ulmoides seed oil powder electuaries and preparation method thereof, with Cortex Eucommiae wing Fruit is raw material, and eucommia ulmoides seed oil is first extracted from Eucommia；Then it is raw material rationally to utilize the waste seed of bark of eucommia dregs of rice after carrying oil, Using technologies such as mechanical ball mill activation, super-high-pressure homogenization processing, spray drying, prepares rich in small molecular protein, starch and contain There is a small amount of gutta-percha, while there is the seed dregs of rice activity powder of preferably embedding effect and emulsifiability；Further, using eucommia ulmoides seed oil as core Material, seed dregs of rice activity powder be wall material handled by micronization, vacuum spray drying, mobility, favorable dispersibility can be prepared Powdered oil, and have reducing blood lipid, blood pressure lowering promotes the development of nervous system, brain and retina, prevents senile dementia and mistake Quick disease and other effects.
A kind of preparation method of eucommia ulmoides seed oil powder electuary, it is characterised in that include the following steps：
1) pretreatment of raw material：Eucommia is dried to water content and is less than 12%, peels off powder after the shell of Eucommia It is 10~20 mesh to be broken to granularity, obtains Eucommia powder；
2) vacuum microwave humid heat treatment：In the surface spray clear water for the Eucommia powder that step (1) obtains, while constantly stirring It mixes uniformly, until the final water content of Eucommia powder is 25~35%, is transferred to later in microwave cavity body, it is micro- to carry out vacuum The moisture of wave processing, control Eucommia powder is 9%~12%；In the prior art, grease is extracted using supercritical extract It only needs raw material drying and crushes, controlling raw material granularity and moisture, (usual granularity is too small, and the permeability of entrainer becomes Difference；Granularity is too big, and the fat in raw material is not easily disconnected from；Moisture is too high, and product oil moisture is high；Moisture is too low, Dry difficulty and cost increase)；The residual oil content of grouts is 2%~4% after general supercritical extract, in order to further decrease cake Dregs of rice residual oil content can only adjust extraction process, but use more harsh extraction process, such as extend extraction time, increase extraction pressure Power etc. can be such that cost is significantly increased or relatively difficult to achieve；And above-mentioned steps through the invention, Eucommia powder can be made micro- in vacuum During wave humid heat treatment, first water absorption and swelling (surface spray clear water) is then acted on by vacuum microwave, makes moisture content in rapid steaming Molecular channel is formed while hair, and grease is entrained with, and can improve the yield of follow-up supercritical extract and reduces grouts Residual oil content.The residual oil content data of supercritical extract after vacuum microwave humid heat treatment are shown in particular in embodiment 2.
3) supercritical extract carries oil：The Eucommia powder obtained using step (2) carries oil as raw material using supercritical extract, Obtain eucommia ulmoides seed oil and the seed of bark of eucommia dregs of rice；
4) mechanical ball mill activates：Take the seed of bark of eucommia dregs of rice that step (3) obtains and clear water in mass ratio 1:3~7 are uniformly mixed, it It is homogenized repeatedly using colloid mill afterwards, making slurries by weight 95% or more can lead to and sieve with 100 mesh sieve, and obtain seed dregs of rice slurries；By seed Dregs of rice slurries sieve with 100 mesh sieve, and collect screenings and are added in ball mill, carry out mechanical ball mill, centrifuge later, obtain upper layer activation seed dregs of rice slurry Liquid and lower sediment；By the step, can make protein, starch in seed dregs of rice slurries etc. mechanical ball mill friction, touch Hit, impact etc. under mechanical forces, crystal structure and physical and chemical performance is made to change, as breaks down proteins at small molecular protein, Destroying starch lattice structure makes its denaturation, to form the active matter with preferably embedding, emulsifying effectiveness；
5) super-high-pressure homogenization is handled：The activation seed dregs of rice slurries that step (4) obtains are crossed into 200 mesh sieve, extracting screen underflow in 120~ Super-high-pressure homogenization processing is carried out under conditions of 150Mpa, and the granularity of activation seed dregs of rice slurries is made to be less than 200nm；Further pass through the step Suddenly, under the action of super-pressure, can make activation seed dregs of rice slurries granularity reach nanoscale, be further formed with preferably embedding, The active matter of emulsifying effectiveness；
6) it is concentrated and dried：Will through step (5) treated activation seed dregs of rice slurries be concentrated into solid content be 15%~ 25%, it is spray-dried powder processed later, obtains seed dregs of rice activity powder；
7) drying is allocated：After taking eucommia ulmoides seed oil, the seed dregs of rice activity powder of step (6) acquisition, clear water that step (3) obtains to mix High-speed stirred is carried out, carries out micronization processing under conditions of 150~180Mpa later, the granularity of lotion is made to be less than 120nm, Then vacuum and low temperature is spray-dried powder processed, you can；In the step, seed dregs of rice activity powder can be completed to Cortex Eucommiae by being handled by micronization The embedding of seed oil, and eucommia ulmoides seed oil, seed dregs of rice activity powder, clear water is made to form nano level homogeneous latex emulsion, make the product tool after drying Standby excellent dispersibility, mobility and dissolubility；Further, it is spray-dried using vacuum and low temperature in the step, can avoid Cortex Eucommiae Leukotrienes is by Oxidative demage in seed oil；Vacuum and low temperature spray drying condition be preferably：0.80~0.98MPa of vacuum degree, air inlet 80~95 DEG C of temperature；
For through the above steps：Pretreatment of raw material, vacuum microwave humid heat treatment, supercritical extract put forward oil, mechanical ball mill Activation super-high-pressure homogenization processing, is concentrated and dried, the dry eucommia ulmoides seed oil powder electuary prepared of allotment, and Du is given in embodiment 3 The data of embedding rate, dissolubility, peroxide value, the moisture content of secondary seed oil powder electuary etc.；
In above-mentioned steps, the granularity of lotion uses GB/T19627- in activation seed dregs of rice slurries, step (7) in step (5) 2005 " grain size analysis-photon correlation spectroscopy " (PCS methods) are detected, and granularity uses median (D50) to indicate；Moisture The detection of content, fixture content uses 105 DEG C of oven drying methods of normal pressure.
As specific technical solution, in the step (2), the condition of vacuum microwave processing is：Vacuum degree 0.90~ 0.98MPa, microwave dose are 0.25~5kw/kg.
As specific technical solution, in the step (3), the condition of supercritical extract is：30~45MPa of extracting pressure, 1~3h of extraction time, 42~55 DEG C of extraction temperature, 28~32 DEG C of separation temperature, CO225~30kg/h of flow.
As specific technical solution, in the step (4), the process conditions of ball milling are：80~500r/ of drum's speed of rotation Min, ball-milling medium filling rate 8%~30%, 1~4h of Ball-milling Time.
As optimal technical scheme, in the step (4), the process conditions of ball milling are：220~300r/ of drum's speed of rotation Min, ball-milling medium filling rate 10%~12%, 2~3h of Ball-milling Time.
As specific technical solution, in the step (7), eucommia ulmoides seed oil, seed dregs of rice activity powder, the ratio of clear water in mass It is 2~5:5~10:40~50.
Further include that functional component and eucommia ulmoides seed oil, seed dregs of rice activity is added in the step (7) as specific technical solution Powder, clear water mixing；The functional component contains：
1) one or more in kudzu root extract, haw thorn extract, extract of soybean, black tea extract；
2) one or more in vitamin E, Rosmarinus officinalis extract, tea polyphenols；By above-mentioned compatibility, in eucommia ulmoides seed oil On the basis of, kudzu root extract, haw thorn extract, extract of soybean, black tea extract with effect for reducing blood fat can be added, it can be with The effect of further enhancing the reducing blood lipid of product, to produce the health products with auxiliary effect for reducing blood fat；Resist in addition, being added and having Vitamin E, Rosmarinus officinalis extract, the tea polyphenols of oxidation, can prevent the oxidation of the eucommia ulmoides seed oil of high linolenic content, with The effect of extending the shelf life of product, maintaining product is stablized.
Further include that nutrition fortifier is added to live with eucommia ulmoides seed oil, the seed dregs of rice in the step (7) as specific technical solution Property powder, clear water mixing；The nutrition fortifier at least contains：Protein, carbohydrate, alpha lactalbumin, 22 carbon six Olefin(e) acid, probiotics, nucleotide, lecithin, whey calcium, arachidonic acid；Eucommia ulmoides seed oil is rich in leukotrienes, can be provided for human body Abundant leukotrienes, in addition protein, carbohydrate, alpha lactalbumin, docosahexaenoic acid, probiotics, nucleotide, ovum Phosphatide, whey calcium, arachidonic acid etc. are the nutrient substances needed for infant's growth；Therefore by above-mentioned compatibility, make this Product can be used as infant food use.
As specific technical solution, in the step (7), further include be added microcapsule wall material, emulsifier and eucommia ulmoides seed oil, Seed dregs of rice activity powder, clear water mixing；The microcapsule wall material is one or more of cyclodextrine, Arabic gum, chitosan；Institute It is glycerin monostearate, sucrose fatty ester to state emulsifier；It is different, diverse when adding other performance in product formula After functional component, nutrition fortifier, in order to further improve and stablize the quality of final products, conventional microcapsules can be used Wall material, emulsifier etc..
The eucommia ulmoides seed oil powder electuary prepared using any of the above-described the method.
Specific implementation mode
The present invention is described further With reference to embodiment, it is pointed out that following implementation is only It is the indicative explaination done to the present invention in the form of enumerating, but protection scope of the present invention is not limited to that, Suo Youben The technical staff in field each falls within protection scope of the present invention with the equivalent replacement that the spirit of the present invention is the present invention.
Embodiment 1
A kind of preparation method of eucommia ulmoides seed oil powder electuary, includes the following steps：
1) pretreatment of raw material：Eucommia is dried with electric drying oven with forced convection to water content and is less than 12%, peels off Cortex Eucommiae It is 10~20 mesh to be crushed to granularity using microphyte pulverizer after the shell of samara, obtains Eucommia powder；
2) vacuum microwave humid heat treatment：In the surface spray clear water for the Eucommia powder that step (1) obtains, while constantly stirring It mixes uniformly, until the final water content of Eucommia powder is 25~35%, is transferred to later in microwave cavity body, in vacuum degree 0.90~0.98MPa, microwave dose carry out vacuum microwave processing under the conditions of being 1.5kw/kg, the moisture of control Eucommia powder contains Amount is 9%~12%；
3) supercritical extract carries oil：Using step (2) obtain Eucommia powder as raw material, using supercritical extracting equipment in Extracting pressure 42MPa, extraction time 2h, 45 DEG C of extraction temperature, 30 DEG C of separation temperature, CO2Under conditions of 25~30kg/h of flow Oil is carried, eucommia ulmoides seed oil and the seed of bark of eucommia dregs of rice are obtained；After testing, the eucommia ulmoides seed oil peroxide value obtained is 1.23mmol/kg, and acid value is 0.18mg/g；In the seed of bark of eucommia dregs of rice contain protein 36.53%, starch-containing 18.32%；
4) mechanical ball mill activates：Take the seed of bark of eucommia dregs of rice that step (3) obtains and clear water in mass ratio 1:3~7 are uniformly mixed, it It is homogenized repeatedly using colloid mill afterwards, making slurries by weight 95% or more can lead to and sieve with 100 mesh sieve, and obtain seed dregs of rice slurries；By seed Dregs of rice slurries sieve with 100 mesh sieve, and collect screenings and are added in ball mill, are filled in 220~300r/min of drum's speed of rotation, ball-milling medium Mechanical ball mill is carried out under rate 10%~12%, 2~3h of Ball-milling Time, is centrifuged later, upper layer activation seed dregs of rice slurries is obtained and lower layer is heavy It forms sediment；
5) super-high-pressure homogenization is handled：The activation seed dregs of rice slurries that step (4) obtains are crossed into 200 mesh sieve, extracting screen underflow in 120~ Super-high-pressure homogenization processing is carried out using nanometer ram machine under conditions of 150Mpa, the granularity of activation seed dregs of rice slurries is made to be less than 200nm；
6) it is concentrated and dried：Will through step (5) treated activation seed dregs of rice slurries be concentrated into solid content be 15%~ 25%, spray drying powder processed is carried out under conditions of 160~185 DEG C of inlet air temperature later, obtains seed dregs of rice activity powder；
7) drying is allocated：After taking eucommia ulmoides seed oil, the seed dregs of rice activity powder of step (6) acquisition, clear water that step (3) obtains to mix Carry out high-speed stirred, later under conditions of 150~180Mpa using nanometer ram machine progress 90 DEG C of micronization under conditions of It carries out vacuum and low temperature and is spray-dried powder processed, you can；
In above-mentioned steps, primary raw material Eucommia is provided by Xiangxi Laodie Biology Co., Ltd.；Key instrument equipment：It is micro- Type plant pulverizer, FZ102 types, Tianjin Stettlen Instrument Ltd.；Electric drying oven with forced convection, 101-2AB types, Tianjin Stettlen Instrument Ltd.；Supercritical extracting equipment, model HA420-40-96, the limited public affairs of Nantong City Huaan supercritical extract Department；Nanometer ram machine, 20/150D types, Langfang Tongyong Machinery Manufacturing Co., Ltd.；Spray dryer, SD-04 types, the long sea of sand are insulted Bio tech ltd；
In above-mentioned steps, the granularity of lotion uses GB/T19627- in activation seed dregs of rice slurries, step (7) in step (5) 2005 " grain size analysis-photon correlation spectroscopy " (PCS methods) are detected, and granularity uses median (D50) to indicate；Moisture The detection of content, fixture content uses 105 DEG C of oven drying methods of normal pressure；The method that the measurement of peroxide value uses GB/T 5538；Acid The method that the measurement of valence uses GB/T 5530；The measurement of protein content uses micro-Kjeldahl；The measurement of content of starch Using the method for GB/T 5009.9.
Embodiment 2
Vacuum microwave humid heat treatment influences to measure on the residual oil content of supercritical extract.
1, the preparation of the seed of bark of eucommia dregs of rice
Vacuum microwave humid heat treatment group：Using the method for embodiment 1, the seed of bark of eucommia dregs of rice that are obtained after taking supercritical extract to carry oil Measure residual oil content；
Conventional method control group：Using the method for embodiment 1, but without vacuum microwave humid heat treatment, take overcritical extraction The seed of bark of eucommia dregs of rice obtained after carrying oil are taken to measure residual oil content.
2, the measurement of residual oil content
Every group takes 3 parts of sample detections, the measurement of residual oil content to use soxhlet extraction methods.
3, interpretation of result
1 vacuum microwave humid heat treatment of table influences the residual oil content of supercritical extract
As shown in Table 1, overcritical after first carrying out vacuum microwave humid heat treatment to Eucommia powder using the method for the present invention The residue seed of bark of eucommia dregs of rice residual oil content of extraction is lower.
Embodiment 3
The indexs such as embedding rate, mobility, dissolubility, peroxide value, the moisture content of eucommia ulmoides seed oil powder electuary of the present invention It measures.
1, the measurement of embedding rate
Embedding rate=(1- surface oil contents/total content oil) × 100%
Eucommia ulmoides seed oil powder electuary surface oil content measures：Using petroleum ether as solvent, 5.0g seed of bark of eucommia oil powders are accurately weighed Last electuary sample, 120mL petroleum ethers are added in three times, and fully oscillation, filtering, merging filtrate, filtrate are dense through depressurizing every time After contracting, grease obtained quality is eucommia ulmoides seed oil powder electuary surface oil content.
Eucommia ulmoides seed oil powder electuary total oil content measures fixed：Make solvent, precise 5.0g seed of bark of eucommia oil powders with anhydrous ether 150~180mL anhydrous ethers are added in last electuary sample, and 4~6h of Soxhlet extraction collects anhydrous ether vacuum distillation, grease obtained Quality is that the measurement of eucommia ulmoides seed oil powder electuary total oil content is fixed.
2, dissolubility
Take 1g eucommia ulmoides seed oil powder electuaries (m1) in 50mL beakers, 10mL distilled water (25 DEG C) is added, is started with stopwatch Timing keeps 60s, takes the eucommia ulmoides seed oil powder electuary 1mL after rehydration in the aluminium box of constant weight immediately, is put into 105 ± 2 DEG C of baking Dry 4h in case, weigh (m2), its dissolubility is then calculated as follows, while being compared with commercially available dried milk powder.
In formula：
m1, eucommia ulmoides seed oil powder electuary quality, g；
m2, the eucommia ulmoides seed oil powder electuary quality after rehydration drying, g.
3, the measurement of mobility
Funnel is fixed and keeps vertical, bell mouth about 8cm high from desktop, desktop places blank sheet of paper, by 50g eucommia ulmoides seed oil powder Electuary is added from funnel, measures the base diameter of free-falling formed taper on blank sheet of paper, differentiates it with the size of diameter The size of mobility.It is compared simultaneously with commercially available dried milk powder, diameter is bigger, and expression mobility is better.
4, peroxide value, the measurement of water content
The peroxide value of eucommia ulmoides seed oil powder electuary is measured according to the method for GB/T 5538；Water content uses 105 DEG C of normal pressures Seasoning.
5, measurement result
Embedding rate, mobility, dissolubility, peroxide value, the moisture content of 2 eucommia ulmoides seed oil powder electuary of the present invention of table
Project Commercially available dried milk powder Eucommia ulmoides seed oil powder electuary of the present invention
Embedding rate/% - 86.4
Dissolubility/% 86.8 78.9
Mobility/cm 9.86 9.72
Peroxide value/(mmol/kg) - 1.38
Water content/% - 6.75
As shown in Table 2, the embedding rate of eucommia ulmoides seed oil powder electuary of the present invention is 86.4%, is in higher level, is illustrated logical Cross mechanical ball mill activation, super-high-pressure homogenization treated seed dregs of rice activity powder has preferable embedding effect；Eucommia ulmoides seed oil of the present invention The mobility of powder electuary is 9.72cm, little with commercially available dried milk powder difference, and solubility is 78.8%, slightly less than commercially available dried milk powder； In addition, the peroxide value of eucommia ulmoides seed oil powder electuary of the present invention is relatively low, it is 1.38mmol/kg, illustrates to pass through seed dregs of rice activity powder pair The embedding of eucommia ulmoides seed oil and vacuum and low temperature spray drying, can effectively inhibit the oxidation deterioration of eucommia ulmoides seed oil.

Claims (10)

1. a kind of preparation method of eucommia ulmoides seed oil powder electuary, it is characterised in that include the following steps：
1) pretreatment of raw material：Eucommia is dried to water content and is less than 12%, the shell for peelling off Eucommia is crushed to later Granularity is 10~20 mesh, obtains Eucommia powder；
2) vacuum microwave humid heat treatment：In the surface spray clear water for the Eucommia powder that step (1) obtains, while being stirred continuously It is even, until the final water content of Eucommia powder is 25~35%, it is transferred in microwave cavity body, is carried out at vacuum microwave later The moisture of reason, control Eucommia powder is 9%~12%；
3) supercritical extract carries oil：The Eucommia powder obtained using step (2) carries oil as raw material using supercritical extract, obtains Eucommia ulmoides seed oil and the seed of bark of eucommia dregs of rice；
4) mechanical ball mill activates：Take the seed of bark of eucommia dregs of rice that step (3) obtains and clear water in mass ratio 1:3~7 are uniformly mixed, Zhi Houli It is homogenized repeatedly with colloid mill, making slurries by weight 95% or more can lead to and sieve with 100 mesh sieve, and obtain seed dregs of rice slurries；The seed dregs of rice are starched Liquid sieves with 100 mesh sieve, collect screenings be added ball mill in, carry out mechanical ball mill, centrifuge later, obtain upper layer activation seed dregs of rice slurries and Lower sediment；
5) super-high-pressure homogenization is handled：The activation seed dregs of rice slurries that step (4) obtains are crossed into 200 mesh sieve, extracting screen underflow in 120~ Super-high-pressure homogenization processing is carried out under conditions of 150Mpa, and the granularity of activation seed dregs of rice slurries is made to be less than 200nm；
6) it is concentrated and dried：Will through step (5) treated activation seed dregs of rice slurries be concentrated into solid content be 15%~25%, it It is spray-dried powder processed afterwards, obtains seed dregs of rice activity powder；
7) drying is allocated：Eucommia ulmoides seed oil, the seed dregs of rice activity powder of step (6) acquisition, clear water that step (3) obtains is taken to be carried out after mixing High-speed stirred carries out micronization processing under conditions of 150~180Mpa later, so that the granularity of lotion is less than 120nm, then Vacuum and low temperature is spray-dried powder processed, you can.
2. a kind of eucommia ulmoides seed oil powder electuary as described in claim 1, it is characterised in that in the step (2), vacuum microwave The condition of processing is：Vacuum degree is 0.90~0.98MPa, microwave dose is 0.25~5kw/kg.
3. a kind of eucommia ulmoides seed oil powder electuary as described in claim 1, it is characterised in that in the step (3), overcritical extraction The condition taken is：30~45MPa of extracting pressure, 1~3h of extraction time, 42~55 DEG C of extraction temperature, 28~32 DEG C of separation temperature, CO225~30kg/h of flow.
4. a kind of eucommia ulmoides seed oil powder electuary as described in claim 1, it is characterised in that in the step (4), the work of ball milling Skill condition is：80~500r/min of drum's speed of rotation, ball-milling medium filling rate 8%~30%, 1~4h of Ball-milling Time.
5. a kind of eucommia ulmoides seed oil powder electuary as claimed in claim 4, it is characterised in that in the step (4), the work of ball milling Skill condition is：220~300r/min of drum's speed of rotation, ball-milling medium filling rate 10%~12%, 2~3h of Ball-milling Time.
6. a kind of eucommia ulmoides seed oil powder electuary as described in claim 1, it is characterised in that in the step (7), eucommia ulmoides seed oil, Seed dregs of rice activity powder, the ratio of clear water in mass are 2~5:5~10:40~50.
7. a kind of eucommia ulmoides seed oil powder electuary as described in claim 1, it is characterised in that further include adding in the step (7) Enter functional component to mix with eucommia ulmoides seed oil, seed dregs of rice activity powder, clear water；The functional component contains：
1) one or more in kudzu root extract, haw thorn extract, extract of soybean, black tea extract；
2) one or more in vitamin E, Rosmarinus officinalis extract, tea polyphenols.
8. a kind of eucommia ulmoides seed oil powder electuary as described in claim 1, it is characterised in that further include adding in the step (7) Enter nutrition fortifier to mix with eucommia ulmoides seed oil, seed dregs of rice activity powder, clear water；The nutrition fortifier at least contains：Protein, carbon water Compound, alpha lactalbumin, docosahexaenoic acid, probiotics, nucleotide, lecithin, whey calcium, arachidonic acid.
9. a kind of eucommia ulmoides seed oil powder electuary as described in claim 1, it is characterised in that further include adding in the step (7) Enter microcapsule wall material, emulsifier is mixed with eucommia ulmoides seed oil, seed dregs of rice activity powder, clear water；The microcapsule wall material be cyclodextrine, Ah Draw one or more of primary glue, chitosan；The emulsifier is glycerin monostearate, sucrose fatty ester.
10. the eucommia ulmoides seed oil powder electuary prepared using any the method for claim 1~9.
CN201810282404.2A 2018-04-02 2018-04-02 A kind of eucommia ulmoides seed oil powder electuary and preparation method thereof Pending CN108703340A (en)

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Application publication date: 20181026