CN108703159A - A kind of composition pesticide containing nicosulfuron and Prochloraz - Google Patents
A kind of composition pesticide containing nicosulfuron and Prochloraz Download PDFInfo
- Publication number
- CN108703159A CN108703159A CN201810812576.6A CN201810812576A CN108703159A CN 108703159 A CN108703159 A CN 108703159A CN 201810812576 A CN201810812576 A CN 201810812576A CN 108703159 A CN108703159 A CN 108703159A
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- parts
- prochloraz
- nicosulfuron
- composition pesticide
- adhesive
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/32—Ingredients for reducing the noxious effect of the active substances to organisms other than pests, e.g. toxicity reducing compositions, self-destructing compositions
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/36—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< directly attached to at least one heterocyclic ring; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/38—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< where at least one nitrogen atom is part of a heterocyclic ring; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
Abstract
The present invention provides a kind of composition pesticide containing nicosulfuron and Prochloraz, is related to composition pesticide field, including the raw material composition of following parts by weight:Nicosulfuron:5-8 parts, Prochloraz:5-8 parts, anisomycin:5-8 parts, class graphite phase carbon nitride:4-5 parts, Spina Gleditsiae extract:4-5 parts, adhesive:12-15 parts, talcum powder:20-25 parts, the present invention can reduce plantation soil and plant the pesticide residue on plant while ensureing high-efficiency low-toxicity.
Description
Technical field
The present invention relates to composition pesticide fields, and in particular to a kind of pesticide combination containing nicosulfuron and Prochloraz
Object.
Background technology
Nicosulfuron is a kind of common farm chemical ingredients being widely used in maize diseases prevention, can be effectively removed to medicine
The strong weeds of sensibility are with a wide range of applications such as And-gather grass, green bristlegrass, wild oat.
Prochloraz is a kind of wide-spectrum bactericide, is had to various crop disease caused by sac fungus and Fungi Imperfecti apparent
Preventive effect, often mixed with the Insecticides (tech) & Herbicides (tech) of other kinds, the insect pest disease occurred when multiple kinds of crops can be inhibited to grow
Evil, is a kind of widely used sterilization component,
Leek originates in the Asia southeast, is most normal on food market and Chinese's dining table in the big plantation extensively on the ground of China
One of vegetable variety seen, therefore there is the huge market demand, however in the developmental process of leek, but often there is leek
Gray mold, downy mildew, this causes serious blow to leek yield.
It is also further strong for the pursuit of health meanwhile with the increasingly raising of living standards of the people, although pesticide is applied
Add the disease that can prevent crops in growth course, but pesticide residue not only causes crops that poisoning occurs, more to ring
The health of border and eater cause many burdens.
Invention content
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of composition pesticide containing nicosulfuron and Prochloraz,
While ensureing high-efficiency low-toxicity, plantation soil can be reduced and plant the pesticide residue on plant.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic
Sulphur is grand:5-8 parts, Prochloraz:5-8 parts, anisomycin:5-8 parts, class graphite phase carbon nitride:4-5 parts, Spina Gleditsiae extract:4-5
Part, adhesive:12-15 parts, talcum powder:20-25 parts.
Preferably, including the raw material of following parts by weight forms:Nicosulfuron:6-7 parts, Prochloraz:7-8 parts, fennel it is mould
Element:5-6 parts, class graphite phase carbon nitride:4-5 parts, Spina Gleditsiae extract:4-5 parts, adhesive:13-14 parts, talcum powder:22-24
Part.
Preferably, including the raw material of following parts by weight forms:Nicosulfuron:6 parts, Prochloraz:7 parts, anisomycin:5
Part, class graphite phase carbon nitride:5 parts, Spina Gleditsiae extract:4 parts, adhesive:14 parts, talcum powder:23 parts.
Preferably, the adhesive is 1799 aqueous solution of polyvinyl alcohol of mass fraction 5%.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, which is characterized in that including following
Step:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight
Enter in grinder and grind, after grinding 20-30min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing,
Pure water, Prochloraz is added, under the mixing speed of 100-150r/min after heating stirring 70-90min, compression moulding is dry
After obtain final product.
Preferably, heating described in step (2) is increases temperature to keeping the temperature after 50-70 DEG C.
(3) advantageous effect
The present invention provides a kind of composition pesticide containing nicosulfuron and Prochloraz, has the advantages that:
First, the selected ingredient in existing sterilization and disinsection formula, nicosulfuron, Prochloraz itself, which have, centainly to kill
Worm effect, compounding superposition after bactericidal and Insecticidal effect further enhance, for leek gray mold cause of disease the pathogen of Botrytis cinerea and
The cause of disease downy mildew of downy mildew passes through itself and nicosulfuron, miaow by increasing anisomycin, Spina Gleditsiae extract in ingredient
The synergistic function of fresh amine improves the bactericidal effect for the pathogen of Botrytis cinerea, downy mildew.
Secondly, increase class graphite phase carbon nitride, it is cheap, and can be under sun light action to the phonetic sulphur of remaining cigarette
The farm chemical ingredients such as grand, Prochloraz carry out degradation decomposition, effectively reduce plantation soil and plant the pesticide residue on plant, meet the modern times
The public demands for low pesticide residue crops.
Finally, the present invention has the characteristics that active ingredient is more, single active constituent content is few, focuses on each ingredient agent basis
Make the synergistic function used, sprinkling is only needed once to can reach prevention as a result, control effect is good in leek growth course.
Specific implementation mode
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making
The every other embodiment obtained under the premise of creative work, shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic
Sulphur is grand:5 parts, Prochloraz:8 parts, anisomycin:5 parts, class graphite phase carbon nitride:4 parts, Spina Gleditsiae extract:5 parts, adhesive
(1799 aqueous solution of polyvinyl alcohol of mass fraction 5%):12 parts, talcum powder:25 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight
Enter in grinder and grind, after grinding 20min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing,
Pure water, Prochloraz is added, increases temperature to keeping the temperature after 50 DEG C, while after stirring 90min under the mixing speed of 100r/min,
Compression moulding obtains final product after dry.
Embodiment 2:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic
Sulphur is grand:8 parts, Prochloraz:5 parts, anisomycin:8 parts, class graphite phase carbon nitride:5 parts, Spina Gleditsiae extract:4 parts, adhesive
(1799 aqueous solution of polyvinyl alcohol of mass fraction 5%):15 parts, talcum powder:20 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight
Enter in grinder and grind, after grinding 30min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing,
Pure water, Prochloraz is added, increases temperature to keeping the temperature after 70 DEG C, while after stirring 70min under the mixing speed of 150r/min,
Compression moulding obtains final product after dry.
Embodiment 3:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic
Sulphur is grand:7 parts, Prochloraz:7 parts, anisomycin:5 parts, class graphite phase carbon nitride:4 parts, Spina Gleditsiae extract:5 parts, adhesive:
13 parts, talcum powder:24 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight
Enter in grinder and grind, after grinding 25min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing,
Pure water, Prochloraz is added, increases temperature to keeping the temperature after 55 DEG C, while after stirring 80min under the mixing speed of 130r/min,
Compression moulding obtains final product after dry.
Embodiment 4:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic
Sulphur is grand:Nicosulfuron:6 parts, Prochloraz:8 parts, anisomycin:6 parts, class graphite phase carbon nitride:5 parts, Spina Gleditsiae extract:4
Part, adhesive:14 parts, talcum powder:22 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight
Enter in grinder and grind, after grinding 22min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing,
Pure water, Prochloraz is added, increases temperature to keeping the temperature after 55 DEG C, while after stirring 75min under the mixing speed of 135r/min,
Compression moulding obtains final product after dry.
Embodiment 5:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic
Sulphur is grand:6 parts, Prochloraz:7 parts, anisomycin:5 parts, class graphite phase carbon nitride:5 parts, Spina Gleditsiae extract:4 parts, adhesive:
14 parts, talcum powder:23 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight
Enter in grinder and grind, after grinding 28min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing,
Pure water, Prochloraz is added, increases temperature to keeping the temperature after 60 DEG C, while after stirring 85min under the mixing speed of 140r/min,
Compression moulding obtains final product after dry.
Advantageous effect in order to further illustrate the present invention, that selects 1-5 preparations of the embodiment of the present invention contains nicosulfuron
With the composition pesticide of Prochloraz, then the medicine for leek leek gray mold, downy mildew having in the prior art is chosen respectively
Agent, and be labeled as medicament 1, medicament 2 carries out sterilization experiment, specifically, take respectively botrytis, downy mildew fresh cultured
Object is separately added into phosphate buffer, bacteria suspension is obtained after dilution, at 20 DEG C, 1ml bacteria suspensions is taken to pour into sterile test tube respectively
In, while the composition pesticide containing nicosulfuron and Prochloraz, medicament 1 and the medicine for respectively preparing 1-5 of the embodiment of the present invention
Agent 2 is dissolved in water to obtain bactericidal liquid, and 10ml bactericidal liquids is taken to be separately added into different sterile test tubes, mixes well to obtain mixed liquor,
It takes mixed liquor to do count plate culture, sterilizing rate is calculated after 5d, the surplus of farm chemical ingredients in bactericidal liquid, experiment are tested after 30d
Ten experiments are repeated, go average that experimental result is recorded in following table.
Test event | Unit | Botrytis | Downy mildew | Residual quantity |
Medicament 1 | % | 91.3 | / | 64 |
Medicament 2 | % | / | 91.8 | 67 |
Embodiment 1 | % | 96.4 | 96.3 | 22 |
Embodiment 2 | % | 96.9 | 96.8 | 21 |
Embodiment 3 | % | 96.3 | 96.2 | 23 |
Embodiment 4 | % | 96.5 | 96.7 | 21 |
Embodiment 5 | % | 96.3 | 96.4 | 22 |
It should be noted that herein, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also include other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions, the element limited including sentence "including a ...", it is not excluded that
There is also other identical elements in the process, method, article or apparatus that includes the element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations, although with reference to the foregoing embodiments
Invention is explained in detail, it will be understood by those of ordinary skill in the art that:It still can be to aforementioned each implementation
Technical solution recorded in example is modified or equivalent replacement of some of the technical features;And these modification or
It replaces, the spirit and scope for various embodiments of the present invention technical solution that it does not separate the essence of the corresponding technical solution.
Claims (6)
1. a kind of composition pesticide containing nicosulfuron and Prochloraz, which is characterized in that include the raw material of following parts by weight
Composition:Nicosulfuron:5-8 parts, Prochloraz:5-8 parts, anisomycin:5-8 parts, class graphite phase carbon nitride:4-5 parts, spina gleditsiae carries
Take object:4-5 parts, adhesive:12-15 parts, talcum powder:20-25 parts.
2. the composition pesticide containing nicosulfuron and Prochloraz as described in claim 1, which is characterized in that including following heavy
Measure the raw material composition of number:Nicosulfuron:6-7 parts, Prochloraz:7-8 parts, anisomycin:5-6 parts, class graphite phase carbon nitride:4-
5 parts, Spina Gleditsiae extract:4-5 parts, adhesive:13-14 parts, talcum powder:22-24 parts.
3. the composition pesticide containing nicosulfuron and Prochloraz as described in claim 1, which is characterized in that including following heavy
Measure the raw material composition of number:Nicosulfuron:6 parts, Prochloraz:7 parts, anisomycin:5 parts, class graphite phase carbon nitride:5 parts, gleditsia sinensis
Pierce extract:4 parts, adhesive:14 parts, talcum powder:23 parts.
4. the composition pesticide containing nicosulfuron and Prochloraz as described in claim 1, which is characterized in that the adhesive
For 1799 aqueous solution of polyvinyl alcohol of mass fraction 5%.
5. the preparation method of the composition pesticide as described in claim 1 containing nicosulfuron and Prochloraz, which is characterized in that
Include the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to be sequentially placed into and grind according to parts by weight
It is ground in grinding machine, after grinding 20-30min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) it takes talcum powder, adhesive to be added in blender, while putting into mixed powder according to parts by weight, after mixing, is added
Pure water, Prochloraz, under the mixing speed of 100-150r/min after heating stirring 70-90min, compression moulding obtains after dry
To final product.
6. the preparation method of the composition pesticide as claimed in claim 5 containing nicosulfuron and Prochloraz, which is characterized in that
Heating described in step (2) is increases temperature to keeping the temperature after 50-70 DEG C.
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