CN108703159A - A kind of composition pesticide containing nicosulfuron and Prochloraz - Google Patents

A kind of composition pesticide containing nicosulfuron and Prochloraz Download PDF

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Publication number
CN108703159A
CN108703159A CN201810812576.6A CN201810812576A CN108703159A CN 108703159 A CN108703159 A CN 108703159A CN 201810812576 A CN201810812576 A CN 201810812576A CN 108703159 A CN108703159 A CN 108703159A
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CN
China
Prior art keywords
parts
prochloraz
nicosulfuron
composition pesticide
adhesive
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810812576.6A
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Chinese (zh)
Inventor
汪志稳
李霞
赵龙凯
金奎�
尹仕兵
王玉贵
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Anhui Huaxing Chemical Co Ltd
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Anhui Huaxing Chemical Co Ltd
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Application filed by Anhui Huaxing Chemical Co Ltd filed Critical Anhui Huaxing Chemical Co Ltd
Priority to CN201810812576.6A priority Critical patent/CN108703159A/en
Publication of CN108703159A publication Critical patent/CN108703159A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/32Ingredients for reducing the noxious effect of the active substances to organisms other than pests, e.g. toxicity reducing compositions, self-destructing compositions
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/36Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< directly attached to at least one heterocyclic ring; Thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/38Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< where at least one nitrogen atom is part of a heterocyclic ring; Thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia

Abstract

The present invention provides a kind of composition pesticide containing nicosulfuron and Prochloraz, is related to composition pesticide field, including the raw material composition of following parts by weight:Nicosulfuron:5-8 parts, Prochloraz:5-8 parts, anisomycin:5-8 parts, class graphite phase carbon nitride:4-5 parts, Spina Gleditsiae extract:4-5 parts, adhesive:12-15 parts, talcum powder:20-25 parts, the present invention can reduce plantation soil and plant the pesticide residue on plant while ensureing high-efficiency low-toxicity.

Description

A kind of composition pesticide containing nicosulfuron and Prochloraz
Technical field
The present invention relates to composition pesticide fields, and in particular to a kind of pesticide combination containing nicosulfuron and Prochloraz Object.
Background technology
Nicosulfuron is a kind of common farm chemical ingredients being widely used in maize diseases prevention, can be effectively removed to medicine The strong weeds of sensibility are with a wide range of applications such as And-gather grass, green bristlegrass, wild oat.
Prochloraz is a kind of wide-spectrum bactericide, is had to various crop disease caused by sac fungus and Fungi Imperfecti apparent Preventive effect, often mixed with the Insecticides (tech) & Herbicides (tech) of other kinds, the insect pest disease occurred when multiple kinds of crops can be inhibited to grow Evil, is a kind of widely used sterilization component,
Leek originates in the Asia southeast, is most normal on food market and Chinese's dining table in the big plantation extensively on the ground of China One of vegetable variety seen, therefore there is the huge market demand, however in the developmental process of leek, but often there is leek Gray mold, downy mildew, this causes serious blow to leek yield.
It is also further strong for the pursuit of health meanwhile with the increasingly raising of living standards of the people, although pesticide is applied Add the disease that can prevent crops in growth course, but pesticide residue not only causes crops that poisoning occurs, more to ring The health of border and eater cause many burdens.
Invention content
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of composition pesticide containing nicosulfuron and Prochloraz, While ensureing high-efficiency low-toxicity, plantation soil can be reduced and plant the pesticide residue on plant.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic Sulphur is grand:5-8 parts, Prochloraz:5-8 parts, anisomycin:5-8 parts, class graphite phase carbon nitride:4-5 parts, Spina Gleditsiae extract:4-5 Part, adhesive:12-15 parts, talcum powder:20-25 parts.
Preferably, including the raw material of following parts by weight forms:Nicosulfuron:6-7 parts, Prochloraz:7-8 parts, fennel it is mould Element:5-6 parts, class graphite phase carbon nitride:4-5 parts, Spina Gleditsiae extract:4-5 parts, adhesive:13-14 parts, talcum powder:22-24 Part.
Preferably, including the raw material of following parts by weight forms:Nicosulfuron:6 parts, Prochloraz:7 parts, anisomycin:5 Part, class graphite phase carbon nitride:5 parts, Spina Gleditsiae extract:4 parts, adhesive:14 parts, talcum powder:23 parts.
Preferably, the adhesive is 1799 aqueous solution of polyvinyl alcohol of mass fraction 5%.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, which is characterized in that including following Step:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight Enter in grinder and grind, after grinding 20-30min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing, Pure water, Prochloraz is added, under the mixing speed of 100-150r/min after heating stirring 70-90min, compression moulding is dry After obtain final product.
Preferably, heating described in step (2) is increases temperature to keeping the temperature after 50-70 DEG C.
(3) advantageous effect
The present invention provides a kind of composition pesticide containing nicosulfuron and Prochloraz, has the advantages that:
First, the selected ingredient in existing sterilization and disinsection formula, nicosulfuron, Prochloraz itself, which have, centainly to kill Worm effect, compounding superposition after bactericidal and Insecticidal effect further enhance, for leek gray mold cause of disease the pathogen of Botrytis cinerea and The cause of disease downy mildew of downy mildew passes through itself and nicosulfuron, miaow by increasing anisomycin, Spina Gleditsiae extract in ingredient The synergistic function of fresh amine improves the bactericidal effect for the pathogen of Botrytis cinerea, downy mildew.
Secondly, increase class graphite phase carbon nitride, it is cheap, and can be under sun light action to the phonetic sulphur of remaining cigarette The farm chemical ingredients such as grand, Prochloraz carry out degradation decomposition, effectively reduce plantation soil and plant the pesticide residue on plant, meet the modern times The public demands for low pesticide residue crops.
Finally, the present invention has the characteristics that active ingredient is more, single active constituent content is few, focuses on each ingredient agent basis Make the synergistic function used, sprinkling is only needed once to can reach prevention as a result, control effect is good in leek growth course.
Specific implementation mode
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention, Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the present invention one Divide embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making The every other embodiment obtained under the premise of creative work, shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic Sulphur is grand:5 parts, Prochloraz:8 parts, anisomycin:5 parts, class graphite phase carbon nitride:4 parts, Spina Gleditsiae extract:5 parts, adhesive (1799 aqueous solution of polyvinyl alcohol of mass fraction 5%):12 parts, talcum powder:25 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight Enter in grinder and grind, after grinding 20min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing, Pure water, Prochloraz is added, increases temperature to keeping the temperature after 50 DEG C, while after stirring 90min under the mixing speed of 100r/min, Compression moulding obtains final product after dry.
Embodiment 2:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic Sulphur is grand:8 parts, Prochloraz:5 parts, anisomycin:8 parts, class graphite phase carbon nitride:5 parts, Spina Gleditsiae extract:4 parts, adhesive (1799 aqueous solution of polyvinyl alcohol of mass fraction 5%):15 parts, talcum powder:20 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight Enter in grinder and grind, after grinding 30min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing, Pure water, Prochloraz is added, increases temperature to keeping the temperature after 70 DEG C, while after stirring 70min under the mixing speed of 150r/min, Compression moulding obtains final product after dry.
Embodiment 3:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic Sulphur is grand:7 parts, Prochloraz:7 parts, anisomycin:5 parts, class graphite phase carbon nitride:4 parts, Spina Gleditsiae extract:5 parts, adhesive: 13 parts, talcum powder:24 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight Enter in grinder and grind, after grinding 25min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing, Pure water, Prochloraz is added, increases temperature to keeping the temperature after 55 DEG C, while after stirring 80min under the mixing speed of 130r/min, Compression moulding obtains final product after dry.
Embodiment 4:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic Sulphur is grand:Nicosulfuron:6 parts, Prochloraz:8 parts, anisomycin:6 parts, class graphite phase carbon nitride:5 parts, Spina Gleditsiae extract:4 Part, adhesive:14 parts, talcum powder:22 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight Enter in grinder and grind, after grinding 22min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing, Pure water, Prochloraz is added, increases temperature to keeping the temperature after 55 DEG C, while after stirring 75min under the mixing speed of 135r/min, Compression moulding obtains final product after dry.
Embodiment 5:
A kind of composition pesticide containing nicosulfuron and Prochloraz includes the raw material composition of following parts by weight:Cigarette is phonetic Sulphur is grand:6 parts, Prochloraz:7 parts, anisomycin:5 parts, class graphite phase carbon nitride:5 parts, Spina Gleditsiae extract:4 parts, adhesive: 14 parts, talcum powder:23 parts.
The preparation method of the above-mentioned composition pesticide containing nicosulfuron and Prochloraz, includes the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to put successively according to parts by weight Enter in grinder and grind, after grinding 28min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) talcum powder, adhesive is taken to be added in blender, while putting into mixed powder according to parts by weight, after mixing, Pure water, Prochloraz is added, increases temperature to keeping the temperature after 60 DEG C, while after stirring 85min under the mixing speed of 140r/min, Compression moulding obtains final product after dry.
Advantageous effect in order to further illustrate the present invention, that selects 1-5 preparations of the embodiment of the present invention contains nicosulfuron With the composition pesticide of Prochloraz, then the medicine for leek leek gray mold, downy mildew having in the prior art is chosen respectively Agent, and be labeled as medicament 1, medicament 2 carries out sterilization experiment, specifically, take respectively botrytis, downy mildew fresh cultured Object is separately added into phosphate buffer, bacteria suspension is obtained after dilution, at 20 DEG C, 1ml bacteria suspensions is taken to pour into sterile test tube respectively In, while the composition pesticide containing nicosulfuron and Prochloraz, medicament 1 and the medicine for respectively preparing 1-5 of the embodiment of the present invention Agent 2 is dissolved in water to obtain bactericidal liquid, and 10ml bactericidal liquids is taken to be separately added into different sterile test tubes, mixes well to obtain mixed liquor, It takes mixed liquor to do count plate culture, sterilizing rate is calculated after 5d, the surplus of farm chemical ingredients in bactericidal liquid, experiment are tested after 30d Ten experiments are repeated, go average that experimental result is recorded in following table.
Test event Unit Botrytis Downy mildew Residual quantity
Medicament 1 % 91.3 / 64
Medicament 2 % / 91.8 67
Embodiment 1 % 96.4 96.3 22
Embodiment 2 % 96.9 96.8 21
Embodiment 3 % 96.3 96.2 23
Embodiment 4 % 96.5 96.7 21
Embodiment 5 % 96.3 96.4 22
It should be noted that herein, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those Element, but also include other elements that are not explicitly listed, or further include for this process, method, article or equipment Intrinsic element.In the absence of more restrictions, the element limited including sentence "including a ...", it is not excluded that There is also other identical elements in the process, method, article or apparatus that includes the element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations, although with reference to the foregoing embodiments Invention is explained in detail, it will be understood by those of ordinary skill in the art that:It still can be to aforementioned each implementation Technical solution recorded in example is modified or equivalent replacement of some of the technical features;And these modification or It replaces, the spirit and scope for various embodiments of the present invention technical solution that it does not separate the essence of the corresponding technical solution.

Claims (6)

1. a kind of composition pesticide containing nicosulfuron and Prochloraz, which is characterized in that include the raw material of following parts by weight Composition:Nicosulfuron:5-8 parts, Prochloraz:5-8 parts, anisomycin:5-8 parts, class graphite phase carbon nitride:4-5 parts, spina gleditsiae carries Take object:4-5 parts, adhesive:12-15 parts, talcum powder:20-25 parts.
2. the composition pesticide containing nicosulfuron and Prochloraz as described in claim 1, which is characterized in that including following heavy Measure the raw material composition of number:Nicosulfuron:6-7 parts, Prochloraz:7-8 parts, anisomycin:5-6 parts, class graphite phase carbon nitride:4- 5 parts, Spina Gleditsiae extract:4-5 parts, adhesive:13-14 parts, talcum powder:22-24 parts.
3. the composition pesticide containing nicosulfuron and Prochloraz as described in claim 1, which is characterized in that including following heavy Measure the raw material composition of number:Nicosulfuron:6 parts, Prochloraz:7 parts, anisomycin:5 parts, class graphite phase carbon nitride:5 parts, gleditsia sinensis Pierce extract:4 parts, adhesive:14 parts, talcum powder:23 parts.
4. the composition pesticide containing nicosulfuron and Prochloraz as described in claim 1, which is characterized in that the adhesive For 1799 aqueous solution of polyvinyl alcohol of mass fraction 5%.
5. the preparation method of the composition pesticide as described in claim 1 containing nicosulfuron and Prochloraz, which is characterized in that Include the following steps:
(1) nicosulfuron, anisomycin, class graphite phase carbon nitride, Spina Gleditsiae extract is taken to be sequentially placed into and grind according to parts by weight It is ground in grinding machine, after grinding 20-30min, oscillation stirring is sufficiently mixed, and obtains mixed powder;
(2) it takes talcum powder, adhesive to be added in blender, while putting into mixed powder according to parts by weight, after mixing, is added Pure water, Prochloraz, under the mixing speed of 100-150r/min after heating stirring 70-90min, compression moulding obtains after dry To final product.
6. the preparation method of the composition pesticide as claimed in claim 5 containing nicosulfuron and Prochloraz, which is characterized in that Heating described in step (2) is increases temperature to keeping the temperature after 50-70 DEG C.
CN201810812576.6A 2018-07-23 2018-07-23 A kind of composition pesticide containing nicosulfuron and Prochloraz Pending CN108703159A (en)

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Application publication date: 20181026