CN108642768B - Preparation method of moisture-absorbing and sweat-releasing fabric based on viscose fibers - Google Patents

Preparation method of moisture-absorbing and sweat-releasing fabric based on viscose fibers Download PDF

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CN108642768B
CN108642768B CN201810622842.9A CN201810622842A CN108642768B CN 108642768 B CN108642768 B CN 108642768B CN 201810622842 A CN201810622842 A CN 201810622842A CN 108642768 B CN108642768 B CN 108642768B
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viscose
sweat
fabric
preparation
moisture
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CN108642768A (en
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刘让同
李亮
刘淑萍
李淑静
别剑龙
胡泽栋
耿长军
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Zhongyuan University of Technology
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/10Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
    • D06B3/18Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics combined with squeezing, e.g. in padding machines
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B15/00Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/248Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
    • D06M13/256Sulfonated compounds esters thereof, e.g. sultones
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402Amides imides, sulfamic acids
    • D06M13/432Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
    • D06M2101/06Vegetal fibres cellulosic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/10Repellency against liquids
    • D06M2200/12Hydrophobic properties

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

The invention relates to the field of textiles, in particular to a preparation method of a moisture absorption and sweat releasing fabric based on viscose, which specifically comprises the following steps: placing the viscose fabric in a water repellent agent with the concentration of 30-60g/L, performing two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-baking at 105 ℃ for 3min, and baking at 150 ℃ for 4 min; placing the water-repellent finished viscose fabric in a hydrophilic agent with the concentration of 30-60g/L, performing two-dipping and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 40 ℃ for 5min, and baking at 60 ℃ for 10min to obtain the viscose fabric with the moisture absorption and sweat releasing functions. The preparation method of the moisture-absorbing and sweat-releasing fabric based on the viscose realizes the moisture-absorbing and sweat-releasing effects of the viscose fabric, improves the added value of the product, and enriches the moisture-absorbing and sweat-releasing fabric.

Description

Preparation method of moisture-absorbing and sweat-releasing fabric based on viscose fibers
Technical Field
The invention relates to the field of textiles, in particular to a preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers.
Background
With the rapid development of society, the pursuit of human beings on the living quality is continuously improved, and as the clothes of necessary products, the pursuit of the color, the hand feeling and the quality is realized, the wearability, the health and the safety and the individuality fashion of the clothes are more emphasized, the phenomenon is particularly obvious in summer, and people hope that the clothes of the people have the functions of moisture absorption and sweat releasing. Of course, for people who are used to sports and leisure life styles, the clothes with the moisture absorption and sweat releasing functions can better meet the pursuit of comfort. The clothes with the functions of absorbing moisture and releasing sweat generally consist of fibers or fabrics with good moisture absorption and moisture conduction, and the clothes can absorb sweat generated by a human body, disperse the sweat outwards through holes in the fibers or gaps among the fibers, and transfer the sweat outwards along the holes in the fibers and the axial direction of the fibers.
The prior garment fabric with the functions of moisture absorption and sweat releasing is mainly realized by the following aspects: firstly, the moisture absorption and moisture transmission performance of the fabric of the clothing is improved by carrying out physical or chemical modification treatment on the fibers, such as: surface micropores, interface irregular sections, surface grooves, introduction of hydrophilic groups and the like; secondly, reasonably designing the fabric tissue of the garment material to ensure that the fabric has more porosity and a capillary effect is formed; and thirdly, the fiber components of the garment fabric are reasonably matched, so that water molecules can be effectively and quickly transferred outwards. Such as: the fiber with excellent moisture absorption performance and the fiber with poor moisture absorption performance are blended, interwoven, wrapped and the like.
The viscose fiber has excellent moisture absorption performance and belongs to a bio-based renewable material, but the fiber product has poor sweat absorption and quick drying performance, and if the fiber product has better moisture absorption and sweat release capability, the application field of the fiber product can be expanded, the additional value of the fiber product is increased, and the types of moisture absorption and sweat release fabrics are further enriched.
Disclosure of Invention
The invention provides a preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers, which solves the moisture absorption and sweat releasing problems of the viscose fiber fabric.
The technical scheme for realizing the invention is as follows: a preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers comprises the following steps:
(1) placing the viscose fabric in a water repellent agent, performing two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 95-105 ℃ for 3min, and baking at 130-150 ℃ for 4 min;
(2) and (3) placing the water-repellent finished viscose fabric into a hydrophilic agent, performing two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 35-45 ℃ for 5min, and baking at 55-65 ℃ for 10min to obtain the viscose fabric with the moisture absorption and sweat releasing functions.
The water repellent is an organic silicon water repellent or an organic fluorine water repellent.
The concentration of the water repellent in the step (1) is 30g/L-60g/L, and the concentration of the hydrophilic agent in the step (2) is 30g/L-60 g/L.
The preparation method of the hydrophilic agent comprises the following steps: mixing denaturant urea, surfactant, strong base and water to prepare a mixed solution, placing the waste wool into the mixed solution, treating at 95-100 ℃ for 3h, adjusting the pH value by using acetic acid after treatment, and performing activated carbon adsorption, suction filtration and spray drying on the adjusted solution to obtain the hydrophilizing agent.
The mass ratio of the denaturant urea to the surfactant to the strong base to the water is 10:1:4: 85.
The surfactant is any one of sodium dodecyl sulfonate, sodium hexadecyl benzene sulfonate or sodium octadecyl benzene sulfonate.
The pH value of the mixed solution is 11, and the pH value after acetic acid adjustment is 5.
The technological parameters of the spray drying are as follows: the drying medium is 150-160 ℃ hot air with the hot air quantity of 60-70m3The feed rate is 0.15 to 0.25ml/s, the feed temperature is 20 to 30 ℃.
Viscose fibers have excellent moisture absorption performance, but poor perspiration performance because hydrophilic groups in the fibers are combined with water molecules through hydrogen bonds to form bound water, so that the water molecules are retained in the fibers and are difficult to discharge. An effective water repellent layer is formed on the surface of the viscose fiber subjected to water repellent treatment, and hydrophilic groups of the viscose fiber are effectively coated, so that water molecules and the hydrophilic groups of the viscose fiber cannot form hydrogen bonds, and the water molecules can only stay on the surface of the viscose fiber, which is beneficial to the transfer and evaporation of the water molecules. However, the water repellent layer formed on the surface of the viscose fiber is not good for the moisture absorption capacity of the viscose fiber, so that the moisture absorption capacity of the viscose fiber is kept by hydrophilic treatment, the moisture absorption performance of the hydrophilic treated water repellent treated viscose fiber is greatly improved, and the moisture absorption and sweat releasing functions of the viscose fiber fabric are further realized.
The invention has the beneficial effects that: the preparation method of the moisture-absorbing and sweat-releasing fabric based on the viscose fibers has good moisture-absorbing and sweat-releasing performance, realizes the moisture-absorbing and sweat-releasing effects of viscose fabrics, improves the added value of the product, and enriches the moisture-absorbing and sweat-releasing fabric.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the drawings without creative efforts.
FIG. 1 is a picture of a water repellent and hydrophilic finishing object of the viscose fabric of the invention.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments of the present invention, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without inventive effort based on the embodiments of the present invention, are within the scope of the present invention.
Example 1
A preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers comprises the following steps:
placing the viscose fabric in a water repellent agent with final concentration of 30g/L, performing two-dipping and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 105 ℃ for 3min, and baking at 150 ℃ for 4 min. And then placing the viscose fabric obtained after the water repellent finishing into a hydrolyzed egg with the concentration of 30g/L, carrying out two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 40 ℃ for 5min, and baking at 60 ℃ for 10min to obtain the moisture-absorbing and sweat-releasing viscose fabric.
TABLE 1 related technical indexes of moisture absorption and sweat releasing performance of fabric
Item Moisture permeability Water absorption rate Wicking height Rate of evaporation Drip spreading time
Common viscose fabric 2557.25g/m2▪d 125% 3.5cm 0.1771g/h 57.8s
Moisture-absorbing sweat-releasing viscose fabric 5237.45g/m2▪d 123% 3.8cm 0.2844g/h 49s
Example 2
A preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers comprises the following steps:
placing the viscose fabric in a water repellent agent with the final concentration of 40g/L, performing two-dipping and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 105 ℃ for 3min, and baking at 150 ℃ for 4 min. And then placing the viscose fabric obtained after the water repellent finishing into a hydrolyzed egg with the concentration of 50g/L, carrying out two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 40 ℃ for 5min, and baking at 60 ℃ for 10min to obtain the moisture-absorbing and sweat-releasing viscose fabric.
Example 3
A preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers comprises the following steps:
placing the viscose fabric in a water repellent agent with the final concentration of 50g/L, performing two-dipping and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 105 ℃ for 3min, and baking at 150 ℃ for 4 min. And then placing the viscose fabric obtained after the water repellent finishing into a hydrolyzed egg with the concentration of 50g/L, carrying out two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 40 ℃ for 5min, and baking at 60 ℃ for 10min to obtain the moisture-absorbing and sweat-releasing viscose fabric.
Example 4
A preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers comprises the following steps:
placing the viscose fabric in a water repellent agent with the final concentration of 60g/L, performing two-dipping and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 105 ℃ for 3min, and baking at 150 ℃ for 4 min. And then placing the viscose fabric obtained after the water repellent finishing into a hydrolyzed egg with the concentration of 50g/L, carrying out two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 40 ℃ for 5min, and baking at 60 ℃ for 10min to obtain the moisture-absorbing and sweat-releasing viscose fabric.
Example 5
A preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers comprises the following steps:
(1) mixing a denaturant urea, sodium hexadecylbenzene sulfonate, sodium hydroxide and water according to a mass ratio of 10:1:4:85 to prepare a mixed solution, placing the waste wool into the mixed solution, treating the mixed solution at 95 ℃ for 3 hours with the pH value of 11, adjusting the pH value to 5 by using acetic acid after treatment, and adsorbing, filtering and spray-drying the adjusted solution by using activated carbon to obtain a hydrophilic agent;
the technological parameters of spray drying are as follows: the drying medium is hot air at 150 deg.C, and the hot air quantity is 60m3H, feed rate of 0.15ml/s, feed temperature of 20 ℃;
(2) placing the viscose fabric in a water repellent agent with the final concentration of 60g/L and the water repellent agent of FG-910, performing two-dipping and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 95 ℃ for 3min, and baking at 130 ℃ for 4 min. And (2) placing the viscose fabric obtained after the water repellent finishing into the hydrophilic agent obtained in the step (1), wherein the concentration of the hydrophilic agent is 30g/L, performing two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 35 ℃ for 5min, and baking at 55 ℃ for 10min to obtain the moisture-absorbing and sweat-releasing viscose fabric.
Example 6
A preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers comprises the following steps:
(1) mixing a denaturant urea, sodium octadecyl benzene sulfonate, sodium hydroxide and water according to a mass ratio of 10:1:4:85 to prepare a mixed solution, placing the waste wool into the mixed solution, treating the mixed solution at 98 ℃ for 3h, adjusting the pH to 5 by using acetic acid after treatment, and adsorbing, filtering and spray-drying the solution by using activated carbon to obtain a hydrophilic agent;
the technological parameters of spray drying are as follows: the drying medium is hot air at 155 deg.C, and the hot air quantity is 65m3Feed rate of 0.20ml/s, feed temperature 25 ℃;
(2) placing the viscose fabric in a water repellent agent with the final concentration of 60g/L, wherein the water repellent agent is HA-210, performing double-soaking and double-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 100 ℃ for 3min, and baking at 140 ℃ for 4 min. And (2) placing the viscose fabric obtained after the water repellent finishing into the hydrophilic agent obtained in the step (1), wherein the concentration of the hydrophilic agent is 30-60g/L, carrying out two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 40 ℃ for 5min, and baking at 60 ℃ for 10min to obtain the moisture-absorbing and sweat-releasing viscose fabric.
Example 7
A preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers comprises the following steps:
(1) mixing denaturant urea, sodium dodecyl sulfate, sodium hydroxide and water according to a mass ratio of 10:1:4:85 to prepare a mixed solution, placing the waste wool into the mixed solution, treating the mixed solution at 100 ℃ for 3 hours with the pH value of 11, adjusting the pH value to 5 by using acetic acid after treatment, and adsorbing, filtering and spray-drying the solution by using activated carbon to obtain a hydrophilic agent;
the technological parameters of spray drying are as follows: the drying medium is hot air of 160 deg.C, and the hot air quantity is 70m3H, feed rate of 0.25ml/s, feed temperature of 30 ℃;
(2) placing the viscose fabric in a water repellent agent with the final concentration of 60g/L and CO, carrying out two-dipping and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 105 ℃ for 3min, and baking at 150 ℃ for 4 min. And (2) placing the viscose fabric obtained after the water repellent finishing into the hydrophilic agent obtained in the step (1), wherein the concentration of the hydrophilic agent is 60g/L, performing two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 45 ℃ for 5min, and baking at 65 ℃ for 10min to obtain the moisture-absorbing and sweat-releasing viscose fabric.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims (3)

1. A preparation method of a moisture absorption and sweat releasing fabric based on viscose fibers is characterized by comprising the following steps:
(1) placing the viscose fabric in a water repellent agent, performing two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-drying at 95-105 ℃ for 3min, and baking at 130-150 ℃ for 4 min; the water repellent is organosilicon water repellent or organic fluorine water repellent, and the concentration of the water repellent is 30-60 g/L;
(2) placing the water-repellent finished viscose fabric into a hydrophilic agent, wherein the concentration of the hydrophilic agent is 30-60 g/L; after two-soaking and two-rolling treatment, keeping the rolling residual rate at 75%, pre-baking at 35-45 ℃ for 5min, and baking at 55-65 ℃ for 10min, the viscose fabric with moisture absorption and sweat releasing functions is obtained;
the preparation method of the hydrophilic agent comprises the following steps: mixing denaturant urea, surfactant, strong base and water to prepare a mixed solution, placing the waste wool into the mixed solution, treating at 95-100 ℃ for 3h, adjusting the pH value by using acetic acid after treatment, and performing activated carbon adsorption, suction filtration and spray drying on the adjusted solution to obtain a hydrophilic agent;
the mass ratio of the denaturant urea to the surfactant to the strong base to the water is 10:1:4: 85;
the technological parameters of the spray drying are as follows: the drying medium is 150-160 ℃ hot air with the hot air quantity of 60-70m3The feed rate is 0.15 to 0.25ml/s, the feed temperature is 20 to 30 ℃.
2. The preparation method of the viscose-based moisture-absorbing and sweat-releasing fabric according to claim 1, wherein the preparation method comprises the following steps: the surfactant is any one of sodium dodecyl sulfonate, sodium hexadecyl benzene sulfonate or sodium octadecyl benzene sulfonate.
3. The preparation method of the viscose-based moisture-absorbing and sweat-releasing fabric according to claim 1, wherein the preparation method comprises the following steps: the pH value of the mixed solution is 11, and the pH value after acetic acid adjustment is 5.
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