CN108634312A - A kind of black pine sealwort tabletting - Google Patents
A kind of black pine sealwort tabletting Download PDFInfo
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- CN108634312A CN108634312A CN201810441189.6A CN201810441189A CN108634312A CN 108634312 A CN108634312 A CN 108634312A CN 201810441189 A CN201810441189 A CN 201810441189A CN 108634312 A CN108634312 A CN 108634312A
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- extract
- black pine
- sealwort
- tabletting
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- 235000005638 Austrian pine Nutrition 0.000 title claims abstract description 47
- 235000008565 Pinus banksiana Nutrition 0.000 title claims abstract description 47
- 244000019397 Pinus jeffreyi Species 0.000 title claims abstract description 47
- 235000013264 Pinus jeffreyi Nutrition 0.000 title claims abstract description 47
- 235000008578 Pinus strobus Nutrition 0.000 title claims abstract description 47
- 235000008585 Pinus thunbergii Nutrition 0.000 title claims abstract description 47
- 235000014030 Podocarpus spicatus Nutrition 0.000 title claims abstract description 47
- 235000017985 rocky mountain lodgepole pine Nutrition 0.000 title claims abstract description 47
- 239000000284 extract Substances 0.000 claims abstract description 87
- 239000002994 raw material Substances 0.000 claims description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 26
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 25
- 239000000243 solution Substances 0.000 claims description 25
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims description 24
- 244000241872 Lycium chinense Species 0.000 claims description 20
- 235000015468 Lycium chinense Nutrition 0.000 claims description 20
- 235000013399 edible fruits Nutrition 0.000 claims description 20
- 235000019441 ethanol Nutrition 0.000 claims description 20
- 241000208340 Araliaceae Species 0.000 claims description 16
- 241001264174 Cordyceps militaris Species 0.000 claims description 16
- 229920000168 Microcrystalline cellulose Polymers 0.000 claims description 16
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims description 16
- 235000003140 Panax quinquefolius Nutrition 0.000 claims description 16
- 235000008434 ginseng Nutrition 0.000 claims description 16
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims description 16
- 239000008108 microcrystalline cellulose Substances 0.000 claims description 16
- 229940016286 microcrystalline cellulose Drugs 0.000 claims description 16
- 239000003595 mist Substances 0.000 claims description 16
- 239000012141 concentrate Substances 0.000 claims description 15
- 238000001035 drying Methods 0.000 claims description 15
- 238000002156 mixing Methods 0.000 claims description 15
- 235000019359 magnesium stearate Nutrition 0.000 claims description 12
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 11
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 11
- 235000021552 granulated sugar Nutrition 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 11
- 239000000706 filtrate Substances 0.000 claims description 10
- 239000008155 medical solution Substances 0.000 claims description 10
- 238000005374 membrane filtration Methods 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 10
- 238000000605 extraction Methods 0.000 claims description 6
- 244000241838 Lycium barbarum Species 0.000 claims description 5
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 5
- 239000006071 cream Substances 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 5
- 230000008014 freezing Effects 0.000 claims description 5
- 238000007710 freezing Methods 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 238000002386 leaching Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 5
- 238000007873 sieving Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- QGXBDMJGAMFCBF-HLUDHZFRSA-N 5α-Androsterone Chemical compound C1[C@H](O)CC[C@]2(C)[C@H]3CC[C@](C)(C(CC4)=O)[C@@H]4[C@@H]3CC[C@H]21 QGXBDMJGAMFCBF-HLUDHZFRSA-N 0.000 abstract description 3
- QGXBDMJGAMFCBF-UHFFFAOYSA-N Etiocholanolone Natural products C1C(O)CCC2(C)C3CCC(C)(C(CC4)=O)C4C3CCC21 QGXBDMJGAMFCBF-UHFFFAOYSA-N 0.000 abstract description 3
- -1 Sphingolipid compound Chemical class 0.000 abstract description 3
- 229940061641 androsterone Drugs 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 3
- 150000004676 glycans Chemical class 0.000 abstract description 3
- 230000036541 health Effects 0.000 abstract description 3
- 230000002401 inhibitory effect Effects 0.000 abstract description 3
- 229920001184 polypeptide Polymers 0.000 abstract description 3
- 229920001282 polysaccharide Polymers 0.000 abstract description 3
- 239000005017 polysaccharide Substances 0.000 abstract description 3
- 102000004196 processed proteins & peptides Human genes 0.000 abstract description 3
- 108090000765 processed proteins & peptides Proteins 0.000 abstract description 3
- 150000003648 triterpenes Chemical class 0.000 abstract description 3
- 201000001320 Atherosclerosis Diseases 0.000 abstract description 2
- 241000304886 Bacilli Species 0.000 abstract description 2
- 241000193830 Bacillus <bacterium> Species 0.000 abstract description 2
- 241000191967 Staphylococcus aureus Species 0.000 abstract description 2
- 208000037386 Typhoid Diseases 0.000 abstract description 2
- 230000032683 aging Effects 0.000 abstract description 2
- 230000003712 anti-aging effect Effects 0.000 abstract description 2
- 230000002929 anti-fatigue Effects 0.000 abstract description 2
- 230000000259 anti-tumor effect Effects 0.000 abstract description 2
- 230000000840 anti-viral effect Effects 0.000 abstract description 2
- 239000003963 antioxidant agent Substances 0.000 abstract description 2
- 230000003078 antioxidant effect Effects 0.000 abstract description 2
- 235000006708 antioxidants Nutrition 0.000 abstract description 2
- 230000007541 cellular toxicity Effects 0.000 abstract description 2
- 230000003750 conditioning effect Effects 0.000 abstract description 2
- 230000002124 endocrine Effects 0.000 abstract description 2
- 230000023597 hemostasis Effects 0.000 abstract description 2
- 201000008297 typhoid fever Diseases 0.000 abstract description 2
- 208000024827 Alzheimer disease Diseases 0.000 abstract 1
- 206010039966 Senile dementia Diseases 0.000 abstract 1
- 230000036039 immunity Effects 0.000 abstract 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
- 241000609666 Tuber aestivum Species 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 229910052749 magnesium Inorganic materials 0.000 description 3
- 241000233866 Fungi Species 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- OIRDTQYFTABQOQ-KQYNXXCUSA-N adenosine Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@@H]1O[C@H](CO)[C@@H](O)[C@H]1O OIRDTQYFTABQOQ-KQYNXXCUSA-N 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- JSPNNZKWADNWHI-PNANGNLXSA-N (2r)-2-hydroxy-n-[(2s,3r,4e,8e)-3-hydroxy-9-methyl-1-[(2r,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoctadeca-4,8-dien-2-yl]heptadecanamide Chemical compound CCCCCCCCCCCCCCC[C@@H](O)C(=O)N[C@H]([C@H](O)\C=C\CC\C=C(/C)CCCCCCCCC)CO[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O JSPNNZKWADNWHI-PNANGNLXSA-N 0.000 description 1
- 239000002126 C01EB10 - Adenosine Substances 0.000 description 1
- YDNKGFDKKRUKPY-JHOUSYSJSA-N C16 ceramide Natural products CCCCCCCCCCCCCCCC(=O)N[C@@H](CO)[C@H](O)C=CCCCCCCCCCCCCC YDNKGFDKKRUKPY-JHOUSYSJSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- CRJGESKKUOMBCT-VQTJNVASSA-N N-acetylsphinganine Chemical compound CCCCCCCCCCCCCCC[C@@H](O)[C@H](CO)NC(C)=O CRJGESKKUOMBCT-VQTJNVASSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 229960005305 adenosine Drugs 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229940106189 ceramide Drugs 0.000 description 1
- ZVEQCJWYRWKARO-UHFFFAOYSA-N ceramide Natural products CCCCCCCCCCCCCCC(O)C(=O)NC(CO)C(O)C=CCCC=C(C)CCCCCCCCC ZVEQCJWYRWKARO-UHFFFAOYSA-N 0.000 description 1
- 229930183167 cerebroside Natural products 0.000 description 1
- RIZIAUKTHDLMQX-UHFFFAOYSA-N cerebroside D Natural products CCCCCCCCCCCCCCCCC(O)C(=O)NC(C(O)C=CCCC=C(C)CCCCCCCCC)COC1OC(CO)C(O)C(O)C1O RIZIAUKTHDLMQX-UHFFFAOYSA-N 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000001963 growth medium Substances 0.000 description 1
- 230000037111 immune power Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- DKXULEFCEORBJK-UHFFFAOYSA-N magnesium;octadecanoic acid Chemical compound [Mg].CCCCCCCCCCCCCCCCCC(O)=O DKXULEFCEORBJK-UHFFFAOYSA-N 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 239000002207 metabolite Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- VVGIYYKRAMHVLU-UHFFFAOYSA-N newbouldiamide Natural products CCCCCCCCCCCCCCCCCCCC(O)C(O)C(O)C(CO)NC(=O)CCCCCCCCCCCCCCCCC VVGIYYKRAMHVLU-UHFFFAOYSA-N 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 150000003408 sphingolipids Chemical class 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L31/00—Edible extracts or preparations of fungi; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Medicines Containing Plant Substances (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses a kind of black pine sealwort tablettings to be related to health product technology field made of the component of following weight percent.Androsterone has supporing yang, the endocrine remarkable efficacy of conditioning in the black pine sealwort tabletting；Sphingolipid compound has apparent activity in terms of preventing senile dementia, atherosclerosis and antitumor cell toxicity；Polysaccharide, polypeptide, triterpene have strengthen immunity, anti-aging, fatigue-resisting function, it can be used for health-care body-nourishing, Rhizoma Polygonati extract has inhibiting effect to typhoid bacillus, staphylococcus aureus, acid-fast bacilli, additionally it is possible to antifatigue, anti-oxidant, slow down aging, hemostasis and antiviral etc..
Description
Technical field
The present invention relates to health product technology field, a kind of specific black pine sealwort tabletting.
Background technology
Tabletting is one kind of dry-press process, and sheet or ring-type are pressed into tablet press machine, can be for molding raw material powder
It is completely dried or has certain humidity.
Black pine, also referred to as ferfas are a kind of wild edible fungis being grown on underground, and appearance is rugged and rough, color and luster between
It is in small convex between dark-brown and black, it is special throughout grey or the texture of light/dark balance and white, smell, it is difficult to shape
Hold, is as far as is known distributed mainly on Alps and the minority area of the Himalaya, modern scientific research data
Display black pine contains abundant protein, 18 kinds of amino acid（The 8 kinds of essential amino acids that cannot be synthesized including human body）, it is unsaturated
The essential trace elements such as aliphatic acid, multivitamin, zinc, manganese, iron, calcium, phosphorus, selenium and sphingolipid, cerebroside, ceramide,
The a large amount of metabolites such as triterpene, androsterone, adenosine, truffle acid, sterol, truffle polysaccharide, truffle polypeptide have high nutrition
Health value.
Invention content
The present invention provides a kind of black pine sealwort tablettings, have outstanding health-care efficacy, wettability is good, is easy to take.
In order to achieve the above object, the present invention is achieved by the following technical programs：It is carried including black pine extract, sealwort
Take object, ostreae testa pulverata, Cordyceps militaris micro mist, ginseng pulverate, Fructus lycii P.E, white granulated sugar, maltose, microcrystalline cellulose and stearic acid
Magnesium, it is characterised in that made of the component of following weight percent：Black pine extract 1~25%, Rhizoma Polygonati extract 1~
15%, ostreae testa pulverata 1~20%, Cordyceps militaris micro mist 1~12%, ginseng pulverate 0.5~8%, Fructus lycii P.E 2~15%, and white granulated sugar 5~
40%, maltose 5~25%, microcrystalline cellulose 3~20%, magnesium stearate 5~30%.
Further, made of the component following weight percent：Black pine extract 5~10%, sealwort extraction
Object 5~15%, ostreae testa pulverata 4~10%, Cordyceps militaris micro mist 6~8%, ginseng pulverate 4~7%, Fructus lycii P.E 3~10%, white granulated sugar 10
~40%, maltose 12~25%, microcrystalline cellulose 10~20%, magnesium stearate 20~30%.
Further, made of the component of following weight percent：Black pine extract 10~20%, Rhizoma Polygonati extract 5
~10%, ostreae testa pulverata 3~9%, Cordyceps militaris micro mist 10~12%, ginseng pulverate 4~8%, Fructus lycii P.E 6~10%, and white granulated sugar 12~
40%, maltose 8~15%, microcrystalline cellulose 10~20%, magnesium stearate 10~14%.
Further, black pine extract is prepared by the following method to obtain：
Black pine is taken, the particle of 3~8mm of diameter is ground into, the water of 10 times of amounts is added, is impregnated 30~60 minutes under room temperature；
Then it decocts 60 minutes, filters to get filtrate at 85~95 DEG C, the water of 10 times of amounts is added in filter residue, decoct 2 times again,
Merge filtrate three times, obtains black pine extracting solution, by membrane filtration, be finally dried to obtain extract with spray-on process.
Further, the Rhizoma Polygonati extract is prepared by the following method to obtain：
Sealwort is cleaned, first with 80% alcohol extracting, then is extracted with water, alcohol extracting is added by being fractionated to obtain extract after the contracting of water concentrate
Alcohol extract is finally dried to obtain extract by membrane filtration with spray-on process.
Further, the Fructus lycii P.E is prepared by the following method to obtain：
The fruit of Chinese wolfberry is removed into impurity, carries out net system；
The fruit of Chinese wolfberry after net system is crushed in freezing crusher, crosses 30 mesh sieve；
In fruit of Chinese wolfberry input supercritical CO 2 extraction device after step is crushed, extracts 1~3 hour, collect extracting solution；
Into the dregs of a decoction, addition quality is the ethyl alcohol that the volumn concentration of 4~6 times of the dregs of a decoction is 60%~80%, is returned in 60 °C~80 °C
Stream 3~6 hours is filtered using 200 mesh silks, collects phegma and residue；
It is 1.20~1.25g/cm3 that obtained phegma, which is concentrated into relative density, obtains concentrate；
The water that 4~6 times of quality of residue are incorporated as into obtained residue decocts 2~3 hours, is filtered using 200 mesh silks, collects
Extracting solution；
It is 1.20~1.25g/cm3 that obtained extracting solution, which is concentrated into relative density, then the extracting solution and step obtained with step 3
Rapid five obtained concentrates are uniformly mixed, and obtain admixing medical solutions；
Obtained admixing medical solutions are placed in and are dried under reduced pressure in case, are dried under reduced pressure under 50 °C~70 °C 2~12 hours, dry leaching is obtained
Cream；
Obtained dry extract is crushed with fluid energy mill, 120 mesh sieve is crossed, obtains dry extract；
Obtained dry extract is mixed 10~15 minutes and is extracted to get the fruit of Chinese wolfberry.
Further, preparation method includes the following steps：
The mixing sieving of S001 raw materials：By black pine extract, Rhizoma Polygonati extract, ostreae testa pulverata, Cordyceps militaris micro mist, ginseng pulverate and matrimony vine
Seed extract crosses 120 mesh sieve respectively, takes out sundries and larger particles, is mixed according to weight percent；
S002 is added auxiliary material and is allocated：The raw material mixed into S001 according to weight percent be added microcrystalline cellulose and
Magnesium stearate；
S003 is stirred：The water that raw material proportion 10~25% is added in the raw material mixed into S002 is stirred mixing, stirs
Mixing 20~30 minutes；
S004 is dried：The raw material that will be stirred in S003, is put into drying box, the temperature control of drying box 60~70 degree into
Row drying；
S005 tablettings：The mixed raw material dried in S004 is put into mold and is press-formed.
Advantageous effect
Androsterone has supporing yang, the endocrine remarkable efficacy of conditioning in black pine sealwort tabletting；Sphingolipid compound is preventing old age
There is apparent activity in terms of dull-witted, atherosclerosis and antitumor cell toxicity；Polysaccharide, polypeptide, triterpene have enhancing immune
Power, anti-aging, fatigue-resisting function, can be used for health-care body-nourishing, and Rhizoma Polygonati extract is to typhoid bacillus, staphylococcus aureus, anti-
Acidfast bacilli has inhibiting effect, sealwort to have different degrees of inhibiting effect to common causative fungi in sabouraud culture medium, additionally it is possible to
It is antifatigue, anti-oxidant, slow down aging, hemostasis and antiviral etc., while the tablet for making slabbing is easy to take and the side of carrying
Just.
Certainly, it implements any of the products of the present invention and does not necessarily require achieving all the advantages described above at the same time.
Specific implementation mode
Embodiment described in the invention is only a part of the embodiment of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Embodiment one
Select black pine extract 1~25%, Rhizoma Polygonati extract 1~15%, ostreae testa pulverata 1~20%, Cordyceps militaris micro mist 1~12%, people
Ginseng powder 0.5~8%, Fructus lycii P.E 2~15%, white granulated sugar 5~40%, maltose 5~25%, microcrystalline cellulose 3~20%, firmly
Fatty acid magnesium 5~30%.
Wherein, black pine extract is prepared by the following method to obtain：
Black pine is taken, the particle of 3~8mm of diameter is ground into, the water of 10 times of amounts is added, is impregnated 30~60 minutes under room temperature；
Then it decocts 60 minutes, filters to get filtrate at 85~95 DEG C, the water of 10 times of amounts is added in filter residue, decoct 2 times again,
Merge filtrate three times, obtains black pine extracting solution, by membrane filtration, be finally dried to obtain extract with spray-on process.
Wherein, the Rhizoma Polygonati extract is prepared by the following method to obtain：
Sealwort is cleaned, first with 80% alcohol extracting, then is extracted with water, alcohol extracting is added by being fractionated to obtain extract after the contracting of water concentrate
Alcohol extract is finally dried to obtain extract by membrane filtration with spray-on process.
Wherein, the Fructus lycii P.E is prepared by the following method to obtain：
The fruit of Chinese wolfberry is removed into impurity, carries out net system；
The fruit of Chinese wolfberry after net system is crushed in freezing crusher, crosses 30 mesh sieve；
In fruit of Chinese wolfberry input supercritical CO 2 extraction device after step is crushed, extracts 1~3 hour, collect extracting solution；
Into the dregs of a decoction, addition quality is the ethyl alcohol that the volumn concentration of 4~6 times of the dregs of a decoction is 60%~80%, is returned in 60 °C~80 °C
Stream 3~6 hours is filtered using 200 mesh silks, collects phegma and residue；
It is 1.20~1.25g/cm3 that obtained phegma, which is concentrated into relative density, obtains concentrate；
The water that 4~6 times of quality of residue are incorporated as into obtained residue decocts 2~3 hours, is filtered using 200 mesh silks, collects
Extracting solution；
It is 1.20~1.25g/cm3 that obtained extracting solution, which is concentrated into relative density, then the extracting solution and step obtained with step 3
Rapid five obtained concentrates are uniformly mixed, and obtain admixing medical solutions；
Obtained admixing medical solutions are placed in and are dried under reduced pressure in case, are dried under reduced pressure under 50 °C~70 °C 2~12 hours, dry leaching is obtained
Cream；
Obtained dry extract is crushed with fluid energy mill, 120 mesh sieve is crossed, obtains dry extract；
Obtained dry extract is mixed 10~15 minutes and is extracted to get the fruit of Chinese wolfberry.
Wherein, preparation method includes the following steps：
The mixing sieving of S001 raw materials：By black pine extract, Rhizoma Polygonati extract, ostreae testa pulverata, Cordyceps militaris micro mist, ginseng pulverate and matrimony vine
Seed extract crosses 120 mesh sieve respectively, takes out sundries and larger particles, is mixed according to weight percent；
S002 is added auxiliary material and is allocated：The raw material mixed into S001 according to weight percent be added microcrystalline cellulose and
Magnesium stearate；
S003 is stirred：The water that raw material proportion 10~25% is added in the raw material mixed into S002 is stirred mixing, stirs
Mixing 20~30 minutes；
S004 is dried：The raw material that will be stirred in S003, is put into drying box, the temperature control of drying box 60~70 degree into
Row drying；
S005 tablettings：The mixed raw material dried in S004 is put into mold and is press-formed.
Embodiment two
Select black pine extract 5~10%, Rhizoma Polygonati extract 5~15%, ostreae testa pulverata 4~10%, Cordyceps militaris micro mist 6~8%, ginseng
Powder 4~7%, Fructus lycii P.E 3~10%, white granulated sugar 10~40%, maltose 12~25%, microcrystalline cellulose 10~20% are stearic
Sour magnesium 20~30%.
Wherein, black pine extract is prepared by the following method to obtain：
Black pine is taken, the particle of 3~8mm of diameter is ground into, the water of 10 times of amounts is added, is impregnated 30~60 minutes under room temperature；
Then it decocts 60 minutes, filters to get filtrate at 85~95 DEG C, the water of 10 times of amounts is added in filter residue, decoct 2 times again,
Merge filtrate three times, obtains black pine extracting solution, by membrane filtration, be finally dried to obtain extract with spray-on process.
Wherein, the Rhizoma Polygonati extract is prepared by the following method to obtain：
Sealwort is cleaned, first with 80% alcohol extracting, then is extracted with water, alcohol extracting is added by being fractionated to obtain extract after the contracting of water concentrate
Alcohol extract is finally dried to obtain extract by membrane filtration with spray-on process.
Wherein, the Fructus lycii P.E is prepared by the following method to obtain：
The fruit of Chinese wolfberry is removed into impurity, carries out net system；
The fruit of Chinese wolfberry after net system is crushed in freezing crusher, crosses 30 mesh sieve；
In fruit of Chinese wolfberry input supercritical CO 2 extraction device after step is crushed, extracts 1~3 hour, collect extracting solution；
Into the dregs of a decoction, addition quality is the ethyl alcohol that the volumn concentration of 4~6 times of the dregs of a decoction is 60%~80%, is returned in 60 °C~80 °C
Stream 3~6 hours is filtered using 200 mesh silks, collects phegma and residue；
It is 1.20~1.25g/cm3 that obtained phegma, which is concentrated into relative density, obtains concentrate；
The water that 4~6 times of quality of residue are incorporated as into obtained residue decocts 2~3 hours, is filtered using 200 mesh silks, collects
Extracting solution；
It is 1.20~1.25g/cm3 that obtained extracting solution, which is concentrated into relative density, then the extracting solution and step obtained with step 3
Rapid five obtained concentrates are uniformly mixed, and obtain admixing medical solutions；
Obtained admixing medical solutions are placed in and are dried under reduced pressure in case, are dried under reduced pressure under 50 °C~70 °C 2~12 hours, dry leaching is obtained
Cream；
Obtained dry extract is crushed with fluid energy mill, 120 mesh sieve is crossed, obtains dry extract；
Obtained dry extract is mixed 10~15 minutes and is extracted to get the fruit of Chinese wolfberry.
Wherein, preparation method includes the following steps：
The mixing sieving of S001 raw materials：By black pine extract, Rhizoma Polygonati extract, ostreae testa pulverata, Cordyceps militaris micro mist, ginseng pulverate and matrimony vine
Seed extract crosses 120 mesh sieve respectively, takes out sundries and larger particles, is mixed according to weight percent；
S002 is added auxiliary material and is allocated：The raw material mixed into S001 according to weight percent be added microcrystalline cellulose and
Magnesium stearate；
S003 is stirred：The water that raw material proportion 10~25% is added in the raw material mixed into S002 is stirred mixing, stirs
Mixing 20~30 minutes；
S004 is dried：The raw material that will be stirred in S003, is put into drying box, the temperature control of drying box 60~70 degree into
Row drying；
S005 tablettings：The mixed raw material dried in S004 is put into mold and is press-formed.
Embodiment three
Select black pine extract 10~20%, Rhizoma Polygonati extract 5~10%, ostreae testa pulverata 3~9%, Cordyceps militaris micro mist 10~12%, people
Ginseng powder 4~8%, Fructus lycii P.E 6~10%, white granulated sugar 12~40%, maltose 8~15%, microcrystalline cellulose 10~20%, firmly
Fatty acid magnesium 10~14%.
Wherein, black pine extract is prepared by the following method to obtain：
Black pine is taken, the particle of 3~8mm of diameter is ground into, the water of 10 times of amounts is added, is impregnated 30~60 minutes under room temperature；
Then it decocts 60 minutes, filters to get filtrate at 85~95 DEG C, the water of 10 times of amounts is added in filter residue, decoct 2 times again,
Merge filtrate three times, obtains black pine extracting solution, by membrane filtration, be finally dried to obtain extract with spray-on process.
Wherein, the Rhizoma Polygonati extract is prepared by the following method to obtain：
Sealwort is cleaned, first with 80% alcohol extracting, then is extracted with water, alcohol extracting is added by being fractionated to obtain extract after the contracting of water concentrate
Alcohol extract is finally dried to obtain extract by membrane filtration with spray-on process.
Wherein, the Fructus lycii P.E is prepared by the following method to obtain：
The fruit of Chinese wolfberry is removed into impurity, carries out net system；
The fruit of Chinese wolfberry after net system is crushed in freezing crusher, crosses 30 mesh sieve；
In fruit of Chinese wolfberry input supercritical CO 2 extraction device after step is crushed, extracts 1~3 hour, collect extracting solution；
Into the dregs of a decoction, addition quality is the ethyl alcohol that the volumn concentration of 4~6 times of the dregs of a decoction is 60%~80%, is returned in 60 °C~80 °C
Stream 3~6 hours is filtered using 200 mesh silks, collects phegma and residue；
It is 1.20~1.25g/cm3 that obtained phegma, which is concentrated into relative density, obtains concentrate；
The water that 4~6 times of quality of residue are incorporated as into obtained residue decocts 2~3 hours, is filtered using 200 mesh silks, collects
Extracting solution；
It is 1.20~1.25g/cm3 that obtained extracting solution, which is concentrated into relative density, then the extracting solution and step obtained with step 3
Rapid five obtained concentrates are uniformly mixed, and obtain admixing medical solutions；
Obtained admixing medical solutions are placed in and are dried under reduced pressure in case, are dried under reduced pressure under 50 °C~70 °C 2~12 hours, dry leaching is obtained
Cream；
Obtained dry extract is crushed with fluid energy mill, 120 mesh sieve is crossed, obtains dry extract；
Obtained dry extract is mixed 10~15 minutes and is extracted to get the fruit of Chinese wolfberry.
Wherein, preparation method includes the following steps：
The mixing sieving of S001 raw materials：By black pine extract, Rhizoma Polygonati extract, ostreae testa pulverata, Cordyceps militaris micro mist, ginseng pulverate and matrimony vine
Seed extract crosses 120 mesh sieve respectively, takes out sundries and larger particles, is mixed according to weight percent；
S002 is added auxiliary material and is allocated：The raw material mixed into S001 according to weight percent be added microcrystalline cellulose and
Magnesium stearate；
S003 is stirred：The water that raw material proportion 10~25% is added in the raw material mixed into S002 is stirred mixing, stirs
Mixing 20~30 minutes；
S004 is dried：The raw material that will be stirred in S003, is put into drying box, the temperature control of drying box 60~70 degree into
Row drying；
S005 tablettings：The mixed raw material dried in S004 is put into mold and is press-formed.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (7)
1. a kind of black pine sealwort tabletting, including black pine extract, Rhizoma Polygonati extract, ostreae testa pulverata, Cordyceps militaris micro mist, ginseng
Powder, Fructus lycii P.E, white granulated sugar, maltose, microcrystalline cellulose and magnesium stearate, it is characterised in that by following weight percent
Component made of：
Black pine extract 1~25%,
Rhizoma Polygonati extract 1~15%,
Ostreae testa pulverata 1~20%,
Cordyceps militaris micro mist 1~12%,
Ginseng pulverate 0.5~8%,
Fructus lycii P.E 2~15%,
White granulated sugar 5~40%,
Maltose 5~25%,
Microcrystalline cellulose 3~20%,
Magnesium stearate 5~30%.
2. a kind of black pine sealwort tabletting according to claim 1, it is characterised in that by the component of following weight percent
It is manufactured：
Black pine extract 5~10%,
Rhizoma Polygonati extract 5~15%,
Ostreae testa pulverata 4~10%,
Cordyceps militaris micro mist 6~8%,
Ginseng pulverate 4~7%,
Fructus lycii P.E 3~10%,
White granulated sugar 10~40%,
Maltose 12~25%,
Microcrystalline cellulose 10~20%,
Magnesium stearate 20~30%.
3. a kind of black pine sealwort tabletting according to claim 1, it is characterised in that by the component of following weight percent
It is manufactured：
Black pine extract 10~20%,
Rhizoma Polygonati extract 5~10%,
Ostreae testa pulverata 3~9%,
Cordyceps militaris micro mist 10~12%,
Ginseng pulverate 4~8%,
Fructus lycii P.E 6~10%,
White granulated sugar 12~40%,
Maltose 8~15%,
Microcrystalline cellulose 10~20%,
Magnesium stearate 10~14%.
4. a kind of black pine sealwort tabletting according to claim 1, it is characterised in that black pine extract is by following
What method was prepared：
Black pine is taken, the particle of 3~8mm of diameter is ground into, the water of 10 times of amounts is added, is impregnated 30~60 minutes under room temperature；
Then it decocts 60 minutes, filters to get filtrate at 85~95 DEG C, the water of 10 times of amounts is added in filter residue, decoct 2 times again,
Merge filtrate three times, obtains black pine extracting solution, by membrane filtration, be finally dried to obtain extract with spray-on process.
5. a kind of black pine sealwort tabletting according to claim 1, it is characterised in that Rhizoma Polygonati extract is by with lower section
What method was prepared：
Sealwort is cleaned, first with 80% alcohol extracting, then is extracted with water, alcohol extracting is added by being fractionated to obtain extract after the contracting of water concentrate
Alcohol extract is finally dried to obtain extract by membrane filtration with spray-on process.
6. a kind of black pine sealwort tabletting according to claim 1, it is characterised in that Fructus lycii P.E is by following
What method was prepared：
The fruit of Chinese wolfberry is removed into impurity, carries out net system；
The fruit of Chinese wolfberry after net system is crushed in freezing crusher, crosses 30 mesh sieve；
In fruit of Chinese wolfberry input supercritical CO 2 extraction device after step is crushed, extracts 1~3 hour, collect extracting solution；
Into the dregs of a decoction, addition quality is the ethyl alcohol that the volumn concentration of 4~6 times of the dregs of a decoction is 60%~80%, is returned in 60 °C~80 °C
Stream 3~6 hours is filtered using 200 mesh silks, collects phegma and residue；
It is 1.20~1.25g/cm3 that obtained phegma, which is concentrated into relative density, obtains concentrate；
The water that 4~6 times of quality of residue are incorporated as into obtained residue decocts 2~3 hours, is filtered using 200 mesh silks, collects
Extracting solution；
It is 1.20~1.25g/cm3 that obtained extracting solution, which is concentrated into relative density, then the extracting solution and step obtained with step 3
Rapid five obtained concentrates are uniformly mixed, and obtain admixing medical solutions；
Obtained admixing medical solutions are placed in and are dried under reduced pressure in case, are dried under reduced pressure under 50 °C~70 °C 2~12 hours, dry leaching is obtained
Cream；
Obtained dry extract is crushed with fluid energy mill, 120 mesh sieve is crossed, obtains dry extract；
Obtained dry extract is mixed 10~15 minutes and is extracted to get the fruit of Chinese wolfberry.
7. according to a kind of any one black pine sealwort tabletting preparation methods of claim 1-7, it is characterised in that including such as
Lower step：
The mixing sieving of S001 raw materials：By black pine extract, Rhizoma Polygonati extract, ostreae testa pulverata, Cordyceps militaris micro mist, ginseng pulverate and matrimony vine
Seed extract crosses 120 mesh sieve respectively, takes out sundries and larger particles, is mixed according to weight percent；
S002 is added auxiliary material and is allocated：The raw material mixed into S001 according to weight percent be added microcrystalline cellulose and
Magnesium stearate；
S003 is stirred：The water that raw material proportion 10~25% is added in the raw material mixed into S002 is stirred mixing, stirs
Mixing 20~30 minutes；
S004 is dried：The raw material that will be stirred in S003, is put into drying box, the temperature control of drying box 60~70 degree into
Row drying；
S005 tablettings：The mixed raw material dried in S004 is put into mold and is press-formed.
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| CN112022955A (en) * | 2020-09-15 | 2020-12-04 | 安徽三九药业有限公司 | Black truffle, cordyceps sinensis and rhizoma polygonati granules and preparation method thereof |
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