CN108623389A - A kind of preparation method of multifunctional efficient foliar fertilizer - Google Patents
A kind of preparation method of multifunctional efficient foliar fertilizer Download PDFInfo
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- CN108623389A CN108623389A CN201810675844.4A CN201810675844A CN108623389A CN 108623389 A CN108623389 A CN 108623389A CN 201810675844 A CN201810675844 A CN 201810675844A CN 108623389 A CN108623389 A CN 108623389A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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Abstract
The invention discloses a kind of preparation methods of multifunctional efficient foliar fertilizer, are related to foliar fertilizer technical field, include the following steps：It takes recessed native powder to grind, is added glycyrrhizic acid and apiolin mixing after heat temperature raising, under stirring condition, add part natural botanical extraction liquid, after heat temperature raising, insulated and stirred obtains material A；It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after heat temperature raising, add Blumea oil and material B is mixed to obtain；It takes the natural botanical extraction liquid of surplus to heat, under stirring condition, sequentially adds water-soluble highland barley beta glucan, trace element, amino acid powder and stir to obtain material C；Material C is taken, material B mixings are added, material A stirring, ultrasound are added after heating.The foliar fertilizer of the present invention prepares simple and convenient, and disease resisting effect is good, increasing both production and income, high financial profit.
Description
Technical field
The present invention relates to foliar fertilizer technical fields, and in particular to a kind of preparation method of multifunctional efficient foliar fertilizer.
Background technology
Foliar fertilizer refers to that nutrient needed for crop is directly applied to the fertilizer on blade face for the purpose of Foliage Absorption.Foliar fertilizer is
Nutrient is applied to crops blade surface, and a kind of fertilizer type of base function is played by the absorption of blade, plant
Blade has upper layer and lower layer table seed, is made of table seed cell, there is cuticula and wax on table on the outside of cell, can protect table seed group
Mesophyll cell under knitting exercises the functions such as photosynthetic, breathing, is not influenced by the variation of extraneous unfavorable conditions, and there are many more blade performances
Small stomata exercises the function that gas is replaced.Foliar fertilizer can be penetrated by micropore in blade after being applied to leaf surfaces.
But the antibacterial insecticidal effect of foliar fertilizer is not fine at present, causes crop yield to be difficult to be promoted, therefore, develops one
Kind antibacterial desinsection, increasing both production and income corps leaf surface fertilizer quite it is necessary to.
The patent application of Publication No. CN106348942A discloses a kind of insecticidal foliar fertilizer for tripterygium, by following mass fraction
Formula components form：6-8 parts of cypermethrin, 2-4 parts of natural complex, 1-2 parts of bacterium for killing insect, humic acid chelating trace element 3-5
Part, 5-7 parts of amino-oligosaccharide, 2-4 parts of penta chrysanthemum of trichlorine cyanogen, 3-5 parts of tripterygium wilfordii extracting solution, 6-8 parts of corn flour, distilled water 200-
300 parts.This kind of foliar fertilizer can make crop yield higher, but prevention and control of plant diseases, pest control cost is higher in implementation process, foliar fertilizer
The antibacterial insecticidal effect of material is poor.
The patent application for authorizing Publication No. CN102336605B, disclose a kind of amino acid foliar fertilizer for ramie and its
Preparation method, the fertilizer are formulated by the raw material of following weight percentage：Amino acid 1 5~20%, potassium nitrate 0.5~1%,
Potassium sulfate 0.5~1%, calcium nitrate 0.1~0.3%, magnesium sulfate 0.15~0.3%, manganese sulfate 0.05~0.1%, five water sulfuric acid
Copper 0.25~0.5%, white vitriol 0.25~0.5%, ammonium tetramolybdate 0.1~0.2%, ferrous sulfate 0.2~0.5%,
How are NaFeEDTA sodium 0.5~1.5%, boric acid 1~2%, ammonium nitrate 1.5~2.5%, arsenic determination 0.05~0.15%, α-
Acetic acid 0.01~0.03%, compound sodium nitrophenolate 0.1~0.2%, ammonium phosphate 1~5%, remaining be water, the sum of each component be 100%；
Ramie yield and quality can be improved in this kind of foliar fertilizer, but its antibacterial disinsection efficiency also needs to improve.
Invention content
The purpose of the present invention is to provide a kind of preparation method of multifunctional efficient foliar fertilizer, this kind of foliar fertilizer is disease-resistant
Effect is good, increasing both production and income, high financial profit.
In order to achieve the above object, the present invention is achieved through the following technical solutions：
A kind of preparation method of multifunctional efficient foliar fertilizer, includes the following steps：
Ⅰ：It is 300-400 μm to take recessed native powder to be ground to fineness, is heated to 42-46 DEG C, glycyrrhizic acid and apiolin is added
6-8min is mixed, under stirring condition, adds the natural botanical extraction liquid of parts by weight 58-66%, is heated to 48-52
After DEG C, insulated and stirred 10-15min obtains material A；
Ⅱ：Under stirring, take allyl sulfides to be added in propylene glycol and be sufficiently stirred, after being heated to 40-44 DEG C, then to its
Middle addition Blumea oil is slowly mixed together stirring 20-25min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus, is heated to 38-42 DEG C, under stirring condition, sequentially adds water-soluble
Property highland barley Beta-dextran, trace element, amino acid powder, then speed of agitator be 100-120r/min under the conditions of be kept stirring 8-
10min obtains material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 42-46 DEG C, it is mixed to add material A
After closing stirring 2-4min, ultrasonic disperse 8-10min.
Further, the preparation method of above-mentioned foliar fertilizer includes the following steps：
Ⅰ：It is 320-380 μm to take recessed native powder to be ground to fineness, is heated to 43-45 DEG C, glycyrrhizic acid and apiolin is added
6.5-7.5min is mixed, under stirring condition, adds the natural botanical extraction liquid of parts by weight 60-64%, is heated to
After 49-51 DEG C, insulated and stirred 11-14min obtains material A；
Ⅱ：Under stirring, take allyl sulfides to be added in propylene glycol and be sufficiently stirred, after being heated to 41-43 DEG C, then to its
Middle addition Blumea oil is slowly mixed together stirring 21-24min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus, is heated to 39-41 DEG C, under stirring condition, sequentially adds water-soluble
Property highland barley Beta-dextran, trace element, amino acid powder, then speed of agitator be 105-115r/min under the conditions of be kept stirring
8.5-9.5min obtains material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 43-45 DEG C, it is mixed to add material A
After closing stirring 2.5-3.5min, ultrasonic disperse 8.5-9.5min.
Further, the preparation method of above-mentioned foliar fertilizer includes the following steps：
Ⅰ：It is 320 μm to take recessed native powder to be ground to fineness, is heated to 43 DEG C, and glycyrrhizic acid is added and apiolin is mixed
7.5min under stirring condition, adds the natural botanical extraction liquid of parts by weight 60%, after being heated to 49 DEG C, insulated and stirred
14min obtains material A；
Ⅱ：It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after being heated to 41 DEG C, then thereto
Blumea oil is added and is slowly mixed together stirring 24min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus is heated to 39 DEG C, under stirring condition, sequentially adds water solubility
Highland barley Beta-dextran, trace element, amino acid powder are then kept stirring 9.5min under the conditions of speed of agitator is 105r/min,
Obtain material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 43 DEG C, material A mixing is added and stirs
After mixing 3.5min, ultrasonic disperse 9.5min.
Further, above-mentioned foliar fertilizer includes following raw material by weight：
It is 1.8-2.2 parts micro-；
2.4-2.8 parts of allyl sulfides；
4.5-5.5 parts of Blumea oil；
1.2-1.8 parts of glycyrrhizic acid；
1.75-2.3 parts of apiolin；
Recessed 17-19 parts of powder of soil；
6.5-7.5 parts of propylene glycol；
Water-soluble highland barley Beta-dextran 1.15-1.35 parts；
2.25-2.7 parts of composite bacterium powder；
2.8-3.2 parts of amino acid powder；
34-38 parts of natural botanical extraction liquid.
Further, above-mentioned foliar fertilizer is made of following raw material by weight：
1.8 parts of trace element；
2.4 parts of allyl sulfides；
4.5 parts of Blumea oil；
1.2 parts of glycyrrhizic acid；
1.75 parts of apiolin；
Recessed 17 parts of powder of soil；
6.5 parts of propylene glycol；
1.15 parts of water-soluble highland barley Beta-dextran；
2.25 parts of composite bacterium powder；
2.8 parts of amino acid powder；
34 parts of natural botanical extraction liquid.
Preferably, above-mentioned trace element is made of following composition by weight：1.2 parts of ammonium molybdate, manganese sulfate 1.2
Part, 2.4 parts of ferrous sulfate, 2.4 parts of borax, 1.7 parts of zinc sulfate, 4.5 parts of potassium dihydrogen phosphate.
Preferably, above-mentioned composite bacterium powder is using fixed nitrogen series bacillus, streptomyces microflavus, bacillus licheniformis, Su Yunjin
Bacillus is according to mass ratio 1.5:3.5:2.2:1.2 are fully blended.
Preferably, above-mentioned amino acid powder is made of following composition by weight：1.6 parts of glycine, leucine 3.2
Part, 1.4 parts of alanine, 1.2 parts of tryptophan, 2.2 parts of lysine, 2.4 parts of glutamic acid, 1.2 parts of arginine.
Further, above-mentioned natural botanical extraction liquid is made by following steps：By weight 3.5:1.2 take fresh wood
Rhinoceros grass, olive leaf, the water that 4.5 times of its weight is added after being smashed to pieces decoct 35min, ultrasonic extraction 5.2min, after centrifugal filtration
The water that 3.5 times of filter residue weight is added into filter residue decocts 46min, ultrasonic extraction 3.2min, and after centrifugal filtration, merging is filtered twice
Liquid is concentrated into the 1/4 of original volume to obtain the final product.
Further, further include in above-mentioned foliar fertilizer parts by weight be 0.4 surfactant.
The present invention has following advantageous effect：The foliar fertilizer of the present invention by ingenious selection to raw materials for production and its
The inventive improvements of preparation process, the collaboration phase of the compositions such as allyl sulfides, Blumea oil, glycyrrhizic acid, apiolin, recessed native powder in raw material
Interaction makes foliar fertilizer obtained reach following effect in the application：
(1) raw materials for production have preferable dissolubility, dispersibility and compatibility, and product solution stable homogeneous, green is harmless,
Precipitation is not generated, is easily stored；
(2) nutrition is comprehensive, and the fertilizer efficiency duration is long, and utilization rate is high, not easily runs off, absorbent properties are good, can preferably fit
Match, promote plant growth healthy and strong in conjunction with organic fertilizer, improve crop yield and quality, reduce abnormal rate, improves appearance and mouthfeel, warp
It helps profitable；
(3) enhance the anti-adversity ability of crops, disease incidence is low, improves survival rate, reduces the use of agriculture chemical, drops
Low planting cost, further improves crop yield and quality.
Specific implementation mode
The specific implementation mode of the present invention is further described with reference to embodiment, following embodiment is only used for more
Technical scheme of the present invention is clearly demonstrated, and not intended to limit the protection scope of the present invention.
It all raw materials in embodiment and its produces composition and can be obtained by disclosed commercially available channel；
Embodiment 1
The present embodiment is related to a kind of multifunctional efficient foliar fertilizer and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter：
1.5 parts of trace element；
2 parts of allyl sulfides；
4 parts of Blumea oil；
1 part of glycyrrhizic acid；
1.5 parts of apiolin；
Recessed 16 parts of powder of soil；
6 parts of propylene glycol；
1 part of water-soluble highland barley Beta-dextran；
2 parts of composite bacterium powder；
2.5 parts of amino acid powder；
30 parts of natural botanical extraction liquid；
Trace element in the present embodiment, composite bacterium powder and amino acid powder selection and produce as shown in table 1 below：
Table 1
In addition, natural botanical extraction liquid is made by following steps：By weight 3:1 takes fresh reseda, olive leaf,
The water that 4 times of its weight is added after being smashed to pieces decocts 34min, ultrasonic extraction 5min, and 3 times of filters are added after centrifugal filtration into filter residue
The water of slag weight decocts 45min, ultrasonic extraction 3min, after centrifugal filtration, merges filtrate twice, is concentrated into the 1/4 of original volume i.e.
.
The preparation method of foliar fertilizer is carried out according to following general steps in the present embodiment：
Ⅰ：It is 300 μm to take recessed native powder to be ground to fineness, is heated to 42 DEG C, and glycyrrhizic acid is added and apiolin is mixed
8min under stirring condition, adds the natural botanical extraction liquid of parts by weight 58%, after being heated to 48 DEG C, insulated and stirred
15min obtains material A；
Ⅱ：It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after being heated to 40 DEG C, then thereto
Blumea oil is added and is slowly mixed together stirring 25min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus is heated to 38 DEG C, under stirring condition, sequentially adds water solubility
Highland barley Beta-dextran, trace element, amino acid powder are then kept stirring 10min under the conditions of speed of agitator is 100r/min, obtain
Material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 42 DEG C, material A mixing is added and stirs
After mixing 4min, after ultrasonic disperse 10min, remaining other raw material mixings are added.
Embodiment 2
The present embodiment is related to a kind of multifunctional efficient foliar fertilizer and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter：
1.8 parts of trace element；
2.4 parts of allyl sulfides；
4.5 parts of Blumea oil；
1.2 parts of glycyrrhizic acid；
1.75 parts of apiolin；
Recessed 17 parts of powder of soil；
6.5 parts of propylene glycol；
1.15 parts of water-soluble highland barley Beta-dextran；
2.25 parts of composite bacterium powder；
2.8 parts of amino acid powder；
34 parts of natural botanical extraction liquid.
Trace element in the present embodiment, composite bacterium powder and amino acid powder selection and produce as shown in table 2 below：
Table 2
In addition, natural botanical extraction liquid is made by following steps：By weight 3.5:1.2 take fresh reseda, olive
Olive leaf, the water that 4.5 times of its weight is added after being smashed to pieces decoct 35min, ultrasonic extraction 5.2min, after centrifugal filtration into filter residue
The water that 3.5 times of filter residue weight is added decocts 46min, ultrasonic extraction 3.2min, after centrifugal filtration, merges filtrate twice, is concentrated into
The 1/4 of original volume to obtain the final product.
The preparation method of foliar fertilizer is carried out according to following general steps in the present embodiment：
Ⅰ：It is 320 μm to take recessed native powder to be ground to fineness, is heated to 43 DEG C, and glycyrrhizic acid is added and apiolin is mixed
7.5min under stirring condition, adds the natural botanical extraction liquid of parts by weight 60%, after being heated to 49 DEG C, insulated and stirred
14min obtains material A；
Ⅱ：It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after being heated to 41 DEG C, then thereto
Blumea oil is added and is slowly mixed together stirring 24min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus is heated to 39 DEG C, under stirring condition, sequentially adds water solubility
Highland barley Beta-dextran, trace element, amino acid powder are then kept stirring 9.5min under the conditions of speed of agitator is 105r/min,
Obtain material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 43 DEG C, material A mixing is added and stirs
After mixing 3.5min, after ultrasonic disperse 9.5min, remaining other raw material mixings are added.
Embodiment 3
The present embodiment is related to a kind of multifunctional efficient foliar fertilizer and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter：
2 parts of trace element；
2.6 parts of allyl sulfides；
5 parts of Blumea oil；
1.5 parts of glycyrrhizic acid；
2 parts of apiolin；
Recessed 18 parts of powder of soil；
7 parts of propylene glycol；
1.25 parts of water-soluble highland barley Beta-dextran；
2.5 parts of composite bacterium powder；
3 parts of amino acid powder；
35 parts of natural botanical extraction liquid；
0.4 part of surfactant.
Trace element in the present embodiment, composite bacterium powder, amino acid powder and surfactant selection and produce such as the following table 3
It is shown：
Table 3
In addition, natural botanical extraction liquid is made by following steps：By weight 4:1.5 take fresh reseda, olive
Leaf, the water that 5 times of its weight is added after being smashed to pieces decoct 36min, and ultrasonic extraction 5.5min is added after centrifugal filtration into filter residue
The water of 4 times of filter residue weight decocts 48min, ultrasonic extraction 3.5min, after centrifugal filtration, merges filtrate twice, is concentrated into original volume
1/4 to obtain the final product.
The preparation method of foliar fertilizer is carried out according to following general steps in the present embodiment：
Ⅰ：It is 350 μm to take recessed native powder to be ground to fineness, is heated to 44 DEG C, and glycyrrhizic acid is added and apiolin is mixed
7min under stirring condition, adds the natural botanical extraction liquid of parts by weight 62%, after being heated to 50 DEG C, insulated and stirred
12.5min obtains material A；
Ⅱ：It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after being heated to 42 DEG C, then thereto
Blumea oil is added and is slowly mixed together stirring 23min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus is heated to 40 DEG C, under stirring condition, sequentially adds water solubility
Highland barley Beta-dextran, trace element, amino acid powder are then kept stirring 9min under the conditions of speed of agitator is 110r/min, obtain
Material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 44 DEG C, material A mixing is added and stirs
After mixing 3min, after ultrasonic disperse 9min, remaining other raw material mixings are added.
Embodiment 4
The present embodiment is related to a kind of multifunctional efficient foliar fertilizer and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter：
2.2 parts of trace element；
2.8 parts of allyl sulfides；
5.5 parts of Blumea oil；
1.8 parts of glycyrrhizic acid；
2.3 parts of apiolin；
Recessed 19 parts of powder of soil；
7.5 parts of propylene glycol；
1.35 parts of water-soluble highland barley Beta-dextran；
2.7 parts of composite bacterium powder；
3.2 parts of amino acid powder；
38 parts of natural botanical extraction liquid；
0.5 part of surfactant.
Trace element in the present embodiment, composite bacterium powder, amino acid powder and surfactant selection and produce such as the following table 4
It is shown：
Table 4
In addition, natural botanical extraction liquid is made by following steps：By weight 4.5:1.8 take fresh reseda, olive
Olive leaf, the water that 5.5 times of its weight is added after being smashed to pieces decoct 37min, ultrasonic extraction 5.8min, after centrifugal filtration into filter residue
The water that 4.5 times of filter residue weight is added decocts 49min, ultrasonic extraction 3.6min, after centrifugal filtration, merges filtrate twice, is concentrated into
The 1/4 of original volume to obtain the final product.
The preparation method of foliar fertilizer is carried out according to following general steps in the present embodiment：
Ⅰ：It is 380 μm to take recessed native powder to be ground to fineness, is heated to 45 DEG C, and glycyrrhizic acid is added and apiolin is mixed
6.5min under stirring condition, adds the natural botanical extraction liquid of parts by weight 64%, after being heated to 51 DEG C, insulated and stirred
11min obtains material A；
Ⅱ：It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after being heated to 43 DEG C, then thereto
Blumea oil is added and is slowly mixed together stirring 21min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus is heated to 41 DEG C, under stirring condition, sequentially adds water solubility
Highland barley Beta-dextran, trace element, amino acid powder are then kept stirring 8.5min under the conditions of speed of agitator is 115r/min,
Obtain material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 45 DEG C, material A mixing is added and stirs
After mixing 2.5min, after ultrasonic disperse 8.5min, remaining other raw material mixings are added.
Embodiment 5
The present embodiment is related to a kind of multifunctional efficient foliar fertilizer and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter：
2.5 parts of trace element；
3.5 parts of allyl sulfides；
6 parts of Blumea oil；
2 parts of glycyrrhizic acid；
2.5 parts of apiolin；
Recessed 20 parts of powder of soil；
8 parts of propylene glycol；
1.5 parts of water-soluble highland barley Beta-dextran；
3 parts of composite bacterium powder；
3.5 parts of amino acid powder；
40 parts of natural botanical extraction liquid；
0.6 part of surfactant.
Trace element in the present embodiment, composite bacterium powder, amino acid powder and surfactant selection and produce such as the following table 5
It is shown：
Table 5
In addition, natural botanical extraction liquid is made by following steps：By weight 5:2 take fresh reseda, olive leaf,
The water that 6 times of its weight is added after being smashed to pieces decocts 38min, ultrasonic extraction 6min, and 5 times of filters are added after centrifugal filtration into filter residue
The water of slag weight decocts 50min, ultrasonic extraction 4min, after centrifugal filtration, merges filtrate twice, is concentrated into the 1/4 of original volume i.e.
.
The preparation method of foliar fertilizer is carried out according to following general steps in the present embodiment：
Ⅰ：It is 400 μm to take recessed native powder to be ground to fineness, is heated to 46 DEG C, and glycyrrhizic acid is added and apiolin is mixed
6min under stirring condition, adds the natural botanical extraction liquid of parts by weight 66%, after being heated to 52 DEG C, insulated and stirred
10min obtains material A；
Ⅱ：It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after being heated to 44 DEG C, then thereto
Blumea oil is added and is slowly mixed together stirring 20min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus is heated to 42 DEG C, under stirring condition, sequentially adds water solubility
Highland barley Beta-dextran, trace element, amino acid powder are then kept stirring 8min under the conditions of speed of agitator is 120r/min, obtain
Material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 46 DEG C, material A mixing is added and stirs
After mixing 2min, after ultrasonic disperse 8min, remaining other raw material mixings are added.
Comparative example 1
This comparative example is related to a kind of foliar fertilizer, is added to making for trace element less relative to embodiment 1, in component
With other compositions and content all same, preparation method is close with embodiment 1, i.e., has lacked trace element in step III
It is prepared by addition.
Comparative example 2
This comparative example is related to a kind of foliar fertilizer, relative to embodiment 2, is added to making for composite bacterium powder in component less
With other compositions and content all same, preparation method is close with embodiment 2, i.e., has lacked composite bacterium powder in step IV
It is prepared by addition.
Comparative example 3
This comparative example is related to a kind of foliar fertilizer, relative to embodiment 3, is added to making for amino acid powder in component less
With other compositions and content all same, preparation method is close with embodiment 3, i.e., has lacked amino acid powder in step III
It is prepared by addition.
Comparative example 4
This comparative example is related to a kind of preparation method of foliar fertilizer, relative to embodiment 4, ingredient and its content in component
All same, but preparation method is different from embodiment 4, is operated using the method being simply blended, it is as follows：Propylene glycol is taken, is added
Enter allyl sulfides, Blumea oil, after being thoroughly mixed, be heated to 42 DEG C, adds natural botanical extraction liquid stirring
Remaining other raw material mixings are added later under agitation in 15min.
Comparative example 5
This comparative example is related to a kind of foliar fertilizer, relative to embodiment 5, is added to allyl sulfides, folium artemisiae argyi in component less
The use of oil, glycyrrhizic acid, apiolin, other compositions and content all same, preparation method adjust accordingly, as follows：It takes
Surfactant, trace element, propylene glycol, water-soluble highland barley Beta-dextran, composite bacterium powder and amino acid powder is added in recessed soil powder
It is sufficiently mixed, obtains prefabricated material；Natural botanical extraction liquid is taken, is heated to 42 DEG C, under agitation slowly by prefabricated material
It is added to mixing in natural botanical extraction liquid.
Comparative example 6
This comparative example is related to a kind of foliar fertilizer comprising composition by weight percentage below：Amino acid 1 5~
20%, potassium nitrate 0.5~1%, potassium sulfate 0.5~1%, calcium nitrate 0.1~0.3%, magnesium sulfate 0.15~0.3%, manganese sulfate
0.05~0.1%, cupric sulfate pentahydrate 0.25~0.5%, white vitriol 0.25~0.5%, ammonium tetramolybdate 0.1~0.2%, sulphur
Sour ferrous iron 0.2~0.5%, NaFeEDTA sodium 0.5~1.5%, boric acid 1~2%, ammonium nitrate 1.5~2.5%, arsenic determination
0.05~0.15%, α-niacin 0.01~0.03%, compound sodium nitrophenolate 0.1~0.2%, ammonium phosphate 1~5%, remaining be water, respectively
The sum of component is 100%.
Implementation result
To verify the advantageous effect of the present invention, using foliar fertilizer made from above-described embodiment 1-5 and comparative example 1-6 as gumbo
And the foliage dressing in the growth period of pomelo shaddock, and carry out the test of following test operation and index substantially：
Test operation：In gumbo, the pomelo shaddock growth most productive period is sprayed, and (embodiment 1-5 corresponds to experimental field 1-5, comparative example
1-6 corresponds to experimental field 6-11, experimental field planting conditions all same), in conjunction with organic composite base fertilizer, gumbo uses and was sprayed every 20 days
Foliar fertilizer is primary, and the amount of spraying is 280g/ mus, and (foliar fertilizer is 1 with water dilution rate ratio:25), pomelo shaddock uses sprayed leaf every 16 days
Leaven is primary, and the amount of spraying is 320g/ mus, and (foliar fertilizer is 1 with water dilution rate ratio:25), experimental period, does not use agriculture chemical additionally
The prevention of growth promotion and pest and disease damage is carried out, experimental period is until crop maturity, record crop yield, disease and quality conditions.
Gumbo
One, about crop yield situation, 6 be see the table below；
Table 6：
| Object | Kg/ mus of yield | Rate of growth (%) when compared to previous harvest |
| Experimental field 1 | 3720 | 55.00 |
| Experimental field 2 | 3770 | 57.08 |
| Experimental field 3 | 3810 | 58.75 |
| Experimental field 4 | 3750 | 56.25 |
| Experimental field 5 | 3640 | 51.67 |
| Experimental field 6 | 3210 | 33.75 |
| Experimental field 7 | 3350 | 39.58 |
| Experimental field 8 | 3100 | 29.17 |
| Experimental field 9 | 3420 | 42.50 |
| Experimental field 10 | 2730 | 13.75 |
| Experimental field 11 | 2890 | 20.41 |
Illustrate, previous common foliar fertilizer per mu yield is about in 2400kg or so；
By upper table 6 it is found that in the growing and cultivation of gumbo, foliar fertilizer of the invention is improved compared to comparative example in rate of growth
9.17-45 percentage points, there is significant yield increase effect, can preferably improve the economic well-being of workers and staff of peasant household.
Two, about crop disease situation, 7 be see the table below；
Table 7：
By upper table 7 it is found that in the growing and cultivation of gumbo, foliar fertilizer of the invention is compared to comparative example in disease incidence
On reduce 2.09-11.28 percentage points, survival rate improves 6.02-15.84 percentage points, no agriculture chemical the case where
Under, disease prevention effect is more preferable, survival rate higher.
Three, about crop quality situation, 8 be see the table below；
Table 8：
By upper table 8 it is found that in the growing and cultivation of gumbo, foliar fertilizer of the invention compared to comparative example appearance condition with
And it is more preferable in mouthfeel situation, and 2.89-11.33 percentage points is reduced on gumbo abnormal rate, gumbo crop quality obtains
Preferably effectively promoted.
Pomelo shaddock
One, about crop yield situation, 9 be see the table below；
Table 9：
| Object | Kg/ mus of yield | Rate of growth (%) when compared to previous harvest |
| Experimental field 1 | 4340 | 35.63 |
| Experimental field 2 | 4270 | 33.44 |
| Experimental field 3 | 4520 | 41.25 |
| Experimental field 4 | 4450 | 39.06 |
| Experimental field 5 | 4260 | 33.13 |
| Experimental field 6 | 3810 | 19.06 |
| Experimental field 7 | 3850 | 20.31 |
| Experimental field 8 | 3770 | 17.81 |
| Experimental field 9 | 4080 | 27.50 |
| Experimental field 10 | 3440 | 6.25 |
| Experimental field 11 | 3790 | 18.44 |
Illustrate, previous common foliar fertilizer per mu yield is about in 3200kg or so；
By upper table 9 it is found that in the growing and cultivation of pomelo shaddock, foliar fertilizer of the invention is compared to comparative example in rate of growth
5.63-35.00 percentage points are improved, there is significant yield increase effect, can preferably improve the economic well-being of workers and staff of peasant household.Two, it closes
In crop disease situation, 10 are see the table below；
Table 10：
By upper table 10 it is found that in the growing and cultivation of pomelo shaddock, foliar fertilizer of the invention is sent out compared to comparative example in disease
5.02-14.44 percentage points is reduced in raw rate, survival rate improves 3.64-13.67 percentage points, in no agriculture chemical
In the case of, disease prevention effect is more preferable, survival rate higher.
Three, about crop quality situation, 11 be see the table below；
Table 11：
By upper table 11 it is found that in the growing and cultivation of pomelo shaddock, the pomelo shaddock that foliar fertilizer of the invention obtains is compared to comparison
Example more preferably, and will reduce 2.25-17.20 percentage points on appearance condition and mouthfeel situation on pomelo's shaddock abnormal rate,
Pomelo's shaddock crop quality obtains preferably effectively being promoted.
In conjunction with the excellent effect of the present invention, applicant is illustrated the constituent part and preparation method of the present invention：
(1) micro-：Trace element is one of nutriment necessary to plant growth, have it is a variety of, including
Iron (Fe), manganese (Mn), zinc (Zn), copper (Cu), boron (B), molybdenum (Mo), chlorine (Cl), sodium (Na), nickel (Ni) etc., trace element in institute
Number containing ingredient and its content is all different the growth effect of Different Crop, some trace element formulas, Ke Nenggeng
Suitable for the development of certain crop, growth can be promoted, improved the yield and quality, but this kind of trace element formula, it is also possible to no
Suitable for the utilization of another crop, very little is helped to crop growth, if possibly even leading to yield product if excess
The problem of matter declines；Therefore, applicant has allotted the trace element of the present invention through many experiments group after the above situation is contemplated
Formula, it is verified to obtain this kind of trace element formula and be applied in foliar fertilizer, it can preferably improve gumbo and pomelo shaddock
Yield and quality；If wherein certain ingredient change, addition or/and missing beneficial effects of the present invention and mesh will be not achieved
's.
(2) amino acid powder：Why aminoacid ingredient is contained in the foliar fertilizer of the present invention, and mainly applicant considers ammonia
Base acid as constitute protein smallest molecule can preferably be present in the present invention foliar fertilizer system in, have be easier to by
The characteristics of crop absorbs；Applicant has been surprisingly found that during preparing Amino Acid Composition, according to following parts by weight：Glycine 1.5-
2.5 parts, 3-4 parts of leucine, 1-2 parts of alanine, 1-2 parts of tryptophan, 2-3 parts of lysine, 2-3 parts of glutamic acid, arginine 1-2
Part, the amino acid powder assembled can improve crop resistance, improve fertilising crop quality, stimulation and the adjusting fast fast-growing of crop
It is long, promote plant growth healthy and strong, promotes its absorption to nutriment；The selection of above-mentioned Amino Acid Composition is not applicant
Arbitrarily, combination without thinking obtains, such as：Glycine is selected to allow for it not only and can improve gumbo and pomelo shaddock
Resistance can also increase chlorophyll content of plant, improve the activity of enzyme, promote the infiltration of carbon dioxide, make photosynthesis more
It is vigorous, play the role of to raising crop quality positive；Gumbo can not only be promoted by for example selecting tryptophan to allow for it again
With the growth of pomelo shaddock, also it can resist and eliminate crop and be encroached on by germ：It is similar as tyrosine, histidine, egg without selecting
The reason of propylhomoserin etc. is, smaller to the growth and development effect of gumbo and pomelo shaddock.
(3) composite bacterium powder：It is well known that microorganism species can secrete amino acid needed for crop, comb acid, vitamin group,
Hormone etc. is directly or indirectly absorbed for crop, and in numerous microbial inoculums, applicant selects with fixed nitrogen series bacillus, thin yellow chain
Mould, bacillus licheniformis, bacillus thuringiensis are according to mass ratio (1-3):(3-5):(2-3):What (1-2) was blended answers
Combined bacteria powder is worthy of careful study, and applicant cleverly uses three kinds of microbial inoculum collaborations in foliar fertilizer, can reach volume increase and increase
It receives, inhibits disease, improves the effect of quality, and change that make the strain of other types be not all right, the change of composition and content also can
Gumbo, the condition of pomelo shaddock, mouthfeel and nutrient content is set to have a greatly reduced quality.
(4) recessed native powder：Inorganic carrier matrices of the present invention using recessed native powder as liquid foliar fertilizer, it is contemplated that its with compared with
Adsorptivity well, caking property, can preserve the nutritional ingredient in fertilizer, prevent its loss that is affected by the external environment well,
And the stability and application of fertilizer system of the present invention can be improved.
(5) disease prevention ingredient：Applicant attempts to select the association of allyl sulfides, Blumea oil, four kinds of glycyrrhizic acid, apiolin ingredients
Antibacterial disease prevention active ingredient of the same-action as foliar fertilizer is unexpectedly obtained than preferably being imitated in terms of previous disease prevention
Fruit, and it is natural, green, non-hazardous, additionally it is possible to the mouthfeel and nutritive value content of gumbo and pomelo shaddock are improved, it is more at one stroke
With, be highly suitable for the present invention foliar fertilizer system.
Certainly, because of the requirement of the mentality of designing and goal of the invention of foliar fertilizer of the present invention, remaining of the invention component selection and
Content selection is obviously also non-obvious, and those skilled in the art combine the prior art that can readily occur in absolutely not.This
Have further embodiment in terms of the preparation process of foliar fertilizer of the present invention, in conjunction with the embodiment of the present invention it can be seen that, it is of the invention
Preparation method is designed using I-IV four step, and raw material is added by several times in batches, and step is simple and orderly, rather than uses the prior art
Conventional is added at one time, and this technique is adapted with the special proportioning of fertilizer production raw material components of the present invention, is only adopted
With this technique, it just can guarantee that the smooth sequential of foliar fertilizer reaction system carries out, ensure the foliar fertilizer finally prepared
Excellent specific property.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although with reference to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution recorded in example is modified or equivalent replacement of some of the technical features.All essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (10)
1. a kind of preparation method of multifunctional efficient foliar fertilizer, which is characterized in that include the following steps：
Ⅰ：It is 300-400 μm to take recessed native powder to be ground to fineness, is heated to 42-46 DEG C, glycyrrhizic acid and apiolin mixing is added
6-8min is stirred, under stirring condition, the natural botanical extraction liquid of parts by weight 58-66% is added, is heated to 48-52 DEG C
Afterwards, insulated and stirred 10-15min obtains material A；
Ⅱ：It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after being heated to 40-44 DEG C, then add thereto
Enter Blumea oil and be slowly mixed together stirring 20-25min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus, is heated to 38-42 DEG C, under stirring condition, sequentially adds water-soluble blueness
Highland barley beta glucan, trace element, amino acid powder are then kept stirring 8- under the conditions of speed of agitator is 100-120r/min
10min obtains material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 42-46 DEG C, material A mixing is added and stirs
After mixing 2-4min, ultrasonic disperse 8-10min.
2. a kind of preparation method of multifunctional efficient foliar fertilizer according to claim 1, which is characterized in that including following
Step：
Ⅰ：It is 320-380 μm to take recessed native powder to be ground to fineness, is heated to 43-45 DEG C, glycyrrhizic acid and apiolin mixing is added
6.5-7.5min is stirred, under stirring condition, the natural botanical extraction liquid of parts by weight 60-64% is added, is heated to 49-51
After DEG C, insulated and stirred 11-14min obtains material A；
Ⅱ：It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after being heated to 41-43 DEG C, then add thereto
Enter Blumea oil and be slowly mixed together stirring 21-24min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus, is heated to 39-41 DEG C, under stirring condition, sequentially adds water-soluble blueness
Highland barley beta glucan, trace element, amino acid powder are then kept stirring 8.5- under the conditions of speed of agitator is 105-115r/min
9.5min obtains material C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 43-45 DEG C, material A mixing is added and stirs
After mixing 2.5-3.5min, ultrasonic disperse 8.5-9.5min.
3. a kind of preparation method of multifunctional efficient foliar fertilizer according to claim 1, which is characterized in that including following
Step：
Ⅰ：It is 320 μm to take recessed native powder to be ground to fineness, is heated to 43 DEG C, and glycyrrhizic acid is added and apiolin is mixed
7.5min under stirring condition, adds the natural botanical extraction liquid of parts by weight 60%, after being heated to 49 DEG C, insulated and stirred
14min obtains material A；
Ⅱ：It under stirring, takes allyl sulfides to be added in propylene glycol and is sufficiently stirred, after being heated to 41 DEG C, then be added thereto
Blumea oil is slowly mixed together stirring 24min, obtains material B；
Ⅲ：The natural botanical extraction liquid for taking surplus is heated to 39 DEG C, under stirring condition, sequentially adds water-soluble highland barley
Beta glucan, trace element, amino acid powder are then kept stirring 9.5min under the conditions of speed of agitator is 105r/min, obtain object
Expect C；
Ⅳ：Material C is taken, material B mixings are first added thereto, are then heated to 43 DEG C, adds material A mixing
After 3.5min, ultrasonic disperse 9.5min.
4. a kind of preparation method of multifunctional efficient foliar fertilizer according to claim 1, which is characterized in that the blade face
Fertilizer includes following raw material by weight：
It is 1.8-2.2 parts micro-；
2.4-2.8 parts of allyl sulfides；
4.5-5.5 parts of Blumea oil；
1.2-1.8 parts of glycyrrhizic acid；
1.75-2.3 parts of apiolin；
Recessed 17-19 parts of powder of soil；
6.5-7.5 parts of propylene glycol；
Water-soluble highland barley Beta-dextran 1.15-1.35 parts；
2.25-2.7 parts of composite bacterium powder；
2.8-3.2 parts of amino acid powder；
34-38 parts of natural botanical extraction liquid.
5. a kind of preparation method of multifunctional efficient foliar fertilizer according to claim 4, which is characterized in that the blade face
Fertilizer is made of following raw material by weight：
1.8 parts of trace element；
2.4 parts of allyl sulfides；
4.5 parts of Blumea oil；
1.2 parts of glycyrrhizic acid；
1.75 parts of apiolin；
Recessed 17 parts of powder of soil；
6.5 parts of propylene glycol；
1.15 parts of water-soluble highland barley Beta-dextran；
2.25 parts of composite bacterium powder；
2.8 parts of amino acid powder；
34 parts of natural botanical extraction liquid.
6. a kind of preparation method of multifunctional efficient foliar fertilizer according to claim 1, which is characterized in that described micro
Element is made of following composition by weight：1.2 parts of ammonium molybdate, 1.2 parts of manganese sulfate, 2.4 parts of ferrous sulfate, borax 2.4
Part, 1.7 parts of zinc sulfate, 4.5 parts of potassium dihydrogen phosphate.
7. a kind of preparation method of multifunctional efficient foliar fertilizer according to claim 1, which is characterized in that described compound
Bacterium powder is fixed nitrogen series bacillus, streptomyces microflavus, bacillus licheniformis, bacillus thuringiensis according to mass ratio 1.5:3.5:
2.2:1.2 are fully blended.
8. a kind of preparation method of multifunctional efficient foliar fertilizer according to claim 1, which is characterized in that the amino
Sour powder is made of following composition by weight：1.6 parts of glycine, 3.2 parts of leucine, 1.4 parts of alanine, tryptophan 1.2
Part, 2.2 parts of lysine, 2.4 parts of glutamic acid, 1.2 parts of arginine.
9. a kind of preparation method of multifunctional efficient foliar fertilizer according to claim 1, which is characterized in that described natural
Plant extraction liquid is made by following steps：By weight 3.5:1.2 take fresh reseda, olive leaf, add after being smashed to pieces
The water for entering 4.5 times of its weight decocts 35min, ultrasonic extraction 5.2min, and 3.5 times of filter residue weight are added after centrifugal filtration into filter residue
Water decoct 46min, ultrasonic extraction 3.2min, after centrifugal filtration, merge filtrate twice, be concentrated into the 1/4 of original volume to obtain the final product.
10. a kind of preparation method of multifunctional efficient foliar fertilizer according to claim 4, which is characterized in that the leaf
It further include the surfactant that parts by weight are 0.4 in leaven material.
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| CN105010346A (en) * | 2015-07-15 | 2015-11-04 | 四川国光农化股份有限公司 | Plant growth regulating composition and preparation and application thereof |
| CN106386871A (en) * | 2016-08-31 | 2017-02-15 | 山东胜伟园林科技有限公司 | Rooting agent containing celery extract and preparation method thereof |
| CN107129403A (en) * | 2017-07-03 | 2017-09-05 | 合肥卓畅农业科技有限公司 | A kind of fruit special foliar fertilizer and preparation method thereof |
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2018
- 2018-06-27 CN CN201810675844.4A patent/CN108623389A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101057953A (en) * | 2006-04-21 | 2007-10-24 | 陈祖辉 | Multi-target cooperative control preparation for treating virus infectious disease |
| CN105010346A (en) * | 2015-07-15 | 2015-11-04 | 四川国光农化股份有限公司 | Plant growth regulating composition and preparation and application thereof |
| CN106386871A (en) * | 2016-08-31 | 2017-02-15 | 山东胜伟园林科技有限公司 | Rooting agent containing celery extract and preparation method thereof |
| CN107129403A (en) * | 2017-07-03 | 2017-09-05 | 合肥卓畅农业科技有限公司 | A kind of fruit special foliar fertilizer and preparation method thereof |
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Application publication date: 20181009 |