CN108619219A - Cloudy gel of the pure natural shield of one kind and preparation method thereof - Google Patents

Cloudy gel of the pure natural shield of one kind and preparation method thereof Download PDF

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Publication number
CN108619219A
CN108619219A CN201810541628.0A CN201810541628A CN108619219A CN 108619219 A CN108619219 A CN 108619219A CN 201810541628 A CN201810541628 A CN 201810541628A CN 108619219 A CN108619219 A CN 108619219A
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pure natural
gel
chinese juniper
natural shield
shield
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柯青
林爱明
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Findin (xiamen) Biotechnology Co Ltd
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Findin (xiamen) Biotechnology Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/13—Coniferophyta (gymnosperms)
    • A61K36/14—Cupressaceae (Cypress family), e.g. juniper or cypress
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/185—Acids; Anhydrides, halides or salts thereof, e.g. sulfur acids, imidic, hydrazonic or hydroximic acids
    • A61K31/19—Carboxylic acids, e.g. valproic acid
    • A61K31/194—Carboxylic acids, e.g. valproic acid having two or more carboxyl groups, e.g. succinic, maleic or phthalic acid
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/33—Heterocyclic compounds
    • A61K31/335—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin
    • A61K31/35—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom
    • A61K31/352—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom condensed with carbocyclic rings, e.g. methantheline 
    • A61K31/353—3,4-Dihydrobenzopyrans, e.g. chroman, catechin
    • A61K31/355—Tocopherols, e.g. vitamin E
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/34—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polyesters, polyamino acids, polysiloxanes, polyphosphazines, copolymers of polyalkylene glycol or poloxamers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/0012—Galenical forms characterised by the site of application
    • A61K9/0034—Urogenital system, e.g. vagina, uterus, cervix, penis, scrotum, urethra, bladder; Personal lubricants
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/06—Ointments; Bases therefor; Other semi-solid forms, e.g. creams, sticks, gels
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P15/00—Drugs for genital or sexual disorders; Contraceptives
    • A61P15/02—Drugs for genital or sexual disorders; Contraceptives for disorders of the vagina
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/02—Local antiseptics
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/04—Antibacterial agents
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/10—Antimycotics
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P33/00—Antiparasitic agents
    • A61P33/02—Antiprotozoals, e.g. for leishmaniasis, trichomoniasis, toxoplasmosis
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30—Extraction of the material
    • A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Animal Behavior & Ethology (AREA)
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  • Public Health (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Epidemiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
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  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
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  • Communicable Diseases (AREA)
  • Oncology (AREA)
  • Engineering & Computer Science (AREA)
  • Botany (AREA)
  • Gynecology & Obstetrics (AREA)
  • Alternative & Traditional Medicine (AREA)
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  • Microbiology (AREA)
  • Mycology (AREA)
  • Reproductive Health (AREA)
  • Biotechnology (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • Urology & Nephrology (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Inorganic Chemistry (AREA)
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  • Endocrinology (AREA)
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Abstract

The present invention relates to cloudy gels of a kind of pure natural shield and preparation method thereof, the cloudy gel of pure natural shield includes 30 55 weight % of Chinese juniper extract, 1 weight % of natto gum 17ppm, 23 weight % of sodium citrate, 0.2 0.5 weight % of vitamin E, 12 20 weight % of dimethyl silicone polymer and excess water.The cloudy gel of pure natural shield of the present invention is used as main formula using natural harmless material, can effectively lubricating moisturizing vagina mucosa, and there is Chinese juniper wood polyphenol powde natural faint scent and fungistatic effect, auxiliary vagina plays self-cleaning action, with preferable market prospects.

Description

Cloudy gel of the pure natural shield of one kind and preparation method thereof
Technical field
The present invention relates to disinfecting articles for use, especially a kind of cloudy gel of pure natural shield and preparation method thereof.
Background technology
There are many floras to exist for intravaginal, and wherein lactic acid bacteria is dominant, maintains intravaginal acidic environment, inhibits other and causes a disease The growth of bacterium makes intravaginal colony balance, keeps vagina health.Daily vaginadouche can upset intravaginal colony balance, acid Basicity changes, and conducive to the growth of pathogenic bacteria, cause the generation of vaginitis.It is trusted for this purpose, vagina condensation becomes safer Vagina anti-inflammatory product.
It is another one is using chlorhexidine acetate as the synthetic agent of representative currently, vagina condensation in the market is divided into two kinds Kind is the gel mixture using metronidazole as representative, however chlorhexidine acetate and metronidazole all have certain toxicity, to vagina There is interference in the breeding of normal strain, long-time service will appear multiple complications, such as inflammation repeatedly, anorexia, abdominal discomfort, Sense of taste change etc..
Patent CN103520262B discloses a kind of lipid soluble gynecological gel, is made in parts by weight of following raw material：L- 8~15 parts of ascorbyl palmitate, 10~23 parts of frutus cnidii, 7~17 parts of kuh-seng, 2~8 parts of borneol, 2~6 parts of vitamin e. Mentioned component reaches antiinflammation using traditional Chinese medicine ingredients, and there is borneol certain toxicity, Ascorbyl Palmitate to be insoluble in Water is easy that precipitation is precipitated, causes vagina internally dry, not only use feeling is poor, but also some users is caused to be mistakenly considered human body Metabolite.
Invention content
Problem to be solved by this invention is to overcome the shortcomings of the prior art, provide a kind of pure natural shield the moon gel and Preparation method.
In the present invention, Chinese juniper extract is the water extract of Chinese juniper wood, containing Chinese juniper wood polyphenol powde, not only has aromatic odor, energy Package odor molecules are quickly neutralized, and have clean effect, and have effects that anti-inflammation and sterilization.
Natto gum mainly contains Poly-L-glutamic acid, and γ-PGA have the function of lubricating moisturizing vagina mucosa, and molecular weight exists 100-400 ten thousand has preferable moistening effect, the preferably natto gum of 300-400 ten thousand, has with Chinese juniper extract preferable compatible Effect.
Vagina pH is adjusted to normal range (NR) by sodium citrate, while having the effect of stable gel.Vitamin E coordinates natto Glue protects mucous membrane and improves peculiar smell.
Concrete scheme is as follows：
A kind of cloudy gel of pure natural shield, including following components：
Wherein, the Chinese juniper extract is the water extract of Chinese juniper wood.
Further, pure natural shield the moon gel includes following components：
Further, pure natural shield the moon gel includes following components：
Further, the Chinese juniper extract is water extract of the Chinese juniper wood at 80-95 DEG C.
Further, the molecular weight of the natto gum is 100-400 ten thousand.
Further, the molecular weight of the natto gum is 300-400 ten thousand.
The present invention also provides the preparation methods of pure natural shield the moon gel, include the following steps：
1) fresh Chinese juniper wood is taken, is added to the water after broken and carries out distillation extraction, collect fraction, obtain Chinese juniper extract；
2) natto gum, dimethyl silicone polymer and water is added into Chinese juniper extract while hot, stirs evenly；
3) sodium citrate and vitamin E is added, is uniformly mixed, stands 8-12h, obtains pure natural shield the moon gel.
Further, the temperature that extraction is distilled described in step 1) is 80-95 DEG C.
Further, the time stirred described in step 2) is 20-30min.
The present invention also protects pure natural shield the moon gel that the preparation method of pure natural shield the moon gel is prepared.
Advantageous effect：The cloudy gel of pure natural shield of the present invention uses natural harmless material as main formula, can Effectively lubricating moisturizing vagina mucosa, and there is Chinese juniper wood polyphenol powde natural faint scent and fungistatic effect, auxiliary vagina plays self-cleaning action, With preferable market prospects.
Specific implementation mode
Technical solution of the present invention is further elaborated with reference to embodiment.Particular technique or item are not specified in embodiment Part person carries out according to technology or condition described in document in the art or according to product description.Agents useful for same or instrument Production firm person is not specified in device, and being can be with conventional products that are commercially available.
Embodiment 1
The cloudy gel of pure natural shield is prepared according to the following steps,
1) fresh Chinese juniper wood is taken, is added to the water after broken and carries out distillation extraction, 85 DEG C of collection fractions is heated to, obtains Chinese juniper and carry Take object；
2) natto gum, dimethyl silicone polymer and water is added into Chinese juniper extract while hot, stirring 30min occurs sticky；
3) sodium citrate and vitamin E is added, is uniformly mixed, stand 8h to get.
Wherein, each raw material dosage situation is shown in Table 1, and the molecular weight of natto gum is 4,000,000, prepared pure natural shield the moon gel Have the effect of lubricating moisturizing vagina mucosa to be colorless and transparent, after use, alleviates the moon such as dryness and burning pain of the eye caused by colpitis Portion is uncomfortable, and without side-effects using pure natural formula, Chinese juniper extract not only has fragrance, improves private parts peculiar smell, and have Fungistatic effect, external germ experiment show suppression of the prepared cloudy gel of natural shield to Candida albicans, staphylococcus aureus Bacterium rate is respectively 65.2% and 80.5%.
1 raw material dosage table (parts by weight) of table
Embodiment 2
The cloudy gel of pure natural shield is prepared according to the following steps,
1) fresh Chinese juniper wood is taken, is added to the water after broken and carries out distillation extraction, 90 DEG C of collection fractions is heated to, obtains Chinese juniper and carry Take object；
2) natto gum, dimethyl silicone polymer and water is added into Chinese juniper extract while hot, stirring 30min occurs sticky；
3) sodium citrate and vitamin E is added, is uniformly mixed, stand 8h to get.
Wherein, each raw material dosage situation is shown in Table 1, and the molecular weight of natto gum is 3,000,000, prepared pure natural shield the moon gel Have the effect of lubricating moisturizing vagina mucosa to be colorless and transparent, after use, alleviates the moon such as dryness and burning pain of the eye caused by colpitis Portion is uncomfortable, and without side-effects using pure natural formula, Chinese juniper extract not only has fragrance, improves private parts peculiar smell, and have Fungistatic effect, external germ experiment show suppression of the prepared cloudy gel of natural shield to Candida albicans, staphylococcus aureus Bacterium rate is respectively 67.4% and 81.2%.
Embodiment 3
The cloudy gel of pure natural shield is prepared according to the following steps,
1) fresh Chinese juniper wood is taken, is added to the water after broken and carries out distillation extraction, 80 DEG C of collection fractions is heated to, obtains Chinese juniper and carry Take object；
2) natto gum, dimethyl silicone polymer and water is added into Chinese juniper extract while hot, stirring 20min occurs sticky；
3) sodium citrate and vitamin E is added, is uniformly mixed, stand 10h to get.
Wherein, each raw material dosage situation is shown in Table 1, and the molecular weight of natto gum is 4,000,000, prepared pure natural shield the moon gel Have the effect of lubricating moisturizing vagina mucosa to be colorless and transparent, after use, alleviates the moon such as dryness and burning pain of the eye caused by colpitis Portion is uncomfortable, and without side-effects using pure natural formula, Chinese juniper extract not only has fragrance, improves private parts peculiar smell, and have Fungistatic effect, external germ experiment show suppression of the prepared cloudy gel of natural shield to Candida albicans, staphylococcus aureus Bacterium rate is respectively 65.0% and 78.4%.
Embodiment 4
The cloudy gel of pure natural shield is prepared according to the following steps,
1) fresh Chinese juniper wood is taken, is added to the water after broken and carries out distillation extraction, 85 DEG C of collection fractions is heated to, obtains Chinese juniper and carry Take object；
2) natto gum, dimethyl silicone polymer and water is added into Chinese juniper extract while hot, stirring 30min occurs sticky；
3) sodium citrate and vitamin E is added, is uniformly mixed, stand 8h to get.
Wherein, each raw material dosage situation is shown in Table 1, and the molecular weight of natto gum is 1,000,000, prepared pure natural shield the moon gel Have the effect of lubricating moisturizing vagina mucosa to be colorless and transparent, after use, alleviates the moon such as dryness and burning pain of the eye caused by colpitis Portion is uncomfortable, and without side-effects using pure natural formula, Chinese juniper extract not only has fragrance, improves private parts peculiar smell, and have Fungistatic effect, external germ experiment show suppression of the prepared cloudy gel of natural shield to Candida albicans, staphylococcus aureus Bacterium rate is respectively 74.8% and 88.5%.
Embodiment 5
The cloudy gel of pure natural shield is prepared according to the following steps,
1) fresh Chinese juniper wood is taken, is added to the water after broken and carries out distillation extraction, 80 DEG C of collection fractions is heated to, obtains Chinese juniper and carry Take object；
2) natto gum, dimethyl silicone polymer and water is added into Chinese juniper extract while hot, stirring 30min occurs sticky；
3) sodium citrate and vitamin E is added, is uniformly mixed, stand 12h to get.
Wherein, each raw material dosage situation is shown in Table 1, and the molecular weight of natto gum is 2,000,000, prepared pure natural shield the moon gel Have the effect of lubricating moisturizing vagina mucosa to be colorless and transparent, after use, alleviates the moon such as dryness and burning pain of the eye caused by colpitis Portion is uncomfortable, and without side-effects using pure natural formula, Chinese juniper extract not only has fragrance, improves private parts peculiar smell, and have Fungistatic effect, external germ experiment show suppression of the prepared cloudy gel of natural shield to Candida albicans, staphylococcus aureus Bacterium rate is respectively 64.3% and 79.5%.
Clinical trial
Experimental subjects：Choose vaginitis patient 30, wherein colpomycosis 10, trichomonas vaginitis 8, bacterium Property vaginitis 12, the generality data no significant difference such as age, course of disease of patient randomly selects 25 from 30 For patient as experimental group, another 4 are used as blank control group.
Application method：Experimental group squeezes into vagina using pure natural shield the moon gel prepared by embodiment 1 using ancillary equipment After lie low 5 minutes, once in the morning and once at night, using 1 month, control group was without processing.
Effective evaluation standard：It cures：Clinical symptoms completely disappear, and cause of disease inspection loses pathogen；It is effective：Clinical symptoms are bright Aobvious to improve, patient feels and is obviously improved or without abnormal sense；In vain, patient without improvement or aggravates.
After one month, 21 are cured in experimental group, effective 4, control group is invalid without improvement, i.e. effective evaluation.
Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example Property, it is not considered as limiting the invention, those skilled in the art are not departing from the principle of the present invention and objective In the case of can make changes, modifications, alterations, and variations to the above described embodiments within the scope of the invention.

Claims (10)

1. a kind of cloudy gel of pure natural shield, it is characterised in that：Including following components：
Wherein, the Chinese juniper extract is the water extract of Chinese juniper wood.
2. the cloudy gel of pure natural shield according to claim 1, it is characterised in that：Including following components：
3. the cloudy gel of pure natural shield according to claim 1, it is characterised in that：Including following components：
4. the cloudy gel of pure natural shield according to claim 1, it is characterised in that：The Chinese juniper extract is Chinese juniper wood in 80-95 DEG C water extract.
5. the cloudy gel of pure natural shield according to claim 1, it is characterised in that：The molecular weight of the natto gum is 100- 4000000.
6. the cloudy gel of pure natural shield according to claim 5, it is characterised in that：The molecular weight of the natto gum is 300- 4000000.
7. the preparation method of the cloudy gel of pure natural shield described in claim 1, it is characterised in that：Include the following steps：1) it takes new Fresh Chinese juniper wood, is added to the water after broken and carries out distillation extraction, collect fraction, obtain Chinese juniper extract；
2) natto gum, dimethyl silicone polymer and water is added into Chinese juniper extract while hot, stirs evenly；
3) sodium citrate and vitamin E is added, is uniformly mixed, stands 8-12h, obtains pure natural shield the moon gel.
8. the preparation method of pure natural shield the moon gel described in claim 7, it is characterised in that：Extraction is distilled described in step 1) Temperature be 80-95 DEG C.
9. the preparation method of pure natural shield the moon gel described in claim 7, it is characterised in that：Stirred described in step 2) when Between be 20-30min.
10. pure natural shield the moon gel that the preparation method of pure natural shield the moon gel described in claim 7-9 is prepared.
CN201810541628.0A 2018-05-30 2018-05-30 Cloudy gel of the pure natural shield of one kind and preparation method thereof Pending CN108619219A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102925291A (en) * 2012-11-22 2013-02-13 广西森呼吸科技工程有限公司 Variable pressure distillation method for extracting pythoncidere and essential oil from Chamaecyparis plants
CN105411975A (en) * 2015-12-09 2016-03-23 南京轩凯生物科技有限公司 Oil-phase dispersed polyglutamic acid and preparation method and application thereof
CN107216949A (en) * 2017-07-29 2017-09-29 安徽扬子生物科技有限公司 The transformation distillating method of polyphenol powde and essential oil is extracted in a kind of wood from Chinese juniper

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102925291A (en) * 2012-11-22 2013-02-13 广西森呼吸科技工程有限公司 Variable pressure distillation method for extracting pythoncidere and essential oil from Chamaecyparis plants
CN105411975A (en) * 2015-12-09 2016-03-23 南京轩凯生物科技有限公司 Oil-phase dispersed polyglutamic acid and preparation method and application thereof
CN107216949A (en) * 2017-07-29 2017-09-29 安徽扬子生物科技有限公司 The transformation distillating method of polyphenol powde and essential oil is extracted in a kind of wood from Chinese juniper

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
郭雪飞: "与医药保健品有关的几种林产化学品研究现状", 《生物质化学工程》 *

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