CN107216949A - The transformation distillating method of polyphenol powde and essential oil is extracted in a kind of wood from Chinese juniper - Google Patents
The transformation distillating method of polyphenol powde and essential oil is extracted in a kind of wood from Chinese juniper Download PDFInfo
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- CN107216949A CN107216949A CN201710633908.XA CN201710633908A CN107216949A CN 107216949 A CN107216949 A CN 107216949A CN 201710633908 A CN201710633908 A CN 201710633908A CN 107216949 A CN107216949 A CN 107216949A
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- CN
- China
- Prior art keywords
- chinese juniper
- essential oil
- wood
- polyphenol powde
- raw material
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The invention discloses the transformation distillating method that polyphenol powde and essential oil are extracted in a kind of wood from Chinese juniper, the transformation distillating method that polyphenol powde and essential oil should be extracted from Chinese juniper wood is comprised the following steps that：S1：The acquisition of raw material, S2：Drying process, S3：Pulverization process, S4：Low-pressure steam processing, S5：Distillation is handled, S6：The processing of condensate liquid, S7：Water-oil separating.The present invention is by the way of transformation, using decompression mode, the polyphenol powde and essential oil that can aid in Chinese juniper wood ooze out, using oozing out under atmospheric pressure normality, coordinate the processing of interval decompression, polyphenol powde and essential oil can be allowd preferably to ooze out, need to steam raw material progress low temperature before distillation processing procedure simultaneously, so that saturated with water in raw material, more conducively polyphenol powde and essential oil is dissolved in water, the later stage, which distills, simultaneously causes polyphenol powde and essential oil as vapor is discharged, Low Temperature Steam can be protected to the stability of polyphenol powde and essential oil simultaneously, reduce the destruction to polyphenol powde and essential oil.
Description
Technical field
It is specially extraction polyphenol powde and essential oil in a kind of wood from Chinese juniper the present invention relates to polyphenol powde and extraction of essential oil technical field
Transformation distillating method.
Background technology
During essential oil is the flower from plant, leaf, stem, root or fruit, pass through steam distillation, extrusion, cold-maceration or molten
Agent extraction method refines the volatile flavor of extraction.It is used for people after being extracted containing substantial amounts of essential oil and polyphenol powde in Chinese juniper wood
Use, contribute to people's healthy, while it is that we need research to carry out distillation to Chinese juniper wood to extract essential oil and polyphenol powde
The problem of, the convenience of distillation is improved, the yield for increasing essential oil and polyphenol powde is all to need the problem of we study, so as to improve
The utilization rate of essential oil and polyphenol powde in Chinese juniper wood.
The content of the invention
, should be from Chinese juniper it is an object of the invention to provide the transformation distillating method that polyphenol powde and essential oil are extracted in a kind of wood from Chinese juniper
Polyphenol powde is extracted in wood and the transformation distillating method of essential oil is comprised the following steps that：
S1：The acquisition of raw material, the Chinese juniper carpentery workshop that 50 years are at least from the age of tree is raw material, while need to detect Chinese juniper wood,
Chinese juniper wood needs the Chinese juniper wood for health, and Hui Mushang is disease-free, in case harm influence Chinese juniper wood extracts the quality of polyphenol powde and essential oil；
S2：Drying process, is dried by the way of air-heater auxiliary is air-dried, drying is aided in using air-heater in ventilation,
Drying temperature is controlled between 30-50 DEG C, and the moisture in Chinese juniper wood is less than 10%；
S3：Pulverization process, Chinese juniper wood raw material is crushed, and the Chinese juniper wood raw material mesh number after crushing is 80-100 mesh；
S4：Low-pressure steam processing, Chinese juniper wood raw material is placed in low-pressure tank and carries out steam and smokes the pressure in processing, low-pressure tank and be
The half of atmospheric value so that steam is in progress steam under low-temperature condition and steamed, and steaming time was controlled at 10-15 minutes, together
When low-pressure tank in vapor (steam) temperature be less than 85 DEG C；
S5：Distillation is handled, and material is put into alembic and distilled, and needs to carry out the control of pressure in alembic, in order to
Polyphenol powde and essential oil are separated out, and the pressure range carried out in steam pressure tank is：
0.1MPa voltage stabilizings 5-10 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 10-15 minutes,
0.05MPa boosts to 0.1MPa, voltage stabilizing 3-5 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 50-60 minutes；
S6：The processing of condensate liquid, carries out filtration treatment, filtration treatment will be miscellaneous in mixed liquor by the oil mixing with water condensate liquid of acquisition
Matter is removed；
S7：Water-oil separating, water-oil separating is carried out by the oil-water mixture of filtration treatment, so as to obtain polyphenol powde and essential oil, is obtained
Sealing storage is carried out after polyphenol powde and essential oil, so as to complete technical process.
It is preferred that, Chinese juniper wood raw material passes through slicing treatment before the drying process, contributes to Chinese juniper wood raw material to dry, cuts
Chinese juniper wood raw material thickness after piece is at 0.5-1 centimetres, and length is at 20-30 centimetres.
It is preferred that, it is pure water that steam, which steams the middle water used, in the S4 and S5, it is to avoid impurities in water is to last
Finished product is impacted.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention is by the way of transformation, using decompression mode,
The polyphenol powde and essential oil that can aid in Chinese juniper wood ooze out, and using oozing out under atmospheric pressure normality, coordinate the processing of interval decompression,
Polyphenol powde and essential oil can be allowd preferably to ooze out, while needing to carry out low temperature to raw material before distillation processing procedure
Steam so that saturated with water in raw material, more conducively polyphenol powde and essential oil are dissolved in water, at the same the later stage distill cause polyphenol powde and
Essential oil is discharged with vapor, while Low Temperature Steam can be protected to the stability of polyphenol powde and essential oil, reduction pair
The destruction of polyphenol powde and essential oil.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.
Embodiment 1
The transformation distillating method of polyphenol powde and essential oil is extracted in a kind of wood from Chinese juniper, the change of polyphenol powde and essential oil should be extracted from Chinese juniper wood
Pressure distillating method is comprised the following steps that：
S1：The acquisition of raw material, the Chinese juniper carpentery workshop that 50 years are at least from the age of tree is raw material, while need to detect Chinese juniper wood,
Chinese juniper wood needs the Chinese juniper wood for health, and Hui Mushang is disease-free, in case harm influence Chinese juniper wood extracts the quality of polyphenol powde and essential oil；
S2：Drying process, is dried by the way of air-heater auxiliary is air-dried, drying is aided in using air-heater in ventilation,
Moisture of the drying temperature control in 40 DEG C, Chinese juniper wood is less than 10%；
S3：Pulverization process, Chinese juniper wood raw material is crushed, and the Chinese juniper wood raw material mesh number after crushing is 90 mesh；
S4：Low-pressure steam processing, Chinese juniper wood raw material is placed in low-pressure tank and carries out steam and smokes the pressure in processing, low-pressure tank and be
The half of atmospheric value so that steam is in progress steam under low-temperature condition and steamed, and steaming time was controlled at 13 minutes, while low
The vapor (steam) temperature in tank is pressed to be less than 85 DEG C；
S5：Distillation is handled, and material is put into alembic and distilled, and needs to carry out the control of pressure in alembic, in order to
Polyphenol powde and essential oil are separated out, and the pressure range carried out in steam pressure tank is：
0.1MPa voltage stabilizings 8 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 13 minutes,
0.05MPa boosts to 0.1MPa, voltage stabilizing 4 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 55 minutes；
S6：The processing of condensate liquid, carries out filtration treatment, filtration treatment will be miscellaneous in mixed liquor by the oil mixing with water condensate liquid of acquisition
Matter is removed；
S7：Water-oil separating, water-oil separating is carried out by the oil-water mixture of filtration treatment, so as to obtain polyphenol powde and essential oil, is obtained
Sealing storage is carried out after polyphenol powde and essential oil, so as to complete technical process.
Chinese juniper wood raw material passes through slicing treatment before the drying process, contributes to Chinese juniper wood raw material to dry, after section
Chinese juniper wood raw material thickness is at 0.8 centimetre, and length is at 25 centimetres.It is pure water that steam, which steams the middle water used, in the S4 and S5,
Impurities in water is avoided to impact last finished product.
Embodiment 2
The transformation distillating method of polyphenol powde and essential oil is extracted in a kind of wood from Chinese juniper, the change of polyphenol powde and essential oil should be extracted from Chinese juniper wood
Pressure distillating method is comprised the following steps that：
S1：The acquisition of raw material, the Chinese juniper carpentery workshop that 50 years are at least from the age of tree is raw material, while need to detect Chinese juniper wood,
Chinese juniper wood needs the Chinese juniper wood for health, and Hui Mushang is disease-free, in case harm influence Chinese juniper wood extracts the quality of polyphenol powde and essential oil；
S2：Drying process, is dried by the way of air-heater auxiliary is air-dried, drying is aided in using air-heater in ventilation,
Moisture of the drying temperature control in 30 DEG C, Chinese juniper wood is less than 10%；
S3：Pulverization process, Chinese juniper wood raw material is crushed, and the Chinese juniper wood raw material mesh number after crushing is 80 mesh；
S4：Low-pressure steam processing, Chinese juniper wood raw material is placed in low-pressure tank and carries out steam and smokes the pressure in processing, low-pressure tank and be
The half of atmospheric value so that steam is in progress steam under low-temperature condition and steamed, and steaming time was controlled at 10 minutes, while low
The vapor (steam) temperature in tank is pressed to be less than 85 DEG C；
S5：Distillation is handled, and material is put into alembic and distilled, and needs to carry out the control of pressure in alembic, in order to
Polyphenol powde and essential oil are separated out, and the pressure range carried out in steam pressure tank is：
0.1MPa voltage stabilizings 5 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 10 minutes,
0.05MPa boosts to 0.1MPa, voltage stabilizing 3 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 50 minutes；
S6：The processing of condensate liquid, carries out filtration treatment, filtration treatment will be miscellaneous in mixed liquor by the oil mixing with water condensate liquid of acquisition
Matter is removed；
S7：Water-oil separating, water-oil separating is carried out by the oil-water mixture of filtration treatment, so as to obtain polyphenol powde and essential oil, is obtained
Sealing storage is carried out after polyphenol powde and essential oil, so as to complete technical process.
Chinese juniper wood raw material passes through slicing treatment before the drying process, contributes to Chinese juniper wood raw material to dry, after section
Chinese juniper wood raw material thickness is at 0.5 centimetre, and length is at 20 centimetres.It is pure water that steam, which steams the middle water used, in the S4 and S5,
Impurities in water is avoided to impact last finished product.
Embodiment 3
The transformation distillating method of polyphenol powde and essential oil is extracted in a kind of wood from Chinese juniper, the change of polyphenol powde and essential oil should be extracted from Chinese juniper wood
Pressure distillating method is comprised the following steps that：
S1：The acquisition of raw material, the Chinese juniper carpentery workshop that 50 years are at least from the age of tree is raw material, while need to detect Chinese juniper wood,
Chinese juniper wood needs the Chinese juniper wood for health, and Hui Mushang is disease-free, in case harm influence Chinese juniper wood extracts the quality of polyphenol powde and essential oil；
S2：Drying process, is dried by the way of air-heater auxiliary is air-dried, drying is aided in using air-heater in ventilation,
Moisture of the drying temperature control in 50 DEG C, Chinese juniper wood is less than 10%；
S3：Pulverization process, Chinese juniper wood raw material is crushed, and the Chinese juniper wood raw material mesh number after crushing is 100 mesh；
S4：Low-pressure steam processing, Chinese juniper wood raw material is placed in low-pressure tank and carries out steam and smokes the pressure in processing, low-pressure tank and be
The half of atmospheric value so that steam is in progress steam under low-temperature condition and steamed, and steaming time was controlled at 15 minutes, while low
The vapor (steam) temperature in tank is pressed to be less than 85 DEG C；
S5：Distillation is handled, and material is put into alembic and distilled, and needs to carry out the control of pressure in alembic, in order to
Polyphenol powde and essential oil are separated out, and the pressure range carried out in steam pressure tank is：
0.1MPa voltage stabilizings 10 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 15 minutes,
0.05MPa boosts to 0.1MPa, voltage stabilizing 5 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 60 minutes；
S6：The processing of condensate liquid, carries out filtration treatment, filtration treatment will be miscellaneous in mixed liquor by the oil mixing with water condensate liquid of acquisition
Matter is removed；
S7：Water-oil separating, water-oil separating is carried out by the oil-water mixture of filtration treatment, so as to obtain polyphenol powde and essential oil, is obtained
Sealing storage is carried out after polyphenol powde and essential oil, so as to complete technical process.
Chinese juniper wood raw material passes through slicing treatment before the drying process, contributes to Chinese juniper wood raw material to dry, after section
Chinese juniper wood raw material thickness is at 1 centimetre, and length is at 30 centimetres.It is pure water that steam, which steams the middle water used, in the S4 and S5, is kept away
Exempt from impurities in water to impact last finished product.
The present invention is by the way of transformation, using decompression mode, and the polyphenol powde and essential oil that can aid in Chinese juniper wood ooze out,
Using oozing out under atmospheric pressure normality, coordinate the processing of interval decompression, polyphenol powde and essential oil can be allowd preferably to ooze out,
Need to steam raw material progress low temperature before distillation processing procedure simultaneously so that saturated with water in raw material, be more conducive to fragrant many
Essence and essential oil are dissolved in water, while the later stage, which distills, causes polyphenol powde and essential oil as vapor is discharged, while Low Temperature Steam
The stability of polyphenol powde and essential oil can be protected, reduce the destruction to polyphenol powde and essential oil.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (3)
1. the transformation distillating method of polyphenol powde and essential oil is extracted in a kind of wood from Chinese juniper, it is characterised in that：It should extract fragrant from Chinese juniper wood
The transformation distillating method of many essences and essential oil is comprised the following steps that：
S1：The acquisition of raw material, the Chinese juniper carpentery workshop that 50 years are at least from the age of tree is raw material, while need to detect Chinese juniper wood,
Chinese juniper wood needs the Chinese juniper wood for health, and Hui Mushang is disease-free, in case harm influence Chinese juniper wood extracts the quality of polyphenol powde and essential oil；
S2：Drying process, is dried by the way of air-heater auxiliary is air-dried, drying is aided in using air-heater in ventilation,
Drying temperature is controlled between 30-50 DEG C, and the moisture in Chinese juniper wood is less than 10%；
S3：Pulverization process, Chinese juniper wood raw material is crushed, and the Chinese juniper wood raw material mesh number after crushing is 80-100 mesh；
S4：Low-pressure steam processing, Chinese juniper wood raw material is placed in low-pressure tank and carries out steam and smokes the pressure in processing, low-pressure tank and be
The half of atmospheric value so that steam is in progress steam under low-temperature condition and steamed, and steaming time was controlled at 10-15 minutes, together
When low-pressure tank in vapor (steam) temperature be less than 85 DEG C；
S5：Distillation is handled, and material is put into alembic and distilled, and needs to carry out the control of pressure in alembic, in order to
Polyphenol powde and essential oil are separated out, and the pressure range carried out in steam pressure tank is：
0.1MPa voltage stabilizings 5-10 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 10-15 minutes,
0.05MPa boosts to 0.1MPa, voltage stabilizing 3-5 minutes,
0.1MPa is depressurized to 0.05MPa, voltage stabilizing 50-60 minutes；
S6：The processing of condensate liquid, carries out filtration treatment, filtration treatment will be miscellaneous in mixed liquor by the oil mixing with water condensate liquid of acquisition
Matter is removed；
S7：Water-oil separating, water-oil separating is carried out by the oil-water mixture of filtration treatment, so as to obtain polyphenol powde and essential oil, is obtained
Sealing storage is carried out after polyphenol powde and essential oil, so as to complete technical process.
2. extracting the transformation distillating method of polyphenol powde and essential oil in a kind of wood from Chinese juniper according to claim 1, its feature exists
In：Chinese juniper wood raw material passes through slicing treatment before the drying process, contributes to Chinese juniper wood raw material to dry, and the Chinese juniper wood after section is former
Thickness is expected at 0.5-1 centimetres, and length is at 20-30 centimetres.
3. extracting the transformation distillating method of polyphenol powde and essential oil in a kind of wood from Chinese juniper according to claim 1, its feature exists
In：It is pure water that steam, which steams the middle water used, in the S4 and S5, it is to avoid impurities in water is impacted to last finished product.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107805546A (en) * | 2017-11-13 | 2018-03-16 | 南宁科城汇信息科技有限公司 | A kind of method that polyphenol powde and essential oil are extracted in the wood from Chinese juniper |
| CN108619219A (en) * | 2018-05-30 | 2018-10-09 | 芬多精（厦门）生物技术有限公司 | Cloudy gel of the pure natural shield of one kind and preparation method thereof |
| CN109321363A (en) * | 2018-09-30 | 2019-02-12 | 四川桧元素生物科技有限公司 | A kind of method that low-temperature negative-pressure extracts Chinese juniper another name for oil and polyphenol powde |
| CN110540906A (en) * | 2019-09-24 | 2019-12-06 | 亓桐月 | method for preparing fendorin extracting solution |
| CN110742912A (en) * | 2019-11-05 | 2020-02-04 | 深圳市芬多精纳米生物科技有限公司 | Method for preparing nano fendorin |
| CN111349520A (en) * | 2020-03-20 | 2020-06-30 | 谭宇航 | Distillation preparation method of plant essential oil |
| CN113845978A (en) * | 2021-11-03 | 2021-12-28 | 上海木汗实业有限公司 | Volatile liquid of hinoki extract and processing method thereof |
| CN114657023A (en) * | 2021-09-08 | 2022-06-24 | 广州东智盟化妆品有限公司 | Extraction method and application of juniper essential oil |
| CN115251448A (en) * | 2022-08-22 | 2022-11-01 | 江西中烟工业有限责任公司 | Efficient tobacco essential oil extraction equipment and method thereof |
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| CN102925291A (en) * | 2012-11-22 | 2013-02-13 | 广西森呼吸科技工程有限公司 | Variable pressure distillation method for extracting pythoncidere and essential oil from Chamaecyparis plants |
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| KR20040026152A (en) * | 2002-09-23 | 2004-03-30 | 엔바이타(주) | Distillation method of Japanese Cypress(Chamaecyparis obtusa essential oil alleviating against blood pressure by promoted heating system |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107805546A (en) * | 2017-11-13 | 2018-03-16 | 南宁科城汇信息科技有限公司 | A kind of method that polyphenol powde and essential oil are extracted in the wood from Chinese juniper |
| CN108619219A (en) * | 2018-05-30 | 2018-10-09 | 芬多精（厦门）生物技术有限公司 | Cloudy gel of the pure natural shield of one kind and preparation method thereof |
| CN109321363A (en) * | 2018-09-30 | 2019-02-12 | 四川桧元素生物科技有限公司 | A kind of method that low-temperature negative-pressure extracts Chinese juniper another name for oil and polyphenol powde |
| CN109321363B (en) * | 2018-09-30 | 2022-02-08 | 四川桧元素生物科技有限公司 | Method for extracting juniper essential oil and phytoncide at low temperature under negative pressure |
| CN110540906A (en) * | 2019-09-24 | 2019-12-06 | 亓桐月 | method for preparing fendorin extracting solution |
| CN110742912A (en) * | 2019-11-05 | 2020-02-04 | 深圳市芬多精纳米生物科技有限公司 | Method for preparing nano fendorin |
| CN111349520A (en) * | 2020-03-20 | 2020-06-30 | 谭宇航 | Distillation preparation method of plant essential oil |
| CN114657023A (en) * | 2021-09-08 | 2022-06-24 | 广州东智盟化妆品有限公司 | Extraction method and application of juniper essential oil |
| CN113845978A (en) * | 2021-11-03 | 2021-12-28 | 上海木汗实业有限公司 | Volatile liquid of hinoki extract and processing method thereof |
| CN115251448A (en) * | 2022-08-22 | 2022-11-01 | 江西中烟工业有限责任公司 | Efficient tobacco essential oil extraction equipment and method thereof |
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Application publication date: 20170929 |