CN108578293A - A kind of environment-friendly type has the shampoo and preparation method thereof of anti-dandruff and itching-relieving efficacies - Google Patents
A kind of environment-friendly type has the shampoo and preparation method thereof of anti-dandruff and itching-relieving efficacies Download PDFInfo
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Abstract
The invention discloses the shampoo that a kind of environment-friendly type has anti-dandruff and itching-relieving efficacies, including below according to the raw material of parts by weight：Herb Gynostemmae Pentaphylli extract, Lignum Aquilariae Resinatum extract, deionized water, olive oil, guar gum, surfactant, olein, quaternized oligofructose, sodium chloride, preservative, Rosemary Oil, EDETATE SODIUM, citric acid.The invention also discloses the preparation methods that the environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies.Shampoo prepared by the present invention has excellent anti-dandruff and itching-relieving effect, it is cooperated by Lignum Aquilariae Resinatum extract and Herb Gynostemmae Pentaphylli extract, play apparent synergistic function, anti-dandruff and itching-relieving effect can be effectively improved, meanwhile natural origin raw material accounts for 96% or more of shampoo total weight, asepsis environment-protecting, also there are good antibacterial and anti-inflammation functions, have a vast market foreground.
Description
Technical field
The present invention relates to cleaning supplies field, specifically a kind of environment-friendly type has the shampoo and its system of anti-dandruff and itching-relieving efficacies
Preparation Method.
Background technology
Shampoo is also known as shampoo or shampoo, shampoo, is the hair being most widely used and scalp basic nursing
Cosmetic product.Currently, shampoo in the market is various in style, still, it is generally only to have the function of cleaning scalp and hair, enters
Weather is gradually dried after winter, and it is very universal that dandruff increases and itch phenomenon, not only affects people’s lives, can also be easy to cause
Alopecia, common shampoo cannot be satisfied the demand of people, meanwhile, the shampoo of domestic market uses chemically synthesized original mostly
Material is produced, and security risk bigger may be used for a long time to health there are security risk.Therefore, research and development one kind is with day
Environment-friendly type based on right source raw material has the shampoo of anti-dandruff and itching-relieving efficacies, the problem of becoming urgent need to resolve.
Invention content
The purpose of the present invention is to provide a kind of environment-friendly type have anti-dandruff and itching-relieving efficacies shampoo and preparation method thereof, with
Solve the problems mentioned above in the background art.
To achieve the above object, the present invention provides the following technical solutions：
A kind of environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies, including below according to the raw material of parts by weight：Gynostemma pentaphylla carries
Take 4-12 parts of object, 8-16 parts of Lignum Aquilariae Resinatum extract, 70-85 parts of deionized water, 0.8-2 parts of olive oil, 0.1-0.8 parts of guar gum, table
Activating agent 10-22 parts of face, 0.1-0.7 parts of olein, oligofructose 0.1-0.7 parts quaternized, 0.1-0.7 parts of sodium chloride,
0.05-0.4 parts of preservative, 0.2-1 parts of Rosemary Oil, 0.05-0.15 parts of EDETATE SODIUM, 0.02-0.1 parts of citric acid.
As a further solution of the present invention：Including below according to the raw material of parts by weight：5-10 parts of Herb Gynostemmae Pentaphylli extract sinks
Fragrant extract 10-15 parts, 72-80 parts of deionized water, 1-1.5 parts of olive oil, 0.2-0.5 parts of guar gum, surfactant 12-18
Part, 0.2-0.5 parts of olein, oligofructose 0.2-0.5 parts quaternized, 0.2-0.5 parts of sodium chloride, preservative 0.1-0.3
Part, 0.3-0.8 parts of Rosemary Oil, 0.08-0.12 parts of EDETATE SODIUM, 0.04-0.08 parts of citric acid.
As further scheme of the invention：Including below according to the raw material of parts by weight：7 parts of Herb Gynostemmae Pentaphylli extract sinks
14 parts of fragrant extract, 78 parts of deionized water, 1.3 parts of olive oil, 0.4 part of guar gum, 15 parts of surfactant, olein
0.4 part, 0.4 part of quaternized oligofructose, 0.4 part of sodium chloride, 0.2 part of preservative, 0.6 part of Rosemary Oil, EDETATE SODIUM 0.1
Part, 0.06 part of citric acid.
As further scheme of the invention：The surfactant be sodium alginate, Cocoamidopropyl betaine,
Lauroyl glutamate, carragheen and soybean lecithin press 5:3:1:2:2 ratio mixes；The preservative is polyquaternary amine
Salt -7.
As further scheme of the invention：The preparation method of the Herb Gynostemmae Pentaphylli extract is that gynostemma pentaphylla is dried
Processing is crushed to 10-80 mesh, and the deionized water of 6-12 times of weight is added, is ultrasonically treated using supersonic wave wall breaking technology, institute
The condition for stating supersound process is ultrasonic power 80-250W, ultrasonic time 10-50min, after the completion of being ultrasonically treated depressurize dense
Contracting, then filtered to get the Herb Gynostemmae Pentaphylli extract through 800 mesh.
As further scheme of the invention：The preparation method of the Lignum Aquilariae Resinatum extract is that agalloch eaglewood deionized water is clear
It washes 3-5 times, dries, the deionized water of 20-30 times of weight is then added, carrying out high temperature and pressure using steam pressure cooker equipment carries
It takes, the pressure of the high temperature and pressure extraction is 0.4-0.8MPa, and time 20-30min, extracting solution is concentrated under reduced pressure, then is passed through
800 mesh filter to get the Lignum Aquilariae Resinatum extract.
The environment-friendly type has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, and steps are as follows：
1) deionized water is weighed according to parts by weight, surfactant, ultrasonic disperse 10- under conditions of 70-90 DEG C is added
40min obtains mixture A；
2) the mixture A obtained in step 1) is sequentially added into olive oil, guar gum, olein under agitation
With quaternized oligofructose, mechanical agitation is carried out under the conditions of 40-60 DEG C, obtains mixture B；
3) citric acid and EDETATE SODIUM are weighed according to parts by weight, are added into Rosemary Oil, ultrasonic vibration 20-30min,
Obtain mixture C；
4) the mixture B obtained in step 2) is uniformly mixed with the mixture C obtained in step 3), sequentially adds anti-corrosion
Agent and sodium chloride, are heated to 70-90 DEG C, continue stirring to being completely dissolved, obtain mixture D；
5) the mixture D obtained in step 4) is cooled to 40 DEG C hereinafter, adding strand according to the rate of temperature fall of 4 DEG C/min
The blue extract of stock and Lignum Aquilariae Resinatum extract, be uniformly mixed to get.
As further scheme of the invention：In step 1), the supersonic frequency of the ultrasonic disperse is 30-50kHz.
As further scheme of the invention：In step 2), the churned mechanically time is 10-30min.
The environment-friendly type has purposes of the shampoo of anti-dandruff and itching-relieving efficacies in preparing shampoo.
Gynostemma pentaphylla, taste micro-sweet, cool in nature, return lung, spleen, kidney channel have and replenish qi to invigorate the spleen, preventing phlegm from forming and stopping coughing, and heat-clearing toxin-expelling functions are right
In physically weak weak, nephrasthenia emission, leukopenia, hyperlipidemia, virus hepatitis, chronic gastroenteritis, chronic bronchitis etc.
With good therapeutic effect.
Agalloch eaglewood, acrid flavour, hardship, slightly warm in nature, returns spleen, stomach, kidney channel there is reconciliation strength, benefit to mend internal organs, operation qi and blood equivalent
Fruit has antibacterial anti-inflammatory, anti-inflammation, anti-spasm, adjusts internal system, boosts metabolism, body and mind of releiving, improving immunity energy
The effects that power.
Compared with prior art, the beneficial effects of the invention are as follows：
Shampoo prepared by the present invention has excellent anti-dandruff and itching-relieving effect, passes through Lignum Aquilariae Resinatum extract and Herb Gynostemmae Pentaphylli extract
It cooperates, plays apparent synergistic function, anti-dandruff and itching-relieving effect can be effectively improved, meanwhile, natural original
Material accounts for 96% or more of shampoo total weight, and asepsis environment-protecting also has good antibacterial and anti-inflammation functions, before having a vast market
Scape.
Specific implementation mode
Technical scheme of the present invention is described in more detail With reference to embodiment.
Embodiment 1
A kind of environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies, including below according to the raw material of parts by weight：Gynostemma pentaphylla carries
Take 4 parts of object, 8 parts of Lignum Aquilariae Resinatum extract, 70 parts of deionized water, 0.8 part of olive oil, 0.1 part of guar gum, 10 parts of surfactant, oil
0.1 part of acid glyceride, 0.1 part of quaternized oligofructose, 0.1 part of sodium chloride, 0.05 part of preservative, 0.2 part of Rosemary Oil,
0.05 part of EDETATE SODIUM, 0.02 part of citric acid.Wherein, the surfactant be sodium alginate, Cocoamidopropyl betaine,
Lauroyl glutamate, carragheen and soybean lecithin press 5:3:1:2:2 ratio mixes；The preservative is polyquaternary amine
Salt -7；The preparation method of the Herb Gynostemmae Pentaphylli extract is that processing is dried in gynostemma pentaphylla, is crushed to 30 mesh, and 8 times of weight are added
Deionized water, be ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 120W,
Ultrasonic time 30min is concentrated under reduced pressure after the completion of being ultrasonically treated, then is filtered to get the Herb Gynostemmae Pentaphylli extract through 800 mesh；
The preparation method of the Lignum Aquilariae Resinatum extract is clean 5 times agalloch eaglewood with deionized water, is dried, then 25 times of weight of addition go from
Sub- water carries out high temperature and pressure extraction using steam pressure cooker equipment, and the pressure of high temperature and pressure extraction is 0.6MPa, and the time is
25min, extracting solution are concentrated under reduced pressure, then are filtered to get the Lignum Aquilariae Resinatum extract through 800 mesh.
In the present embodiment, the environment-friendly type has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, and steps are as follows：
1) deionized water is weighed according to parts by weight, surfactant is added, with the supersonic frequency of 40kHz under conditions of 80 DEG C
Rate carries out ultrasonic disperse 25min, obtains mixture A；
2) the mixture A obtained in step 1) is sequentially added into olive oil, guar gum, olein under agitation
With quaternized oligofructose, mechanical agitation 20min is carried out under the conditions of 50 DEG C, obtains mixture B；
3) citric acid and EDETATE SODIUM are weighed according to parts by weight, be added into Rosemary Oil, ultrasonic vibration 25min is obtained
Mixture C；
4) the mixture B obtained in step 2) is uniformly mixed with the mixture C obtained in step 3), sequentially adds anti-corrosion
Agent and sodium chloride are heated to 80 DEG C, continue stirring to being completely dissolved, obtain mixture D；
5) the mixture D obtained in step 4) is cooled to 35 DEG C according to the rate of temperature fall of 4 DEG C/min, adds gynostemma pentaphylla
Extract and Lignum Aquilariae Resinatum extract, be uniformly mixed to get.
Embodiment 2
A kind of environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies, including below according to the raw material of parts by weight：Gynostemma pentaphylla carries
Take 12 parts of object, 16 parts of Lignum Aquilariae Resinatum extract, 85 parts of deionized water, 2 parts of olive oil, 0.8 part of guar gum, 22 parts of surfactant, oil
0.7 part of acid glyceride, 0.7 part of quaternized oligofructose, 0.7 part of sodium chloride, 0.4 part of preservative, 1 part of Rosemary Oil, EDTA
0.15 part of disodium, 0.1 part of citric acid.Wherein, the surfactant is sodium alginate, Cocoamidopropyl betaine, bay
Acyl glutamate, carragheen and soybean lecithin press 5:3:1:2:2 ratio mixes；The preservative is polyquaternium -7；
The preparation method of the Herb Gynostemmae Pentaphylli extract is that processing is dried in gynostemma pentaphylla, is crushed to 30 mesh, 8 times of weight of addition go from
Sub- water is ultrasonically treated using supersonic wave wall breaking technology, and the condition of the supersound process is ultrasonic power 120W, when ultrasonic
Between 30min, be ultrasonically treated after the completion of be concentrated under reduced pressure, then through 800 mesh filter to get the Herb Gynostemmae Pentaphylli extract；It is described heavy
The preparation method of fragrant extract is to clean agalloch eaglewood 5 times with deionized water, is dried, and the deionized water of 25 times of weight is then added,
High temperature and pressure extraction is carried out using steam pressure cooker equipment, the pressure of high temperature and pressure extraction is 0.6MPa, and the time is
25min, extracting solution are concentrated under reduced pressure, then are filtered to get the Lignum Aquilariae Resinatum extract through 800 mesh.
In the present embodiment, the environment-friendly type has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, and steps are as follows：
1) deionized water is weighed according to parts by weight, surfactant is added, with the supersonic frequency of 40kHz under conditions of 80 DEG C
Rate carries out ultrasonic disperse 25min, obtains mixture A；
2) the mixture A obtained in step 1) is sequentially added into olive oil, guar gum, olein under agitation
With quaternized oligofructose, mechanical agitation 20min is carried out under the conditions of 50 DEG C, obtains mixture B；
3) citric acid and EDETATE SODIUM are weighed according to parts by weight, be added into Rosemary Oil, ultrasonic vibration 25min is obtained
Mixture C；
4) the mixture B obtained in step 2) is uniformly mixed with the mixture C obtained in step 3), sequentially adds anti-corrosion
Agent and sodium chloride are heated to 80 DEG C, continue stirring to being completely dissolved, obtain mixture D；
5) the mixture D obtained in step 4) is cooled to 35 DEG C according to the rate of temperature fall of 4 DEG C/min, adds gynostemma pentaphylla
Extract and Lignum Aquilariae Resinatum extract, be uniformly mixed to get.
Embodiment 3
A kind of environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies, including below according to the raw material of parts by weight：Gynostemma pentaphylla carries
Take 8 parts of object, 12 parts of Lignum Aquilariae Resinatum extract, 77.5 parts of deionized water, 1.4 parts of olive oil, 0.45 part of guar gum, surfactant 16
Part, 0.4 part of olein, 0.4 part of quaternized oligofructose, 0.4 part of sodium chloride, 0.225 part of preservative, Rosemary Oil
0.6 part, 0.1 part of EDETATE SODIUM, 0.06 part of citric acid.Wherein, the surfactant is sodium alginate, cocamidopropyl propyl amide sweet tea
Dish alkali, lauroyl glutamate, carragheen and soybean lecithin press 5:3:1:2:2 ratio mixes；The preservative is poly-
Quaternary ammonium salt -7；The preparation method of the Herb Gynostemmae Pentaphylli extract is that processing is dried in gynostemma pentaphylla, is crushed to 30 mesh, is added 8 times
The deionized water of weight is ultrasonically treated using supersonic wave wall breaking technology, and the condition of the supersound process is ultrasonic power
120W, ultrasonic time 30min are concentrated under reduced pressure after the completion of being ultrasonically treated, then are filtered through 800 mesh and carried to get the gynostemma pentaphylla
Take object；The preparation method of the Lignum Aquilariae Resinatum extract is to clean agalloch eaglewood 5 times with deionized water, is dried, and 25 times of weight are then added
Deionized water, high temperature and pressure extraction is carried out using steam pressure cooker equipment, the pressure of high temperature and pressure extraction is 0.6MPa,
Time is 25min, and extracting solution is concentrated under reduced pressure, then is filtered to get the Lignum Aquilariae Resinatum extract through 800 mesh.
In the present embodiment, the environment-friendly type has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, and steps are as follows：
1) deionized water is weighed according to parts by weight, surfactant is added, with the supersonic frequency of 40kHz under conditions of 80 DEG C
Rate carries out ultrasonic disperse 25min, obtains mixture A；
2) the mixture A obtained in step 1) is sequentially added into olive oil, guar gum, olein under agitation
With quaternized oligofructose, mechanical agitation 20min is carried out under the conditions of 50 DEG C, obtains mixture B；
3) citric acid and EDETATE SODIUM are weighed according to parts by weight, be added into Rosemary Oil, ultrasonic vibration 25min is obtained
Mixture C；
4) the mixture B obtained in step 2) is uniformly mixed with the mixture C obtained in step 3), sequentially adds anti-corrosion
Agent and sodium chloride are heated to 80 DEG C, continue stirring to being completely dissolved, obtain mixture D；
5) the mixture D obtained in step 4) is cooled to 35 DEG C according to the rate of temperature fall of 4 DEG C/min, adds gynostemma pentaphylla
Extract and Lignum Aquilariae Resinatum extract, be uniformly mixed to get.
Embodiment 4
A kind of environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies, including below according to the raw material of parts by weight：Gynostemma pentaphylla carries
Take 5 parts of object, 10 parts of Lignum Aquilariae Resinatum extract, 72 parts of deionized water, 1 part of olive oil, 0.2 part of guar gum, 12 parts of surfactant, oleic acid
0.2 part of glyceride, 0.2 part of quaternized oligofructose, 0.2 part of sodium chloride, 0.1 part of preservative, 0.3 part of Rosemary Oil, EDTA
0.08 part of disodium, 0.04 part of citric acid.Wherein, the surfactant is sodium alginate, Cocoamidopropyl betaine, bay
Acyl glutamate, carragheen and soybean lecithin press 5:3:1:2:2 ratio mixes；The preservative is polyquaternium -7；
The preparation method of the Herb Gynostemmae Pentaphylli extract is that processing is dried in gynostemma pentaphylla, is crushed to 30 mesh, 8 times of weight of addition go from
Sub- water is ultrasonically treated using supersonic wave wall breaking technology, and the condition of the supersound process is ultrasonic power 120W, when ultrasonic
Between 30min, be ultrasonically treated after the completion of be concentrated under reduced pressure, then through 800 mesh filter to get the Herb Gynostemmae Pentaphylli extract；It is described heavy
The preparation method of fragrant extract is to clean agalloch eaglewood 5 times with deionized water, is dried, and the deionized water of 25 times of weight is then added,
High temperature and pressure extraction is carried out using steam pressure cooker equipment, the pressure of high temperature and pressure extraction is 0.6MPa, and the time is
25min, extracting solution are concentrated under reduced pressure, then are filtered to get the Lignum Aquilariae Resinatum extract through 800 mesh.
In the present embodiment, the environment-friendly type has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, and steps are as follows：
1) deionized water is weighed according to parts by weight, surfactant is added, with the supersonic frequency of 40kHz under conditions of 80 DEG C
Rate carries out ultrasonic disperse 25min, obtains mixture A；
2) the mixture A obtained in step 1) is sequentially added into olive oil, guar gum, olein under agitation
With quaternized oligofructose, mechanical agitation 20min is carried out under the conditions of 50 DEG C, obtains mixture B；
3) citric acid and EDETATE SODIUM are weighed according to parts by weight, be added into Rosemary Oil, ultrasonic vibration 25min is obtained
Mixture C；
4) the mixture B obtained in step 2) is uniformly mixed with the mixture C obtained in step 3), sequentially adds anti-corrosion
Agent and sodium chloride are heated to 80 DEG C, continue stirring to being completely dissolved, obtain mixture D；
5) the mixture D obtained in step 4) is cooled to 35 DEG C according to the rate of temperature fall of 4 DEG C/min, adds gynostemma pentaphylla
Extract and Lignum Aquilariae Resinatum extract, be uniformly mixed to get.
Embodiment 5
A kind of environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies, including below according to the raw material of parts by weight：Gynostemma pentaphylla carries
Take 10 parts of object, 15 parts of Lignum Aquilariae Resinatum extract, 80 parts of deionized water, 1.5 parts of olive oil, 0.5 part of guar gum, 18 parts of surfactant,
0.5 part of olein, 0.5 part of quaternized oligofructose, 0.5 part of sodium chloride, 0.3 part of preservative, 0.8 part of Rosemary Oil,
0.12 part of EDETATE SODIUM, 0.08 part of citric acid.Wherein, the surfactant be sodium alginate, Cocoamidopropyl betaine,
Lauroyl glutamate, carragheen and soybean lecithin press 5:3:1:2:2 ratio mixes；The preservative is polyquaternary amine
Salt -7；The preparation method of the Herb Gynostemmae Pentaphylli extract is that processing is dried in gynostemma pentaphylla, is crushed to 30 mesh, and 8 times of weight are added
Deionized water, be ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 120W,
Ultrasonic time 30min is concentrated under reduced pressure after the completion of being ultrasonically treated, then is filtered to get the Herb Gynostemmae Pentaphylli extract through 800 mesh；
The preparation method of the Lignum Aquilariae Resinatum extract is clean 5 times agalloch eaglewood with deionized water, is dried, then 25 times of weight of addition go from
Sub- water carries out high temperature and pressure extraction using steam pressure cooker equipment, and the pressure of high temperature and pressure extraction is 0.6MPa, and the time is
25min, extracting solution are concentrated under reduced pressure, then are filtered to get the Lignum Aquilariae Resinatum extract through 800 mesh.
In the present embodiment, the environment-friendly type has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, and steps are as follows：
1) deionized water is weighed according to parts by weight, surfactant is added, with the supersonic frequency of 40kHz under conditions of 80 DEG C
Rate carries out ultrasonic disperse 25min, obtains mixture A；
2) the mixture A obtained in step 1) is sequentially added into olive oil, guar gum, olein under agitation
With quaternized oligofructose, mechanical agitation 20min is carried out under the conditions of 50 DEG C, obtains mixture B；
3) citric acid and EDETATE SODIUM are weighed according to parts by weight, be added into Rosemary Oil, ultrasonic vibration 25min is obtained
Mixture C；
4) the mixture B obtained in step 2) is uniformly mixed with the mixture C obtained in step 3), sequentially adds anti-corrosion
Agent and sodium chloride are heated to 80 DEG C, continue stirring to being completely dissolved, obtain mixture D；
5) the mixture D obtained in step 4) is cooled to 35 DEG C according to the rate of temperature fall of 4 DEG C/min, adds gynostemma pentaphylla
Extract and Lignum Aquilariae Resinatum extract, be uniformly mixed to get.
Embodiment 6
A kind of environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies, including below according to the raw material of parts by weight：Gynostemma pentaphylla carries
Take 7.5 parts of object, 12.5 parts of Lignum Aquilariae Resinatum extract, 76 parts of deionized water, 1.25 parts of olive oil, 0.35 part of guar gum, surfactant
15 parts, 0.35 part of olein, 0.35 part of quaternized oligofructose, 0.35 part of sodium chloride, 0.2 part of preservative, rosemary essence
0.55 part of oil, 0.1 part of EDETATE SODIUM, 0.06 part of citric acid.Wherein, the surfactant is sodium alginate, coconut oleoyl amine third
Base glycine betaine, lauroyl glutamate, carragheen and soybean lecithin press 5:3:1:2:2 ratio mixes；The preservative
For polyquaternium -7；The preparation method of the Herb Gynostemmae Pentaphylli extract is that processing is dried in gynostemma pentaphylla, is crushed to 30 mesh, is added
The deionized water of 8 times of weight is ultrasonically treated using supersonic wave wall breaking technology, and the condition of the supersound process is ultrasonic wave work(
Rate 120W, ultrasonic time 30min are concentrated under reduced pressure after the completion of being ultrasonically treated, then are filtered to get the gynostemma pentaphylla through 800 mesh
Extract；The preparation method of the Lignum Aquilariae Resinatum extract is to clean agalloch eaglewood 5 times with deionized water, is dried, and 25 times of weights are then added
The deionized water of amount carries out high temperature and pressure extraction using steam pressure cooker equipment, and the pressure of the high temperature and pressure extraction is
0.6MPa, time 25min, extracting solution are concentrated under reduced pressure, then are filtered to get the Lignum Aquilariae Resinatum extract through 800 mesh.
In the present embodiment, the environment-friendly type has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, and steps are as follows：
1) deionized water is weighed according to parts by weight, surfactant is added, with the supersonic frequency of 40kHz under conditions of 80 DEG C
Rate carries out ultrasonic disperse 25min, obtains mixture A；
2) the mixture A obtained in step 1) is sequentially added into olive oil, guar gum, olein under agitation
With quaternized oligofructose, mechanical agitation 20min is carried out under the conditions of 50 DEG C, obtains mixture B；
3) citric acid and EDETATE SODIUM are weighed according to parts by weight, be added into Rosemary Oil, ultrasonic vibration 25min is obtained
Mixture C；
4) the mixture B obtained in step 2) is uniformly mixed with the mixture C obtained in step 3), sequentially adds anti-corrosion
Agent and sodium chloride are heated to 80 DEG C, continue stirring to being completely dissolved, obtain mixture D；
5) the mixture D obtained in step 4) is cooled to 35 DEG C according to the rate of temperature fall of 4 DEG C/min, adds gynostemma pentaphylla
Extract and Lignum Aquilariae Resinatum extract, be uniformly mixed to get.
Embodiment 7
A kind of environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies, including below according to the raw material of parts by weight：Gynostemma pentaphylla carries
Take 7 parts of object, 14 parts of Lignum Aquilariae Resinatum extract, 78 parts of deionized water, 1.3 parts of olive oil, 0.4 part of guar gum, 15 parts of surfactant, oil
0.4 part of acid glyceride, 0.4 part of quaternized oligofructose, 0.4 part of sodium chloride, 0.2 part of preservative, 0.6 part of Rosemary Oil,
0.1 part of EDETATE SODIUM, 0.06 part of citric acid.Wherein, the surfactant be sodium alginate, Cocoamidopropyl betaine,
Lauroyl glutamate, carragheen and soybean lecithin press 5:3:1:2:2 ratio mixes；The preservative is polyquaternary amine
Salt -7；The preparation method of the Herb Gynostemmae Pentaphylli extract is that processing is dried in gynostemma pentaphylla, is crushed to 30 mesh, and 8 times of weight are added
Deionized water, be ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 120W,
Ultrasonic time 30min is concentrated under reduced pressure after the completion of being ultrasonically treated, then is filtered to get the Herb Gynostemmae Pentaphylli extract through 800 mesh；
The preparation method of the Lignum Aquilariae Resinatum extract is clean 5 times agalloch eaglewood with deionized water, is dried, then 25 times of weight of addition go from
Sub- water carries out high temperature and pressure extraction using steam pressure cooker equipment, and the pressure of high temperature and pressure extraction is 0.6MPa, and the time is
25min, extracting solution are concentrated under reduced pressure, then are filtered to get the Lignum Aquilariae Resinatum extract through 800 mesh.
In the present embodiment, the environment-friendly type has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, and steps are as follows：
1) deionized water is weighed according to parts by weight, surfactant is added, with the supersonic frequency of 40kHz under conditions of 80 DEG C
Rate carries out ultrasonic disperse 25min, obtains mixture A；
2) the mixture A obtained in step 1) is sequentially added into olive oil, guar gum, olein under agitation
With quaternized oligofructose, mechanical agitation 20min is carried out under the conditions of 50 DEG C, obtains mixture B；
3) citric acid and EDETATE SODIUM are weighed according to parts by weight, be added into Rosemary Oil, ultrasonic vibration 25min is obtained
Mixture C；
4) the mixture B obtained in step 2) is uniformly mixed with the mixture C obtained in step 3), sequentially adds anti-corrosion
Agent and sodium chloride are heated to 80 DEG C, continue stirring to being completely dissolved, obtain mixture D；
5) the mixture D obtained in step 4) is cooled to 35 DEG C according to the rate of temperature fall of 4 DEG C/min, adds gynostemma pentaphylla
Extract and Lignum Aquilariae Resinatum extract, be uniformly mixed to get.
Comparative example 1
Compared with Example 7, Herb Gynostemmae Pentaphylli extract is free of, other are same as Example 7.
Comparative example 2
Compared with Example 7, Lignum Aquilariae Resinatum extract is free of, other are same as Example 7.
Comparative example 3
Compared with Example 7, Herb Gynostemmae Pentaphylli extract and Lignum Aquilariae Resinatum extract are free of, other are same as Example 7.
Performance test
There is the shampoo of anti-dandruff and itching-relieving efficacies to carry out performance detection environment-friendly type prepared by embodiment 7 and comparative example 1-3,
Specific detection method according to《The foundation and application study of the anti-dandruff effect detection evaluation method of shampoo》Disclosed method into
Row inhibition zone diameter is tested, and is evaluated anti-dandruff effect of shampoo product, and inhibition zone diameter is bigger, and anti-dandruff effect is better,
Specific testing result is as shown in table 1.
Wherein, " foundation and application study of the anti-dandruff effect detection evaluation method of shampoo ", where, Wang Tan, Jia Zebao, flood
Know roc, Peng Jin, research and development department of Si Bao daily use chemicals Co., Ltd, household chemicals science, o. 11th in 2009.
Gynostemma pentaphylla, taste micro-sweet, cool in nature, return lung, spleen, kidney channel have and replenish qi to invigorate the spleen, preventing phlegm from forming and stopping coughing, and heat-clearing toxin-expelling functions are right
In physically weak weak, nephrasthenia emission, leukopenia, hyperlipidemia, virus hepatitis, chronic gastroenteritis, chronic bronchitis etc.
With good therapeutic effect.
Agalloch eaglewood, acrid flavour, hardship, slightly warm in nature, returns spleen, stomach, kidney channel there is reconciliation strength, benefit to mend internal organs, operation qi and blood equivalent
Fruit has antibacterial anti-inflammatory, anti-inflammation, anti-spasm, adjusts internal system, boosts metabolism, body and mind of releiving, improving immunity energy
The effects that power.
1 testing result table of table
| Group | Inhibition zone diameter (mm) |
| Embodiment 7 | 24.8 |
| Comparative example 1 | 19.4 |
| Comparative example 2 | 14.3 |
| Comparative example 3 | 11.6 |
It, can from can be seen that the present invention in the data comparison of embodiment 7 and comparative example 2 by adding Lignum Aquilariae Resinatum extract
Effectively improve anti-dandruff effect；Pass through addition gynostemma pentaphylla from can be seen that the present invention in the data comparison of embodiment 7 and comparative example 1
Extract can improve anti-dandruff effect to a certain extent；In addition, can from data comparison of the embodiment 7 with comparative example 1-3
Go out, the present invention is cooperated by Lignum Aquilariae Resinatum extract and Herb Gynostemmae Pentaphylli extract, plays apparent synergistic function, Neng Gouyou
Effect improves anti-dandruff effect, can remove dandruff, stop scalp pruritus, removes hair oil, salubrious using rear hair naturally, the viscous puzzlement of oil-free, eliminates
With the trouble of hair conditioner, at the same can dephlogistication and promoting nuscle growth, effectively reduce depilation phenomenon.
As can be seen that the shampoo of environment-friendly type with anti-dandruff and itching-relieving efficacies of the invention prepared is with excellent from result above
Different anti-dandruff and itching-relieving effect is cooperated by Lignum Aquilariae Resinatum extract and Herb Gynostemmae Pentaphylli extract, plays apparent synergistic work
With, anti-dandruff and itching-relieving effect can be effectively improved, meanwhile, natural origin raw material accounts for 96% or more of shampoo total weight, no poison ring
It protects, also there are good antibacterial and anti-inflammation functions, have a vast market foreground.
The better embodiment of the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
Formula, one skilled in the relevant art within the scope of knowledge, can also be without departing from the purpose of the present invention
Various changes can be made.There is no necessity and possibility to exhaust all the enbodiments.And it thus amplifies out apparent
Variation or variation be still in the protection scope of this invention.
Claims (10)
1. a kind of environment-friendly type has the shampoo of anti-dandruff and itching-relieving efficacies, which is characterized in that including below according to the raw material of parts by weight：
4-12 parts of Herb Gynostemmae Pentaphylli extract, 8-16 parts of Lignum Aquilariae Resinatum extract, 70-85 parts of deionized water, 0.8-2 parts of olive oil, guar gum 0.1-
0.8 part, 10-22 parts of surfactant, 0.1-0.7 parts of olein, oligofructose 0.1-0.7 parts quaternized, sodium chloride
0.1-0.7 parts, 0.05-0.4 parts of preservative, 0.2-1 parts of Rosemary Oil, 0.05-0.15 parts of EDETATE SODIUM, citric acid 0.02-
0.1 part.
2. environment-friendly type according to claim 1 has the shampoo of anti-dandruff and itching-relieving efficacies, which is characterized in that including pressing below
According to the raw material of parts by weight：5-10 parts of Herb Gynostemmae Pentaphylli extract, 10-15 parts of Lignum Aquilariae Resinatum extract, 72-80 parts of deionized water, olive oil 1-
1.5 parts, 0.2-0.5 parts of guar gum, 12-18 parts of surfactant, 0.2-0.5 parts of olein, quaternized oligofructose
0.2-0.5 parts, 0.2-0.5 parts of sodium chloride, 0.1-0.3 parts of preservative, 0.3-0.8 parts of Rosemary Oil, EDETATE SODIUM 0.08-
0.12 part, 0.04-0.08 parts of citric acid.
3. environment-friendly type according to claim 2 has the shampoo of anti-dandruff and itching-relieving efficacies, which is characterized in that including pressing below
According to the raw material of parts by weight：7 parts of Herb Gynostemmae Pentaphylli extract, 14 parts of Lignum Aquilariae Resinatum extract, 78 parts of deionized water, 1.3 parts of olive oil, guar gum
0.4 part, 15 parts of surfactant, 0.4 part of olein, 0.4 part of quaternized oligofructose, 0.4 part of sodium chloride, preservative
0.2 part, 0.6 part of Rosemary Oil, 0.1 part of EDETATE SODIUM, 0.06 part of citric acid.
4. environment-friendly type according to claim 1 or 2 or 3 has the shampoo of anti-dandruff and itching-relieving efficacies, which is characterized in that described
Surfactant is that sodium alginate, Cocoamidopropyl betaine, lauroyl glutamate, carragheen and soybean lecithin press 5:3:
1:2:2 ratio mixes；The preservative is polyquaternium -7.
5. environment-friendly type according to claim 3 has the shampoo of anti-dandruff and itching-relieving efficacies, which is characterized in that the gynostemma pentaphylla
The preparation method of extract is that processing is dried in gynostemma pentaphylla, is crushed to 10-80 mesh, and the deionization of 6-12 times of weight is added
Water is ultrasonically treated using supersonic wave wall breaking technology, and the condition of the supersound process is ultrasonic power 80-250W, ultrasound
Time 10-50min is concentrated under reduced pressure after the completion of being ultrasonically treated, then is filtered to get the Herb Gynostemmae Pentaphylli extract through 800 mesh.
6. environment-friendly type according to claim 3 has the shampoo of anti-dandruff and itching-relieving efficacies, which is characterized in that the agalloch eaglewood carries
It is to clean agalloch eaglewood 3-5 times with deionized water to take the preparation method of object, is dried, and the deionized water of 20-30 times of weight is then added,
High temperature and pressure extraction is carried out using steam pressure cooker equipment, the pressure of high temperature and pressure extraction is 0.4-0.8MPa, and the time is
20-30min, extracting solution are concentrated under reduced pressure, then are filtered to get the Lignum Aquilariae Resinatum extract through 800 mesh.
7. a kind of environment-friendly type as described in claim 1-6 is any has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies,
It is characterized in that, steps are as follows：
1）Deionized water is weighed according to parts by weight, surfactant, ultrasonic disperse 10- under conditions of 70-90 DEG C is added
40min obtains mixture A；
2）By step 1）In obtained mixture A sequentially add olive oil, guar gum, olein and season under agitation
Ammonium oligofructose carries out mechanical agitation under the conditions of 40-60 DEG C, obtains mixture B；
3）Citric acid and EDETATE SODIUM are weighed according to parts by weight, is added into Rosemary Oil, ultrasonic vibration 20-30min is obtained mixed
Close material C；
4）By step 2）In obtained mixture B and step 3）In obtained mixture C be uniformly mixed, sequentially add preservative and
Sodium chloride is heated to 70-90 DEG C, continues stirring to being completely dissolved, obtains mixture D；
5）By step 4）In obtained mixture D be cooled to 40 DEG C hereinafter, adding gynostemma pentaphylla according to the rate of temperature fall of 4 DEG C/min
Extract and Lignum Aquilariae Resinatum extract, be uniformly mixed to get.
8. environment-friendly type according to claim 7 has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, which is characterized in that
Step 1）In, the supersonic frequency of the ultrasonic disperse is 30-50kHz.
9. environment-friendly type according to claim 8 has the preparation method of the shampoo of anti-dandruff and itching-relieving efficacies, which is characterized in that
Step 2）In, the churned mechanically time is 10-30min.
10. there is a kind of environment-friendly type as described in claim 1-6 is any the shampoo of anti-dandruff and itching-relieving efficacies to prepare shampoo
In purposes.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109303729A (en) * | 2018-11-23 | 2019-02-05 | 茂名市和香种植科技有限公司 | A kind of preparation method of Chinese medicine agalloch eaglewood shampoo |
| CN111826659A (en) * | 2020-07-30 | 2020-10-27 | 上海源育节能环保科技有限公司 | Green environment-friendly antirust agent and preparation method thereof |
| WO2021140111A1 (en) | 2020-01-10 | 2021-07-15 | Lyneline Sàrl | Hair conditioner allowing the use of soap as shampoo |
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| JP2009073773A (en) * | 2007-09-21 | 2009-04-09 | Alpen Sogo Kenkyusho:Kk | Composition for hair-scalp and hair treatment, color treatment, pore-cleaning agent, shampoo and soap comprising the same composition for hair-scalp |
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| CN109303729A (en) * | 2018-11-23 | 2019-02-05 | 茂名市和香种植科技有限公司 | A kind of preparation method of Chinese medicine agalloch eaglewood shampoo |
| WO2021140111A1 (en) | 2020-01-10 | 2021-07-15 | Lyneline Sàrl | Hair conditioner allowing the use of soap as shampoo |
| CN111826659A (en) * | 2020-07-30 | 2020-10-27 | 上海源育节能环保科技有限公司 | Green environment-friendly antirust agent and preparation method thereof |
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Application publication date: 20180928 |