CN108578281A - A kind of compound essential oil and preparation method thereof for turning joint nursing - Google Patents
A kind of compound essential oil and preparation method thereof for turning joint nursing Download PDFInfo
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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Abstract
The present invention relates to a kind of compound essential oils for turning joint nursing, it is raw material by using camphor tree oil, antrodia fruiting body extract, caryophyllus oil, evening primrose oil, ginger oil, cinnamon oil and carries out suitable weight proportion, camphor tree oil acts synergistically with caryophyllus oil in side, play the role of lenitive, antrodia fruiting body extract, evening primrose oil and ginger oil all play the role of promoting blood circulation and removing blood stasis, and cinnamon oil and caryophyllus oil can make one to feel pleasant.The compound essential oil for turning joint nursing being finally prepared, a variety of different component synergistic effects, can effectively adjust fatigue, discomfort or damage of the physical activity joint caused by activity, nursing role is played to turning joint.Compound essential oil of the present invention completely remains the active ingredient in each raw material, is acted through skin, channels and collaterals, acupuncture point osmotic absorption, significant effect, safe without toxic side effect, and smell is good, while nursing activity joint, moreover it is possible to have the function that pleasure mood, relieve stress.
Description
Technical field
The invention belongs to cosmetic technical fields, and in particular to a kind of compound essential oil and its system for turning joint nursing
Preparation Method.
Background technology
Turning joint is the place that can be connected between movable bone and bone.Lesion, age increase, joint itself is changed in quality, fortune
It rubs caused by dynamic and lacking corresponding sports causes musculature inability etc. that can all bring uncomfortable or damage to turning joint, sternly
The degeneration for causing function of joint when weight, influences health and daily life, for this purpose, daily need to nurse turning joint.
Invention content
In order to solve the above-mentioned problems in the prior art, the present invention provides a kind of compound for turning joint nursing
Essential oil and preparation method thereof.
The technical scheme is that：
A kind of compound essential oil for turning joint nursing, raw material components include：
Camphor tree oil 7-15 parts by weight, antrodia fruiting body extract 4-20 parts by weight, caryophyllus oil 2-7 parts by weight, evening primrose oil
35-80 parts by weight, ginger oil 2-8 parts by weight, cinnamon oil 5-15 parts by weight.
The further preferred compound essential oil for turning joint nursing, raw material components include：
Camphor tree oil 8-13 parts by weight, antrodia fruiting body extract 5-15 parts by weight, caryophyllus oil 2-4 parts by weight, evening primrose oil
55-75 parts by weight, ginger oil 2-6 parts by weight, cinnamon oil 6-8 parts by weight.
The further preferred compound essential oil for turning joint nursing, raw material components include：
Camphor tree oil 8 parts by weight, 5 parts by weight of antrodia fruiting body extract, 2 parts by weight of caryophyllus oil, 75 parts by weight of evening primrose oil,
2 parts by weight of ginger oil, 8 parts by weight of cinnamon oil.
The extracting method of the antrodia fruiting body extract includes the following steps：
(1) it crushes：Antrodia fructification is chilled under the conditions of nitrogen ultra low temperature, Lowtemperaturepulverizer crushes, and obtains antrodia
Entity fine powder；
(2) it extracts：Antrodia fructification fine powder is packed into supercritical CO2It is entrainment with absolute ethyl alcohol in the extraction kettle of extraction
Agent is extracted, and is then transferred to separating still 1 successively and separating still 2 is detached, the mixing of liquid and ethyl alcohol after being detached
Liquid；
(3) it detaches：The mixed liquor of liquid and ethyl alcohol after separation is heated, ethyl alcohol is made to be volatilized completely to get described
Antrodia fruiting body extract.
In step (1), the liquid nitrogen pump amount of infusion is 6-7L/min, and the rotating speed of the Lowtemperaturepulverizer is 24000-
The time of 30000r/min, the low-temperature grinding are 10-50s.
In step (2),
The mass ratio of the absolute ethyl alcohol and antrodia fructification fine powder is 9:1-5:1；
The extraction temperature for carrying out the extraction is 65-70 DEG C, extracting pressure 37-42MPa, CO2Flow is 45-66L/h,
Extraction time is 1.2-1.8h；
The temperature of the separating still 1 is 75-80 DEG C, pressure 28-35MPa；
The temperature of the separating still 2 is 80-85 DEG C, pressure 18-25MPa.
In step (3), the temperature for carrying out the heating is 92-95 DEG C.
A method of the compound essential oil for turning joint nursing is prepared, is included the following steps：
(1) evening primrose oil is added reactor, under stirring condition, sequentially adds camphor tree oil, antrodia fruiting body extract, fourth
Sesame oil, ginger oil and cinnamon oil；
(2) continue stirring to being sufficiently mixed uniformly, up to the compound essential oil for turning joint nursing after standing.
In step (1), the speed for carrying out the stirring is 40-80rmp, and the time for carrying out the stirring is 10-30min,
The temperature for carrying out the stirring is 20-25 DEG C.
In step (2), the speed for carrying out the stirring is 40-80rmp, and the time for carrying out the stirring is 10-30min,
The time for carrying out the standing is 1-6h.
To facilitate the understanding of the present invention, now in the present invention bulk pharmaceutical chemicals and drug effect be further elaborated.
Camphor tree oil：Main component includes the terpenoid substances such as borneol, linalool, terpinol, has antibacterial bacteriostatic activity, right
Various bacteria has inhibiting effect, also has to a variety of fungies and is acted on compared with high inhibition, can treat various bacterial infection diseases.Together
When have the function of it is anti-inflammatory, analgesia, promote infiltration, can effectively administer skin trauma, be good natural nursing health care material, extensively
General is applied to medicine etc..
Antrodia fruiting body extract：Main component is ganoderma lucidum triterpene compounds and ganoderma lucidum polysaccharide, and having reduces blood platelet
Stickiness, the effect for inhibiting platelet aggregation, can be used for anticoagulation, meanwhile, it is also equipped with antiallergy, antifatigue, beautifying face and moistering lotion, delays
The effect of aging.
Caryophyllus oil：Smell is good, has excellent lenitive effect, frequently as the original of fast pain relief drug
Material, main component include eugenol, and eugenol is a kind of natural bacteria and pain inhibitory agents.
Evening primrose oil：A kind of grease of reconciliation base oil and essential oil, has blood coagulation resisting function, can promote blood circulation,
The delay of fatty wall in the blood vessels is reduced, dissipation atherosis spot prevents blood vessel internal membrane damage, prevents and treats artery sclerosis；
Help to treat eczema and dermatitis, there is anti-inflammatory effect；Eliminate rheumatic arthritis；It can exclude to have saved courage in the cell
Sterol reduces triglyceride, blood cholesterol levels, the content of B- lipoprotein；The metabolism of sebaceous glands is adjusted, moisturizes the skin, improved
Quick constitution, muscle reinforcing and bone strengthening, alleviation have a pain in the back, the symptom that trick is tingle.
Ginger oil：By being extracted in race, the Multiple components such as including gingerol have effects that releive, and can adjust mood so that
It is in a cheerful frame of mind；The superfluous grease of absorption, makes skin pleasant pure and fresh；Promoting blood circulation channels and collaterals dispel moisture and cold air, for the extravasated blood that dissipates, control
Treatment trauma.
Cinnamon oil：The bark of canella Chinese cassia tree, branch, leaf are yellow or brown color through distilling obtained aromatic oil
Supernatant liquid and a kind of Chinese medicine have the special fragrance of Chinese cassia tree, can treat rheumatism and skin itching.
Beneficial effects of the present invention are：
Compound essential oil of the present invention for turning joint nursing is modulated by a variety of natural plant extracts, is led to
It crosses and uses camphor tree oil, antrodia fruiting body extract, caryophyllus oil, evening primrose oil, ginger oil, cinnamon oil as raw material and carry out suitable
Weight proportion, camphor tree oil not only can effectively inhibit bacterium or fungi to bring damage to the human body in side, moreover it is possible to be cooperateed with caryophyllus oil
Effect, plays the role of lenitive, and antrodia fruiting body extract, evening primrose oil and ginger oil can all prevent blood clotting, rises
To effect promoting blood circulation and removing blood stasis, while skin metabolism can be adjusted, antifatigue and alleviation skin aging.Cinnamon oil all has good with caryophyllus oil
Good odour can make one to feel pleasant, while cinnamon oil can effectively treat turning joint because of the skin caused by movement or slight illness
Itch, can also releive sensitive skin first contacts essential oil when discomfort.The answering for turning joint nursing being finally prepared
Square essential oil, a variety of different components synergistic effect, can effectively adjust fatigue of the physical activity joint caused by activity, discomfort or
Damage, nursing role is played to turning joint.Completely retain provided by the present invention for the compound essential oil of turning joint nursing
Active ingredient in each raw material, acts, significant effect through skin, channels and collaterals, acupuncture point osmotic absorption, safe and non-toxic secondary to make
With and smell is good, while nursing activity joint, moreover it is possible to have the function that pleasure mood, relieve stress.
Specific implementation mode
Below by specific embodiment, the invention will be further described.
Embodiment 1
The present embodiment provides a kind of compound essential oil for turning joint nursing, raw material components include：
Camphor tree oil 7ml, antrodia fruiting body extract 4ml, caryophyllus oil 2ml, evening primrose oil 80ml, ginger oil 2ml, cinnamon oil
6ml。
Further, a kind of extracting method of the antrodia fruiting body extract is provided, is included the following steps：
(1) it crushes：Antrodia fructification is -196 DEG C in temperature, and liquid nitrogen pump amount of infusion is the nitrogen ultra low temperature condition of 6L/min
50s is crushed through 24000r/min Lowtemperaturepulverizers obtain antrodia fructification fine powder after lower freezing；
(2) it extracts：Antrodia fructification fine powder is packed into supercritical CO2It is entrainment with absolute ethyl alcohol in the extraction kettle of extraction
Agent is extracted, and the mass ratio of absolute ethyl alcohol and antrodia fructification fine powder is 9:1, extraction temperature is 65 DEG C, and extracting pressure is
37MPa, CO2Flow is 45L/h, extraction time 1.2h, and it is 75 DEG C to be then transferred to temperature successively, and pressure is the separation of 28MPa
The separating still 2 that kettle 1 and temperature are 80 DEG C, pressure is 18MPa is detached, the mixed liquor of liquid and ethyl alcohol after being detached；
(3) it detaches：The mixed liquor of liquid and ethyl alcohol after separation is heated to 92 DEG C, ethyl alcohol is made to be volatilized completely to get institute
The antrodia fruiting body extract stated.
Further, a kind of method preparing the compound essential oil for turning joint nursing is provided, is included the following steps：
(1) reactor is added in evening primrose oil, sequentially added under stirring camphor tree oil, antrodia fruiting body extract, caryophyllus oil,
Ginger oil and cinnamon oil, control mixing speed are 40rmp, and mixing time 10min, whipping temp is 20 DEG C；
(2) continue to stir 10min with the mixing speed of 40rmp, be nursed for turning joint up to described after standing 1h
Compound essential oil.
Embodiment 2
The present embodiment provides a kind of compound essential oil for turning joint nursing, raw material components include：
Camphor tree oil 15ml, antrodia fruiting body extract 15ml, caryophyllus oil 4ml, evening primrose oil 55ml, ginger oil 6ml, Chinese cassia tree
Oily 5ml.
Further, a kind of extracting method of the antrodia fruiting body extract is provided, is included the following steps：
(1) it crushes：Antrodia fructification is -196 DEG C in temperature, and liquid nitrogen pump amount of infusion is the nitrogen ultra low temperature condition of 6L/min
After lower freezing, 10s is crushed through 30000r/min Lowtemperaturepulverizers, obtains antrodia fructification fine powder；
(2) it extracts：Antrodia fructification fine powder is packed into supercritical CO2It is entrainment with absolute ethyl alcohol in the extraction kettle of extraction
Agent is extracted, and the mass ratio of absolute ethyl alcohol and antrodia fructification fine powder is 5:1, extraction temperature is 70 DEG C, and extracting pressure is
42MPa, CO2Flow is 66L/h, extraction time 1.8h, and it is 80 DEG C to be then transferred to temperature successively, and pressure is the separation of 35MPa
The separating still 2 that kettle 1 and temperature are 85 DEG C, pressure is 25MPa is detached, the mixed liquor of liquid and ethyl alcohol after being detached；
(3) it detaches：The mixed liquor of liquid and ethyl alcohol after separation is heated to 95 DEG C, ethyl alcohol is made to be volatilized completely to get institute
The antrodia fruiting body extract stated.
Further, a kind of method preparing the compound essential oil for turning joint nursing is provided, is included the following steps：
(1) reactor is added in evening primrose oil, sequentially added under stirring camphor tree oil, antrodia fruiting body extract, caryophyllus oil,
Ginger oil and cinnamon oil, control mixing speed are 80rmp, and mixing time 30min, whipping temp is 25 DEG C；
(2) continue to stir 30min with the mixing speed of 80rmp, be nursed for turning joint up to described after standing 6h
Compound essential oil.
Embodiment 3
The present embodiment provides a kind of compound essential oil for turning joint nursing, raw material components include：
Camphor tree oil 13ml, antrodia fruiting body extract 20ml, caryophyllus oil 7ml, evening primrose oil 35ml, ginger oil 8ml, Chinese cassia tree
Oily 15ml.
Further, a kind of extracting method of the antrodia fruiting body extract is provided, is included the following steps：
(1) it crushes：Antrodia fructification is -196 DEG C in temperature, and liquid nitrogen pump amount of infusion is the nitrogen ultra low temperature condition of 7L/min
After lower freezing, 40s is crushed through 26000r/min Lowtemperaturepulverizers, obtains antrodia fructification fine powder；
(2) it extracts：Antrodia fructification fine powder is packed into supercritical CO2It is entrainment with absolute ethyl alcohol in the extraction kettle of extraction
Agent is extracted, and the mass ratio of absolute ethyl alcohol and antrodia fructification fine powder is 8:1, extraction temperature is 65 DEG C, and extracting pressure is
38MPa, CO2Flow is 50L/h, extraction time 1.3h, and it is 75 DEG C to be then transferred to temperature successively, and pressure is the separation of 30MPa
The separating still 2 that kettle 1 and temperature are 80 DEG C, pressure is 20MPa is detached, the mixed liquor of liquid and ethyl alcohol after being detached；
(3) it detaches：The mixed liquor of liquid and ethyl alcohol after separation is heated to 92 DEG C, ethyl alcohol is made to be volatilized completely to get institute
The antrodia fruiting body extract stated.
Further, a kind of method preparing the compound essential oil for turning joint nursing is provided, is included the following steps：
(1) reactor is added in evening primrose oil, sequentially added under stirring camphor tree oil, antrodia fruiting body extract, caryophyllus oil,
Ginger oil and cinnamon oil, control mixing speed are 60rmp, and mixing time 15min, whipping temp is 21 DEG C；
(2) continue to stir 15min with the mixing speed of 60rmp, be nursed for turning joint up to described after standing 2h
Compound essential oil.
Embodiment 4
The present embodiment provides a kind of compound essential oil for turning joint nursing, raw material components include：
Camphor tree oil 13ml, antrodia fruiting body extract 5ml, caryophyllus oil 7ml, evening primrose oil 55ml, ginger oil 6ml, Chinese cassia tree
Oily 15ml.
Further, a kind of extracting method of the antrodia fruiting body extract is provided, is included the following steps：
(1) it crushes：Antrodia fructification is -196 DEG C in temperature, and liquid nitrogen pump amount of infusion is the nitrogen ultra low temperature condition of 7L/min
After lower freezing, 20s is crushed through 28000r/min Lowtemperaturepulverizers, obtains antrodia fructification fine powder；
(2) it extracts：Antrodia fructification fine powder is packed into supercritical CO2It is entrainment with absolute ethyl alcohol in the extraction kettle of extraction
Agent is extracted, and the mass ratio of absolute ethyl alcohol and antrodia fructification fine powder is 7:1, extraction temperature is 70 DEG C, and extracting pressure is
40MPa, CO2Flow is 60L/h, extraction time 1.7h, and it is 80 DEG C to be then transferred to temperature successively, and pressure is the separation of 35MPa
The separating still 2 that kettle 1 and temperature are 85 DEG C, pressure is 25MPa is detached, the mixed liquor of liquid and ethyl alcohol after being detached；
(3) it detaches：The mixed liquor of liquid and ethyl alcohol after separation is heated to 95 DEG C, ethyl alcohol is made to be volatilized completely to get institute
The antrodia fruiting body extract stated.
Further, a kind of method preparing the compound essential oil for turning joint nursing is provided, is included the following steps：
(1) reactor is added in evening primrose oil, sequentially added under stirring camphor tree oil, antrodia fruiting body extract, caryophyllus oil,
Ginger oil and cinnamon oil, control mixing speed are 70rmp, and mixing time 25min, whipping temp is 23 DEG C；
(2) continue to stir 25min with the mixing speed of 70rmp, be nursed for turning joint up to described after standing 5h
Compound essential oil.
Embodiment 5
The present embodiment provides a kind of compound essential oil for turning joint nursing, raw material components include：
Camphor tree oil 8ml, antrodia fruiting body extract 5ml, caryophyllus oil 2ml, evening primrose oil 75ml, ginger oil 2ml, cinnamon oil
8ml。
Further, a kind of extracting method of the antrodia fruiting body extract is provided, is included the following steps：
(1) it crushes：Antrodia fructification is -196 DEG C in temperature, and liquid nitrogen pump amount of infusion is the nitrogen ultra low temperature condition of 7L/min
After lower freezing, 30s is crushed through 27000r/min Lowtemperaturepulverizers, obtains antrodia fructification fine powder；
(2) it extracts：Antrodia fructification fine powder is packed into supercritical CO2It is entrainment with absolute ethyl alcohol in the extraction kettle of extraction
Agent is extracted, and the mass ratio of absolute ethyl alcohol and antrodia fructification fine powder is 6:1, extraction temperature is 65 DEG C, and extracting pressure is
39MPa, CO2Flow is 55L/h, extraction time 1.5h, and it is 75 DEG C to be then transferred to temperature successively, and pressure is the separation of 32MPa
The separating still 2 that kettle 1 and temperature are 80 DEG C, pressure is 22MPa is detached, the mixed liquor of liquid and ethyl alcohol after being detached；
(3) it detaches：The mixed liquor of liquid and ethyl alcohol after separation is heated to 93 DEG C, ethyl alcohol is made to be volatilized completely to get institute
The antrodia fruiting body extract stated.
Further, a kind of method preparing the compound essential oil for turning joint nursing is provided, is included the following steps：
(1) reactor is added in evening primrose oil, sequentially added under stirring camphor tree oil, antrodia fruiting body extract, caryophyllus oil,
Ginger oil and cinnamon oil, control mixing speed are 50rmp, and mixing time 20min, whipping temp is 22 DEG C；
(2) continue to stir 20min with the mixing speed of 50rmp, be nursed for turning joint up to described after standing 4h
Compound essential oil.
Typical case：
Case 1：Certain Ms, 46 years old, Nanjing Human was ailing with knee joint, and anchylosis, hair are felt when every morning gets up
Tightly, activity is by obstacle, and leg cannot stretch, feel like jelly completely when walking.After this compound essential oil 15 days, stiff, stiff feeling has
Be relieved, after 30 days, when walking legs feel completely without.
Case 2：Certain Ms, 58 years old, people from Zhengzhou lifted difficult when hand, the active and passive limitation of activity of elbow joint, elbow joint tool
There is a sense of aching, pain aggravates when ancon activity.After this compound essential oil 15 days, sense of aching is relieved, after 30 days, joint
Activity is freely.
Case 3：Certain man, 63 years old, people from Suzhou suffered from gonalgia symptom all the year round, and joint will appear when bending motion
Friction sound between bone and bone.After this compound essential oil 18-20 days, feeling of pain is mitigated, after 30-35 days, sense of aching
It is relieved.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of compound essential oil for turning joint nursing, which is characterized in that raw material components include：
Camphor tree oil 7-15 parts by weight, antrodia fruiting body extract 4-20 parts by weight, caryophyllus oil 2-7 parts by weight, evening primrose oil 35-80
Parts by weight, ginger oil 2-8 parts by weight, cinnamon oil 5-15 parts by weight.
2. the compound essential oil according to claim 1 for turning joint nursing, which is characterized in that raw material components include：
Camphor tree oil 8-13 parts by weight, antrodia fruiting body extract 5-15 parts by weight, caryophyllus oil 2-4 parts by weight, evening primrose oil 55-75
Parts by weight, ginger oil 2-6 parts by weight, cinnamon oil 6-8 parts by weight.
3. the compound essential oil according to claim 1 for turning joint nursing, which is characterized in that raw material components include：
8 parts by weight of camphor tree oil, 5 parts by weight of antrodia fruiting body extract, 2 parts by weight of caryophyllus oil, 75 parts by weight of evening primrose oil, race
Oily 2 parts by weight, 8 parts by weight of cinnamon oil.
4. being used for the compound essential oil of turning joint nursing according to claim 1-3 any one of them, which is characterized in that the camphor tree
The extracting method of sesame fruiting body extract includes the following steps：
(1) it crushes：Antrodia fructification is chilled under the conditions of nitrogen ultra low temperature, Lowtemperaturepulverizer crushes, and obtains antrodia fructification
Fine powder；
(2) it extracts：Antrodia fructification fine powder is packed into supercritical CO2In the extraction kettle of extraction, carried out by entrainer of absolute ethyl alcohol
Extraction, is then transferred to separating still 1 and separating still 2 is detached successively, the mixed liquor of liquid and ethyl alcohol after being detached；
(3) it detaches：The mixed liquor of liquid and ethyl alcohol after separation is heated, ethyl alcohol is made to be volatilized completely to get the camphor tree
Sesame fruiting body extract.
5. the compound essential oil according to claim 4 for turning joint nursing, which is characterized in that described in step (1)
Liquid nitrogen pump amount of infusion is 6-7L/min, and the rotating speed of the Lowtemperaturepulverizer is 24000-30000r/min, the low-temperature grinding
Time is 10-50s.
6. the compound essential oil according to claim 4 for turning joint nursing, which is characterized in that in step (2),
The mass ratio of the absolute ethyl alcohol and antrodia fructification fine powder is 9:1-5:1；
The extraction temperature for carrying out the extraction is 65-70 DEG C, extracting pressure 37-42MPa, CO2Flow is 45-66L/h, extraction
Time is 1.2-1.8h；
The temperature of the separating still 1 is 75-80 DEG C, pressure 28-35MPa；
The temperature of the separating still 2 is 80-85 DEG C, pressure 18-25MPa.
7. the compound essential oil according to claim 4 for turning joint nursing, which is characterized in that in step (3), carry out
The temperature of the heating is 92-95 DEG C.
8. a kind of method preparing claim 1-7 any one of them for the compound essential oil that turning joint is nursed, feature
It is, includes the following steps：
(1) evening primrose oil is added reactor, under stirring condition, sequentially adds camphor tree oil, antrodia fruiting body extract, cloves
Oil, ginger oil and cinnamon oil；
(2) continue stirring to being sufficiently mixed uniformly, up to the compound essential oil for turning joint nursing after standing.
9. the method according to claim 8 for preparing the compound essential oil for turning joint nursing, which is characterized in that step
(1) in, the speed for carrying out the stirring is 40-80rmp, and the time for carrying out the stirring is 10-30min, carries out the stirring
Temperature be 20-25 DEG C.
10. the method according to claim 8 for preparing the compound essential oil for turning joint nursing, which is characterized in that step
Suddenly in (2), the speed for carrying out the stirring is 40-80rmp, and the time for carrying out the stirring is 10-30min, is carried out described quiet
The time set is 1-6h.
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Application publication date: 20180928 |