CN108559659A - Antibacterial anti-colour contamination liquid detergent of one kind and preparation method thereof - Google Patents
Antibacterial anti-colour contamination liquid detergent of one kind and preparation method thereof Download PDFInfo
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- CN108559659A CN108559659A CN201810644576.XA CN201810644576A CN108559659A CN 108559659 A CN108559659 A CN 108559659A CN 201810644576 A CN201810644576 A CN 201810644576A CN 108559659 A CN108559659 A CN 108559659A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/1213—Oxides or hydroxides, e.g. Al2O3, TiO2, CaO or Ca(OH)2
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3707—Polyethers, e.g. polyalkyleneoxides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/008—Polymeric surface-active agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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- Health & Medical Sciences (AREA)
- Inorganic Chemistry (AREA)
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Abstract
The invention discloses a kind of antibacterial anti-colour contamination liquid detergents and preparation method thereof, volatile essential oil is rich in pericarpium zanthoxyli schinifolii shell, main chemical compositions are linalool, the terpenoid substances such as limonene, with excellent antibacterial effect, the present invention is acted synergistically using pericarpium zanthoxyli schinifolii extracting solution and nano-titanium dioxide, significant antibacterial effect can be reached, simultaneously, nano-titanium dioxide can enter the internal voids of apparel fabrics fiber using its nano-scale, not only increase the completeness of antibacterial, also fixation is further improved, the effect of anti-colour contamination, injury is not generated to clothing and skin.
Description
Technical field
The invention belongs to liquid detergent technical fields, and in particular to antibacterial anti-colour contamination liquid detergent of one kind and preparation method thereof.
Background technology
Liquid detergent is the personal clothing articles for washing quickly grown in recent years, compared with washing powder, liquid detergent dissolving is rapid,
Simple production process, without dust pollution, and it is suitble to cold washing and mechanization washing, therefore be the following hair of laundry detergent compositions
Direction is opened up, since the advantages that its water and electric saving, detergency height, saving resource is increasingly doted on by people.But it is washed with it
It is easy colour contamination when washing dark clothing, fades, enables consumer's worries endlessly.
Common liquid detergent is only used as cleaning agent currently on the market, without efficient antibacterial and anti-colour contamination while decontamination
Function, therefore, exploitation is a kind of not only to have higher dirt-removing power, but also the liquid detergent with antibacterial and anti-colour contamination is with wide
Application prospect.
Invention content
In view of the above-mentioned problems, the present invention is intended to provide a kind of not only having higher dirt-removing power, but also there is antibacterial and anti-string
The liquid detergent of color, and preparation method thereof.
The invention is realized by the following technical scheme：
A kind of antibacterial anti-colour contamination liquid detergent, is made of the raw material of following parts by weight：
Pericarpium zanthoxyli schinifolii extracting solution 5-10, nano-titanium dioxide 5-10, polyethylene glycol-400 3-5, sodium chloride 4-8, laruyl alcohol polyoxy second
Alkene ether 10-20, Cocoamidopropyl betaine 10-15, essence 0.5-3, guar gum 5-10.
Further, preparation method includes the following steps：
（1）Ninety percent pericarpium zanthoxyli schinifolii ripe, that nothing is mildew and rot is chosen to be placed in 0~-10 DEG C of environment and freeze after distilled water flushing 1-2 times
3-6h is ground after taking-up, until granularity is 50-500 μm, obtains pericarpium zanthoxyli schinifolii powder, pericarpium zanthoxyli schinifolii powder is placed in microwave device
Middle carry out microwave treatment, is then added in the extracting solution of 30-50 times of its volume, using 20-40min is ultrasonically treated, then turns
Enter in reflux, flow back 5-10h at 70-85 DEG C, filtering；
（2）Nano-titanium dioxide is first subjected to microwave treatment 5-10s, is then dispersed in the deionized water of 20-50 times of its volume,
Polyethylene glycol-400 is added, while being stirred under the rotating speed of 300-600rpm, while being warming up to 60-65 DEG C, step is then added（1）
Gains, sodium chloride, ethoxylated dodecyl alcohol, Cocoamidopropyl betaine continue to stir with the rotating speed of 400-800rpm
2-4h is eventually adding essence, guar gum, continues to stir 20-30min.
Further, step（1）The microwave treatment conditions are 800-1500W, processing time 10-30s.
Further, step（1）The extracting solution is distilled water and ethyl alcohol with 10:The mixed liquor of 1-3 mixing.
Further, step（1）The ultrasound condition is 30-50Hz, 500-1200W.
Further, step（2）The microwave treatment conditions are 500-1000W.
Further, step（2）The essence is Lavender, aloe essential oil or cape jasmine flower essential oil.
Beneficial effects of the present invention：Volatile essential oil is rich in pericarpium zanthoxyli schinifolii shell, main chemical compositions are linalool, lemon
There is the terpenoid substances such as alkene excellent antibacterial effect, the present invention to be assisted using pericarpium zanthoxyli schinifolii extracting solution and nano-titanium dioxide
Same-action can reach significant antibacterial effect, meanwhile, nano-titanium dioxide can enter apparel fabrics using its nano-scale
The internal voids of fiber, not only increase the completeness of antibacterial, fixation, the effect of anti-colour contamination are also further improved, to clothing
Injury is not generated with skin.
Specific implementation mode
Illustrate the present invention with specific embodiment below, but is not limitation of the present invention.
Embodiment 1
A kind of antibacterial anti-colour contamination liquid detergent, is made of the raw material of following parts by weight：
Pericarpium zanthoxyli schinifolii extracting solution 5, nano-titanium dioxide 5, polyethylene glycol-400 3, sodium chloride 4, ethoxylated dodecyl alcohol 10, coconut palm
Oleamide propyl betaine 10, essence 0.5, guar gum 5.
Further, preparation method includes the following steps：
（1）It chooses ninety percent pericarpium zanthoxyli schinifolii ripe, that nothing is mildew and rot to be placed in 0 DEG C of environment after distilled water flushing 1 time and freeze 3h, take out
After be ground, until granularity be 50 μm, obtain pericarpium zanthoxyli schinifolii powder, by pericarpium zanthoxyli schinifolii powder be placed in microwave device carry out microwave at
Reason, is then added in the extracting solution of 30 times of its volume, using 20min is ultrasonically treated, is then transferred in reflux, at 70 DEG C
Flow back 5h, filtering；
（2）Nano-titanium dioxide is first subjected to microwave treatment 5s, is then dispersed in the deionized water of 20 times of its volume, adds
While being stirred under the rotating speed of 300-600rpm, while being warming up to 60 DEG C, step is then added in polyethylene glycol-400（1）Gains, chlorine
Change sodium, ethoxylated dodecyl alcohol, Cocoamidopropyl betaine, continues to stir 2h with the rotating speed of 400-800rpm, finally add
Enter essence, guar gum, continues to stir 20min.
Further, step（1）The microwave treatment conditions are 800W, processing time 10s.
Further, step（1）The extracting solution is distilled water and ethyl alcohol with 10:The mixed liquor of 1 mixing.
Further, step（1）The ultrasound condition is 30Hz, 500W.
Further, step（2）The microwave treatment conditions are 500W.
Further, step（2）The essence is Lavender.
Embodiment 2
A kind of antibacterial anti-colour contamination liquid detergent, is made of the raw material of following parts by weight：
Pericarpium zanthoxyli schinifolii extracting solution 6, nano-titanium dioxide 7, polyethylene glycol-400 4, sodium chloride 5, ethoxylated dodecyl alcohol 15, coconut palm
Oleamide propyl betaine 13, essence 1, guar gum 7.
Further, preparation method includes the following steps：
（1）Ninety percent pericarpium zanthoxyli schinifolii ripe, that nothing is mildew and rot is chosen to be placed in -5 DEG C of environment after distilled water flushing 2 times and freeze 5h, take
It is ground after going out, until granularity is 100 μm, obtains pericarpium zanthoxyli schinifolii powder, pericarpium zanthoxyli schinifolii powder is placed in microwave device and carries out microwave
Processing, is then added in the extracting solution of 40 times of its volume, using 30min is ultrasonically treated, is then transferred in reflux, 80 DEG C
Lower reflux 8h, filtering；
（2）Nano-titanium dioxide is first subjected to microwave treatment 8s, is then dispersed in the deionized water of 40 times of its volume, adds
While being stirred under the rotating speed of 400rpm, while being warming up to 62 DEG C, step is then added in polyethylene glycol-400（1）Gains, chlorination
Sodium, ethoxylated dodecyl alcohol, Cocoamidopropyl betaine continue to stir 3h with the rotating speed of 700rpm, be eventually adding essence,
Guar gum continues to stir 25min.
Further, step（1）The microwave treatment conditions are 1000W, processing time 20s.
Further, step（1）The extracting solution is distilled water and ethyl alcohol with 10:The mixed liquor of 2 mixing.
Further, step（1）The ultrasound condition is 40Hz, 1000W.
Further, step（2）The microwave treatment conditions are 800W.
Further, step（2）The essence is Lavender.
Embodiment 3
A kind of antibacterial anti-colour contamination liquid detergent, is made of the raw material of following parts by weight：
Pericarpium zanthoxyli schinifolii extracting solution 10, nano-titanium dioxide 10, polyethylene glycol-400 5, sodium chloride 8, ethoxylated dodecyl alcohol 20,
Cocoamidopropyl betaine 15, essence 3, guar gum 10.
Further, preparation method includes the following steps：
（1）Ninety percent pericarpium zanthoxyli schinifolii ripe, that nothing is mildew and rot is chosen to be placed in -10 DEG C of environment after distilled water flushing 2 times and freeze 6h, take
It is ground after going out, until granularity is 500 μm, obtains pericarpium zanthoxyli schinifolii powder, pericarpium zanthoxyli schinifolii powder is placed in microwave device and carries out microwave
Processing, is then added in the extracting solution of 50 times of its volume, using 40min is ultrasonically treated, is then transferred in reflux, 85 DEG C
Lower reflux 10h, filtering；
（2）Nano-titanium dioxide is first subjected to microwave treatment 10s, is then dispersed in the deionized water of 50 times of its volume, then is added
Enter polyethylene glycol-400, while being stirred under the rotating speed of 600rpm, while being warming up to 65 DEG C, step is then added（1）Gains, chlorination
Sodium, ethoxylated dodecyl alcohol, Cocoamidopropyl betaine continue to stir 4h with the rotating speed of 800rpm, be eventually adding essence,
Guar gum continues to stir 30min.
Further, step（1）The microwave treatment conditions are 1500W, processing time 30s.
Further, step（1）The extracting solution is distilled water and ethyl alcohol with 10:The mixed liquor of 3 mixing.
Further, step（1）The ultrasound condition is 50Hz, 1200W.
Further, step（2）The microwave treatment conditions are 1000W.
Further, step（2）The essence is Lavender, aloe essential oil or cape jasmine flower essential oil.
Comparative example 1
The addition of nano-titanium dioxide is omitted compared to embodiment 1 in this comparative example, and method and step in addition to this is homogeneous
Together.
Comparative example 2
The addition of pericarpium zanthoxyli schinifolii extracting solution is omitted compared to embodiment 1 in this comparative example, and method and step in addition to this is homogeneous
Together.
Comparative example 3
Compared to embodiment 1 addition of nano-titanium dioxide and pericarpium zanthoxyli schinifolii extracting solution is omitted, in addition to this in this comparative example
Method and step all same.
Control group
Commercial laundry liquid
Experiment：
Detergency ability is tested：The detergency ability of each group sample is with reference to GB/T13174-2008《It dress material detergent detergency and follows
The measurement of ring scourability》It carries out, liquid detergent is to carbon black oil soiled cotton, albumen soiled cotton, sebum soiled cotton decontamination value obtained by each group sample
It is as shown in table 1 with the ratio of standard liquid detergent decontamination value.
Table 1
As shown in Table 1, the liquid detergent that prepared by the present invention has stronger dirt-removing power.
Anti-microbial property test：Antibacterial ability test is with reference to QB/T2738-2012《Daily chemical products antibacterial and fungistatic effect are commented
Valence method》Carry out, liquid detergent obtained by each group sample diluted 100 times, 20 minutes action time, each group sample to Escherichia coli and
The bacteriostasis rate of staphylococcus aureus is as shown in table 2.
Table 2
As can be seen from Table 2, the liquid detergent that prepared by the present invention has significant antibacterial effect, pericarpium zanthoxyli schinifolii extracting solution and nano-silica
Change titanium synergistic effect, antibacterial effect greatly improves.
Dye migration resistant performance test：Dye migration resistant experiment condition is：30 ± 2 DEG C, rotating speed 120r/min of water temperature, washing
Time 20min, 6 × 6cm calico are shuffled with red cloth and each 4 pieces of black cloth.Measured before washing using calico its chromatic value as
Original value measures the chromatic value of calico again after dye migration resistant is tested after drying, dye migration resistant performance is being washed with calico
It washs front and back its and measures chroma difference Δ E and indicate that value is smaller, expression is from there is the dye molecule washed off on painting cloth to be moved to through solution
Amount on calico is fewer, and the dye migration resistant effect of the liquid detergent is better, i.e., anti-colour contamination effect is better.Test result such as 3 institute of table
Show.
Table 3
As can be seen from Table 3, the liquid detergent that prepared by the present invention have excellent dye migration resistant, i.e., anti-colour contamination effect, this be by
The internal voids for being entered apparel fabrics fiber using its nano-scale in nano-titanium dioxide, are attached in gap, are effectively prevented
The migration of dyestuff.
Claims (7)
1. a kind of antibacterial anti-colour contamination liquid detergent, which is characterized in that be made of the raw material of following parts by weight：
Pericarpium zanthoxyli schinifolii extracting solution 5-10, nano-titanium dioxide 5-10, polyethylene glycol-400 3-5, sodium chloride 4-8, laruyl alcohol polyoxy second
Alkene ether 10-20, Cocoamidopropyl betaine 10-15, essence 0.5-3, guar gum 5-10.
2. the antibacterial anti-colour contamination liquid detergent of one kind according to claim 1, which is characterized in that preparation method includes following step
Suddenly：
（1）Ninety percent pericarpium zanthoxyli schinifolii ripe, that nothing is mildew and rot is chosen to be placed in 0~-10 DEG C of environment and freeze after distilled water flushing 1-2 times
3-6h is ground after taking-up, until granularity is 50-500 μm, obtains pericarpium zanthoxyli schinifolii powder, pericarpium zanthoxyli schinifolii powder is placed in microwave device
Middle carry out microwave treatment, is then added in the extracting solution of 30-50 times of its volume, using 20-40min is ultrasonically treated, then turns
Enter in reflux, flow back 5-10h at 70-85 DEG C, filtering；
（2）Nano-titanium dioxide is first subjected to microwave treatment 5-10s, is then dispersed in the deionized water of 20-50 times of its volume,
Polyethylene glycol-400 is added, while being stirred under the rotating speed of 300-600rpm, while being warming up to 60-65 DEG C, step is then added（1）
Gains, sodium chloride, ethoxylated dodecyl alcohol, Cocoamidopropyl betaine continue to stir with the rotating speed of 400-800rpm
2-4h is eventually adding essence, guar gum, continues to stir 20-30min.
3. a kind of preparation method of antibacterial anti-colour contamination liquid detergent according to claim 2, which is characterized in that step（1）Institute
It is 800-1500W, processing time 10-30s to state microwave treatment conditions.
4. a kind of preparation method of antibacterial anti-colour contamination liquid detergent according to claim 1, which is characterized in that step（1）Institute
It is distilled water and ethyl alcohol with 10 to state extracting solution:The mixed liquor of 1-3 mixing.
5. a kind of preparation method of antibacterial anti-colour contamination liquid detergent according to claim 1, which is characterized in that step（1）Institute
It is 30-50Hz, 500-1200W to state ultrasound condition.
6. a kind of preparation method of antibacterial anti-colour contamination liquid detergent according to claim 1, which is characterized in that step（2）Institute
It is 500-1000W to state microwave treatment conditions.
7. a kind of preparation method of antibacterial anti-colour contamination liquid detergent according to claim 1, which is characterized in that step（2）Institute
It is Lavender, aloe essential oil or cape jasmine flower essential oil to state essence.
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Cited By (3)
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| CN111011815A (en) * | 2019-12-24 | 2020-04-17 | 彝良县增垒农业开发有限公司 | Preparation method of green zanthoxylum oil |
| CN111592942A (en) * | 2020-06-11 | 2020-08-28 | 浙江施维康生物医学材料有限公司 | Color-crossing-preventing washing condensation bead and preparation method thereof |
| CN112375631A (en) * | 2020-11-24 | 2021-02-19 | 云南超越日化有限公司 | Antibacterial laundry detergent and preparation method thereof |
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Cited By (4)
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| CN111011815A (en) * | 2019-12-24 | 2020-04-17 | 彝良县增垒农业开发有限公司 | Preparation method of green zanthoxylum oil |
| CN111592942A (en) * | 2020-06-11 | 2020-08-28 | 浙江施维康生物医学材料有限公司 | Color-crossing-preventing washing condensation bead and preparation method thereof |
| CN112375631A (en) * | 2020-11-24 | 2021-02-19 | 云南超越日化有限公司 | Antibacterial laundry detergent and preparation method thereof |
| CN112375631B (en) * | 2020-11-24 | 2021-11-09 | 云南超越日化有限公司 | Antibacterial laundry detergent and preparation method thereof |
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Application publication date: 20180921 |