CN102899185A - Method for preparing high-class wool spinning textile printing detergent - Google Patents
Method for preparing high-class wool spinning textile printing detergent Download PDFInfo
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- CN102899185A CN102899185A CN2012104124413A CN201210412441A CN102899185A CN 102899185 A CN102899185 A CN 102899185A CN 2012104124413 A CN2012104124413 A CN 2012104124413A CN 201210412441 A CN201210412441 A CN 201210412441A CN 102899185 A CN102899185 A CN 102899185A
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- fatty alcohol
- polyoxyethylene ether
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- wool spinning
- detergent
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Abstract
The invention discloses a method for preparing high-class wool spinning textile printing detergent. The method comprises the following steps of: A, sequentially adding fatty alcohol-polyoxyethylene ether-15, fatty alcohol-polyoxyethylene ether-9 and water into a 1000 ml compound kettle, and dissolving by heating and stirring for 0.5-1 hour; and B, sequentially adding maleic acid-acrylate copolymer, dodecanol amide ethyl ester sulfo succinate disodium salt, laureths-9 sodium sulfate, carboxymethyl hydroxyl propyl cellulose, EDTA (Ethylene Diamine Tetraacetic Acid) disodium salt and sodium metasilicate in solution obtained in step A, stirring for 0.5-2 hours under 50-80 DEG C, and finishing. The high-class wool spinning textile printing detergent obtained in the method disclosed by the invention has an excellent biological degradability, the detergent washing performance is excellent, the contamination resistance is strong, the use is safe and non-toxic, the compound effect is excellent, wool and wool fabric after being washed feel smooth and plump, and the high-class wool spinning textile printing detergent can also be used for the detergent washing of wool milling, the soaping of fabrics such as cotton, fiber and silk, and the like.
Description
Technical field:
The present invention relates to a kind of senior wool spinning printing and dyeing lotion, particularly a kind of preparation method of Novel advanced wool spinning printing and dyeing lotion.
Background technology:
Wool fabric is liked by the human consumer deeply with its noble style, superior wear behavior.The consumption of hair woolen material is at increase year after year, and the assortment of linen-cotton fabric also continue to diversified development, yet untrimmed wool fabric is lower through constantly pushing, rubbing when washing, and felting (Felting) can occur.Thereby cause the appearance change such as fabric size is dwindled, face is scared, weavy grain is chaotic, so that wool fabric in taking process, can only be hand-washed or dry-cleaning by low temperature, can not adopt the violent washings such as washing machine, this washing for fabric is nursed and is caused very burden.Therefore, scouring of wool is the important procedure in the wool spinning technology, road processing and final product quality after the scouring of wool quality directly affects.For a long time, the negatively charged ion lotion is adopted in scouring of wool always, and lotion commonly used comprises sodium soap (soap), sodium alkyl benzene sulfonate (ABS), alkyl sodium sulfonate (601) etc.The scouring of wool of external at present many employing nonionic lotions, nonionic lotion scouring of wool quality is better than negatively charged ion lotion, soft, is beneficial to the processing of rear road, but on the high side.There are some researches show: dodecanol acyl ethyl ester amine disodium sulfosuccinate salt, good surface activity, wetting power is good, and strong detergency is a good tensio-active agent.On the basis of this experiment based on broad research dodecanol acid amides ethyl ester disodium sulfosuccinate salt surfactant performance, it is good to develop a complex effect, and biological degradation is easy, moderate senior wool spinning printing and dyeing lotion.
Summary of the invention:
Goal of the invention: the defective for prior art exists the invention provides a kind of washing excellent property, the preparation method of the senior wool spinning printing and dyeing of the environment-friendly type that biological degradability is good lotion.
Technical scheme: for achieving the above object, the present invention by the following technical solutions:
A kind of preparation of senior wool spinning printing and dyeing lotion: A, add successively fatty alcohol-polyoxyethylene ether-15 in the composite still of 1000ml, fatty alcohol-polyoxyethylene ether-9 and water are warming up to 40 ~ 60 ℃, stir 0.5 ~ 1 hour, make its dissolving.B, under vigorous stirring, add successively in the solution that obtains to steps A, maleic acid-acrylic acid copolymer, dodecanol acid amides ethyl ester disodium sulfosuccinate salt, laureth-9 sodium sulfate, carboxymethyl hydroxypropyl cellulose, EDETATE DISODIUM, Starso adds quantitative water again, stirred 0.5 ~ 2 hour at 50 ~ 80 ℃, make solid content and be 20% optimization detergent product.Raw materials used mass fraction is:
Fatty alcohol-polyoxyethylene ether-15:1 ~ 10 part
Fatty alcohol-polyoxyethylene ether-9:1 ~ 15 part
Maleic acid-acrylic acid copolymer: 50 ~ 150 parts
Dodecanol acid amides ethyl ester disodium sulfosuccinate salt: 10 ~ 30 parts
Laureth-9 sodium sulfate: 10 ~ 30 parts
Carboxymethyl hydroxypropyl cellulose: 5 ~ 15 parts
EDETATE DISODIUM: 0.5 ~ 3 part
Starso: 0.5 ~ 3 part
Water: an amount of
In the preparation of described cleaner for wool spinning and milling, fatty alcohol-polyoxyethylene ether-15: fatty alcohol-polyoxyethylene ether-9: maleic acid-acrylic acid copolymer: dodecanol acid amides ethyl ester disodium sulfosuccinate salt: laureth-9 sodium sulfate: carboxymethyl hydroxypropyl cellulose: EDETATE DISODIUM: the mass ratio of Starso is 1:1 ~ 1.5:5 ~ 50:1 ~ 10:1 ~ 10:1 ~ 1.5:0.01 ~ 1:0.01 ~ 1.
According to above technical scheme, can realize following beneficial effect: compared with prior art, the present invention has the following advantages: the present invention obtains senior wool spinning printing and dyeing lotion: have good biological degradability, the washing excellent performance, anti-contamination ability is strong, safety non-toxic, complex effect is good and moderate, reach international standards, hair and wool textile slippery feel, plentiful through washing, and this lotion both can be used for the washing of wool spinning fulling, also can be used for soaping of the fabrics such as cotton, fiber crops, silk.
Embodiment:
Below in conjunction with embodiment the present invention is done further detailed description, but the scope of protection of present invention is not limited to the scope that embodiment represents.
Embodiment 1:
Add successively 5g fatty alcohol-polyoxyethylene ether-15 in the composite still of 1000ml, 6g fatty alcohol-polyoxyethylene ether-9 and 500ml water are warming up to 40 ~ 60 ℃, stir 0.5 ~ 1 hour, make its dissolving.Under vigorous stirring, in mentioned solution, add successively the 120g maleic acid-acrylic acid copolymer, 18g dodecanol acid amides ethyl ester disodium sulfosuccinate salt, 12g laureth-9 sodium sulfate, 8g carboxymethyl hydroxypropyl cellulose, 1.8g EDETATE DISODIUM, 1.2g Starso, add again 180ml water, stirred 0.5 ~ 2 hour at 50 ~ 80 ℃, make solid content and be 20% optimization detergent product.
Claims (2)
1. the preparation method of a senior wool spinning printing and dyeing lotion is characterized in that: A, add successively fatty alcohol-polyoxyethylene ether-15 in the composite still of 1000ml, fatty alcohol-polyoxyethylene ether-9 and water are warming up to 40 ~ 60 ℃, stir 0.5 ~ 1 hour, make its dissolving; B, under vigorous stirring, add successively in the solution that obtains to steps A, maleic acid-acrylic acid copolymer, dodecanol acid amides ethyl ester disodium sulfosuccinate salt, laureth-9 sodium sulfate, carboxymethyl hydroxypropyl cellulose, EDETATE DISODIUM, Starso adds quantitative water again, stirred 0.5 ~ 2 hour at 50 ~ 80 ℃, make solid content and be 20% optimization detergent product; Raw materials used mass fraction is:
Fatty alcohol-polyoxyethylene ether-15:1 ~ 10 part
Fatty alcohol-polyoxyethylene ether-9:1 ~ 15 part
Maleic acid-acrylic acid copolymer: 50 ~ 150 parts
Dodecanol acid amides ethyl ester disodium sulfosuccinate salt: 10 ~ 30 parts
Laureth-9 sodium sulfate: 10 ~ 30 parts
Carboxymethyl hydroxypropyl cellulose: 5 ~ 15 parts
EDETATE DISODIUM: 0.5 ~ 3 part
Starso: 0.5 ~ 3 part
Water: an amount of.
2. the preparation method of described senior wool spinning printing and dyeing lotion according to claim 1, it is characterized in that: fatty alcohol-polyoxyethylene ether-15: fatty alcohol-polyoxyethylene ether-9: maleic acid-acrylic acid copolymer: dodecanol acid amides ethyl ester disodium sulfosuccinate salt: laureth-9 sodium sulfate: carboxymethyl hydroxypropyl cellulose: EDETATE DISODIUM: the mass ratio of Starso is 1:1 ~ 1.5:5 ~ 50:1 ~ 10:1 ~ 10:1 ~ 1.5:0.01 ~ 1:0.01 ~ 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2012104124413A CN102899185A (en) | 2012-10-25 | 2012-10-25 | Method for preparing high-class wool spinning textile printing detergent |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012104124413A CN102899185A (en) | 2012-10-25 | 2012-10-25 | Method for preparing high-class wool spinning textile printing detergent |
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| CN102899185A true CN102899185A (en) | 2013-01-30 |
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| CN2012104124413A Pending CN102899185A (en) | 2012-10-25 | 2012-10-25 | Method for preparing high-class wool spinning textile printing detergent |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105802753A (en) * | 2016-04-12 | 2016-07-27 | 湖州吉昌丝绸有限公司 | Soaping agent applicable to wool fabric |
| CN106544165A (en) * | 2016-10-28 | 2017-03-29 | 济宁锦祥化工科技有限公司 | A kind of preparation method of textile printing and dyeing with green deoiling decontaminant |
| CN106635512A (en) * | 2016-10-28 | 2017-05-10 | 济宁锦祥化工科技有限公司 | Preparation method for green soaping agent for spinning printing and dyeing |
| CN110184820A (en) * | 2019-05-30 | 2019-08-30 | 江苏尼美达科技有限公司 | A kind of Multifunctional washing-free milling agent and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1648327A (en) * | 2004-11-01 | 2005-08-03 | 上海市印染技术研究所 | Anti-soil detergent for textile white ground |
-
2012
- 2012-10-25 CN CN2012104124413A patent/CN102899185A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1648327A (en) * | 2004-11-01 | 2005-08-03 | 上海市印染技术研究所 | Anti-soil detergent for textile white ground |
Non-Patent Citations (2)
| Title |
|---|
| 主领地等: "《化工产品手册.精细化工助剂》", 31 August 2008, 化学工业出版社 * |
| 李东光等: "《精细化学品配方.1》", 31 January 2004, 江苏科学技术出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105802753A (en) * | 2016-04-12 | 2016-07-27 | 湖州吉昌丝绸有限公司 | Soaping agent applicable to wool fabric |
| CN106544165A (en) * | 2016-10-28 | 2017-03-29 | 济宁锦祥化工科技有限公司 | A kind of preparation method of textile printing and dyeing with green deoiling decontaminant |
| CN106635512A (en) * | 2016-10-28 | 2017-05-10 | 济宁锦祥化工科技有限公司 | Preparation method for green soaping agent for spinning printing and dyeing |
| CN110184820A (en) * | 2019-05-30 | 2019-08-30 | 江苏尼美达科技有限公司 | A kind of Multifunctional washing-free milling agent and preparation method thereof |
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| C06 | Publication | ||
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20130130 |