CN108559605A - A kind of preparation method of environmentally protective mine hydraulic support fluid - Google Patents
A kind of preparation method of environmentally protective mine hydraulic support fluid Download PDFInfo
- Publication number
- CN108559605A CN108559605A CN201810512407.0A CN201810512407A CN108559605A CN 108559605 A CN108559605 A CN 108559605A CN 201810512407 A CN201810512407 A CN 201810512407A CN 108559605 A CN108559605 A CN 108559605A
- Authority
- CN
- China
- Prior art keywords
- hydraulic support
- preparation
- environmentally protective
- acid
- mixing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000012530 fluid Substances 0.000 title claims abstract description 28
- 230000001681 protective effect Effects 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- 238000002156 mixing Methods 0.000 claims abstract description 24
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 18
- 239000002253 acid Substances 0.000 claims abstract description 18
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 16
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 150000003973 alkyl amines Chemical class 0.000 claims abstract description 11
- 239000013556 antirust agent Substances 0.000 claims abstract description 10
- 239000002199 base oil Substances 0.000 claims abstract description 10
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 10
- 239000011707 mineral Substances 0.000 claims abstract description 10
- 239000011734 sodium Substances 0.000 claims abstract description 10
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 10
- 125000001931 aliphatic group Chemical group 0.000 claims abstract description 9
- ZZVUWRFHKOJYTH-UHFFFAOYSA-N diphenhydramine Chemical compound C=1C=CC=CC=1C(OCCN(C)C)C1=CC=CC=C1 ZZVUWRFHKOJYTH-UHFFFAOYSA-N 0.000 claims abstract description 8
- 230000000855 fungicidal effect Effects 0.000 claims abstract description 8
- 239000000417 fungicide Substances 0.000 claims abstract description 8
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims abstract description 6
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000012964 benzotriazole Substances 0.000 claims abstract description 6
- 229940028356 diethylene glycol monobutyl ether Drugs 0.000 claims abstract description 6
- JCGNDDUYTRNOFT-UHFFFAOYSA-N oxolane-2,4-dione Chemical compound O=C1COC(=O)C1 JCGNDDUYTRNOFT-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000003208 petroleum Substances 0.000 claims abstract description 5
- -1 boric acid amine salt Chemical class 0.000 claims description 39
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 12
- 150000001412 amines Chemical class 0.000 claims description 9
- 239000003921 oil Substances 0.000 claims description 9
- 235000019198 oils Nutrition 0.000 claims description 9
- 125000000217 alkyl group Chemical group 0.000 claims description 6
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 claims description 6
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 6
- 150000002148 esters Chemical class 0.000 claims description 6
- 229930195729 fatty acid Natural products 0.000 claims description 6
- 239000000194 fatty acid Substances 0.000 claims description 6
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 229910019142 PO4 Inorganic materials 0.000 claims description 4
- 239000004615 ingredient Substances 0.000 claims description 4
- 239000012875 nonionic emulsifier Substances 0.000 claims description 4
- IOQPZZOEVPZRBK-UHFFFAOYSA-N octan-1-amine Chemical compound CCCCCCCCN IOQPZZOEVPZRBK-UHFFFAOYSA-N 0.000 claims description 4
- 239000010452 phosphate Substances 0.000 claims description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 4
- 239000008158 vegetable oil Substances 0.000 claims description 4
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims description 3
- 239000003899 bactericide agent Substances 0.000 claims description 3
- 229960003237 betaine Drugs 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 3
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 2
- KANAPVJGZDNSCZ-UHFFFAOYSA-N 1,2-benzothiazole 1-oxide Chemical compound C1=CC=C2S(=O)N=CC2=C1 KANAPVJGZDNSCZ-UHFFFAOYSA-N 0.000 claims description 2
- HXKKHQJGJAFBHI-UHFFFAOYSA-N 1-aminopropan-2-ol Chemical compound CC(O)CN HXKKHQJGJAFBHI-UHFFFAOYSA-N 0.000 claims description 2
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 2
- LWEAHXKXKDCSIE-UHFFFAOYSA-M 2,3-di(propan-2-yl)naphthalene-1-sulfonate Chemical compound C1=CC=C2C(S([O-])(=O)=O)=C(C(C)C)C(C(C)C)=CC2=C1 LWEAHXKXKDCSIE-UHFFFAOYSA-M 0.000 claims description 2
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 2
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 2
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 2
- XBPCUCUWBYBCDP-UHFFFAOYSA-N Dicyclohexylamine Chemical compound C1CCCCC1NC1CCCCC1 XBPCUCUWBYBCDP-UHFFFAOYSA-N 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- REYJJPSVUYRZGE-UHFFFAOYSA-N Octadecylamine Chemical compound CCCCCCCCCCCCCCCCCCN REYJJPSVUYRZGE-UHFFFAOYSA-N 0.000 claims description 2
- 239000005642 Oleic acid Substances 0.000 claims description 2
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 2
- 235000019082 Osmanthus Nutrition 0.000 claims description 2
- 241000333181 Osmanthus Species 0.000 claims description 2
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 2
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical class [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 claims description 2
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 2
- SLINHMUFWFWBMU-UHFFFAOYSA-N Triisopropanolamine Chemical compound CC(O)CN(CC(C)O)CC(C)O SLINHMUFWFWBMU-UHFFFAOYSA-N 0.000 claims description 2
- BKDZVPVJIXZYBH-UHFFFAOYSA-N [Na].C(C)(=O)O.NC(=N)N Chemical compound [Na].C(C)(=O)O.NC(=N)N BKDZVPVJIXZYBH-UHFFFAOYSA-N 0.000 claims description 2
- 125000002252 acyl group Chemical group 0.000 claims description 2
- 235000004279 alanine Nutrition 0.000 claims description 2
- 239000010775 animal oil Substances 0.000 claims description 2
- 239000004327 boric acid Substances 0.000 claims description 2
- JGIATAMCQXIDNZ-UHFFFAOYSA-N calcium sulfide Chemical compound [Ca]=S JGIATAMCQXIDNZ-UHFFFAOYSA-N 0.000 claims description 2
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 2
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 2
- 229940043237 diethanolamine Drugs 0.000 claims description 2
- VPNOHCYAOXWMAR-UHFFFAOYSA-N docosan-1-amine Chemical compound CCCCCCCCCCCCCCCCCCCCCCN VPNOHCYAOXWMAR-UHFFFAOYSA-N 0.000 claims description 2
- JRBPAEWTRLWTQC-UHFFFAOYSA-N dodecylamine Chemical compound CCCCCCCCCCCCN JRBPAEWTRLWTQC-UHFFFAOYSA-N 0.000 claims description 2
- 235000019387 fatty acid methyl ester Nutrition 0.000 claims description 2
- 150000004665 fatty acids Chemical class 0.000 claims description 2
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 2
- 239000000787 lecithin Substances 0.000 claims description 2
- 229940067606 lecithin Drugs 0.000 claims description 2
- 235000010445 lecithin Nutrition 0.000 claims description 2
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 2
- 229920000570 polyether Polymers 0.000 claims description 2
- 229920001296 polysiloxane Polymers 0.000 claims description 2
- WBHHMMIMDMUBKC-XLNAKTSKSA-N ricinelaidic acid Chemical compound CCCCCC[C@@H](O)C\C=C\CCCCCCCC(O)=O WBHHMMIMDMUBKC-XLNAKTSKSA-N 0.000 claims description 2
- 229960003656 ricinoleic acid Drugs 0.000 claims description 2
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 claims description 2
- 150000003918 triazines Chemical class 0.000 claims description 2
- 235000013311 vegetables Nutrition 0.000 claims description 2
- 239000002202 Polyethylene glycol Substances 0.000 claims 2
- LVTYICIALWPMFW-UHFFFAOYSA-N diisopropanolamine Chemical compound CC(O)CNCC(C)O LVTYICIALWPMFW-UHFFFAOYSA-N 0.000 claims 2
- 229940043276 diisopropanolamine Drugs 0.000 claims 2
- 229920001223 polyethylene glycol Polymers 0.000 claims 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims 1
- 229920001732 Lignosulfonate Polymers 0.000 claims 1
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 claims 1
- SYKNUAWMBRIEKB-UHFFFAOYSA-N [Cl].[Br] Chemical compound [Cl].[Br] SYKNUAWMBRIEKB-UHFFFAOYSA-N 0.000 claims 1
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 claims 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 229940117986 sulfobetaine Drugs 0.000 claims 1
- 239000007788 liquid Substances 0.000 abstract description 5
- 239000000126 substance Substances 0.000 abstract description 5
- 238000003912 environmental pollution Methods 0.000 abstract description 3
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 8
- 230000008901 benefit Effects 0.000 description 5
- 235000010288 sodium nitrite Nutrition 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 3
- 238000005065 mining Methods 0.000 description 3
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 239000008233 hard water Substances 0.000 description 2
- 229910001385 heavy metal Inorganic materials 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 1
- 208000005623 Carcinogenesis Diseases 0.000 description 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 241000132456 Haplocarpha Species 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- MOFINMJRLYEONQ-UHFFFAOYSA-N [N].C=1C=CNC=1 Chemical class [N].C=1C=CNC=1 MOFINMJRLYEONQ-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 125000005605 benzo group Chemical group 0.000 description 1
- 230000036952 cancer formation Effects 0.000 description 1
- 231100000504 carcinogenesis Toxicity 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000001808 coupling effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 230000009970 fire resistant effect Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- OHMBHFSEKCCCBW-UHFFFAOYSA-N hexane-2,5-diol Chemical compound CC(O)CCC(C)O OHMBHFSEKCCCBW-UHFFFAOYSA-N 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 125000002819 montanyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M173/00—Lubricating compositions containing more than 10% water
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/06—Metal compounds
- C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/04—Ethers; Acetals; Ortho-esters; Ortho-carbonates
- C10M2207/046—Hydroxy ethers
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
- C10M2207/402—Castor oils
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/108—Polyethers, i.e. containing di- or higher polyoxyalkylene groups etherified
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/109—Polyethers, i.e. containing di- or higher polyoxyalkylene groups esterified
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/221—Six-membered rings containing nitrogen and carbon only
- C10M2215/222—Triazines
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/042—Sulfate esters
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/10—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring
- C10M2219/104—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring containing sulfur and carbon with nitrogen or oxygen in the ring
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2225/00—Organic macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2225/04—Organic macromolecular compounds containing phosphorus as ingredients in lubricant compositions obtained by phosphorisation of macromolecualr compounds not containing phosphorus in the monomers
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- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
- C10M2229/04—Siloxanes with specific structure
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
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Abstract
The invention discloses a kind of preparation methods of environmentally protective mine hydraulic support fluid, comprise the following steps that successively：By water, 0.1~1.0 part of sodium hydroxide, 2~15 parts of antirust agent, 0~8 part of hydramine, 0.1~0.8 part of benzotriazole, tetra- sodium of EDTA, 0~12 part of mixing, the solution I of homogeneous transparent is obtained；3~30 parts of mineral base oil, 1~5 part of diethylene glycol monobutyl ether, 2~20 parts of emulsifier, 0~10 part of alkylamine, 2~15 parts of aliphatic acid are added in solution I, is mixed, obtains the solution II of homogeneous transparent；0.1~3 part of fungicide, 0.01~0.8 part of antifoaming agent are added in solution II, is mixed, obtains the solution III of homogeneous transparent.A kind of preparation method of environmentally protective mine hydraulic support fluid of the present invention, preparation process is simple, the holder liquid appearance transparent of acquisition, the non-volatile substance of odorlessness, it is environmentally protective, it is applicable to different quality, freeze-thaw resistance property is excellent, saves petroleum resources and can reduce environmental pollution.
Description
【Technical field】
The present invention relates to the technical field of hydraulic support fluid more particularly to a kind of systems of environmentally protective mine hydraulic support fluid
Preparation Method.
【Background technology】
Mine hydraulic support fluid is a kind of to be developed for advanced mine hydraulic support and other industrial quarters hydraulic pressure systems
Fire-resistant hydraulic fluid, mine hydraulic support liquid energy are effectively protected hydraulic system, extend hydraulic support service life.Mine at present
For hydraulic support fluid largely using sodium nitrite as rust-inhibiting additive, sodium nitrite has rust-proof effect as rust-inhibiting additive
Good, at low cost feature, but sodium nitrite has stimulation and carcinogenesis to human body, jeopardizes personal health and pollution environment.And
Mine hydraulic support fluid is there is also resistance to hard water stability is poor at present, the undesirable disadvantage of freeze-thaw resistance property.Therefore, it is necessary to
It proposes that one kind is environmentally protective, resistance to hard water stability is good, and meets the hydraulic support fluid of mining demand.
【Invention content】
The purpose of the present invention is exactly to solve the problems of the prior art, a kind of environmentally protective mine hydraulic support fluid of proposition
Preparation method, preparation process is simple, the holder liquid appearance transparent that the method for the present invention obtains, and the non-volatile substance of odorlessness has good
Good stability is free of sodium nitrite, and the harmful substances such as heavy metal ensure that worker's body is without damage, environmentally protective, applicable
In different quality, freeze-thaw resistance property is excellent, meets the requirement of mine long-wall mining, and use cost is low, and saving petroleum resources simultaneously can
It reduces environmental pollution, is a kind of good oil emulsion substitute products, can be widely used in coal production, have apparent economical
Benefit and social benefit.
To achieve the above object, the present invention proposes a kind of preparation method of environmentally protective mine hydraulic support fluid, successively
It comprises the following steps that：
A) by 6.4~59.49 parts of water, 0.1~1.0 part of sodium hydroxide, 2~15 parts of antirust agent, 0~8 part of hydramine, benzo three
0.1~0.8 part of nitrogen azoles, 0~12 part of tetra- sodium of EDTA are added sequentially to be mixed 15~60 minutes in reaction kettle, obtain uniformly thoroughly
Bright solution I；
B) by 3~30 parts of mineral base oil, 1~5 part of diethylene glycol monobutyl ether, 2~20 parts of emulsifier, alkylamine 0~10
Part, 2~15 parts of aliphatic acid are added sequentially in solution I, are mixed 15~60 minutes, are obtained the solution II of homogeneous transparent；
C) 0.1~3 part of fungicide, 0.01~0.8 part of antifoaming agent are added sequentially in solution II, are mixed 15~60
Minute, obtain the solution III of homogeneous transparent.
Preferably, the mixing speed in described step a, b, c is 60~80r/min.
Preferably, the antirust agent is water-based antirust, the antirust agent is organic amine acid salt or ester, boric acid
Amine salt either one or more mixing in ester, dodecenylsuccinic acid amine salt or ester.
Preferably, the hydramine is monoethanolamine, diethanol amine, triethanolamine, monoisopropanolamine, diisopropanol
One or more mixing in amine, triisopropanolamine.The hydramine maintains the stabilization of solution pH value.
Preferably, the benzotriazole plays anti-non-ferrous metal discoloration.
Preferably, tetra- sodium of EDTA is chelating agent, the hardness of water is reduced, keeps emulsion stability.
Preferably, the mineral base oil is paraffinic base, intermediate base or naphthenic mineral type base oil, it is from stone
The ingredient being extract in oil.
Preferably, the emulsifier is one kind in ionic emulsifying agent, nonionic emulsifier, amphoteric emulsifier
Or a variety of mixing, the ionic emulsifying agent be fatty alcohol ether sulfate salt, fatty alcohol sulfate salt, sodium alkyl sulfonate,
It is alkyl ether carboxylic acid, aromatic radical ether carboxylic acid, fatty alcohol carboxylate, petroleum sodium sulfonate, oil sulphur calcium, nekal, wooden
Plain sulfonate, octadecyl trimethyl chlorine (bromine) change one or more mixing in ammonium, and the nonionic emulsifier is poly-
Ethylene oxide fatty alcohol ether, polyoxyethylene fatty acid esters, sorbitan fatty acid ester, gathers polyoxyethylene nonyl phenyl vinethene
Ethylene oxide fat alcohol phosphate, anhydrous sorbitol phosphate, polyoxyethylene nonyl phenyl ethylene phosphate, fatty acid methyl ester polyoxyethylene
One or more mixing in ether, the amphoteric emulsifier are alkyl betaine, Cocoamidopropyl betaine, weight ratio
In glycine betaine, lecithin, osmanthus acyl both sexes guanidine-acetic acid sodium, alkyl aminopropionic mono-sodium salt, ethoxy iso-octyl alanine mono-sodium salt
One or more mixing.
Preferably, the alkylamine mixes for one or more of alkyl line style amine and the ring-like amine of alkyl, institute
The alkylamine stated is octyl amine, lauryl amine, octadecylamine, two octyl amine, docosyl amine, octacosyl
One or more mixing in amine, cyclohexylamine, dicyclohexyl amine, tricyclohexyltin amine.The alkylamine and butyl glycol ether plays coupling
Effect, it is ensured that water phase and oil phase are transparent.
Preferably, the aliphatic acid is that either vegetable fatty acid is refined from animal oil or vegetable oil to animal
Ingredient out, the aliphatic acid are animal oleic acid, vegetable oil acid, ricinoleic acid, one kind in ready denier oil acid or more
Kind mixing, the aliphatic acid play antirust and lubrication.
Preferably, the fungicide is benzoisothiazolinone, dimethylene diamines series bactericidal agent, triazines sterilization
One or more mixing in agent.
Preferably, the antifoaming agent be water-soluble poly ether defoaming agent and one kind in efficient polysiloxane defoaming agent or
A variety of mixing.
Preferably, being diluted with water adjusting concentration, it is recommended to use a concentration of 4~5%V/V.
Beneficial effects of the present invention：A kind of preparation method of environmentally protective mine hydraulic support fluid of the present invention, preparation process
Simply, the holder liquid appearance transparent that the method for the present invention obtains, the non-volatile substance of odorlessness is with good stability, without Asia
Sodium nitrate, the harmful substances such as heavy metal ensure that worker's body is without damage, environmentally protective, are applicable to different quality, freeze-thawing resistant
It has excellent performance, meets the requirement of mine long-wall mining, use cost is low, saves petroleum resources and can reduce environmental pollution, is one
The good oil emulsion substitute products of kind, can be widely used in coal production, have apparent economic benefit and social benefit.
The feature and advantage of the present invention will be described in detail by embodiment.
【Specific implementation mode】
Embodiment one：
A kind of preparation method of environmentally protective mine hydraulic support fluid, comprises the following steps that successively：
A) water, 0.5 part of sodium hydroxide, 8 parts of antirust agent, 0.5 part of benzotriazole are added sequentially to mix in reaction kettle
Stirring 15~60 minutes, obtains the solution I of homogeneous transparent；
B) by 8 parts of mineral base oil, 2.5 parts of diethylene glycol monobutyl ether, 4 parts of emulsifier, 5 parts of alkylamine, 4 parts of aliphatic acid according to
It is secondary to be added in solution I, it is mixed 15~60 minutes, obtains the solution II of homogeneous transparent；
C) 1 part of fungicide, 0.01 part of antifoaming agent are added sequentially in solution II, are mixed 15~60 minutes, obtain
The solution III of homogeneous transparent.
Holder liquid detection knot obtained by a kind of preparation method embodiment one of environmentally protective mine hydraulic support fluid of table one
Fruit
Embodiment two：
A kind of preparation method of environmentally protective mine hydraulic support fluid, comprises the following steps that successively：
A) by water, 0.5 part of sodium hydroxide, 8 parts of antirust agent, 2 parts of hydramine, 0.5 part of benzotriazole, 1 part of tetra- sodium of EDTA according to
Secondary be added in reaction kettle is mixed 15~60 minutes, obtains the solution I of homogeneous transparent；
B) by 8 parts of mineral base oil, 2.5 parts of diethylene glycol monobutyl ether, 7 parts of emulsifier, 2 parts of alkylamine, 4 parts of aliphatic acid according to
It is secondary to be added in solution I, it is mixed 15~60 minutes, obtains the solution II of homogeneous transparent；
C) 1 part of fungicide, 0.01 part of antifoaming agent are added sequentially in solution II, are mixed 15~60 minutes, obtain
The solution III of homogeneous transparent.
Embodiment three：
A kind of preparation method of environmentally protective mine hydraulic support fluid, comprises the following steps that successively：
B) by water, 0.8 part of sodium hydroxide, 10 parts of antirust agent, 5 parts of hydramine, 0.3 part of benzotriazole, 8 parts of tetra- sodium of EDTA according to
Secondary be added in reaction kettle is mixed 15~60 minutes, obtains the solution I of homogeneous transparent；
B) by 8 parts of mineral base oil, 3 parts of diethylene glycol monobutyl ether, 7 parts of emulsifier, 6 parts of alkylamine, 12 parts of aliphatic acid according to
It is secondary to be added in solution I, it is mixed 15~60 minutes, obtains the solution II of homogeneous transparent；
C) 1 part of fungicide, 0.2 part of antifoaming agent are added sequentially in solution II, are mixed 15~60 minutes, obtained
Even transparent solution III.
Above-described embodiment is the description of the invention, is not limitation of the invention, it is any to simple transformation of the present invention after
Scheme all belong to the scope of protection of the present invention.
Claims (10)
1. a kind of preparation method of environmentally protective mine hydraulic support fluid, it is characterised in that：It comprises the following steps that successively：
A) by 6.4~59.49 parts of water, 0.1~1.0 part of sodium hydroxide, 2~15 parts of antirust agent, 0~8 part of hydramine, benzotriazole
0.1~0.8 part, 0~12 part of tetra- sodium of EDTA be added sequentially to be mixed 15~60 minutes in reaction kettle, obtain homogeneous transparent
Solution I；
B) by 3~30 parts of mineral base oil, 1~5 part of diethylene glycol monobutyl ether, 2~20 parts of emulsifier, 0~10 part of alkylamine, fat
2~15 parts of fat acid is added sequentially in solution I, is mixed 15~60 minutes, is obtained the solution II of homogeneous transparent；
C) 0.1~3 part of fungicide, 0.01~0.8 part of antifoaming agent are added sequentially in solution II, are mixed 15~60 points
Clock obtains the solution III of homogeneous transparent.
2. a kind of preparation method of environmentally protective mine hydraulic support fluid as described in claim 1, it is characterised in that：It is described
Step a, b, c in mixing speed be 60~80r/min.
3. a kind of preparation method of environmentally protective mine hydraulic support fluid as described in claim 1, it is characterised in that：It is described
Antirust agent be water-based antirust, the antirust agent is organic amine acid salt either ester, boric acid amine salt or ester, laurylene base fourth
One or more mixing in two amine acid salts or ester.
4. a kind of preparation method of environmentally protective mine hydraulic support fluid as described in claim 1, it is characterised in that：It is described
Hydramine be monoethanolamine, diethanol amine, triethanolamine, monoisopropanolamine, diisopropanolamine (DIPA), one kind in triisopropanolamine or
A variety of mixing.
5. a kind of preparation method of environmentally protective mine hydraulic support fluid as described in claim 1, it is characterised in that：It is described
Mineral base oil be paraffinic base, intermediate base or naphthenic mineral type base oil, be the ingredient being extract from oil.
6. a kind of preparation method of environmentally protective mine hydraulic support fluid as described in claim 1, it is characterised in that：It is described
Emulsifier be ionic emulsifying agent, nonionic emulsifier, the mixing of one or more of amphoteric emulsifier, it is described from
Subtype emulsifier is fatty alcohol ether sulfate salt, fatty alcohol sulfate salt, sodium alkyl sulfonate, alkyl ether carboxylic acid, aromatic radical ether carboxylic
Acid, fatty alcohol carboxylate, petroleum sodium sulfonate, oil sulphur calcium, nekal, lignosulfonates, octadecyl front three
Base chlorine (bromine) changes one or more mixing in ammonium, and the nonionic emulsifier is polyoxyethylene aliphatic alcohol ether, nonyl
Phenol polyethylene glycol oxide ether, sorbitan fatty acid ester, polyethylene glycol oxide fat alcohol phosphate, loses polyoxyethylene fatty acid esters
One or more mixing in water sorbierite phosphate, polyoxyethylene nonyl phenyl ethylene phosphate, fatty acid methyl ester APEO,
The amphoteric emulsifier is alkyl betaine, Cocoamidopropyl betaine, hydroxyl sulfo betaine, lecithin, osmanthus acyl two
One or more mixing in property guanidine-acetic acid sodium, alkyl aminopropionic mono-sodium salt, ethoxy iso-octyl alanine mono-sodium salt.
7. a kind of preparation method of environmentally protective mine hydraulic support fluid as described in claim 1, it is characterised in that：It is described
Alkylamine be one or more of alkyl line style amine and the ring-like amine of alkyl mixing, the alkylamine be octyl amine,
Lauryl amine, octadecylamine, two octyl amine, docosyl amine, octacosyl amine, cyclohexylamine, dicyclohexyl amine, three
One or more mixing in cyclohexylamine.
8. a kind of preparation method of environmentally protective mine hydraulic support fluid as described in claim 1, it is characterised in that：It is described
Aliphatic acid be that either vegetable fatty acid is the ingredient being extract from animal oil or vegetable oil, the fat to animal
Acid is one or more mixing in animal oleic acid, vegetable oil acid, ricinoleic acid, ready denier oil acid.
9. a kind of preparation method of environmentally protective mine hydraulic support fluid as described in claim 1, it is characterised in that：It is described
Fungicide be benzoisothiazolinone, dimethylene diamines series bactericidal agent, one or more mixing in triazine series bactericidal agent.
10. a kind of preparation method of environmentally protective mine hydraulic support fluid as described in claim 1, it is characterised in that：Institute
The antifoaming agent stated is one or more mixing in water-soluble poly ether defoaming agent and efficient polysiloxane defoaming agent.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109456824A (en) * | 2018-11-27 | 2019-03-12 | 辽宁泰克诺美科技有限公司 | A kind of mine hydraulic support oil emulsion |
| CN109777582A (en) * | 2019-03-20 | 2019-05-21 | 富地润滑科技股份有限公司 | A kind of mine hydraulic support fluid and preparation method thereof of green environment protective biological degradation |
| CN111518608A (en) * | 2020-05-27 | 2020-08-11 | 中国石油化工股份有限公司 | Emulsified oil composition for low-temperature-resistant hydraulic support, preparation method and application |
| CN112029564A (en) * | 2020-09-09 | 2020-12-04 | 南京科润工业介质股份有限公司 | Neutral water-based antirust agent |
| CN113136177A (en) * | 2021-04-08 | 2021-07-20 | 煤炭科学技术研究院有限公司 | Efficient anti-freezing solution for hydraulic support and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1208072A1 (en) * | 1984-03-01 | 1986-01-30 | Всесоюзный Ордена Трудового Красного Знамени Научно-Исследовательский Институт Горной Геомеханики И Маркшейдерского Дела | Working fluid for hydraulic systems of powered supports |
| CN101029273A (en) * | 2007-02-15 | 2007-09-05 | 大同云雁石化有限公司 | Liquefied concentrate for hydraulic stand |
| CN102839038A (en) * | 2012-09-13 | 2012-12-26 | 济南库伦特科技有限公司 | Additive composition for producing emulsified oil, preparation method of additive composition and application of additive composition |
| CN103074150A (en) * | 2012-12-26 | 2013-05-01 | 山东梁山三晶石化有限责任公司 | Emulsified oil for hydraulic support for mines and preparation method |
| CN108048182A (en) * | 2017-12-18 | 2018-05-18 | 煤炭科学技术研究院有限公司 | A kind of complex function additive and preparation method for hydraulic support oil emulsion |
-
2018
- 2018-05-25 CN CN201810512407.0A patent/CN108559605A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1208072A1 (en) * | 1984-03-01 | 1986-01-30 | Всесоюзный Ордена Трудового Красного Знамени Научно-Исследовательский Институт Горной Геомеханики И Маркшейдерского Дела | Working fluid for hydraulic systems of powered supports |
| CN101029273A (en) * | 2007-02-15 | 2007-09-05 | 大同云雁石化有限公司 | Liquefied concentrate for hydraulic stand |
| CN102839038A (en) * | 2012-09-13 | 2012-12-26 | 济南库伦特科技有限公司 | Additive composition for producing emulsified oil, preparation method of additive composition and application of additive composition |
| CN103074150A (en) * | 2012-12-26 | 2013-05-01 | 山东梁山三晶石化有限责任公司 | Emulsified oil for hydraulic support for mines and preparation method |
| CN108048182A (en) * | 2017-12-18 | 2018-05-18 | 煤炭科学技术研究院有限公司 | A kind of complex function additive and preparation method for hydraulic support oil emulsion |
Non-Patent Citations (2)
| Title |
|---|
| 刘金林: "《工业润滑剂》", 31 March 1989, 武汉出版社 * |
| 陈仪本等: "《工业杀菌剂》", 31 May 2001, 化学工业出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109456824A (en) * | 2018-11-27 | 2019-03-12 | 辽宁泰克诺美科技有限公司 | A kind of mine hydraulic support oil emulsion |
| CN109777582A (en) * | 2019-03-20 | 2019-05-21 | 富地润滑科技股份有限公司 | A kind of mine hydraulic support fluid and preparation method thereof of green environment protective biological degradation |
| CN111518608A (en) * | 2020-05-27 | 2020-08-11 | 中国石油化工股份有限公司 | Emulsified oil composition for low-temperature-resistant hydraulic support, preparation method and application |
| CN112029564A (en) * | 2020-09-09 | 2020-12-04 | 南京科润工业介质股份有限公司 | Neutral water-based antirust agent |
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Application publication date: 20180921 |