CN108546506A - A kind of anti-dazzle optical coating and preparation method thereof - Google Patents
A kind of anti-dazzle optical coating and preparation method thereof Download PDFInfo
- Publication number
- CN108546506A CN108546506A CN201810440154.0A CN201810440154A CN108546506A CN 108546506 A CN108546506 A CN 108546506A CN 201810440154 A CN201810440154 A CN 201810440154A CN 108546506 A CN108546506 A CN 108546506A
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- Prior art keywords
- parts
- optical coating
- dazzle optical
- cooled
- solvent
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D177/00—Coating compositions based on polyamides obtained by reactions forming a carboxylic amide link in the main chain; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/327—Aluminium phosphate
Abstract
The present invention relates to functional paint technical fields, and in particular to a kind of anti-dazzle optical coating and preparation method thereof.Anti-dazzle optical coating is made of 20 45 parts of butylene terephthalate, 5 10 parts of PA hot melt adhesive, 15 parts of calcium carbonate, 35 parts of aluminium triphosphate, 10 20 parts of solvent, 37 parts of curing agent, 34 parts of cyanidenon etc..Butylene terephthalate, PA hot melt adhesive, calcium carbonate, aluminium triphosphate, solvent, curing agent, cyanidenon and pyraflufen-ethyl are added into consersion unit first, 180 200 DEG C are warming up to react 15 hours, it is cooled to room temperature step by step, control rotating speed is 800 1200rpm/min, is stirred 5 10 hours；Filtering, inflated with nitrogen packaging.The present invention can eliminate dazzle pollution by rationally designing the component and proportioning of anti-dazzle optical coating to keep the anti-glare effect of anti-dazzle optical coating preferable, meanwhile, coating is phenomena such as painted surfaces appearance is not in striped.
Description
Technical field
The present invention relates to functional paint technical fields, and in particular to a kind of anti-dazzle optical coating and preparation method thereof.
Background technology
Coating is to be coated in the body surface protected or decorated, and can form the continuous thin of firm attachment with coated article
Film adds or does not add pigment, filler typically based on resin or oil or lotion, adds corresponding additive, uses organic solvent
Or the thick liquid that water is formulated.
In the prior art, the coating with anti-dazzle function is not deposited generally.
Invention content
In order to solve the technical problems existing in the prior art, the present invention proposes a kind of anti-dazzle optical coating and its preparation side
Method has more excellent anti-glare function.
The technical scheme is that：A kind of anti-dazzle optical coating, is made of the raw material of following parts by weight：
It is 20-45 parts of butylene terephthalate, 5-10 parts of PA hot melt adhesive, 1-5 parts of calcium carbonate, 3-5 parts of aluminium triphosphate, molten
1-2 parts of 10-20 parts of agent, 3-7 parts of curing agent, 3-4 parts of cyanidenon and pyraflufen-ethyl.
As the preferred embodiment of the present invention, it is made of the raw material of following parts by weight：
40 parts of butylene terephthalate, 3 parts of calcium carbonate, 4 parts of aluminium triphosphate, 15 parts of solvent, is consolidated 7 parts of PA hot melt adhesive
1.8 parts of 4 parts of agent, 3.5 parts of cyanidenon and pyraflufen-ethyl.
A method of anti-dazzle optical coating being prepared, steps are as follows：
1., first by butylene terephthalate, PA hot melt adhesive, calcium carbonate, aluminium triphosphate, solvent, curing agent, sweet-scented osmanthus
Careless element and pyraflufen-ethyl are added into consersion unit, are warming up to 180-200 DEG C and react 1-5 hours, be cooled to room temperature step by step, control turns
Speed is 800-1200rpm/min, is stirred 5-10 hours；
2., filtering, inflated with nitrogen packaging.
As the preferred embodiment of preparation method, the processing step being cooled to room temperature step by step is：First, in accordance with dropping per hour
Low 40 DEG C of rate of temperature fall allows to cool to 120 DEG C, then allows to cool to 50 again with the rate of temperature fall for reducing by 20 DEG C per hour
DEG C, finally it is cooled to room temperature with the rate of temperature fall for reducing by 10 DEG C per hour.
Beneficial effects of the present invention are shown：
By rationally designing the component and proportioning of anti-dazzle optical coating, to keep the anti-glare effect of anti-dazzle optical coating preferable,
Dazzle pollution can be eliminated, meanwhile, coating is phenomena such as painted surfaces appearance is not in striped.
Specific implementation mode
Embodiment 1
A kind of anti-dazzle optical coating, is made of the raw material of following parts by weight：
20 parts of butylene terephthalate, 1 part of calcium carbonate, 3 parts of aluminium triphosphate, 20 parts of solvent, is consolidated 10 parts of PA hot melt adhesive
1 part of 3 parts of agent, 4 parts of cyanidenon and pyraflufen-ethyl.
A method of anti-dazzle optical coating being prepared, steps are as follows：
1., first by butylene terephthalate, PA hot melt adhesive, calcium carbonate, aluminium triphosphate, solvent, curing agent, sweet-scented osmanthus
Careless element and pyraflufen-ethyl are added into consersion unit, are warming up to 200 DEG C and react 1 hour, are cooled to room temperature step by step, and control rotating speed is
1200rpm/min is stirred 5 hours；
The processing step being cooled to room temperature step by step is：It is allowed to cool to first, in accordance with the rate of temperature fall for reducing by 40 DEG C per hour
120 DEG C, 50 DEG C then are allowed to cool to reduce by 20 DEG C of rate of temperature fall per hour again, finally to reduce by 10 DEG C of drop per hour
Warm rate is cooled to room temperature；
2., filtering, inflated with nitrogen packaging.
Embodiment 2
A kind of anti-dazzle optical coating, is made of the raw material of following parts by weight：
45 parts of butylene terephthalate, 5 parts of calcium carbonate, 5 parts of aluminium triphosphate, 10 parts of solvent, is consolidated 5 parts of PA hot melt adhesive
2 parts of 7 parts of agent, 3 parts of cyanidenon and pyraflufen-ethyl.
A method of anti-dazzle optical coating being prepared, steps are as follows：
1., first by butylene terephthalate, PA hot melt adhesive, calcium carbonate, aluminium triphosphate, solvent, curing agent, sweet-scented osmanthus
Careless element and pyraflufen-ethyl are added into consersion unit, are warming up to 180 DEG C and react 5 hours, are cooled to room temperature step by step, and control rotating speed is
800rpm/min is stirred 10 hours；
The processing step being cooled to room temperature step by step is：It is allowed to cool to first, in accordance with the rate of temperature fall for reducing by 40 DEG C per hour
120 DEG C, 50 DEG C then are allowed to cool to reduce by 20 DEG C of rate of temperature fall per hour again, finally to reduce by 10 DEG C of drop per hour
Warm rate is cooled to room temperature；
2., filtering, inflated with nitrogen packaging.
Embodiment 3
A kind of anti-dazzle optical coating, is made of the raw material of following parts by weight：
40 parts of butylene terephthalate, 3 parts of calcium carbonate, 4 parts of aluminium triphosphate, 15 parts of solvent, is consolidated 7 parts of PA hot melt adhesive
1.8 parts of 4 parts of agent, 3.5 parts of cyanidenon and pyraflufen-ethyl.
A method of anti-dazzle optical coating being prepared, steps are as follows：
1., first by butylene terephthalate, PA hot melt adhesive, calcium carbonate, aluminium triphosphate, solvent, curing agent, sweet-scented osmanthus
Careless element and pyraflufen-ethyl are added into consersion unit, are warming up to 190 DEG C and react 3 hours, are cooled to room temperature step by step, and control rotating speed is
1000rpm/min is stirred 8 hours；
The processing step being cooled to room temperature step by step is：It is allowed to cool to first, in accordance with the rate of temperature fall for reducing by 40 DEG C per hour
120 DEG C, 50 DEG C then are allowed to cool to reduce by 20 DEG C of rate of temperature fall per hour again, finally to reduce by 10 DEG C of drop per hour
Warm rate is cooled to room temperature；
2., filtering, inflated with nitrogen packaging.
The above content is just an example and description of the concept of the present invention, affiliated those skilled in the art
It makes various modifications or additions to the described embodiments or substitutes by a similar method, without departing from invention
Design or beyond the scope defined by this claim, be within the scope of protection of the invention.
Claims (4)
1. a kind of anti-dazzle optical coating, which is characterized in that be made of the raw material of following parts by weight：
20-45 parts of butylene terephthalate, 5-10 parts of PA hot melt adhesive, 1-5 parts of calcium carbonate, 3-5 parts of aluminium triphosphate, solvent
1-2 parts of 10-20 parts, 3-7 parts of curing agent, 3-4 parts of cyanidenon and pyraflufen-ethyl.
2. anti-dazzle optical coating as described in claim 1, which is characterized in that be made of the raw material of following parts by weight：
40 parts of butylene terephthalate, 7 parts of PA hot melt adhesive, 3 parts of calcium carbonate, 4 parts of aluminium triphosphate, 15 parts of solvent, curing agent 4
1.8 parts of part, 3.5 parts of cyanidenon and pyraflufen-ethyl.
3. a kind of method preparing anti-dazzle optical coating as claimed in claim 1 or 2, which is characterized in that steps are as follows：
1., first by butylene terephthalate, PA hot melt adhesive, calcium carbonate, aluminium triphosphate, solvent, curing agent, cyanidenon
It is added into consersion unit with pyraflufen-ethyl, is warming up to 180-200 DEG C and reacts 1-5 hours, be cooled to room temperature step by step, control rotating speed is
800-1200rpm/min is stirred 5-10 hours；
2., filtering, inflated with nitrogen packaging.
4. preparation method as claimed in claim 3, which is characterized in that the processing step being cooled to room temperature step by step is：It presses first
120 DEG C are allowed to cool to according to the rate of temperature fall for reducing by 40 DEG C per hour, is then made again with the rate of temperature fall for reducing by 20 DEG C per hour
It is cooled to 50 DEG C, is finally cooled to room temperature with the rate of temperature fall for reducing by 10 DEG C per hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810440154.0A CN108546506A (en) | 2018-05-10 | 2018-05-10 | A kind of anti-dazzle optical coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810440154.0A CN108546506A (en) | 2018-05-10 | 2018-05-10 | A kind of anti-dazzle optical coating and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108546506A true CN108546506A (en) | 2018-09-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810440154.0A Pending CN108546506A (en) | 2018-05-10 | 2018-05-10 | A kind of anti-dazzle optical coating and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN108546506A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112876953A (en) * | 2021-01-18 | 2021-06-01 | 唐山润峰复合材料有限公司 | Anti-dazzle daylighting panel |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103819954A (en) * | 2013-11-12 | 2014-05-28 | 北京科技大学 | Preparation method of poly-luteolin antibacterial coatings and antibacterial effect testing method |
| CN105017548A (en) * | 2015-07-10 | 2015-11-04 | 浙江欧仁新材料有限公司 | Digital printing advertisement base material and preparation method thereof |
| CN105860738A (en) * | 2016-06-13 | 2016-08-17 | 张悦 | Self-luminous road sign marking coating and application thereof |
| CN106675224A (en) * | 2016-12-28 | 2017-05-17 | 山西长达交通材料科技股份有限公司 | Anti-cracking type hot-melting paint of road mark |
| CN106947361A (en) * | 2017-04-18 | 2017-07-14 | 德阳森华新材料科技有限公司 | Low-temperature fast-curing epoxy coating |
-
2018
- 2018-05-10 CN CN201810440154.0A patent/CN108546506A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103819954A (en) * | 2013-11-12 | 2014-05-28 | 北京科技大学 | Preparation method of poly-luteolin antibacterial coatings and antibacterial effect testing method |
| CN105017548A (en) * | 2015-07-10 | 2015-11-04 | 浙江欧仁新材料有限公司 | Digital printing advertisement base material and preparation method thereof |
| CN105860738A (en) * | 2016-06-13 | 2016-08-17 | 张悦 | Self-luminous road sign marking coating and application thereof |
| CN106675224A (en) * | 2016-12-28 | 2017-05-17 | 山西长达交通材料科技股份有限公司 | Anti-cracking type hot-melting paint of road mark |
| CN106947361A (en) * | 2017-04-18 | 2017-07-14 | 德阳森华新材料科技有限公司 | Low-temperature fast-curing epoxy coating |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112876953A (en) * | 2021-01-18 | 2021-06-01 | 唐山润峰复合材料有限公司 | Anti-dazzle daylighting panel |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180918 |
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| RJ01 | Rejection of invention patent application after publication |