CN108485286A - A kind of preparation method of antibacterial damp-proof floor wax - Google Patents
A kind of preparation method of antibacterial damp-proof floor wax Download PDFInfo
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- CN108485286A CN108485286A CN201810290692.6A CN201810290692A CN108485286A CN 108485286 A CN108485286 A CN 108485286A CN 201810290692 A CN201810290692 A CN 201810290692A CN 108485286 A CN108485286 A CN 108485286A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
- C08L91/06—Waxes
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2206—Oxides; Hydroxides of metals of calcium, strontium or barium
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention discloses a kind of preparation methods of antibacterial damp-proof floor wax, belong to floor wax preparing technical field.Beeswax and fruit wax are mixed first, and stirring melting at high temperature, it is blended with sierozem power after melting, so that system is not easy to dewax and crack, to improve the moisture resistance of floor wax, in addition the present invention uses beeswax, fruit wax fusion cream jasmin france is made, shrimp shell is put into the fermentation tank with yeast powder by the present invention ferments, and produce self-control chitosan, it wherein makes by oneself and contains a large amount of hydroxyl and amino in chitosan molecule, the present invention is using nano-titanium dioxide through overactivation, by itself and silane coupling agent, fermentation is blended in vegetable oil and bed-silt, can directly attack bacteria cell, cause the organic matter degradation in bacterial cell, bacterium is killed with this, and it is allowed to decompose, the moisture resistance and antibiotic property for being conducive to floor wax are improved, it is with a wide range of applications.
Description
Technical field
The invention discloses a kind of preparation methods of antibacterial damp-proof floor wax, belong to floor wax preparing technical field.
Background technology
The advanced solid wax of floor wax white oiliness, band fragrance, high temperature are in oiliness semisolid, and low temperature is in hard solid, can be quickly
The pore for penetrating into material, is processed by shot blasting with high-speed glazing machine or floor-cleaning machine, and ground is made to have very strong glossiness, higher
Wearability and feud effect, so that rough earth is formed hard protective film, it is especially anti-skidding, anti-scratch, wear-resisting, be effectively prevented water
Part, greasy dirt and other materials corrode.
In recent years, as the improvement of people's living standards, people are also higher and higher to the requirement for fitting up product, meanwhile, people
To environmental protection and health have higher more urgent demand.
Floor decorative is the essential part of house fitting-up, room can be made to seem graceful using wood floor decoration household.
With people's living standard raising and the continuous improvement of shelter environment, select the family of timber floor finishing increasing.Woodenly
The advantages of plate is because of beautiful natural, pollution-free, easy processing, good heat preservation performance is liked by consumer, but wood floors but exist firmly
Spend that low, resistance to corrosion is poor, easy the defects of damaging by worms.If not paying attention to the maintenance of timber floor, it is easy to so that it is worn, or even hair
Mould or dumb light is eclipsed.Floor wax is one of present house decoration regular supplies, can remove floor stain, makes material by waxing
Material itself and air exclusion reduce and are damaged caused by the harmful substance in oxidation or ingress of air is material, reach extension material
Expect service life and beautiful bright and clean purpose, it is often more important that its special durable of specular surface formed can prevent from washing
The injuries such as agent, cut, heel friction.
Currently, common floor wax is mostly solid or liquid wax on the market, general main component is oil extract and has
Solvent need to add essence and increase its fragrance to cover the taste of wax work itself, and organic solvent is evaporate into air, to people
Body health is unfavorable, and there are also watersoluble floor polish this lifes, though such floor wax does not contain organic solvent, but it is to floor
Protection, cleaning, blast the floor wax of effect and traditional organic solvent there are some gaps, and durability is not strong, need
Floor-cleaning nursing is often carried out repeatedly.
Therefore, inventing a kind of antibacterial damp-proof floor wax standby technical field waxed to floor has positive effect.
Invention content
The technical problems to be solved by the invention：For current common floor wax there are moisture resistance difference and antibiotic property are poor, separately
Outer common floor wax is mostly solid or liquid wax, and general main component is oil extract and organic solvent, wherein organic solvent
It can volatilize, air quality is caused to decline, the defect being also harmful to human health provides a kind of system of antibacterial damp-proof floor wax
Preparation Method.
In order to solve the above technical problems, the present invention is using technical solution as described below：
A kind of preparation method of antibacterial damp-proof floor wax, it is characterised in that specifically preparation process is：
（1）Beeswax, fruit wax and deionized water are mixed to be placed in beaker and stir melting, obtains melting mixing wax, then melting is mixed
It closes wax and sierozem power is mixed, obtain modified melting mixing wax；
（2）It weighs 80~100g shrimp shells to grind, obtains shrimp shell powder, then shrimp shell powder quality is added into shrimp shell powder
0.6% yeast powder, is fitted into fermentation tank, is sealed by fermentation, and after fermentation, takes out tunning, as makes chitosan by oneself, will
It makes chitosan by oneself and acetum is mixed, obtain self-control chitosan-acetic acid solution；
（3）It weighs 45~51g nano-titanium dioxides and pours into high temperature carbonization furnace and activate, obtain activation nano-titanium dioxide, then will
It activates nano-titanium dioxide and silane coupling agent KH-560 is mixed, obtain mixture, continue that mixing is added into mixture
The bed-silt of the beet oil and mixture quality 0.8% of amount of substance 5%, is fitted into fermentation tank, is sealed by fermentation, fermentation ends
Afterwards, tunning is taken out, grinding discharging obtains modified nano-titanium dioxide powder；
（4）It counts in parts by weight, it is molten to weigh 27~32 parts of modified melting mixing waxes, 10~12 parts of self-control chitosan acetic acid respectively
Liquid, 6~8 parts of modified nano-titanium dioxide powder, 2~4 parts of lauryl sodium sulfate, 3~5 parts of hydroxyethyl celluloses, 2~4 parts
Ethylene glycol and 1~3 part of cream jasmin france, first will modified melting mixing wax, self-control chitosan-acetic acid solution, modified nano-titanium dioxide
Powder and lauryl sodium sulfate mixing are placed in reaction kettle and stir, and cool down after stirring, then add hydroxyethyl cellulose, ethylene glycol
And cream jasmin france, continue to keep rotating speed that reaction is mixed, cooled to room temperature discharges to get antibacterial damp-proof floor wax.
Step（1）The mass ratio of the beeswax, fruit wax and deionized water is 5：3：2, stirring melting temperature is 85~90
DEG C, the stirring melting time is 10~12min, and the mass ratio of melting mixing wax and sierozem power is 4：1, be mixed the time be 4~
6min。
Step（2）The time that grinds is 7~9min, and fermentation temperature is 32~35 DEG C, and fermentation time is 9~11
It, the mass ratio for making the acetum that chitosan and mass fraction are 12% by oneself is 1：3, mixing time is 6~8min.
Step（3）The activation temperature is 185~190 DEG C, and soak time is 12~16min, activates nanometer titanium dioxide
Titanium and the mass ratio of silane coupling agent KH-560 are 5：1, the mixing time is 4~6min, and fermentation temperature is 35~45 DEG C, hair
The ferment time is 11~13 days.
Step（4）The whipping temp be 85~90 DEG C, speed of agitator be 240~300r/min, mixing time be 1~
2h, cooling temperature is 65~70 DEG C, continues to be stirred to react the time as 24~32min.
Compared with other methods, advantageous effects are the present invention：
（1）The present invention makes chitosan-acetic acid solution and modified nano-titanium dioxide powder by oneself to be modified melting mixing wax as base material
As modifying agent, and it is aided with hydroxyethyl cellulose, ethylene glycol etc. and antibacterial damp-proof floor wax is prepared, first by beeswax and fruit
Wax mixes, and stirring melting at high temperature, is blended with sierozem power after melting, and wherein sierozem power main component is calcium hydroxide, by
After sierozem power is dispersed in substrate surface, calcium hydroxide can absorb the carbon dioxide in air, and carburizing reagent occurs,
The calcium carbonate crystal net closely to interweave is formed, the water resistance and adhesive strength of system are increased so that system is not easy to dewax and crack,
To improve the moisture resistance of floor wax, in addition the present invention is made using beeswax, fruit wax fusion cream jasmin france, and product distributes day
Right jasmine is fragrant, has no irritating odor, and reduces the defect that traditional chemical floor wax is hazardous to the human body, and product is semi liquid state
Lotion, solves the defect that traditional floor wax can only make solid or liquid, and use is easy to operate；
（2）Shrimp shell is put into the fermentation tank with yeast powder by the present invention ferments, and produces self-control chitosan, wherein making by oneself
Contain a large amount of hydroxyl and amino in chitosan molecule, since the positive charge of amino on self-control chitosan is easy and bacterium surface institute
The negative electrical charge of band is combined, to inhibit the mobility of bacterium so that the growth inhibition of bacterium, while making chitosan energy by oneself
Enough penetration cell walls inhibit the formation of mRNA in its cell into the intracellular of bacterium, can also inhibit the growth of bacterium, favorably
It is improved in the antibiotic property of floor wax, then self-control chitosan is immersed in acetum, obtain having after being completely dissolved viscous
The self-control chitosan-acetic acid solution of property, promotes the adhesive strength of base material and filler；
（3）Using nano-titanium dioxide, through overactivation, hair is blended with silane coupling agent, vegetable oil and bed-silt in it by the present invention
Ferment forms tough and tensile porous nano titanium dioxide, and plant oil decomposition is generated lipophile ester group using microorganism in bed-silt,
And make lipophile ester group be grafted to nano-titanium dioxide surface under the self-crosslinking of microorganism, make it have waterproof energy
Power, since nano-titanium dioxide generates the very strong superoxide anion radical of chemical activity and hydrogen-oxygen certainly when being illuminated by the light
By base, can direct attack bacteria cell, cause the organic matter degradation in bacterial cell, bacterium killed with this, and be allowed to point
Solution, the moisture resistance and antibiotic property for being conducive to floor wax are improved, are with a wide range of applications.
Specific implementation mode
It is 5 in mass ratio：3：2 are placed in the mixing of beeswax, fruit wax and deionized water in beaker, in the case where temperature is 85~90 DEG C
Stirring 10~12min of melting, obtains melting mixing wax, then by melting mixing wax and sierozem power is 4 in mass ratio：1 is mixed 4
~6min obtains modified melting mixing wax；It weighs 80~100g shrimp shells and grinds 7~9min, obtain shrimp shell powder, then to shrimp
The yeast powder of shrimp shell powder quality 0.6% is added in shell powder, is fitted into fermentation tank, it is close under conditions of temperature is 32~35 DEG C
Seal ferment 9~11 days takes out tunning, as makes chitosan by oneself, be in mass ratio 1 after fermentation：3 gather self-control shell
6~8min is mixed in the acetum that sugar and mass fraction are 12%, obtains self-control chitosan-acetic acid solution；Weigh 45~
51g nano-titanium dioxides pour into high temperature carbonization furnace, activate 12~16min at being 185~190 DEG C in temperature, obtain activation and receive
Rice titanium dioxide, then be 5 in mass ratio：1 will activation nano-titanium dioxide and silane coupling agent KH-560 be mixed 4~
6min obtains mixture, continues the river that the beet oil and mixture quality 0.8% of mixture quality 5% are added into mixture
Bottom mud, is fitted into fermentation tank, is sealed by fermentation under conditions of temperature is 35~45 DEG C 11~13 days, after fermentation, takes out
Tunning, grinding discharging, obtains modified nano-titanium dioxide powder；It counts in parts by weight, weighs 27~32 parts of modifications respectively
Melting mixing wax, 10~12 parts of self-control chitosan-acetic acid solutions, 6~8 parts of modified nano-titanium dioxide powder, 2~4 parts of dodecanes
Base sodium sulphate, 3~5 parts of hydroxyethyl celluloses, 2~4 parts of ethylene glycol and 1~3 part of cream jasmin france, first will modified melting mixing wax,
Self-control chitosan-acetic acid solution, modified nano-titanium dioxide powder and lauryl sodium sulfate mixing are placed in reaction kettle, in temperature
1~2h is stirred under conditions of degree is 85~90 DEG C, rotating speed is 240~300r/min, 65~70 DEG C is cooled to after stirring, then add
Hydroxyethyl cellulose, ethylene glycol and cream jasmin france continue to keep rotating speed that 24~32min of reaction is mixed, naturally cool to room
Temperature discharges to get antibacterial damp-proof floor wax.
It is 5 in mass ratio：3：2 are placed in the mixing of beeswax, fruit wax and deionized water in beaker, are stirred at being 85 DEG C in temperature
10min is melted, obtains melting mixing wax, then by melting mixing wax and sierozem power is 4 in mass ratio：1 is mixed 4min, obtains
Modified melting mixing wax；It weighs 80g shrimp shells and grinds 7min, obtain shrimp shell powder, then shrimp shell meal is added into shrimp shell powder
The yeast powder of last quality 0.6%, is fitted into fermentation tank, sealing and fermenting 9 days under conditions of temperature is 32 DEG C, after fermentation,
Tunning is taken out, chitosan is as made by oneself, is in mass ratio 1：3 will to make the acetic acid that chitosan and mass fraction are 12% by oneself molten
6min is mixed in liquid, obtains self-control chitosan-acetic acid solution；45g nano-titanium dioxides are weighed to pour into high temperature carbonization furnace,
Temperature is to activate 12min at 185 DEG C, obtains activation nano-titanium dioxide, then is 5 in mass ratio：1 will activate nano-titanium dioxide
4min is mixed with silane coupling agent KH-560, obtains mixture, continues the sweet tea that mixture quality 5% is added into mixture
The bed-silt of rape oil and mixture quality 0.8%, is fitted into fermentation tank, and 11 are sealed by fermentation under conditions of temperature is 35 DEG C
It takes out tunning after fermentation, and grinding discharging obtains modified nano-titanium dioxide powder；It counts in parts by weight, point
Also known as take 27 parts of modified melting mixing waxes, 10 parts make by oneself chitosan-acetic acid solutions, 6 parts of modified nano-titanium dioxide powder, 2 part ten
Sodium dialkyl sulfate, 3 parts of hydroxyethyl celluloses, 2 parts of ethylene glycol and 1 part of cream jasmin france, first will modified melting mixing wax, self-control shell
Glycan acetum, modified nano-titanium dioxide powder and lauryl sodium sulfate mixing are placed in reaction kettle, are 85 in temperature
DEG C, rotating speed be 240r/min under conditions of stir 1h, 65 DEG C are cooled to after stirring, then add hydroxyethyl cellulose, ethylene glycol and
Cream jasmin france continues to keep rotating speed that reaction 24min is mixed, and cooled to room temperature discharges to get antibacterial damp-proof floor
Wax.
It is 5 in mass ratio：3：2 are placed in the mixing of beeswax, fruit wax and deionized water in beaker, are stirred at being 87 DEG C in temperature
11min is melted, obtains melting mixing wax, then by melting mixing wax and sierozem power is 4 in mass ratio：1 is mixed 5min, obtains
Modified melting mixing wax；It weighs 90g shrimp shells and grinds 8min, obtain shrimp shell powder, then shrimp shell meal is added into shrimp shell powder
The yeast powder of last quality 0.6%, is fitted into fermentation tank, sealing and fermenting 10 days under conditions of temperature is 34 DEG C, after fermentation,
Tunning is taken out, chitosan is as made by oneself, is in mass ratio 1：3 will to make the acetic acid that chitosan and mass fraction are 12% by oneself molten
7min is mixed in liquid, obtains self-control chitosan-acetic acid solution；48g nano-titanium dioxides are weighed to pour into high temperature carbonization furnace,
Temperature is to activate 14min at 187 DEG C, obtains activation nano-titanium dioxide, then is 5 in mass ratio：1 will activate nano-titanium dioxide
5min is mixed with silane coupling agent KH-560, obtains mixture, continues the sweet tea that mixture quality 5% is added into mixture
The bed-silt of rape oil and mixture quality 0.8%, is fitted into fermentation tank, and 12 are sealed by fermentation under conditions of temperature is 40 DEG C
It takes out tunning after fermentation, and grinding discharging obtains modified nano-titanium dioxide powder；It counts in parts by weight, point
Also known as take 30 parts of modified melting mixing waxes, 11 parts make by oneself chitosan-acetic acid solutions, 7 parts of modified nano-titanium dioxide powder, 3 part ten
Sodium dialkyl sulfate, 4 parts of hydroxyethyl celluloses, 3 parts of ethylene glycol and 2 parts of cream jasmin frances, first will modified melting mixing wax, self-control shell
Glycan acetum, modified nano-titanium dioxide powder and lauryl sodium sulfate mixing are placed in reaction kettle, are 87 in temperature
DEG C, rotating speed be 260/min under conditions of stir 1.5h, 67 DEG C are cooled to after stirring, then add hydroxyethyl cellulose, ethylene glycol and
Cream jasmin france continues to keep rotating speed that reaction 28min is mixed, and cooled to room temperature discharges to get antibacterial damp-proof floor
Wax.
It is 5 in mass ratio：3：2 are placed in the mixing of beeswax, fruit wax and deionized water in beaker, are stirred at being 90 DEG C in temperature
12min is melted, obtains melting mixing wax, then by melting mixing wax and sierozem power is 4 in mass ratio：1 is mixed 6min, obtains
Modified melting mixing wax；It weighs 100g shrimp shells and grinds 9min, obtain shrimp shell powder, then shrimp shell meal is added into shrimp shell powder
The yeast powder of last quality 0.6%, is fitted into fermentation tank, sealing and fermenting 11 days under conditions of temperature is 35 DEG C, after fermentation,
Tunning is taken out, chitosan is as made by oneself, is in mass ratio 1：3 will to make the acetic acid that chitosan and mass fraction are 12% by oneself molten
8min is mixed in liquid, obtains self-control chitosan-acetic acid solution；51g nano-titanium dioxides are weighed to pour into high temperature carbonization furnace,
Temperature is to activate 16min at 190 DEG C, obtains activation nano-titanium dioxide, then is 5 in mass ratio：1 will activate nano-titanium dioxide
6min is mixed with silane coupling agent KH-560, obtains mixture, continues the sweet tea that mixture quality 5% is added into mixture
The bed-silt of rape oil and mixture quality 0.8%, is fitted into fermentation tank, and 13 are sealed by fermentation under conditions of temperature is 45 DEG C
It takes out tunning after fermentation, and grinding discharging obtains modified nano-titanium dioxide powder；It counts in parts by weight, point
Also known as take 32 parts of modified melting mixing waxes, 12 parts make by oneself chitosan-acetic acid solutions, 8 parts of modified nano-titanium dioxide powder, 4 part ten
Sodium dialkyl sulfate, 5 parts of hydroxyethyl celluloses, 4 parts of ethylene glycol and 3 parts of cream jasmin frances, first will modified melting mixing wax, self-control shell
Glycan acetum, modified nano-titanium dioxide powder and lauryl sodium sulfate mixing are placed in reaction kettle, are 90 in temperature
DEG C, rotating speed be 300r/min under conditions of stir 2h, 70 DEG C are cooled to after stirring, then add hydroxyethyl cellulose, ethylene glycol and
Cream jasmin france continues to keep rotating speed that reaction 32min is mixed, and cooled to room temperature discharges to get antibacterial damp-proof floor
Wax.
With the antibacterial damp-proof floor wax of Shanghai company production as a comparison case to antibacterial damp-proof produced by the present invention
Antibacterial damp-proof floor wax in floor wax and comparative example carries out performance detection, and testing result is as shown in table 1：
Test method：
Escherichia coli be averaged bacterium number test by JC/T897-2002 regulation progress bacteriostasis property detection；
Staphylococcus aureus be averaged bacterium number test by JC/T897-2002 regulation progress bacteriostasis property detection；
The test of Candida albicans bacteriostasis rate carries out performance detection by the regulation of GB/T20944.2-2007；
Floor surface luminance test is detected using floor glossiness tester；
Water resistance testing method：By the floor wax in example 1~3 and comparative example on identical floor, after its drying, use
Water wipes it, observes surface situation of change；
Air quality standard GB is pressed in air pollution index API tests：3095 are detected.
1 floor wax performance measurement result of table
| Test event | Example 1 | Example 2 | Example 3 | Comparative example |
| Escherichia coli bacteriostasis rate（%） | 99.64 | 99.85 | 99.99 | 82.45 |
| Staphylococcus aureus bacteriostasis rate（%） | 99.75 | 99.88 | 99.99 | 81.32 |
| Candida albicans bacteriostasis rate（%） | 99.35 | 99.74 | 99.99 | 81.76 |
| Floor surface brightness | 51 | 51 | 52 | 40 |
| Water resistance | Crack-free | Crack-free | Crack-free | Slight rupture |
| API indexes | 19 | 16 | 15 | 29 |
Note：It is acceptable level, to Health Impact unobvious when API values are less than 32；When reaching 50, chronic respiratory can be made
Tract disease patient symptom is aggravated；When reaching 100, heart disease and respiratory disease patient are seriously threatened, also had to healthy person
Slight effect；When 50~75, the measure of pollution abatement should be given a warning and must taken.
Good according to the antibacterial damp-proof floor wax antibiotic property produced by the present invention of data among the above, moisture resistance is good, will not
Air quality is influenced, is had broad application prospects.
Claims (5)
1. a kind of preparation method of antibacterial damp-proof floor wax, it is characterised in that specifically preparation process is：
（1）Beeswax, fruit wax and deionized water are mixed to be placed in beaker and stir melting, obtains melting mixing wax, then melting is mixed
It closes wax and sierozem power is mixed, obtain modified melting mixing wax；
（2）It weighs 80~100g shrimp shells to grind, obtains shrimp shell powder, then shrimp shell powder quality is added into shrimp shell powder
0.6% yeast powder, is fitted into fermentation tank, is sealed by fermentation, and after fermentation, takes out tunning, as makes chitosan by oneself, will
It makes chitosan by oneself and acetum is mixed, obtain self-control chitosan-acetic acid solution；
（3）It weighs 45~51g nano-titanium dioxides and pours into high temperature carbonization furnace and activate, obtain activation nano-titanium dioxide, then will
It activates nano-titanium dioxide and silane coupling agent KH-560 is mixed, obtain mixture, continue that mixing is added into mixture
The bed-silt of the beet oil and mixture quality 0.8% of amount of substance 5%, is fitted into fermentation tank, is sealed by fermentation, fermentation ends
Afterwards, tunning is taken out, grinding discharging obtains modified nano-titanium dioxide powder；
（4）It counts in parts by weight, it is molten to weigh 27~32 parts of modified melting mixing waxes, 10~12 parts of self-control chitosan acetic acid respectively
Liquid, 6~8 parts of modified nano-titanium dioxide powder, 2~4 parts of lauryl sodium sulfate, 3~5 parts of hydroxyethyl celluloses, 2~4 parts
Ethylene glycol and 1~3 part of cream jasmin france, first will modified melting mixing wax, self-control chitosan-acetic acid solution, modified nano-titanium dioxide
Powder and lauryl sodium sulfate mixing are placed in reaction kettle and stir, and cool down after stirring, then add hydroxyethyl cellulose, ethylene glycol
And cream jasmin france, continue to keep rotating speed that reaction is mixed, cooled to room temperature discharges to get antibacterial damp-proof floor wax.
2. a kind of preparation method of antibacterial damp-proof floor wax according to claim 1, it is characterised in that：Step（1）Institute
The mass ratio of beeswax, fruit wax and the deionized water stated is 5：3：2, stirring melting temperature be 85~90 DEG C, stirring the melting time be
The mass ratio of 10~12min, melting mixing wax and sierozem power is 4：1, the mixing time is 4~6min.
3. a kind of preparation method of antibacterial damp-proof floor wax according to claim 1, it is characterised in that：Step（2）Institute
The time that grinds stated is 7~9min, and fermentation temperature is 32~35 DEG C, and fermentation time is 9~11 days, makes chitosan and matter by oneself
The mass ratio for measuring the acetum that score is 12% is 1：3, mixing time is 6~8min.
4. a kind of preparation method of antibacterial damp-proof floor wax according to claim 1, it is characterised in that：Step（3）Institute
The activation temperature stated is 185~190 DEG C, and soak time is 12~16min, activates nano-titanium dioxide and silane coupling agent KH-
560 mass ratio is 5：1, the mixing time is 4~6min, and fermentation temperature is 35~45 DEG C, and fermentation time is 11~13 days.
5. a kind of preparation method of antibacterial damp-proof floor wax according to claim 1, it is characterised in that：Step（4）Institute
The whipping temp stated be 85~90 DEG C, speed of agitator be 240~300r/min, mixing time be 1~2h, cooling temperature be 65~
70 DEG C, continue to be stirred to react the time as 24~32min.
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