CN108456611A - Bletilla striata wine and preparation method thereof - Google Patents
Bletilla striata wine and preparation method thereof Download PDFInfo
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- CN108456611A CN108456611A CN201810328548.7A CN201810328548A CN108456611A CN 108456611 A CN108456611 A CN 108456611A CN 201810328548 A CN201810328548 A CN 201810328548A CN 108456611 A CN108456611 A CN 108456611A
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
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Abstract
The present invention relates to a kind of preparation of wine of splendid achnatherum, especially a kind of bletilla striata wine and preparation method thereof.The bletilla striata wine calculates the wine and contains white wine 85-90%, bletilla striata extract 10-15% by weight.The step of preparation process of bletilla striata wine is as follows：It is prepared by the drying of the bletilla striata, the preparation of complex enzyme, enzymatic treatment reaction, water extract-alcohol precipitation extraction bletilla polysaccharide, bletilla striata wine.Technical solution of the present invention has the characteristics that：In the preparation process of bletilla striata extract, the bletilla striata is digested using complex enzyme first, is then extracted using existing water extraction and alcohol precipitation method, its recovery rate and purity are greatly improved compared with the prior art；Bletilla striata wine is often drunk on a small quantity, there is certain killing effect to the fungi in stomach, and has the effects that anticancer and anti-cancer；The white wine used in bletilla striata wine is prepared, white wine of the grape skin through distillation gained discarded in red wine production process can be used, accomplishes waste utilization, it is environmentally friendly to wait society and economic effect.
Description
Technical field
The present invention relates to a kind of preparation of wine of splendid achnatherum, especially a kind of bletilla striata wine and preparation method thereof.
Background technology
Bletilla polysaccharide is a kind of water-soluble heteroglycan extracted in bletilla, also known as Bletilla glucomannan, bletilla mannan, by
The glucose of 4 molecule mannoses and 1 molecule glucose composition matches mannosan, also incorporates a small amount of metal ion in molecule, together
When there are three kinds of β -1,4- mannoses, β -1,4- glucose and α -1,6- glucose residues.Its molecular weight distribution is wider, average
Molecular weight is 10-20kD.Bletilla polysaccharide is safe and efficient medical material, the pharmaceutic adjuvant of performance brilliance and before quite having development
The biomedical material of scape is had functional slow-release, local retention, auto-degradation, nonirritant is had no toxic side effect with splendid achnatherum
The features such as.
The Patent No. 200710233470.6 of on 06 20th, 2017 bulletins of China Intellectual Property Office, it is entitled " a kind of
The primary raw material of the patent of invention of the production method of bletilla striata vinegar ", the technique includes sorghum flour 50%, bletilla striata powder 50%.By raw material into
Row processing, steaming, mixed song, fermentation, acetic fermentation, concentration store.Product of the present invention is the bletilla striata vinegar of a nourishing the stomach stomach invigorating,
To fill up the blank of bletilla striata product, long-time service can stomach invigorating control stomach.But bletilla polysaccharide can hydrolyze in acid condition, the bletilla striata
The making of vinegar reduces the content to bletilla polysaccharide to a certain extent, to affect the utilization of bletilla polysaccharide nutritive value.Cause
The bletilla striata is fabricated to a bletilla striata wine by this can reduce the hydrolysis of bletilla polysaccharide, ensure effective content.The bletilla striata is had not yet to see
The production technology or product of wine.
Invention content
The object of the present invention is to provide a kind of containing bletilla striata extract, bletilla striata wine with health role and its preparation sides
Method.
The technical scheme is that：A kind of bletilla striata wine, it is characterised in that calculate the wine by weight and contain white wine 85-
90%, bletilla striata extract 10-15%.
The alcoholic strength of above-mentioned white wine is 20-65%VOL.
The method for preparing bletilla striata wine described in the claims, step of preparation process are as follows：
Step 1：The drying of the bletilla striata：After the fresh bletilla striata is cleaned, slice, the dry weight percent content to moisture are less than etc.
After 30% or so, it is spare to be crushed to 20 mesh or so；
Step 2：The preparation of complex enzyme：Weigh pectase and cellulase respectively, the weight ratio of pectase and cellulase is 1:
Then the above-mentioned pectase weighed and cellulase are added to the water by 10-26 under stirring, the weight of water is above-mentioned pectin
20 times of enzyme and cellulase total weight, the composite enzyme solution prepared is spare；
Step 3：Enzymatic treatment reacts：The above-mentioned bletilla striata powder for being crushed to 20 mesh or so is lowered into above-mentioned complex enzyme in stirring
In solution, after stirring evenly, 50 DEG C or so, after enzymatic treatment reacts 2-3 hours, after above-mentioned enzymatic treatment is reacted are maintained the temperature at
Material to boil inactivation in 2 minutes or so spare；
Step 4：Water extract-alcohol precipitation extracts bletilla polysaccharide：Material after above-mentioned inactivation is repeated into extraction 3 with boiling water bath refluxing extraction
It is secondary, it is filtered after merging extracting solution, after concentrating the filtrate to paste, the heavy of hundred a concentration of 95% ethyl alcohol of volume basis is added
It forms sediment, after suction filtration, 55 DEG C of vacuum drying are to get polysaccharide preparation；
Step 5：It is prepared by bletilla striata wine：The bletilla striata extract of step 4 extraction is added in the white wine that precision is 20-65%VOL, is stirred
It mixes 15-30 minutes, stands 1-24 hours, bletilla striata wine is obtained after filtering.
Above-mentioned precision is that skin slag by being generated in red wine production process is obtained through distillation by the white wine of 20-65%VOL
Alcohol.
Technical solution of the present invention has the characteristics that：1, in the preparation process of bletilla striata extract, complex enzyme is used first
The bletilla striata is digested, is then extracted using existing water extraction and alcohol precipitation method, with prior art than bletilla striata extract --- it is white
The recovery rate of splendid achnatherum polysaccharide can be improved 3-10 percentage points, and content and the purity of bletilla polysaccharide can be improved 3-8 percentage points；2, in
State's spirits culture is of long standing and well established, but excessive consumption of alcohol has damage, the technical program to the stomach of human body, liver to be had only using the bletilla striata
The effects that blood, protection gastric mucosa, antibacterial, antimycotic, anticancer and anti-cancer, organically blend forming bletilla striata wine with white wine, make one
During drinking bletilla striata wine, play the role of certain shield stomach, while often drinking on a small quantity, to the fungi in stomach have one
Fixed killing effect, and have the effects that anticancer and anti-cancer；3, the white wine used in bletilla striata wine is prepared, red wine production can be used
White wine of the discarded grape skin through distillation gained in the process accomplishes waste utilization, environmentally friendly to wait society and economic effect.
Specific implementation mode
Embodiment 1：
Step 1：The drying of the bletilla striata：The fresh bletilla striatas of 9kg are weighed, sorted, cleaning after being sliced, is dried to moisture content 30% or so,
It is 20 mesh to be crushed to granularity；
The moisture content refers to the percentage of the weight of water and bletilla striata total weight in the bletilla striata, and moisture content is thus in following embodiment
Meaning.
Step 2：The preparation of complex enzyme：Cellulase 2.4g and pectase 0.24g are weighed, by cellulase and pectase
It is added in 50kg water under stirring, composite enzyme solution is made；
Step 3：Enzymatic treatment reacts：Bletilla striata powder after crushing is lowered into stirring in above-mentioned composite enzyme solution, at 50 DEG C
Under the conditions of enzymatic treatment react 3 hours after, the material after enzymatic treatment is reacted boil 2 minutes inactivation it is spare；
Step 4：Water extract-alcohol precipitation extracts bletilla polysaccharide：By the material of step 3 boiling water bath refluxing extraction, extraction 3 times is repeated, is closed
And extracting solution, filtrate is placed in Rotary Evaporators after filtration and is concentrated under reduced pressure into paste, adds 3 times of amount volume percents by volume dense
It spends 95% ethanol precipitation, filter, dried to get 1.1kg bletilla polysaccharides under 55 DEG C of vacuum conditions.
Step 5：It is prepared by bletilla striata wine：Above-mentioned 100 grams of the bletilla striata extract-bletilla polysaccharide produced is weighed, is added 20 degree 900
Gram white wine in, stirring 30 minutes after, stand 24 hours, after filtering 20 degree of 1000 grams of bletilla striata wine.
Embodiment 2-5.
On the basis of above-described embodiment 1, the alcoholic strength of bletilla striata wine can be controlled according to demand in 20-65%VOL ranges
It is interior；The weight percent content of bletilla striata extract-bletilla polysaccharide controls in 10-15% range in bletilla striata wine, specific embodiment party
Formula such as table.
| Embodiment | The alcoholic strength of white wine, weight | The weight of bletilla striata extract |
| 2 | 32%VOL, 850 grams | 15 grams |
| 3 | 48%VOL, 860 grams | 14 grams |
| 4 | 52%VOL, 880 grams | 12 grams |
| 5 | 65%VOL, 850 grams | 15 grams |
In the above-described embodiments, white wine uses the white wine that prior art method is obtained.
Embodiment 6：
On the basis of the above embodiments, white wine using the discarded skin slag in red wine production process distilled obtained by wine
Essence.
Specific distillation technique is as follows：
The grape skin 20kg in red wine production process is taken, pours into distiller and is distilled, distillation temperature when single flash
Degree is 80 DEG C or so, and recycling obtains the alcohol 2.4kg of 25%VOL or so, then by 2.4kg alcohol row second distillations, vapo(u)rizing temperature
105 DEG C or so, recycling obtains the alcohol 0.84kg of 65%VOL or so；
As needed, the alcohol of 25%VOL that single flash is obtained or so can be used in the alcohol of configuration bletilla striata wine, can also be used
The alcohol of the 65%VOL that second distillation obtains or so.
Grape skin in the above-mentioned production process using red wine is distilled obtained alcoholic strength can be as needed
It is adjusted.
Embodiment 7-10.
In above-mentioned any embodiment, change mixing time in the moisture content and bletilla striata wine preparation process of the bletilla striata and
Time of repose, equally available bletilla striata wine.
| Embodiment | Bletilla striata moisture content | Mixing time | Time of repose |
| Embodiment 7 | 15% | 18 | 1 |
| Embodiment 8 | 20% | 20 | 12 |
| Embodiment 9 | 25% | 25 | 18 |
| Embodiment 10 | 30% | 30 | 24 |
In the above-described embodiments, the unit of mixing time is minute, and the unit of time of repose is hour.
Claims (4)
1. a kind of bletilla striata wine, it is characterised in that calculate the wine by weight and contain white wine 85-90%, bletilla striata extract 10-15%.
2. a kind of bletilla striata wine according to claim 1, it is characterised in that the alcoholic strength of above-mentioned white wine is 20-65%VOL.
3. the method for preparing bletilla striata wine described in the claims, step of preparation process are as follows：
Step 1：The drying of the bletilla striata：After the fresh bletilla striata is cleaned, slice, the dry weight percent content to moisture are less than etc.
After 30% or so, it is spare to be crushed to 20 mesh or so；
Step 2：The preparation of complex enzyme：Weigh pectase and cellulase respectively, the weight ratio of pectase and cellulase is 1:
Then the above-mentioned pectase weighed and cellulase are added to the water by 10-26 under stirring, the weight of water is above-mentioned pectin
20 times of enzyme and cellulase total weight, the composite enzyme solution prepared is spare；
Step 3：Enzymatic treatment reacts：The above-mentioned bletilla striata powder for being crushed to 20 mesh or so is lowered into above-mentioned complex enzyme in stirring
In solution, after stirring evenly, 50 DEG C or so, after enzymatic treatment reacts 2-3 hours, after above-mentioned enzymatic treatment is reacted are maintained the temperature at
Material to boil inactivation in 2 minutes or so spare；
Step 4：Water extract-alcohol precipitation extracts bletilla polysaccharide：Material after above-mentioned inactivation is repeated into extraction 3 with boiling water bath refluxing extraction
It is secondary, it is filtered after merging extracting solution, after concentrating the filtrate to paste, the heavy of hundred a concentration of 95% ethyl alcohol of volume basis is added
It forms sediment, after suction filtration, 55 DEG C of vacuum drying are to get polysaccharide preparation；
Step 5：It is prepared by bletilla striata wine：The bletilla striata extract of step 4 extraction is added in the white wine that precision is 20-65%VOL, is stirred
It mixes 15-30 minutes, stands 1-24 hours, bletilla striata wine is obtained after filtering.
4. the method according to claim 3 for preparing bletilla striata wine, it is characterised in that above-mentioned precision is the white wine of 20-65%VOL
It is skin slag by being generated in red wine production process through distilling obtained alcohol.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810328548.7A CN108456611A (en) | 2018-04-13 | 2018-04-13 | Bletilla striata wine and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810328548.7A CN108456611A (en) | 2018-04-13 | 2018-04-13 | Bletilla striata wine and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112876573A (en) * | 2020-12-14 | 2021-06-01 | 皖西学院 | Be used for tuber of hyacinth bletilla polysaccharide scale extraction equipment |
Citations (7)
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|---|---|---|---|---|
| CN1042079A (en) * | 1988-10-20 | 1990-05-16 | 南京市鱼品加工厂 | A kind of method and special equipment thereof of producing Pseudobulbus Bletillae (Rhizoma Bletillae) glue |
| CN1150912A (en) * | 1996-09-18 | 1997-06-04 | 罗启伦 | Health-care medicinal liquor for treatment of stomach disease and its technology |
| CN106834039A (en) * | 2017-03-30 | 2017-06-13 | 镇远县道益堂生物科技有限公司 | A kind of preparation method of bletilla striata health liquor |
| CN106832038A (en) * | 2017-03-30 | 2017-06-13 | 镇远县道益堂生物科技有限公司 | A kind of extracting method of bletilla polysaccharide |
| CN106867865A (en) * | 2017-04-11 | 2017-06-20 | 贵州盛茂白芨开发有限公司 | A kind of preparation method of bletilla vinegar |
| CN107522794A (en) * | 2017-09-29 | 2017-12-29 | 贵州同源中药发展有限公司 | A kind of bletilla striata polyoses glue extracting method |
| CN107737046A (en) * | 2017-11-28 | 2018-02-27 | 张夏洋 | A kind of preparation method of beauty extract |
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2018
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Patent Citations (7)
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|---|---|---|---|---|
| CN1042079A (en) * | 1988-10-20 | 1990-05-16 | 南京市鱼品加工厂 | A kind of method and special equipment thereof of producing Pseudobulbus Bletillae (Rhizoma Bletillae) glue |
| CN1150912A (en) * | 1996-09-18 | 1997-06-04 | 罗启伦 | Health-care medicinal liquor for treatment of stomach disease and its technology |
| CN106834039A (en) * | 2017-03-30 | 2017-06-13 | 镇远县道益堂生物科技有限公司 | A kind of preparation method of bletilla striata health liquor |
| CN106832038A (en) * | 2017-03-30 | 2017-06-13 | 镇远县道益堂生物科技有限公司 | A kind of extracting method of bletilla polysaccharide |
| CN106867865A (en) * | 2017-04-11 | 2017-06-20 | 贵州盛茂白芨开发有限公司 | A kind of preparation method of bletilla vinegar |
| CN107522794A (en) * | 2017-09-29 | 2017-12-29 | 贵州同源中药发展有限公司 | A kind of bletilla striata polyoses glue extracting method |
| CN107737046A (en) * | 2017-11-28 | 2018-02-27 | 张夏洋 | A kind of preparation method of beauty extract |
Non-Patent Citations (1)
| Title |
|---|
| 广西壮族自治区食品药品监督管理局培训咨询中心编: "《食品生产企业检验技术大全》", 31 March 2015, 南宁：广西科学技术出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112876573A (en) * | 2020-12-14 | 2021-06-01 | 皖西学院 | Be used for tuber of hyacinth bletilla polysaccharide scale extraction equipment |
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