CN108450487A - A kind of rice with regulatory function compound botanical insecticide and preparation method thereof - Google Patents
A kind of rice with regulatory function compound botanical insecticide and preparation method thereof Download PDFInfo
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- CN108450487A CN108450487A CN201810466472.4A CN201810466472A CN108450487A CN 108450487 A CN108450487 A CN 108450487A CN 201810466472 A CN201810466472 A CN 201810466472A CN 108450487 A CN108450487 A CN 108450487A
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- missible oil
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- essential oil
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds containing nitrogen-to-oxygen bonds
- A01N33/18—Nitro compounds
- A01N33/20—Nitro compounds containing oxygen or sulfur attached to the carbon skeleton containing the nitro group
- A01N33/22—Nitro compounds containing oxygen or sulfur attached to the carbon skeleton containing the nitro group having at least one oxygen or sulfur atom and at least one nitro group directly attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/06—Coniferophyta [gymnosperms], e.g. cypress
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Pest Control & Pesticides (AREA)
- Botany (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of compound botanical insecticides of the rice with regulatory function, including following component:25 35 parts of calamus, 15 25 parts of yellow cinnamon leaf, 12 18 parts of allicin, 46 parts of Celastrus angulatus missible oil, 58 parts of matrine missible oil, 35 parts of jervine alcoholic solution, 8 12 parts of plant anti-mildew ingredient, 30 40 parts of potassium fulvate, 0.8 1.2 parts of compound sodium nitrophenolate, plant compound 24 parts of essential oil.The rice of the present invention is reasonable with compound botanical insecticidal formulation, using the compoundings such as active components of plants and allicin, plant anti-mildew ingredient, potassium fulvate, dosage reduces, reduce cost, it is environmentally safe, not only insecticidal effect is preferable, also has preferable effect to improving rice quality and growth.
Description
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of rice with regulatory function compound botanical insecticide
And preparation method thereof.
Background technology
Insecticide is a kind of special product, it can prevent agricultural pest and disease damage, also can be to making while killing off the insect pests
The growth of object generates harm;And commonly using insecticide or it is an excess amount of use insecticide, to the growing environment and work of crop
All it is a kind of burden for object itself, fights the enemy 1,000 from damage 800 although not reaching, nocuity is still very big and right
People and animals, environment are also a kind of injury.
Invention content
In view of the foregoing, it is an object to provide a kind of rice with regulatory function compound botanical desinsection
Agent and preparation method thereof, compound botanical insecticidal formulation is reasonable, and the more existing insecticide of dosage reduces, insecticidal effect compared with
It is good, also there is preferable effect to improving rice quality and growth, and preparation method is simple, it is easily operated.
To achieve the goals above, the technical solution adopted by the present invention is:A kind of rice compounding with regulatory function
Vegetable insecticide is made of the raw material of following parts by weight:
25-35 parts of calamus, 15-25 parts of yellow cinnamon leaf, 12-18 parts of allicin, 4-6 parts of Celastrus angulatus missible oil, matrine missible oil
5-8 parts, 3-5 parts of jervine alcoholic solution, 8-12 parts of plant anti-mildew ingredient, 30-40 parts of potassium fulvate, 0.8-1.2 parts of compound sodium nitrophenolate,
Plant compounds 2-4 parts of essential oil.
The plant anti-mildew ingredient is the mixing of taraxol extract, dwarf sheareria herb alcohol extracting thing and chrysanthemol extract
Object;Wherein, the weight proportion of taraxol extract, dwarf sheareria herb alcohol extracting thing and chrysanthemol extract is 1:(0.5-0.8):
(0.8-1.0)。
The plant compounding essential oil is the compound of deodar essential oil and chenopodium ambrosiodies essential oil;Wherein, deodar essential oil and chenopodium ambrosiodies
The weight proportion of essential oil is 1:(0.5-0.8).
The Celastrus angulatus missible oil is 1% Celastrus angulatus missible oil, and matrine missible oil is 0.38% matrine missible oil, jervine
Alcoholic solution is 0.5% jervine alcoholic solution.
The above-mentioned rice with regulatory function compound botanical insecticide, including following preparation process:
(1) according to formula rate, calamus and yellow cinnamon leaf are weighed, cleaning shreds to obtain mixed material after drying, by mixed material
6-10h is impregnated in water, is heated to 90-100 DEG C, extraction 2 times, the 1st time plus 20-30 times is decocted and measures water, extracts 2-3h, the 2nd time
Add 15-25 times to measure water, extract 1.5-2.5h, four layers of gauze filtration, merging filtrate, filtrate are concentrated into mixed material weight every time
4-7 times, filtering is spare;
(2) according to formula rate, allicin, Celastrus angulatus missible oil, matrine missible oil, jervine alcoholic solution, plant are weighed
Anti-mildew ingredient and plant compound essential oil, are added in the concentrate obtained by step (1), are uniformly mixed after mixing;
(3) according to formula rate, potassium fulvate and compound sodium nitrophenolate are added in the mixed liquor obtained by step (2), stirring is mixed
It closes uniform;
(4) mixture obtained by step (3) is crushed with airslide disintegrating mill, then test package finished product.
In use, being diluted to the above-mentioned prepared rice clear water that 80-100 times is added in compound botanical insecticide
Sprinkling, and it is generally used in rice seedlings early growth period, it is used in conjunction 2-3 times, every minor tick 7-10 days, control effect is more satisfactory.
Beneficial effects of the present invention:The present invention rice it is reasonable with compound botanical insecticidal formulation, using vegetable active at
Point and the compoundings such as allicin, plant anti-mildew ingredient, potassium fulvate, dosage reduces for existing insecticide, and subtracts
Few cost, environmentally safe, not only insecticidal effect is preferable, also has preferable effect to improving rice quality and growth
Fruit;Meanwhile preparation method is simple, it is easily operated.
Specific implementation mode
Below in conjunction with specific embodiment, the invention will be further described, but protection scope of the present invention is not limited to following reality
Apply example.In embodiment, all raw materials are commercially available product.
Embodiment 1
A kind of rice with regulatory function compound botanical insecticide, is made of the raw material of following parts by weight:
33 parts of calamus, 22 parts of yellow cinnamon leaf, 16 parts of allicin, 5 parts of Celastrus angulatus missible oil, 6 parts of matrine missible oil, jervine alcohol
4 parts of solution, 10 parts of plant anti-mildew ingredient, 36 parts of potassium fulvate, 1.0 parts of compound sodium nitrophenolate, plant compound 3 parts of essential oil.
The plant anti-mildew ingredient is the mixing of taraxol extract, dwarf sheareria herb alcohol extracting thing and chrysanthemol extract
Object;Wherein, the weight proportion of taraxol extract, dwarf sheareria herb alcohol extracting thing and chrysanthemol extract is 1:0.5:1.0.
The plant compounding essential oil is the compound of deodar essential oil and chenopodium ambrosiodies essential oil;Wherein,
The weight proportion of deodar essential oil and chenopodium ambrosiodies essential oil is 1:0.5.
The Celastrus angulatus missible oil is 1% Celastrus angulatus missible oil, and matrine missible oil is 0.38% matrine missible oil, jervine
Alcoholic solution is 0.5% jervine alcoholic solution.
The above-mentioned rice with regulatory function compound botanical insecticide, including following preparation process:
(1) according to formula rate, calamus and yellow cinnamon leaf are weighed, cleaning shreds to obtain mixed material after drying, by mixed material
8h is impregnated in water, is heated to 100 DEG C, decocts 2 times, the 1st time plus 26 times amount water of extraction, extracts 3h, the 2nd time plus 22 times amount water,
2h is extracted, four layers of gauze filtration, merging filtrate, filtrate are concentrated into 5 times of mixed material weight every time, filter, spare;
(2) according to formula rate, allicin, Celastrus angulatus missible oil, matrine missible oil, jervine alcoholic solution, plant are weighed
Anti-mildew ingredient and plant compound essential oil, are added in the concentrate obtained by step (1), are uniformly mixed after mixing;
(3) according to formula rate, potassium fulvate and compound sodium nitrophenolate are added in the mixed liquor obtained by step (2), stirring is mixed
It closes uniform;
(4) mixture obtained by step (3) is crushed with airslide disintegrating mill, then test package finished product.
In use, 90 times of clear water dilution is added into above-mentioned prepared rice compound botanical insecticide to spray
It spills, and is generally used in rice seedlings early growth period, be used in conjunction 3 times, every minor tick 10 days, control effect 89.6%.
Embodiment 2
A kind of rice with regulatory function compound botanical insecticide, is made of the raw material of following parts by weight:
35 parts of calamus, 23 parts of yellow cinnamon leaf, 16 parts of allicin, 5 parts of Celastrus angulatus missible oil, 7 parts of matrine missible oil, jervine alcohol
4 parts of solution, 10 parts of plant anti-mildew ingredient, 38 parts of potassium fulvate, 1.0 parts of compound sodium nitrophenolate, plant compound 3.6 parts of essential oil.
The plant anti-mildew ingredient is the mixing of taraxol extract, dwarf sheareria herb alcohol extracting thing and chrysanthemol extract
Object;Wherein, the weight proportion of taraxol extract, dwarf sheareria herb alcohol extracting thing and chrysanthemol extract is 1:0.6:0.9.
The plant compounding essential oil is the compound of deodar essential oil and chenopodium ambrosiodies essential oil;Wherein, deodar essential oil and chenopodium ambrosiodies
The weight proportion of essential oil is 1:0.8.
The Celastrus angulatus missible oil is 1% Celastrus angulatus missible oil, and matrine missible oil is 0.38% matrine missible oil, jervine
Alcoholic solution is 0.5% jervine alcoholic solution.
The above-mentioned rice with regulatory function compound botanical insecticide, including following preparation process:
(1) according to formula rate, calamus and yellow cinnamon leaf are weighed, cleaning shreds to obtain mixed material after drying, by mixed material
10h is impregnated in water, is heated to 100 DEG C, decocts 2 times, the 1st time plus 30 times amount water of extraction, extracts 3h, the 2nd time plus 25 times amount water,
2.5h is extracted, four layers of gauze filtration, merging filtrate, filtrate are concentrated into 6 times of mixed material weight every time, filter, spare;
(2) according to formula rate, allicin, Celastrus angulatus missible oil, matrine missible oil, jervine alcoholic solution, plant are weighed
Anti-mildew ingredient and plant compound essential oil, are added in the concentrate obtained by step (1), are uniformly mixed after mixing;
(3) according to formula rate, potassium fulvate and compound sodium nitrophenolate are added in the mixed liquor obtained by step (2), stirring is mixed
It closes uniform;
(4) mixture obtained by step (3) is crushed with airslide disintegrating mill, then test package finished product.
In use, 100 times of clear water dilution is added into above-mentioned prepared rice compound botanical insecticide to spray
It spills, and is generally used in rice seedlings early growth period, be used in conjunction 3 times, every minor tick 10 days, control effect 90.2%.
Claims (5)
1. a kind of rice with regulatory function compound botanical insecticide, which is characterized in that by the raw material group of following parts by weight
At:25-35 parts of calamus, 15-25 parts of yellow cinnamon leaf, 12-18 parts of allicin, 4-6 parts of Celastrus angulatus missible oil, 5-8 parts of matrine missible oil,
3-5 parts of jervine alcoholic solution, 8-12 parts of plant anti-mildew ingredient, 30-40 parts of potassium fulvate, 0.8-1.2 parts of compound sodium nitrophenolate, plant are multiple
With 2-4 parts of essential oil.
2. a kind of rice with regulatory function compound botanical insecticide according to claim, which is characterized in that institute
Plant anti-mildew ingredient is stated as taraxol extract, the mixture of dwarf sheareria herb alcohol extracting thing and chrysanthemol extract;Wherein, Pu
The weight proportion of public English alcohol extracting thing, dwarf sheareria herb alcohol extracting thing and chrysanthemol extract is 1:(0.5-0.8):(0.8-1.0).
3. a kind of rice with regulatory function compound botanical insecticide according to claim, which is characterized in that institute
State the compound that plant compounding essential oil is deodar essential oil and chenopodium ambrosiodies essential oil;Wherein, the weight of deodar essential oil and chenopodium ambrosiodies essential oil
Proportioning is 1:(0.5-0.8).
4. a kind of rice with regulatory function compound botanical insecticide according to claim, which is characterized in that institute
It is 1% Celastrus angulatus missible oil to state Celastrus angulatus missible oil, and matrine missible oil is 0.38% matrine missible oil, and jervine alcoholic solution is
0.5% jervine alcoholic solution.
5. a kind of rice with regulatory function compound botanical insecticide according to any one of claims 1-4,
It is characterized in that, including following preparation process:
(1) according to formula rate, calamus and yellow cinnamon leaf are weighed, cleaning shreds to obtain mixed material after drying, by mixed material in water
Middle immersion 6-10h, is heated to 90-100 DEG C, decocts extraction 2 times, the 1st time plus 20-30 times and measures water, extracts 2-3h, the 2nd time plus 15-
25 times of amount water, extract 1.5-2.5h, and four layers of gauze filtration, merging filtrate, filtrate are concentrated into the 4-7 of mixed material weight every time
Times, filtering is spare;
(2) according to formula rate, allicin, Celastrus angulatus missible oil, matrine missible oil, jervine alcoholic solution, plant anti-mildew are weighed
Ingredient and plant compound essential oil, are added in the concentrate obtained by step (1), are uniformly mixed after mixing;
(3) according to formula rate, potassium fulvate and compound sodium nitrophenolate are added in the mixed liquor obtained by step (2), is stirred
It is even;
(4) mixture obtained by step (3) is crushed with airslide disintegrating mill, then test package finished product.
Priority Applications (1)
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CN201810466472.4A CN108450487A (en) | 2018-05-16 | 2018-05-16 | A kind of rice with regulatory function compound botanical insecticide and preparation method thereof |
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CN201810466472.4A CN108450487A (en) | 2018-05-16 | 2018-05-16 | A kind of rice with regulatory function compound botanical insecticide and preparation method thereof |
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Publication Number | Publication Date |
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CN108450487A true CN108450487A (en) | 2018-08-28 |
Family
ID=63214465
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CN201810466472.4A Withdrawn CN108450487A (en) | 2018-05-16 | 2018-05-16 | A kind of rice with regulatory function compound botanical insecticide and preparation method thereof |
Country Status (1)
Country | Link |
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CN (1) | CN108450487A (en) |
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2018
- 2018-05-16 CN CN201810466472.4A patent/CN108450487A/en not_active Withdrawn
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