CN108441392A - A kind of preparation method of anti-oxidant Russule spirit - Google Patents
A kind of preparation method of anti-oxidant Russule spirit Download PDFInfo
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- CN108441392A CN108441392A CN201810582267.4A CN201810582267A CN108441392A CN 108441392 A CN108441392 A CN 108441392A CN 201810582267 A CN201810582267 A CN 201810582267A CN 108441392 A CN108441392 A CN 108441392A
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- russule
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
- C12H1/06—Precipitation by physical means, e.g. by irradiation, vibrations
- C12H1/063—Separation by filtration
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- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
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- Food Science & Technology (AREA)
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- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention belongs to the preparing technical field of wine, more particularly to a kind of preparation method of anti-oxidant Russule spirit, including following preparation process:1) fresh russule is won, is cleaned up, is dried, crushes, obtains russule dry powder;2) white wine of 5 10 times of its weight is added to russule dry powder again, 8 18min are handled under 245 285MPa super-pressure;3) it was aged for 3 June, ultrafiltration is filling to seal up for safekeeping, you can.The Russule spirit that the method for the present invention is prepared has very strong antioxidation, has especially been obviously improved the antioxidation of russule, to promote the value of russule, the preservation that wine is more advantageous to russule is made.
Description
Technical field
The invention belongs to the preparing technical field of wine, more particularly to a kind of preparation method of anti-oxidant Russule spirit.
Background technology
Russule also known as russule, russule are the red vertebra woods soil humic layers formed in the very long years.Russule has
There is blood-nourishing to strengthen the health-care efficacies such as body, skin care U.S. face, cancer-resisting, anti-aging, is rare in the world pure natural health-care
Edible mushroom, deep to be favored by domestic and international consumer, situation of selling well Fujian, Guangdong etc. save and the states such as Japan, Southeast Asian countries, Hong Kong, Macao and Taiwan
Family and area, market sale price raise up year after year.Russule there is no deep processed product at present, all manually dry or dry pin
It sells, has no pollution, be pure natural health-care edible mushroom.
Russule contains other foods containing protein, carbohydrate, minerals, vitamin B, vitamin D, vitamin E
Rare niacin in product, trace elements iron, zinc, selenium, manganese etc..Russule contains the ingredients such as a variety of amino acid necessary to someone, has
Enriching yin, kidney tonifying, moistening lung, promoting blood circulation, brain tonic, beauty treatment and other effects, it is often edible, it can keep fit and healthy, promote longevity.Contained by russule
Protein has 25% or so to be dissolved in water, and 50% or so can be digested and assimilated by people, and only 25% or so cannot
It is absorbed by the body.It contains polysaccharide cancer-resisting substance simultaneously, is conducive to blood circulation, reduces the cholesterol in blood, inhibits cancer
Cell shifts, and treating acute spinal optic nerve disease to treatment also has certain curative effect.Indigestion, children's rickets, energy can also be prevented
The function of improving normal sugar metabolism and immunity of organism, is conducive to the reduction of nursing baby in lactation period for puerpera juice, anaemia etc., there is special food therapy value
Wholefood.
Russule still can not carry out artificial cultivation at present, and the annual yield of the pure natural russule grown naturally has
Limit, and after russule is removed, is easy to oxidation and is decomposed, it is not easy to maintain.Therefore a kind of russule deep processing is researched and developed
Product promotes its value, and more easy to maintain, is necessary.And research and develop a kind of raising russule antioxygenic property
The preparation method of wine, so far unmanned research.
Invention content
Technical problem to be solved by the invention is to provide a kind of preparation methods of anti-oxidant Russule spirit.
To achieve the above object, the present invention adopts the following technical scheme that:
The present invention provides a kind of preparation method of anti-oxidant Russule spirit, including following preparation process:
1) fresh russule is won, is cleaned up, is dried, crushes, obtains russule dry powder;
2) white wine of 5-10 times of its weight is added to russule dry powder again, 8- is handled under 245-285MPa super-pressure
18min;
3) ageing 3-6 months, ultrafiltration is filling to seal up for safekeeping, you can.
Preferably, in step 1) of the present invention, it is 12-20% to be dried to water content.
Preferably, in step 1) of the present invention, it is crushed to 100-200 mesh.
Preferably, in step 2) of the present invention, the alcoholic strength of white wine is 28-35%vol.
Preferably, in step 2) of the present invention, the alcoholic strength of white wine is 30%vol.
Preferably, it in step 2) of the present invention, is handled under 265MPa super-pressure.
Preferably, it in step 3) of the present invention, crosses the hollow-fibre membrane that molecular cut off is 3-6 ten thousand and carries out ultrafiltration.
Preferably, it in step 3) of the present invention, crosses the hollow-fibre membrane that molecular cut off is 50,000 and carries out ultrafiltration.
In the preparation method of the present invention, the pressure difference of super-pressure and the change of other correlation steps-can influence red
The antioxidant effect of vertebra bacterium wine, the study found that each step synergistic effect of wine of the present invention, can promote the antioxygen of russule very well
Change effect.
Compared with prior art, the beneficial effects of the present invention are:
It after the present invention is by specific ultra high pressure treatment, then is aged so that russule dry powder is carried out with white wine ingredient
Complicated reaction, the Russule spirit being finally prepared have very strong antioxidation, have especially been obviously improved russule
Antioxidation the preservation that wine is more advantageous to russule is made to promote the value of russule.
Specific implementation mode
The invention will be further described with reference to embodiments, but the invention is not limited in these embodiments.
Embodiment 1
A kind of preparation method of anti-oxidant Russule spirit, including following preparation process:
1) fresh russule is won, is cleaned up, it is 12% to be dried to water content, is crushed to 200 mesh, obtains russule
Dry powder;
2) white wine that 5 times of alcoholic strengths of its weight are 35%vol is added to russule dry powder again, under 245MPa super-pressure
Manage 18min;
3) it is aged 3 months, crosses the hollow-fibre membrane that molecular cut off is 60,000 and carry out ultrafiltration, it is filling to seal up for safekeeping, you can.
Embodiment 2
A kind of preparation method of anti-oxidant Russule spirit, including following preparation process:
1) fresh russule is won, is cleaned up, it is 16% to be dried to water content, is crushed to 150 mesh, obtains russule
Dry powder;
2) white wine that 7 times of alcoholic strengths of its weight are 30%vol is added to russule dry powder again, under 265MPa super-pressure
Manage 13min;
3) it is aged 5 months, crosses the hollow-fibre membrane that molecular cut off is 50,000 and carry out ultrafiltration, it is filling to seal up for safekeeping, you can.
Embodiment 3
A kind of preparation method of anti-oxidant Russule spirit, including following preparation process:
1) fresh russule is won, is cleaned up, it is 20% to be dried to water content, is crushed to 100 mesh, obtains russule
Dry powder;
2) white wine that 10 times of alcoholic strengths of its weight are 28%vol is added to russule dry powder again, under 285MPa super-pressure
Handle 8min;
3) it is aged 6 months, crosses the hollow-fibre membrane that molecular cut off is 30,000 and carry out ultrafiltration, it is filling to seal up for safekeeping, you can.
Embodiment 4
As different from Example 2:In step 2), handled under 245MPa super-pressure.Remaining is same
Embodiment 2.
Embodiment 5
As different from Example 2:In step 2), handled under 285MPa super-pressure.Remaining is same
Embodiment 2.
Embodiment 6
As different from Example 2:In step 2), white wine alcoholic strength is 28%vol.Remaining is the same as embodiment 2.
Embodiment 7
As different from Example 2:In step 2), white wine alcoholic strength is 35%vol.Remaining is the same as embodiment 2.
Embodiment 8
As different from Example 2:In step 3), it is aged 3 months.Remaining is the same as embodiment 2.
Embodiment 9
As different from Example 2:In step 3), it is aged 5 months.Remaining is the same as embodiment 2.
Comparative example 1
As different from Example 2:In step 2), handled under 225MPa super-pressure.Remaining is same
Embodiment 2.
Comparative example 2
As different from Example 2:In step 2), handled under 305MPa super-pressure.Remaining is same
Embodiment 2.
Comparative example 3
As different from Example 2:In step 2), white wine alcoholic strength is 25%vol.Remaining is the same as embodiment 2.
Comparative example 4
As different from Example 2:In step 2), white wine alcoholic strength is 38%vol.Remaining is the same as embodiment 2.
Comparative example 5
As different from Example 2:In step 3), it is aged 2 months.Remaining is the same as embodiment 2.
Comparative example 6
As different from Example 2:In step 3), it is aged 6 months.Remaining is the same as embodiment 2.
Comparative example 7
As different from Example 2:The step 3) is:Ageing 5 months, it is filling to seal up for safekeeping, you can.Remaining is the same as embodiment 2.
Test example:The Russule spirit antioxygenic property that the method for the present invention is prepared
(8 groups of comparative example is 30 degree of white wine, 9 groups of comparative example for 2 groups of Example, embodiment 4-9 groups, comparative example 1-9 groups respectively
For fresh russule juice), the ability that they remove hydroxyl radical free radical, DPPH, superoxide anion, their survey are measured respectively
The method of determining is:
1) measurement of hydroxyl radical free radical is removed:FeSO4With H2O2Reaction generates OH, and salicylic acid is added in system, can catch
It catches hydroxyl radical free radical and generates coloring matter, which has absorption maximum at 510nm, when there are OH freedom in reaction system
When base scavenger, this oxidation process is suppressed, and absorbance value then reduces.In FeSO4With H2O2In reaction system, it is separately added into
2 groups of the embodiment of the present invention of a concentration of 30ml/ml, embodiment 4-9 groups, comparative example 1-9 group tie substances measure clearance rate.
2) DPPH methods measure health care olive roast pork sauce antioxidant activity:DPPH be in organic solvent a kind of stabilization from
By base, it is widely used in anti-oxidant appraisement system.In system, it is separately added into 2 groups of the embodiment of a concentration of 30ml/ml, implements
Example 4-9 groups, comparative example 1-9 group tie substances, measure clearance rate.
3) superoxide anion is removed to measure:Generating ultra-oxygen anion free radical (O2-) reaction system in, respectively plus
2 groups of the embodiment of the present invention, embodiment 4-9 groups, comparative example 1-9 group tie substances for entering a concentration of 5ml/ml measure them and remove
Rate.
Wherein, 9 groups of russule juice of comparative example are prepared as:Fresh russule is won, the water for going weight equivalent weight is added, beats
Slurry, filtering, filtrate is russule juice.
Measurement result is shown in Table 1.
1 embodiment and comparative example each group substance in vitro anti-oxidation activity rating situation of table
As it can be seen from table 1 the pressure of super-pressure in the method for the present invention, the alcohol concentration of white wine, digestion time, whether surpassing
Filter can all influence the inoxidizability of Russule spirit, and wherein embodiment 2 and embodiment 4-9 antioxygenic properties is significantly higher than comparative example
Group illustrates to prepare Russule spirit by the method for the invention, the antioxidant activity of russule can be improved, to improve russule
Inoxidizability.
Claims (8)
1. a kind of preparation method of anti-oxidant Russule spirit, which is characterized in that including following preparation process:
1) fresh russule is won, is cleaned up, is dried, crushes, obtains russule dry powder;
2) white wine of 5-10 times of its weight is added to russule dry powder again, 8-18min is handled under 245-285MPa super-pressure;
3) ageing 3-6 months, ultrafiltration is filling to seal up for safekeeping, you can.
2. the preparation method of anti-oxidant Russule spirit according to claim 1, it is characterised in that:In the step 1), dry
It is 12-20% to do to water content.
3. the preparation method of anti-oxidant Russule spirit according to claim 1, it is characterised in that:In the step 1), powder
It is broken to 100-200 mesh.
4. the preparation method of anti-oxidant Russule spirit according to claim 1, it is characterised in that:In the step 2), in vain
The alcoholic strength of wine is 28-35%vol.
5. the preparation method of anti-oxidant Russule spirit according to claim 4, it is characterised in that:In the step 2), in vain
The alcoholic strength of wine is 30%vol.
6. the preparation method of anti-oxidant Russule spirit according to claim 1, it is characterised in that:In the step 2),
It is handled under 265MPa super-pressure.
7. the preparation method of anti-oxidant Russule spirit according to claim 1, it is characterised in that:In the step 3), mistake
The hollow-fibre membrane that molecular cut off is 3-6 ten thousand carries out ultrafiltration.
8. the preparation method of anti-oxidant Russule spirit according to claim 7, it is characterised in that:In the step 3), mistake
The hollow-fibre membrane that molecular cut off is 50,000 carries out ultrafiltration.
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CN201810582267.4A CN108441392A (en) | 2018-06-07 | 2018-06-07 | A kind of preparation method of anti-oxidant Russule spirit |
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CN201810582267.4A CN108441392A (en) | 2018-06-07 | 2018-06-07 | A kind of preparation method of anti-oxidant Russule spirit |
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Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101654644A (en) * | 2009-09-15 | 2010-02-24 | 吴宗满 | Russula vinosa king wine |
CN102876531A (en) * | 2012-03-24 | 2013-01-16 | 雷鉴源 | Ultra high pressure (UHP) wine |
CN103275852A (en) * | 2013-03-26 | 2013-09-04 | 浦北县健翔食品厂 | Russule spirit preparation method |
CN103666939A (en) * | 2012-08-31 | 2014-03-26 | 张释文 | Health-care wine for preserving health and preparation technology thereof |
CN104745424A (en) * | 2015-04-01 | 2015-07-01 | 吉林省命之元生物科技有限公司 | Maca health wine and preparation method thereof |
CN107151594A (en) * | 2017-06-09 | 2017-09-12 | 广西浦北龙升红椎菌有限公司 | A kind of Russule spirit |
CN107373306A (en) * | 2017-07-31 | 2017-11-24 | 广西健美乐食品有限公司 | A kind of preparation method of Russulasp. powder |
-
2018
- 2018-06-07 CN CN201810582267.4A patent/CN108441392A/en not_active Withdrawn
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101654644A (en) * | 2009-09-15 | 2010-02-24 | 吴宗满 | Russula vinosa king wine |
CN102876531A (en) * | 2012-03-24 | 2013-01-16 | 雷鉴源 | Ultra high pressure (UHP) wine |
CN103666939A (en) * | 2012-08-31 | 2014-03-26 | 张释文 | Health-care wine for preserving health and preparation technology thereof |
CN103275852A (en) * | 2013-03-26 | 2013-09-04 | 浦北县健翔食品厂 | Russule spirit preparation method |
CN104745424A (en) * | 2015-04-01 | 2015-07-01 | 吉林省命之元生物科技有限公司 | Maca health wine and preparation method thereof |
CN107151594A (en) * | 2017-06-09 | 2017-09-12 | 广西浦北龙升红椎菌有限公司 | A kind of Russule spirit |
CN107373306A (en) * | 2017-07-31 | 2017-11-24 | 广西健美乐食品有限公司 | A kind of preparation method of Russulasp. powder |
Non-Patent Citations (1)
Title |
---|
纵伟主编: "《食品最少破坏加工技术》", 30 April 2006, 东北林业大学出版社 * |
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Application publication date: 20180824 |