CN108359386A - A kind of fire resistant doorsets fireproof gum and preparation method thereof - Google Patents
A kind of fire resistant doorsets fireproof gum and preparation method thereof Download PDFInfo
- Publication number
- CN108359386A CN108359386A CN201810342950.0A CN201810342950A CN108359386A CN 108359386 A CN108359386 A CN 108359386A CN 201810342950 A CN201810342950 A CN 201810342950A CN 108359386 A CN108359386 A CN 108359386A
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- CN
- China
- Prior art keywords
- parts
- fire resistant
- fireproof gum
- resistant doorsets
- liquid
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J1/00—Adhesives based on inorganic constituents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
Abstract
The present invention is a kind of fire resistant doorsets fireproof gum and preparation method thereof, and the component and part of the fireproof gum is as follows：Liquid silicon hydrochlorate：650 850 parts；Redispersible latex powder：15 25 parts；Polypropylene monofilament fiber：2.2 2.8 parts；Silica：110 170 parts；Aluminium oxide：2 25 parts；Iron oxide：3 20 parts；Magnesia：3 25 parts；Calcium oxide：2 10 parts；Aluminum phosphate：15 60 parts；Kaolin：50 500 parts；Aluminium hydroxide：20 40 parts.The present invention has preferable adhesion strength, crack resistance and durability, can high temperature resistant and nontoxic.
Description
Technical field
The present invention relates to fire resistant doorsets fields more particularly to a kind of fire resistant doorsets fireproof gum and preparation method thereof.
Background technology
Fire resistant doorsets are to meet fire stability within a certain period of time, and thermal insulation can prevent fire spreading and diffusion, really
Protect the door of evacuating personnel.Fire resistant doorsets be usually fire-proof plate is bonded on the panel of fire resistant doorsets with fireproof gum made of, commonly
Fireproof gum is polyurethane foam glue and inorganic bond glue, and polyurethane foam glue is inflammable, and the flue gas that when burning generates is harmful,
Inorganic bond glue has cheap, the advantages such as adhesion strength is high, and production smoke toxicity is low, but durability is slightly poor, uses a period of time
Afterwards, the integrality and thermal insulation of fire resistant doorsets are influenced.
Invention content
Present invention seek to address that the deficiencies in the prior art, and a kind of fire resistant doorsets fireproof gum is provided and preparation method thereof.
The present invention to achieve the above object, using following technical scheme：A kind of fire resistant doorsets fireproof gum, the fireproof gum
Component and part is as follows：
Liquid silicon hydrochlorate：650-850 parts；
Redispersible latex powder：15-25 parts；
Polypropylene monofilament fiber：2.2-2.8 part；
Silica：110-170 parts；
Aluminium oxide：2-25 parts；
Iron oxide：3-20 parts；
Magnesia：3-25 parts；
Calcium oxide：2-10 parts；
Aluminum phosphate：15-60 parts；
Kaolin：50-500 parts；
Aluminium hydroxide：20-40 parts.
Particularly, the liquid silicon hydrochlorate is liquid sodium silicate or liquid silicic acid magnesium.
Particularly, the particle diameter of the silica is 1.5-2.8 μm.
Particularly, the length of the polypropylene monofilament fiber is 12-18mm.
A kind of preparation method of fire resistant doorsets fireproof gum, includes the following steps：
(1) liquid silicon hydrochlorate, redispersible latex powder are put into blender, uniform stirring makes emulsification, mixing time
For 130-200min；
(2) liquid after emulsification is filtered；
(3) obtained filtered fluid is poured into high speed dispersor；
(4) silica, aluminium oxide, iron oxide, magnesia, calcium oxide, aluminum phosphate, kaolin and aluminium hydroxide is slow
It is added in high speed dispersor and carries out fully dispersed；
(5) it adds polypropylene monofilament fiber and is disperseed；
(6) liquid after dispersion is filtered.
The beneficial effects of the invention are as follows：The present invention have preferable adhesion strength, crack resistance and durability, can high temperature resistant and
It is nontoxic.
Specific implementation mode
With reference to embodiment, the invention will be further described：
A kind of fire resistant doorsets fireproof gum, the component and part of the fireproof gum are as follows：
Liquid silicon hydrochlorate：650-850 parts；
Redispersible latex powder：15-25 parts；
Polypropylene monofilament fiber：2.2-2.8 part；
Silica：110-170 parts；
Aluminium oxide：2-25 parts；
Iron oxide：3-20 parts；
Magnesia：3-25 parts；
Calcium oxide：2-10 parts；
Aluminum phosphate：15-60 parts；
Kaolin：50-500 parts；
Aluminium hydroxide：20-40 parts.
Particularly, the liquid silicon hydrochlorate is liquid sodium silicate or liquid silicic acid magnesium.
Particularly, the particle diameter of the silica is 1.5-2.8 μm.
Particularly, the length of the polypropylene monofilament fiber is 12-18mm.
A kind of preparation method of fire resistant doorsets fireproof gum, includes the following steps：
(1) liquid silicon hydrochlorate, redispersible latex powder are put into blender, uniform stirring makes emulsification, mixing time
For 130-200min；
(2) liquid after emulsification is filtered；
(3) obtained filtered fluid is poured into high speed dispersor；
(4) silica, aluminium oxide, iron oxide, magnesia, calcium oxide, aluminum phosphate, kaolin and aluminium hydroxide is slow
It is added in high speed dispersor and carries out fully dispersed；
(5) it adds polypropylene monofilament fiber and is disperseed；
(6) liquid after dispersion is filtered.
Embodiment 1
A kind of fire resistant doorsets fireproof gum, the component and part of the fireproof gum are as follows：
Liquid silicon hydrochlorate：650 parts；
Redispersible latex powder：15 parts；
Polypropylene monofilament fiber：2.2 part；
Silica：110 parts；
Aluminium oxide：25 parts；
Iron oxide：3 parts；
Magnesia：3 parts；
Calcium oxide：2 parts；
Aluminum phosphate：15 parts；
Kaolin：50 parts；
Aluminium hydroxide：20 parts.
Particularly, the liquid silicon hydrochlorate is liquid sodium silicate or liquid silicic acid magnesium.
Particularly, the particle diameter of the silica is 1.5 μm.
Particularly, the length of the polypropylene monofilament fiber is 12mm.
A kind of preparation method of fire resistant doorsets fireproof gum, includes the following steps：
(1) liquid silicon hydrochlorate, redispersible latex powder are put into blender, uniform stirring makes emulsification, mixing time
For 130min；
(2) liquid after emulsification is filtered；
(3) obtained filtered fluid is poured into high speed dispersor；
(4) silica, aluminium oxide, iron oxide, magnesia, calcium oxide, aluminum phosphate, kaolin and aluminium hydroxide is slow
It is added in high speed dispersor and carries out fully dispersed；
(5) it adds polypropylene monofilament fiber and is disperseed；
(6) liquid after dispersion is filtered.
Embodiment 2
A kind of fire resistant doorsets fireproof gum, the component and part of the fireproof gum are as follows：
Liquid silicon hydrochlorate：850 parts；
Redispersible latex powder：25 parts；
Polypropylene monofilament fiber：2.8 part；
Silica：170 parts；
Aluminium oxide：2 parts；
Iron oxide：20 parts；
Magnesia：25 parts；
Calcium oxide：10 parts；
Aluminum phosphate：60 parts；
Kaolin：500 parts；
Aluminium hydroxide：40 parts.
Particularly, the liquid silicon hydrochlorate is liquid sodium silicate or liquid silicic acid magnesium.
Particularly, the particle diameter of the silica is 2.8 μm.
Particularly, the length of the polypropylene monofilament fiber is 18mm.
A kind of preparation method of fire resistant doorsets fireproof gum, includes the following steps：
(1) liquid silicon hydrochlorate, redispersible latex powder are put into blender, uniform stirring makes emulsification, mixing time
For 200min；
(2) liquid after emulsification is filtered；
(3) obtained filtered fluid is poured into high speed dispersor；
(4) silica, aluminium oxide, iron oxide, magnesia, calcium oxide, aluminum phosphate, kaolin and aluminium hydroxide is slow
It is added in high speed dispersor and carries out fully dispersed；
(5) it adds polypropylene monofilament fiber and is disperseed；
(6) liquid after dispersion is filtered.
Embodiment 3
A kind of fire resistant doorsets fireproof gum, the component and part of the fireproof gum are as follows：
Liquid silicon hydrochlorate：720 parts；
Redispersible latex powder：20 parts；
Polypropylene monofilament fiber：2.5 part；
Silica：155 parts；
Aluminium oxide：16 parts；
Iron oxide：13 parts；
Magnesia：16 parts；
Calcium oxide：6 parts；
Aluminum phosphate：35 parts；
Kaolin：300 parts；
Aluminium hydroxide：30 parts.
Particularly, the liquid silicon hydrochlorate is liquid sodium silicate or liquid silicic acid magnesium.
Particularly, the particle diameter of the silica is 2 μm.
Particularly, the length of the polypropylene monofilament fiber is 15mm.
A kind of preparation method of fire resistant doorsets fireproof gum, includes the following steps：
(1) liquid silicon hydrochlorate, redispersible latex powder are put into blender, uniform stirring makes emulsification, mixing time
For 160min；
(2) liquid after emulsification is filtered；
(3) obtained filtered fluid is poured into high speed dispersor；
(4) silica, aluminium oxide, iron oxide, magnesia, calcium oxide, aluminum phosphate, kaolin and aluminium hydroxide is slow
It is added in high speed dispersor and carries out fully dispersed；
(5) it adds polypropylene monofilament fiber and is disperseed；
(6) liquid after dispersion is filtered.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above,
As long as using the various improvement of inventive concept and technical scheme of the present invention progress, or not improved directly apply to other fields
It closes, within protection scope of the present invention.
Claims (5)
1. a kind of fire resistant doorsets fireproof gum, which is characterized in that the component and part of the fireproof gum is as follows：
Liquid silicon hydrochlorate：650-850 parts；
Redispersible latex powder：15-25 parts；
Polypropylene monofilament fiber：2.2-2.8 part；
Silica：110-170 parts；
Aluminium oxide：2-25 parts；
Iron oxide：3-20 parts；
Magnesia：3-25 parts；
Calcium oxide：2-10 parts；
Aluminum phosphate：15-60 parts；
Kaolin：50-500 parts；
Aluminium hydroxide：20-40 parts.
2. a kind of fire resistant doorsets fireproof gum according to claim 1, which is characterized in that the liquid silicon hydrochlorate is liquid silicon
Sour sodium or liquid silicic acid magnesium.
3. a kind of fire resistant doorsets fireproof gum according to claim 2, which is characterized in that the particle diameter of the silica
It is 1.5-2.8 μm.
4. a kind of fire resistant doorsets fireproof gum according to claim 3, which is characterized in that the length of the polypropylene monofilament fiber
Degree is 12-18mm.
5. the preparation method of fire resistant doorsets fireproof gum according to claim 4, which is characterized in that include the following steps：
(1) liquid silicon hydrochlorate, redispersible latex powder are put into blender, uniform stirring makes the emulsification, mixing time be
130-200min；
(2) liquid after emulsification is filtered；
(3) obtained filtered fluid is poured into high speed dispersor；
(4) silica, aluminium oxide, iron oxide, magnesia, calcium oxide, aluminum phosphate, kaolin and aluminium hydroxide are slowly added
To in high speed dispersor and carrying out fully dispersed；
(5) it adds polypropylene monofilament fiber and is disperseed；
(6) liquid after dispersion is filtered.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810342950.0A CN108359386A (en) | 2018-04-17 | 2018-04-17 | A kind of fire resistant doorsets fireproof gum and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810342950.0A CN108359386A (en) | 2018-04-17 | 2018-04-17 | A kind of fire resistant doorsets fireproof gum and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108359386A true CN108359386A (en) | 2018-08-03 |
Family
ID=63008474
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810342950.0A Pending CN108359386A (en) | 2018-04-17 | 2018-04-17 | A kind of fire resistant doorsets fireproof gum and preparation method thereof |
Country Status (1)
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| CN (1) | CN108359386A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112322194A (en) * | 2020-11-20 | 2021-02-05 | 北京中科原创节能环保科技有限公司 | Binder for high-temperature environment and preparation method thereof |
| CN115353366A (en) * | 2022-09-06 | 2022-11-18 | 永康市瑞盛科技有限公司 | Foaming adhesive for fireproof door |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1106772A (en) * | 1992-12-22 | 1995-08-16 | 朱宗桓 | Fireproof and insulation composition |
| CN1820034A (en) * | 2002-10-15 | 2006-08-16 | 埃克森美孚化学专利公司 | Polyolefin adhesive compositions and articles made therefrom |
| CN1878835A (en) * | 2005-02-11 | 2006-12-13 | 德古萨公司 | Aqueous compositions |
| CN101365586A (en) * | 2005-10-27 | 2009-02-11 | 埃克森美孚化学专利公司 | Construction comprising tie layer |
| CN103146344A (en) * | 2013-03-25 | 2013-06-12 | 曹大庆 | Aqueous inorganic and fireproof foam adhesive |
| CN104099028A (en) * | 2014-08-04 | 2014-10-15 | 公安部四川消防研究所 | Fire-proof adhesive and application thereof |
| CN104694020A (en) * | 2015-02-16 | 2015-06-10 | 湖州铁佛门窗有限公司 | Modified inorganic fireproof rubber |
-
2018
- 2018-04-17 CN CN201810342950.0A patent/CN108359386A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1106772A (en) * | 1992-12-22 | 1995-08-16 | 朱宗桓 | Fireproof and insulation composition |
| CN1820034A (en) * | 2002-10-15 | 2006-08-16 | 埃克森美孚化学专利公司 | Polyolefin adhesive compositions and articles made therefrom |
| CN1878835A (en) * | 2005-02-11 | 2006-12-13 | 德古萨公司 | Aqueous compositions |
| CN101365586A (en) * | 2005-10-27 | 2009-02-11 | 埃克森美孚化学专利公司 | Construction comprising tie layer |
| CN103146344A (en) * | 2013-03-25 | 2013-06-12 | 曹大庆 | Aqueous inorganic and fireproof foam adhesive |
| CN104099028A (en) * | 2014-08-04 | 2014-10-15 | 公安部四川消防研究所 | Fire-proof adhesive and application thereof |
| CN104694020A (en) * | 2015-02-16 | 2015-06-10 | 湖州铁佛门窗有限公司 | Modified inorganic fireproof rubber |
Non-Patent Citations (2)
| Title |
|---|
| 李凤: "《2014年中国消防协会防火材料分会与建筑防火专业委员会学术会议论文集》", 30 July 2014, 西南交通大学出版社 * |
| 蔡永源: "《高分子材料阻燃技术手册》", 28 February 1993, 化学工业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112322194A (en) * | 2020-11-20 | 2021-02-05 | 北京中科原创节能环保科技有限公司 | Binder for high-temperature environment and preparation method thereof |
| CN115353366A (en) * | 2022-09-06 | 2022-11-18 | 永康市瑞盛科技有限公司 | Foaming adhesive for fireproof door |
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Application publication date: 20180803 |