CN108329891A - A kind of waterproof roll adhesive and preparation method thereof - Google Patents
A kind of waterproof roll adhesive and preparation method thereof Download PDFInfo
- Publication number
- CN108329891A CN108329891A CN201810073080.1A CN201810073080A CN108329891A CN 108329891 A CN108329891 A CN 108329891A CN 201810073080 A CN201810073080 A CN 201810073080A CN 108329891 A CN108329891 A CN 108329891A
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- CN
- China
- Prior art keywords
- parts
- rubber
- waterproof roll
- waterproofing agent
- mixture
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J195/00—Adhesives based on bituminous materials, e.g. asphalt, tar, pitch
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J107/00—Adhesives based on natural rubber
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of waterproof roll adhesives and preparation method thereof, belong to building material technical field.Adhesive includes following raw material component by raw material：100 parts of asphalt, 60 100 parts of rubber, 23 parts of rubber antioxidant, 20 30 parts of size, 1.5 2.2 parts of emulsifier, 220 280 parts of solvent naphtha, 25 parts of tackifier, 0.5 1.5 parts of waterproofing agent, 12 parts of stabilizer.The present invention can effectively improve the intensity of pasting of the adhesive by the way that a certain amount of stabilizer and tackifier are added in formula, ensure buildings waterproof work efficiency, and when saving base's back tender and expense, and water resistance is lasting, water-fast, corrosion resistant performance is good, be suitble to promote.
Description
Technical field
The invention belongs to building material technical fields, more particularly to a kind of waterproof roll adhesive and preparation method thereof.
Background technology
Waterproof material is a kind of prevents in rainwater, underground water, industry and civilian plumbing, corrosive liquids and air
The intrusion building such as moisture, steam material.It is divided according to material character, waterproof material mainly has waterproof roll, 911 poly- ammonia
Ester waterproof material, new polymers cement group water-proofing material three classes, wherein waterproof roll be mainly used for construction wall, roofing, with
And tunnel, highway, refuse landfill etc., play and resist extraneous rainwater, underground water leakage, as engineering foundation and building it
Between ne-leakage connect, be first of barrier of entire engineering waterproofing, entire engineering played a crucial role.Waterproof simultaneously
The water resistance of the coiled material bonding of coiled material and coiled material, the closing of coiled material lapping and coiled material adhesive in the construction process is also shadow
A key factor of coiled material integral waterproofing performance is rung, the current adhesive for waterproof roll is applied in moist base
Work more takes, and the water resistance under long-term moist environment is bad, is easy to lose waterproof energy in a relatively short period of time
Power, to influence the performance of integral waterproofing layer.
Invention content
The purpose of the present invention is to provide a kind of waterproof roll adhesives and preparation method thereof, by the way that one is added in formula
Quantitative stabilizer, tackifier and waterproofing agent solves the problems, such as that existing adhesive water resistance is low and stability is poor.
In order to solve the above technical problems, the present invention is achieved by the following technical solutions：
The present invention is a kind of waterproof roll adhesive, including following raw material component：100 parts of asphalt, rubber
60-100 parts, 2-3 parts of rubber antioxidant, 20-30 parts of size, 1.5-2.2 parts of emulsifier, 220-280 parts of solvent naphtha, tackifier
2-5 parts, 0.5-1.5 parts of waterproofing agent, 1-2 parts of stabilizer.
Further, the rubber is natural rubber or synthesis butyl rubber, neoprene, polyurethane rubber, polypropylene
The mixture of one or more of acid esters rubber.
Further, the solvent naphtha is the mixture of one or more of gasoline, dimethylbenzene or petroleum hydrocarbon.
Further, the size is the mixture of one or more of diesel oil, kerosene, light machine oil or turpentine oil.
Further, the tackifier is one kind or several in phenol-formaldehyde resin modified, modified rosin resin or Petropols
The mixture of kind.
Further, the waterproofing agent is nano-sized carbon silicate compound combined polymerization waterproofing agent, silane coupled waterproofing agent, aluminium
The mixture of one or more of salt water-repellent, higher fatty acids waterproofing agent.
Further, the stabilizer is antioxidant BHT, antioxidant 1010, antioxidant 4010, ultra-violet absorber UV-
9, the mixture of one or more of ultraviolet absorbent UV-531.
A kind of preparation method of waterproof roll adhesive, includes the following steps：
Step 1 prepares each raw material according to recipe requirements；
Step 2 rubber, rubber antioxidant, size, suitable emulsifier and solvent naphtha is added in mixer, in temperature
Stop heating at 60-80 DEG C of degree after insulated and stirred 15-30min, discharging is cooled to room temperature；
Dewatered asphalt first by 100 parts of asphalt thermal dehydrations, then is put into pitch and reacted by step 3
In tank, 140 DEG C are warming up to the speed of 20 DEG C/min under normal pressure, keeps the temperature 15-20min；After stopping heating, sequentially add remaining
Emulsifier and solvent naphtha, average rate are stirred to pitch and are completely dissolved, and ensure the pressure ＜ 0.15MPa in retort in production process；
Step 4 mixes the rubber composition obtained in step 1 with the pitch obtained in step 2 at 15-40 DEG C
Object presses 1:1 ratio is sent into blending tank, and sequentially adds tackifier and stabilizer, then stirs 30-60min under constant speed,
And it is slowly added to waterproofing agent while agitating；It is cooled to room temperature after stirring；
Mixture feeding grinder is ground by step 5, and control fineness of grind is less than 10 μm；It weighs after grinding packing
To obtain the final product.
The invention has the advantages that：
The present invention can effectively improve pasting for the adhesive by the way that a certain amount of stabilizer and tackifier are added in formula
Intensity ensures buildings waterproof work efficiency, and when saving base's back tender and expense, and water resistance is lasting, water-fast, corrosion resistant performance is good；
By the way that a certain amount of waterproofing agent is added, allow the adhesive on wet base and constructs in wide temperature range, fit
For large-scale industrial production.
Certainly, it implements any of the products of the present invention and does not necessarily require achieving all the advantages described above at the same time.
Specific implementation mode
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
All other embodiment that art personnel are obtained without creative efforts belongs to the model that the present invention protects
It encloses.
Embodiment one：
A kind of waterproof roll adhesive, including following raw material component：
100 parts of asphalt, 60-100 parts of rubber, 2-3 parts of rubber antioxidant, 20-30 parts of size, emulsifier 1.5-
2.2 parts, 220-280 parts of solvent naphtha, 2-5 parts of tackifier, 0.5-1.5 parts of waterproofing agent, 1-2 parts of stabilizer.
Wherein, rubber is natural rubber.
Wherein, solvent naphtha is gasoline.
Wherein, size is kerosene.
Wherein, tackifier is phenol-formaldehyde resin modified.
Wherein, waterproofing agent is silane coupled waterproofing agent.
Wherein, stabilizer is antioxidant BHT.
A kind of preparation method of waterproof roll adhesive, includes the following steps：
Step 1 prepares each raw material according to recipe requirements；
Step 2 adds 70 parts of rubber, 1.5 parts of rubber antioxidants, 20 parts of sizes, 1 part of emulsifier and 130 parts of solvent naphthas
Enter in mixer, stop heating after insulated and stirred 15-30min at 60-80 DEG C of temperature, discharging is cooled to room temperature；
Dewatered asphalt first by 100 parts of asphalt thermal dehydrations, then is put into pitch and reacted by step 3
In tank, 140 DEG C are warming up to the speed of 20 DEG C/min under normal pressure, keeps the temperature 15-20min；After stopping heating, 1 part of breast is sequentially added
Agent and 130 parts of solvent naphthas, average rate are stirred to pitch and are completely dissolved, and ensure the pressure ＜ in retort in production process
0.15MPa；
Step 4 mixes the rubber composition obtained in step 1 with the pitch obtained in step 2 at 15-40 DEG C
Object presses 1:1 ratio is sent into blending tank, and sequentially adds 2 parts of tackifiers and 1 part of stabilizer, then stirs 30- under constant speed
60min, and it is slowly added to 0.5 part of waterproofing agent while agitating；It is cooled to room temperature after stirring；
Mixture feeding grinder is ground by step 5, and control fineness of grind is less than 10 μm；It weighs after grinding packing
To obtain the final product.
Embodiment two：
A kind of waterproof roll adhesive, including following raw material component：
100 parts of asphalt, 60-100 parts of rubber, 2-3 parts of rubber antioxidant, 20-30 parts of size, emulsifier 1.5-
2.2 parts, 220-280 parts of solvent naphtha, 2-5 parts of tackifier, 0.5-1.5 parts of waterproofing agent, 1-2 parts of stabilizer.
Wherein, rubber is lactoprene.
Wherein, solvent naphtha is gasoline.
Wherein, size is kerosene.
Wherein, tackifier is Petropols.
Wherein, waterproofing agent is higher fatty acids waterproofing agent.
Wherein, stabilizer is antioxidant 1010.
A kind of preparation method of waterproof roll adhesive, includes the following steps：
Step 1 prepares each raw material according to recipe requirements；
Step 2, by 100 parts of rubber, 3 parts of rubber antioxidants, 30 parts of sizes, 0.9 part of emulsifier and 120 parts of solvent naphthas
It is added in mixer, stops heating after insulated and stirred 15-30min at 60-80 DEG C of temperature, discharging is cooled to room temperature；
Dewatered asphalt first by 100 parts of asphalt thermal dehydrations, then is put into pitch and reacted by step 3
In tank, 140 DEG C are warming up to the speed of 20 DEG C/min under normal pressure, keeps the temperature 15-20min；After stopping heating, 0.9 part is sequentially added
Emulsifier and 130 parts of solvent naphthas, average rate are stirred to pitch and are completely dissolved, and ensure the pressure ＜ in retort in production process
0.15MPa；
Step 4 mixes the rubber composition obtained in step 1 with the pitch obtained in step 2 at 15-40 DEG C
Object presses 1:1 ratio is sent into blending tank, and sequentially adds 2.2 parts of tackifiers and 1.5 parts of stabilizers, then is stirred under constant speed
30-60min, and it is slowly added to 0.8 part of waterproofing agent while agitating；It is cooled to room temperature after stirring；
Mixture feeding grinder is ground by step 5, and control fineness of grind is less than 10 μm；It weighs after grinding packing
To obtain the final product.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment
All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification,
It can make many modifications and variations.These embodiments are chosen and specifically described to this specification, is in order to preferably explain the present invention
Principle and practical application, to enable skilled artisan to be best understood by and utilize the present invention.The present invention is only
It is limited by claims and its full scope and equivalent.
Claims (8)
1. a kind of waterproof roll adhesive, which is characterized in that including following raw material component：
100 parts of asphalt, 60-100 parts of rubber, 2-3 parts of rubber antioxidant, 20-30 parts of size, 1.5-2.2 parts of emulsifier,
220-280 parts of solvent naphtha, 2-5 parts of tackifier, 0.5-1.5 parts of waterproofing agent, 1-2 parts of stabilizer.
2. a kind of waterproof roll adhesive according to claim 1, which is characterized in that the rubber is natural rubber or conjunction
At the mixture of one or more of butyl rubber, neoprene, polyurethane rubber, lactoprene.
3. a kind of waterproof roll adhesive according to claim 1, which is characterized in that the solvent naphtha is gasoline, diformazan
The mixture of one or more of benzene or petroleum hydrocarbon.
4. a kind of waterproof roll adhesive according to claim 1, which is characterized in that the size be diesel oil, kerosene,
The mixture of one or more of light machine oil or turpentine oil.
5. a kind of waterproof roll adhesive according to claim 1, which is characterized in that the tackifier is modified phenolic resin
The mixture of one or more of fat, modified rosin resin or Petropols.
6. a kind of waterproof roll adhesive according to claim 1, which is characterized in that the waterproofing agent is nano-sized carbon silicic acid
One or more of salt compound combined polymerization waterproofing agent, silane coupled waterproofing agent, aluminate water-proof agent, higher fatty acids waterproofing agent
Mixture.
7. a kind of waterproof roll adhesive according to claim 1, which is characterized in that the stabilizer be antioxidant BHT,
The mixing of one or more of antioxidant 1010, antioxidant 4010, ultra-violet absorber UV-9, ultraviolet absorbent UV-531
Object.
8. a kind of preparation method of waterproof roll adhesive, which is characterized in that include the following steps：
Step 1 prepares each raw material according to recipe requirements；
Step 2 rubber, rubber antioxidant, size, suitable emulsifier and solvent naphtha is added in mixer, in temperature
Stop heating at 60-80 DEG C after insulated and stirred 15-30min, discharging is cooled to room temperature；
Dewatered asphalt first by 100 parts of asphalt thermal dehydrations, then is put into pitch retort by step 3
In, 140 DEG C are warming up to the speed of 20 DEG C/min under normal pressure, keeps the temperature 15-20min；After stopping heating, remaining breast is sequentially added
Agent and solvent naphtha, average rate are stirred to pitch and are completely dissolved, and ensure the pressure ＜ 0.15MPa in retort in production process；
Step 4, at 15-40 DEG C, by the rubber composition obtained in step 1 and the asphalt mixture obtained in step 2 by
1:1 ratio is sent into blending tank, and sequentially adds tackifier and stabilizer, then 30-60min is stirred under constant speed, and
Waterproofing agent is slowly added to while stirring；It is cooled to room temperature after stirring；
Mixture feeding grinder is ground by step 5, and control fineness of grind is less than 10 μm；Packing is weighed after grinding i.e.
.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810073080.1A CN108329891A (en) | 2018-01-25 | 2018-01-25 | A kind of waterproof roll adhesive and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810073080.1A CN108329891A (en) | 2018-01-25 | 2018-01-25 | A kind of waterproof roll adhesive and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108329891A true CN108329891A (en) | 2018-07-27 |
Family
ID=62926737
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810073080.1A Pending CN108329891A (en) | 2018-01-25 | 2018-01-25 | A kind of waterproof roll adhesive and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN108329891A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109251542A (en) * | 2018-08-16 | 2019-01-22 | 马鞍山市永固防水科技有限公司 | A kind of waterproof roll and preparation method thereof with compared with high-elongation |
| CN109762516A (en) * | 2019-01-21 | 2019-05-17 | 株洲加美乐素建材有限公司 | A kind of waterproof roll cement base adhesive pulvis and preparation method thereof |
| CN110003670A (en) * | 2019-03-25 | 2019-07-12 | 广东工业大学 | A kind of road hydrophobic maintenance sealing material and preparation method thereof |
| CN110791253A (en) * | 2019-11-22 | 2020-02-14 | 安徽喜宝高分子材料有限公司 | Preparation method of waterproof flame-retardant adhesive for elastic coiled material |
| CN113308127A (en) * | 2021-07-19 | 2021-08-27 | 安徽省奥佳建材有限公司 | Root-resistant asphalt waterproof coiled material |
| CN113528058A (en) * | 2021-06-16 | 2021-10-22 | 山西博润交通科学工程有限公司 | Desulfurized gypsum powder-based pavement water-based crack pouring adhesive and preparation method thereof |
| CN115340845A (en) * | 2022-09-15 | 2022-11-15 | 安徽光智科技有限公司 | Adhesive for finish machining of optical material and preparation method thereof |
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| CN105086932A (en) * | 2015-08-26 | 2015-11-25 | 王伟 | Adhesive for waterproof coils and preparation method thereof |
| CN106893540A (en) * | 2015-12-17 | 2017-06-27 | 天津市亘元科技发展有限公司 | A kind of high-temperature Resistance Adhesives |
| CN107216832A (en) * | 2017-06-16 | 2017-09-29 | 佛山赛威光电技术有限公司 | It is a kind of to consolidate epoxy adhesive and preparation method thereof soon |
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| CN105086932A (en) * | 2015-08-26 | 2015-11-25 | 王伟 | Adhesive for waterproof coils and preparation method thereof |
| CN106893540A (en) * | 2015-12-17 | 2017-06-27 | 天津市亘元科技发展有限公司 | A kind of high-temperature Resistance Adhesives |
| CN107216832A (en) * | 2017-06-16 | 2017-09-29 | 佛山赛威光电技术有限公司 | It is a kind of to consolidate epoxy adhesive and preparation method thereof soon |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109251542A (en) * | 2018-08-16 | 2019-01-22 | 马鞍山市永固防水科技有限公司 | A kind of waterproof roll and preparation method thereof with compared with high-elongation |
| CN109762516A (en) * | 2019-01-21 | 2019-05-17 | 株洲加美乐素建材有限公司 | A kind of waterproof roll cement base adhesive pulvis and preparation method thereof |
| CN110003670A (en) * | 2019-03-25 | 2019-07-12 | 广东工业大学 | A kind of road hydrophobic maintenance sealing material and preparation method thereof |
| CN110003670B (en) * | 2019-03-25 | 2021-03-30 | 广东工业大学 | Hydrophobic curing seal material for roads and preparation method thereof |
| CN110791253A (en) * | 2019-11-22 | 2020-02-14 | 安徽喜宝高分子材料有限公司 | Preparation method of waterproof flame-retardant adhesive for elastic coiled material |
| CN110791253B (en) * | 2019-11-22 | 2021-12-21 | 安徽喜宝高分子材料有限公司 | Preparation method of waterproof flame-retardant adhesive for elastic coiled material |
| CN113528058A (en) * | 2021-06-16 | 2021-10-22 | 山西博润交通科学工程有限公司 | Desulfurized gypsum powder-based pavement water-based crack pouring adhesive and preparation method thereof |
| CN113308127A (en) * | 2021-07-19 | 2021-08-27 | 安徽省奥佳建材有限公司 | Root-resistant asphalt waterproof coiled material |
| CN115340845A (en) * | 2022-09-15 | 2022-11-15 | 安徽光智科技有限公司 | Adhesive for finish machining of optical material and preparation method thereof |
| CN115340845B (en) * | 2022-09-15 | 2024-03-05 | 安徽光智科技有限公司 | Adhesive for finishing optical material and preparation method thereof |
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| PB01 | Publication | ||
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Application publication date: 20180727 |