CN104449381A - Composite emulsified asphalt waterproof coating and preparation method thereof - Google Patents
Composite emulsified asphalt waterproof coating and preparation method thereof Download PDFInfo
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- CN104449381A CN104449381A CN201410804105.2A CN201410804105A CN104449381A CN 104449381 A CN104449381 A CN 104449381A CN 201410804105 A CN201410804105 A CN 201410804105A CN 104449381 A CN104449381 A CN 104449381A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
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- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention relates to a composite emulsified asphalt waterproof coating and a preparation method thereof. The composite emulsified asphalt waterproof coating is prepared from the following raw materials in parts by weight: 150-220 parts of emulsified asphalt, 50-105 parts of a polymeric emulsion, 70-130 parts of inorganic powder, 0.5-2 parts of a stabilizer, 6-10 parts of a dispersant, 2-5 parts of a wetting agent, 1-3 parts of a thickener I, 1-3 parts of a thickener II, 2-7 parts of a defoaming agent and 15-40 parts of water. The invention further relates to a preparation method of the composite emulsified asphalt waterproof coating. The viscosity, strength, application property, solid content and storage stability of the emulsified asphalt waterproof coating are remarkably improved, and the cost is lowered to a great extent.
Description
Technical field
The present invention relates to a kind of water and milk asphalt waterproofing paint and preparation method thereof, be specifically related to a kind of organic/inorganic compound water and milk asphalt waterproofing paint and preparation method thereof.
Background technology
Waterproof paint is the important integral part of water-proof material, and the asphaltic base waterproof paint of China is divided into two classes according to construction temperature: hot-melt application type asphalt waterproofing paint and cold construction type waterproof paint.Wherein, cold construction type is divided into again solvent-borne type asphalt waterproofing paint and emulsified asphalt waterproofing coating.Hot-melting type asphalt waterproofing paint adopts scene to boil, and heat construction method produces a large amount of flue gas, not only easily presence of fire, scald accident, and the problems such as height that consume energy; There is atmospheric pollution in solvent-borne type asphalt waterproofing paint, easily occurs poisoning, the problems such as worker safety difference.Public environmental attitude is more and more stronger now, and emulsified asphalt waterproofing coating that is nontoxic, environmental protection has advantages such as can saving a large amount of solvent, pollution-free, easy construction, can construct on wet base, has become the development trend of asphalt waterproofing paint from now on.
At present, domestic emulsified asphalt waterproofing coating preparation method mainly contains two kinds, one is add polymer emulsion and auxiliary agent preparation after the emulsification by pitch, two is directly add mineral filler again by the basis of adding polymer emulsion and auxiliary agent after asphalt emulsification, but all not to the high speed dispersion process that mineral filler is carried out in advance, and lack concrete preparation technology, particularly do not use the auxiliary agent such as dispersion agent, wetting agent in advance inorganic powder to be carried out to the technique of high speed dispersion.These preparation methods have free settling, segregation, layering, Fen Shui, solid content is low, low, the easy trickling of viscosity, need construct a lot of dry all over, brushing after material soft, intensity is low, cannot walk at coating surface, glue the sticky wheel of pin, in coarse fineless and smooth, the coating of coating, dregs are many, paint film defect is many, and the prices of raw and semifnished materials are high causes the shortcomings such as cost increase.
Such as, prior art CN201310276812.4 discloses a kind of with cement generation chemically crosslinked with the waterproof paint of physics mortise and tenon, comprises the raw material of following parts by weight: synthetic rubber latex 20 ~ 50; Emulsified bitumen 20 ~ 50; Functional aid 0.5 ~ 2; Dispersion agent 0.5 ~ 2; Filler 20 ~ 40; Water 10 ~ 25.This waterproof paint directly adds the mode of filler owing to adopting, although employ dispersion agent, fillers dispersed is very poor, and easily reunite, precipitation, particle is very large; This waterproof paint typical mean solids content is 55.7% simultaneously, and Average Bond Strength is 0.51MPa, makes this waterproof paint film forming thickness, film quality undesirable, need construct a lot of times.CN201310416370.9 discloses thick matter waterproof paint of a kind of modified-high polymer water-latex type asphaltic base and preparation method thereof, this waterproof paint typical mean solids content is 67.3%, Average Bond Strength is 0.62MPa, makes this waterproof paint film forming thickness, film quality undesirable, need construct a lot of times.CN201310133075.2 discloses a kind of High-strength rubber asphalt waterproof paint and preparation method thereof, this waterproof paint is made up of emulsified bitumen, modified latex, filler etc., and its weight percent is: emulsified bitumen 55%-65%, modified latex 25%-35%, filler 5%-10%.This waterproof paint is also directly add filler, makes fillers dispersed very poor.This waterproof paint typical mean solids content is 60% simultaneously, and average tension set is 455%, makes this waterproof paint film forming thickness, film quality undesirable, and is difficult to adapt to rugged environment and weather.
Summary of the invention
Technical problem to be solved by this invention is, provides compound water and milk asphalt waterproofing paint that a kind of solid content is high, intensity is large, application property is good, stability in storage is good and preparation method thereof.
The technical scheme that the present invention solves the employing of its technical problem is:
A kind of Compound Water breast asphalt waterproofing paint of the present invention, be made up of the raw material of following parts by weight: emulsified bitumen 150 ~ 220 parts, polymer emulsion 50 ~ 105 parts, inorganic powder 70 ~ 130 parts, stablizer 0.5 ~ 2 part, dispersion agent 6 ~ 10 parts, wetting agent 2 ~ 5 parts, thickening material I 1 ~ 3 part, thickening material II 1 ~ 3 part, defoamer 2 ~ 7 parts, 15 ~ 40 parts, water.
Further, described emulsified bitumen is selected from the one in anionic emulsified bitumen, cationic emulsified bitumen, non ionic emulsified bitumen and zwitter-ion emulsified bitumen.
Further, described polymer emulsion is selected from one or more the mixture in styrene-acrylate emulsion, acrylic ester emulsion, acetate emulsion, styrene-butadiene latex, nitrile rubber, polychloroprene latex and natural rubber latex.
Further, described inorganic powder is one or more in light calcium carbonate powder, heavy calcium carbonate, talcum powder, wilkinite, kaolin, diatomite, titanium dioxide, silicon powder.
Further, described stablizer is calcium chloride.
Further, described dispersion agent is selected from one or more the mixture in glyceryl monostearate, ethylene group bis-stearamides, Tristearoylglycerol, vinyl bis-stearamides, polyoxyethylene glycol and fatty acid polyglycol ester.
Further, described wetting agent is selected from one or more the mixture in alkyl-sulphate, sulfonate, soap, fatty acid ester vitriol, carboxylic soap, phosphoric acid ester, polyxyethylated alkylphenol and polyoxyethylene aliphatic alcohol ether.
Further, described thickening material I is selected from one or more the mixture in Vltra tears, Xylo-Mucine, Natvosol, polyacrylamide and polyvinyl alcohol; Described thickening material II is selected from one or more the mixture in hydrophobically modified oxyethyl group polyether polyols with reduced unsaturation, hydrophobically modified polyether polymer and hydrophobically modified amino polymer.
Further, described defoamer is selected from silicon ether copolymer, one or more the mixture in organo-siloxane, polyethers and polyether modified siloxane.
The preparation method of a kind of Compound Water breast asphalt waterproofing paint of the present invention, comprises the following steps:
(1) first add inorganic powder, dispersion agent, wetting agent, stablizer, defoamer and water, then high speed dispersor with rotating speed for 1500 ~ 2000r/min, high speed dispersion 30 ~ 40 minutes;
(2) then add emulsified bitumen, high speed dispersor with rotating speed for 100 ~ 500r/min, low rate mixing 5 ~ 10 minutes;
(3) then add polymer emulsion, high speed dispersor with rotating speed for 100 ~ 500r/min, low rate mixing 5 ~ 10 minutes;
(4) then add thickening material I, high speed dispersor with rotating speed for 100 ~ 500r/min, low rate mixing 5 ~ 15 minutes;
(5) finally add thickening material II, high speed dispersor with rotating speed for 100 ~ 500r/min, low rate mixing 5 ~ 15 minutes.
The raw material composition of the compound water and milk asphalt waterproofing paint of the present invention and preparation method adopt the pretreatment technology of inorganic powder, make to be prepared into water and milk bituminous composition fillers dispersed good, do not reunite, do not precipitate, coating is fine and smooth in dregs; Significantly improve the viscosity of water and milk bituminous composition, intensity, application property, solid content, stability in storage, and significantly reduce costs.
The compound water and milk asphalt waterproofing paint of the present invention compared with prior art, has following beneficial effect:
(1) solid content is more than 70%, and most high solids content can reach 77%, not containing organic solvent.
(2) dope viscosity is at more than 90KU, is up to 125KU high, and elevation construction does not trickle, and constructs and can meet the requirements of thickness less than 3 times.
(3) good stability, can 50 DEG C within two months, do not emanate, precipitate.
(4) dry rear intensity is high.
(5) the not sticky pin of coating surface walking, not sticky wheel.
(6) coating exquisiteness, film zero defect.
The waterproof paint of the present invention can be used alone or reinforcement use, also can with asphalt water-proof coiled material compound use.
Embodiment
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
By 30 parts, water, dispersion agent 6 parts, wetting agent 3 parts, stablizer 2 parts, inorganic powder 70 parts, defoamer 2 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 2000r/min, high-speed stirring 40 minutes; Then add emulsified bitumen 220 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 500r/min, low rate mixing 10 minutes; Then add polymer emulsion 60 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 500r/min, low rate mixing 10 minutes; Then add thickening material I 1.5 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 500r/min, low rate mixing 10 minutes; Finally add thickening material II 3 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 500r/min, low rate mixing 15 minutes; Discharging afterwards, obtains organic/inorganic compound water and milk asphalt waterproofing paint.Embodiment 1 compound water and milk asphalt waterproofing paint performance index detect as shown in table 1:
Table 1-embodiment 1 organic/inorganic compound water and milk asphalt waterproofing paint detected result
Embodiment 2
By 15 parts, water, dispersion agent 8 parts, wetting agent 5 parts, stablizer 2 parts, inorganic powder 77 parts, defoamer 2.5 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 1500r/min, high-speed stirring 40 minutes; Then add emulsified bitumen 150 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 100r/min, low rate mixing 10 minutes; Then add polymer emulsion 80 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 100r/min, low rate mixing 10 minutes; Then add thickening material I 1.5 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 100r/min, low rate mixing 10 minutes; Finally add thickening material II 3 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 100r/min, low rate mixing 15 minutes; Discharging afterwards, obtains organic/inorganic compound water and milk asphalt waterproofing paint.Embodiment 2 compound water and milk asphalt waterproofing paint performance index detect as shown in table 2:
Table 2-embodiment 2 organic/inorganic compound water and milk asphalt waterproofing paint detected result
Embodiment 3
By 40 parts, water, dispersion agent 10 parts, wetting agent 2 parts, stablizer 0.5 part, inorganic powder 130 parts, defoamer 7 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 2000r/min, high-speed stirring 30 minutes; Then add emulsified bitumen 200 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 500r/min, low rate mixing 5 minutes; Then add polymer emulsion 105 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 500r/min, low rate mixing 5 minutes; Then add thickening material I 1 part, the Special dispersing machine with dentation dispersion impeller take rotating speed as 500r/min, low rate mixing 5 minutes; Finally add thickening material II 1 part, the Special dispersing machine with dentation dispersion impeller take rotating speed as 500r/min, low rate mixing 5 minutes; Discharging afterwards, obtains organic/inorganic compound water and milk asphalt waterproofing paint.Embodiment 3 compound water and milk asphalt waterproofing paint performance index detect as shown in table 3:
Table 3-embodiment 3 organic/inorganic compound water and milk asphalt waterproofing paint detected result
Embodiment 4
By 20 parts, water, dispersion agent 9 parts, wetting agent 4 parts, stablizer 1 part, inorganic powder 100 parts, defoamer 5 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 1800r/min, high-speed stirring 40 minutes; Then add emulsified bitumen 200 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 300r/min, low rate mixing 10 minutes; Then add polymer emulsion 90 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 300r/min, low rate mixing 10 minutes; Then add thickening material I 2 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 300r/min, low rate mixing 10 minutes; Finally add thickening material II 2 parts, the Special dispersing machine with dentation dispersion impeller take rotating speed as 300r/min, low rate mixing 10 minutes; Discharging afterwards, obtains organic/inorganic compound water and milk asphalt waterproofing paint.Embodiment 4 compound water and milk asphalt waterproofing paint performance index detect as shown in table 4:
Table 4-embodiment 4 organic/inorganic compound water and milk asphalt waterproofing paint detected result
The present invention is not limited to above-mentioned example, within the scope of the Knowledge Attainments of this area industry technology personnel deposit, also can come according to proportioning amplification of the present invention, according to the requirement of different technological standards and different construction environments, corresponding adjustment is made to technical scheme, to obtain the most suitable water and milk asphalt waterproofing paint of performance.
Claims (10)
1. a compound water and milk asphalt waterproofing paint, it is characterized in that, be made up of the raw material of following parts by weight: emulsified bitumen 150 ~ 220 parts, polymer emulsion 50 ~ 105 parts, inorganic powder 70 ~ 130 parts, stablizer 0.5 ~ 2 part, dispersion agent 6 ~ 10 parts, wetting agent 2 ~ 5 parts, thickening material I 1 ~ 3 part, thickening material II 1 ~ 3 part, defoamer 2 ~ 7 parts, 15 ~ 40 parts, water.
2. compound water and milk asphalt waterproofing paint according to claim 1, is characterized in that, described emulsified bitumen is selected from the one in anionic emulsified bitumen, cationic emulsified bitumen, non ionic emulsified bitumen and zwitter-ion emulsified bitumen.
3. compound water and milk asphalt waterproofing paint according to claim 1, it is characterized in that, described polymer emulsion is selected from one or more the mixture in styrene-acrylate emulsion, acrylic ester emulsion, acetate emulsion, styrene-butadiene latex, nitrile rubber, polychloroprene latex and natural rubber latex.
4. compound water and milk asphalt waterproofing paint according to claim 1, is characterized in that, described inorganic powder is one or more in light calcium carbonate powder, heavy calcium carbonate, talcum powder, wilkinite, kaolin, diatomite, titanium dioxide, silicon powder.
5. compound water and milk asphalt waterproofing paint according to claim 1, is characterized in that, described stablizer is calcium chloride.
6. compound water and milk asphalt waterproofing paint according to claim 1, it is characterized in that, described dispersion agent is selected from one or more the mixture in glyceryl monostearate, ethylene group bis-stearamides, Tristearoylglycerol, vinyl bis-stearamides, polyoxyethylene glycol and fatty acid polyglycol ester.
7. compound water and milk asphalt waterproofing paint according to claim 1, it is characterized in that, described wetting agent is selected from one or more the mixture in alkyl-sulphate, sulfonate, soap, fatty acid ester vitriol, carboxylic soap, phosphoric acid ester, polyxyethylated alkylphenol and polyoxyethylene aliphatic alcohol ether.
8. compound water and milk asphalt waterproofing paint according to claim 1, it is characterized in that, described thickening material I is selected from one or more the mixture in Vltra tears, Xylo-Mucine, Natvosol, polyacrylamide and polyvinyl alcohol; Described thickening material II is selected from one or more the mixture in hydrophobically modified oxyethyl group polyether polyols with reduced unsaturation, hydrophobically modified polyether polymer and hydrophobically modified amino polymer.
9. compound water and milk asphalt waterproofing paint according to claim 1, it is characterized in that, described defoamer is selected from silicon ether copolymer, one or more the mixture in organo-siloxane, polyethers and polyether modified siloxane.
10. a preparation method for the compound water and milk asphalt waterproofing paint as described in one of claim 1 ~ 9, is characterized in that, comprise the following steps:
(1) first add inorganic powder, dispersion agent, wetting agent, stablizer, defoamer and water, then high speed dispersor with rotating speed for 1500 ~ 2000r/min, high speed dispersion 30 ~ 40 minutes;
(2) then add emulsified bitumen, high speed dispersor with rotating speed for 100 ~ 500r/min, low rate mixing 5 ~ 10 minutes;
(3) then add polymer emulsion, high speed dispersor with rotating speed for 100 ~ 500r/min, low rate mixing 5 ~ 10 minutes.
(4) then add thickening material I, high speed dispersor with rotating speed for 100 ~ 500r/min, low rate mixing 5 ~ 15 minutes.
(5) finally add thickening material II, high speed dispersor with rotating speed for 100 ~ 500r/min, low rate mixing 5 ~ 15 minutes.
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2014
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Application publication date: 20150325 |