CN109135475A - A kind of preparation method of high-efficient purification air coating - Google Patents

A kind of preparation method of high-efficient purification air coating Download PDF

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Publication number
CN109135475A
CN109135475A CN201810882496.8A CN201810882496A CN109135475A CN 109135475 A CN109135475 A CN 109135475A CN 201810882496 A CN201810882496 A CN 201810882496A CN 109135475 A CN109135475 A CN 109135475A
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China
Prior art keywords
preparation
powder
purification air
efficient purification
coating
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CN201810882496.8A
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Chinese (zh)
Inventor
王志忠
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Dewitt Coatings Ltd
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Dewitt Coatings Ltd
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Priority to CN201810882496.8A priority Critical patent/CN109135475A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04—Homopolymers or copolymers of esters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D103/00—Coating compositions based on starch, amylose or amylopectin or on their derivatives or degradation products
    • C09D103/02—Starch; Degradation products thereof, e.g. dextrin
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D189/00—Coating compositions based on proteins; Coating compositions based on derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/24—Acids; Salts thereof
    • C08K3/26—Carbonates; Bicarbonates
    • C08K2003/265—Calcium, strontium or barium carbonate
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/38—Boron-containing compounds
    • C08K2003/387—Borates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses a kind of preparation methods of high-efficient purification air coating, soyabean protein powder is modified by ultramicro grinding and is mixed with wheat flour, rice bran, tourmaline, aethiops vegetabilis, water charcoal etc. are placed in settling tank later after settling, after being impregnated using strong acid, it is crushed, after being dispersed in suitable water, granulation is blended with modified powder, silica, hydroxylated cellulose；Suitable adjuvant is mixed and obtains the coating with after the mixing and ball millings such as lotion, pitch adjustment coating viscosity.The present invention is utilized using soyabean protein powder and wheat flour, rice bran as raw material, the purification particle for cooperating tourmaline, aethiops vegetabilis, water charcoal to prepare, the coating of preparation has preferable water resistance good with stability, actively adsorbs toxic gas, while carrying out resolution process part formaldehyde.

Description

A kind of preparation method of high-efficient purification air coating
Technical field
The invention belongs to coating manufacture fields, and in particular to a kind of preparation method of high-efficient purification air coating.
Background technique
The dark brown complex mixture that pitch is made of the hydrocarbon and its non metallic derivatives of different molecular weight, It is one kind of high viscosity organic liquid, is in a liquid state, surface is in black, dissolves in carbon disulfide.Pitch be it is a kind of waterproof and dampproof and Corrosion-resistant organic cementitious material.
Tourmaline is again tourmaline by translated name, often shows multiple color on same crystal, is its main characteristics.Tourmaline Be collection " natural negative ion device ", " far infrared transmitter ", " cell activation teacher ", " blood vessel scavenger ", " ecological water reorganizer ", Numerous good reputations such as " life jewel " are.Therefore, tourmaline not only becomes the friend of human health, also becomes and improves people The dazzling scientific and technological nova of one of quality of the life brings Gospel for the health of the mankind.
Summary of the invention
The present invention provides a kind of preparation method of high-efficient purification air coating, and the present invention is utilized with soyabean protein powder and wheat Flour, rice bran are raw material, and purification particle prepared by cooperation tourmaline, aethiops vegetabilis, water charcoal, the coating of preparation has preferable water-fast Property is good with stability, actively adsorbs toxic gas, while carrying out resolution process part formaldehyde.
The present invention is achieved by the following technical solutions:
A kind of preparation method of high-efficient purification air coating, which comprises the following steps:
(1) modified soy-bean protein powder and wheat flour, rice bran
A) disperse soyabean protein powder and wheat flour, rice bran in after ultramicro crushing treatment after mixing 10 times of water In；
B) modifying agent is added into mixed-powder solution sufficiently to be reacted at a temperature of 40-90 DEG C, then is dried under vacuum to constant weight, Grinding, sieving obtain modified powder；
(2) preparation of particle is purified
A) tourmaline, aethiops vegetabilis, water charcoal and sepiolite and attapulgite are respectively placed in settling tank, are settled 24 hours；
B) will be after the mixture filtering after sedimentation and dry, it is impregnated using strong acid solution, filters, is born after dipping The particle for carrying strong acid, is ground into powder；
C) step (1) resulting modified powder is dissolved in suitable water, smashed powder is evenly dispersed in solution In, obtain mixed liquor；
D) it after being spray-dried mixed liquor, is blended, is granulated with silica, hydroxylated cellulose；
(3) mixing of adjuvant
It weighs suitable anti-settling agent, reactive diluent, diatomite, defoaming agent and levelling agent mixing and suitable water dispenser tool low speed is added Stirring to solid is completely dissolved；
(4) coating is prepared
Acrylic acid ester emulsion is mixed with pitch and is added in agitator tank, after being filtered after mixing evenly, is then added to ball mill Carry out dispersion grinding with step (2) resulting particle, be added step (3) resulting auxiliary material and kaolin, precipitated calcium carbonate again into Row fine design, high speed ball milling is until system is uniform, and moderate viscosity is to get high-efficient purification air coating.
The dry protein content of the wheat gluten protein is 75-85%.
The granularity of the ultra micro treated powder is 1400-2000 mesh.
The modifying agent is dodecyl trimethyl ammonium chloride.
The defoaming agent is organic silicon defoaming agent, mineral oil defoaming agent or combinations thereof.
The bitumen is natural minerals pitch or natural rock asphalt.
The invention has the advantages that
Soyabean protein powder is modified by ultramicro grinding and is mixed with wheat flour, rice bran by the present invention, later by tourmaline, sea Algae charcoal, water charcoal etc. are placed in settling tank after sedimentation, after being impregnated using strong acid, are crushed to it, are dispersed in suitable water In after, granulation is blended with modified powder, silica, hydroxylated cellulose；Suitable adjuvant is mixed and is mixed with lotion, pitch etc. The coating is obtained after ball milling adjustment coating viscosity.The present invention passes through using soyabean protein powder and wheat flour, rice bran as raw material After modification, it is added in coating and develops coating for wall surface product, improves the benefit of soyabean protein powder and wheat flour With value and economic value, rice bran is recycled, due to the presence of chain alkyl in modifying agent, so that mixed-powder has parent Oiliness, while one layer of hydrophobic organic monomer is coated on surface, the coating of preparation has preferable water resistance and stability good, electrically Using repulsive interaction between charge after stone, aethiops vegetabilis, water charcoal compounding, it is uniformly dispersed in the solution, keeps nano powder to the maximum extent The independent dispersity of body particle in the solution, while after being handled using strong acid, absorption aperture can be exposed to greatest extent, Toxic gas is actively adsorbed, it is dynamic that air stream can be driven, while carrying out resolution process part formaldehyde, use acrylic acid ester emulsion and day Right pitch is dispersed, therefore coating does not contain noxious material, and the present invention, which is utilized with soyabean protein powder and wheat flour, rice bran, is The coating of raw material, purification particle prepared by cooperation tourmaline, aethiops vegetabilis, water charcoal, preparation has preferable water resistance and stability It is good, toxic gas is actively adsorbed, while carrying out resolution process part formaldehyde.
Specific embodiment
A kind of preparation method of high-efficient purification air coating, which comprises the following steps:
(1) modified soy-bean protein powder and wheat flour, rice bran
A) disperse soyabean protein powder and wheat flour, rice bran in after ultramicro crushing treatment after mixing 10 times of water In；
B) modifying agent is added into mixed-powder solution sufficiently to be reacted at a temperature of 40-90 DEG C, then is dried under vacuum to constant weight, Grinding, sieving obtain modified powder；
(2) preparation of particle is purified
A) tourmaline, aethiops vegetabilis, water charcoal and sepiolite and attapulgite are respectively placed in settling tank, are settled 24 hours；
B) will be after the mixture filtering after sedimentation and dry, it is impregnated using strong acid solution, filters, is born after dipping The particle for carrying strong acid, is ground into powder；
C) step (1) resulting modified powder is dissolved in suitable water, smashed powder is evenly dispersed in solution In, obtain mixed liquor；
D) it after being spray-dried mixed liquor, is blended, is granulated with silica, hydroxylated cellulose；
(3) mixing of adjuvant
It weighs suitable anti-settling agent, reactive diluent, diatomite, defoaming agent and levelling agent mixing and suitable water dispenser tool low speed is added Stirring to solid is completely dissolved；
(4) coating is prepared
Acrylic acid ester emulsion is mixed with pitch and is added in agitator tank, after being filtered after mixing evenly, is then added to ball mill Carry out dispersion grinding with step (2) resulting particle, be added step (3) resulting auxiliary material and kaolin, precipitated calcium carbonate again into Row fine design, high speed ball milling is until system is uniform, and moderate viscosity is to get high-efficient purification air coating.
The dry protein content of the wheat gluten protein is 75-85%.
The granularity of the ultra micro treated powder is 1400-2000 mesh.
The modifying agent is dodecyl trimethyl ammonium chloride.
The defoaming agent is organic silicon defoaming agent, mineral oil defoaming agent or combinations thereof.
The bitumen is natural minerals pitch or natural rock asphalt.

Claims (6)

1. a kind of preparation method of high-efficient purification air coating, which comprises the following steps:
(1) modified soy-bean protein powder and wheat flour, rice bran
A) disperse soyabean protein powder and wheat flour, rice bran in after ultramicro crushing treatment after mixing 10 times of water In；
B) modifying agent is added into mixed-powder solution sufficiently to be reacted at a temperature of 40-90 DEG C, then is dried under vacuum to constant weight, Grinding, sieving obtain modified powder；
(2) preparation of particle is purified
A) tourmaline, aethiops vegetabilis, water charcoal and sepiolite and attapulgite are respectively placed in settling tank, are settled 24 hours；
B) will be after the mixture filtering after sedimentation and dry, it is impregnated using strong acid solution, filters, is born after dipping The particle for carrying strong acid, is ground into powder；
C) step (1) resulting modified powder is dissolved in suitable water, smashed powder is evenly dispersed in solution In, obtain mixed liquor；
D) it after being spray-dried mixed liquor, is blended, is granulated with silica, hydroxylated cellulose；
(3) mixing of adjuvant
It weighs suitable anti-settling agent, reactive diluent, diatomite, defoaming agent and levelling agent mixing and suitable water dispenser tool low speed is added Stirring to solid is completely dissolved；
(4) coating is prepared
Acrylic acid ester emulsion is mixed with pitch and is added in agitator tank, after being filtered after mixing evenly, is then added to ball mill Carry out dispersion grinding with step (2) resulting particle, be added step (3) resulting auxiliary material and kaolin, precipitated calcium carbonate again into Row fine design, high speed ball milling is until system is uniform, and moderate viscosity is to get high-efficient purification air coating.
2. a kind of preparation method of high-efficient purification air coating according to claim 1, which is characterized in that the wheat gluten protein Dry protein content be 75-85%.
3. a kind of preparation method of high-efficient purification air coating according to claim 1, which is characterized in that treated for the ultra micro The granularity of powder is 1400-2000 mesh.
4. a kind of preparation method of high-efficient purification air coating according to claim 1, which is characterized in that the modifying agent is 12 Alkyl trimethyl ammonium chloride.
5. a kind of preparation method of high-efficient purification air coating according to claim 1, which is characterized in that the defoaming agent is to have Machine silicon class defoaming agent, mineral oil defoaming agent or combinations thereof.
6. a kind of preparation method of high-efficient purification air coating according to claim 1, which is characterized in that the bitumen is day Right mineral bitumen or natural rock asphalt.
CN201810882496.8A 2018-08-06 2018-08-06 A kind of preparation method of high-efficient purification air coating Pending CN109135475A (en)

Priority Applications (1)

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CN201810882496.8A CN109135475A (en) 2018-08-06 2018-08-06 A kind of preparation method of high-efficient purification air coating

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810882496.8A CN109135475A (en) 2018-08-06 2018-08-06 A kind of preparation method of high-efficient purification air coating

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CN109135475A true CN109135475A (en) 2019-01-04

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101081933A (en) * 2007-06-06 2007-12-05 湖南大学 Environment-friendly type split mending material for polymer emulsion inorganic powder and nano material composite modified emulsified asphalt
CN101148338A (en) * 2007-09-14 2008-03-26 陈宪宏 Environmental protection inorganic powder material and polymer composite modified emulsification asphalt grouting material
CN104449381A (en) * 2014-12-19 2015-03-25 锦州东方雨虹建筑材料有限责任公司 Composite emulsified asphalt waterproof coating and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101081933A (en) * 2007-06-06 2007-12-05 湖南大学 Environment-friendly type split mending material for polymer emulsion inorganic powder and nano material composite modified emulsified asphalt
CN101148338A (en) * 2007-09-14 2008-03-26 陈宪宏 Environmental protection inorganic powder material and polymer composite modified emulsification asphalt grouting material
CN104449381A (en) * 2014-12-19 2015-03-25 锦州东方雨虹建筑材料有限责任公司 Composite emulsified asphalt waterproof coating and preparation method thereof

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Application publication date: 20190104