CN106317528A - Novel high-performance anticorrosion waterproof environment-friendly material - Google Patents
Novel high-performance anticorrosion waterproof environment-friendly material Download PDFInfo
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- CN106317528A CN106317528A CN201610800657.5A CN201610800657A CN106317528A CN 106317528 A CN106317528 A CN 106317528A CN 201610800657 A CN201610800657 A CN 201610800657A CN 106317528 A CN106317528 A CN 106317528A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L11/00—Compositions of homopolymers or copolymers of chloroprene
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/0427—Coating with only one layer of a composition containing a polymer binder
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2311/00—Characterised by the use of homopolymers or copolymers of chloroprene
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2427/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
- C08J2427/02—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
- C08J2427/12—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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Abstract
The invention discloses a novel high-performance anticorrosion waterproof environment-friendly material, made from, by weight, 20-45 parts of chloroprene rubber, 20-30 parts of polyvinyl chloride resin, 10-15 parts of acrylonitrile-butadiene-styrene resin, 6-10 parts of zinc oxide, 3-8 parts of benzoic acid, 10-15 parts of white carbon black, 4-9 parts of butylated hydroxytoluene, 4-9 parts of zinc soap, 3-8 parts of dihydropyridine, 2-8 parts of a photostabilizer, and 8-15 parts of a water-based waterproof. The novel high-performance anticorrosion waterproof environment-friendly material provided herein is made mainly from the widely used rubber and resin, the composition is simple, the materials are easy to obtain, and the prepared novel material has good corrosion resistance and waterproof property, also has good heat resistance, light resistance and aging resistance, and is widely applicable to various severe environments; the invention also provides a preparation method of the novel high-performance anticorrosion waterproof environment-friendly material, the material is prepared by blending vulcanized rubber with resin and adding aids, and the method is simple to perform, safe, environment-friendly, pollution-free, low in cost and widely applicable.
Description
Technical field
The present invention relates to anticorrosion waterproof material technical field, particularly relate to a kind of high-performance anticorrosion water-proof environmental protection new material.
Background technology
Waterproof material is the general designation of the material of impermeable, seepage and erosion, the building enclosure rainwater to be prevented of building, snow
Water and the infiltration of subsoil water；Dampness, steam and other harmful gass in air to be prevented and the erosion of liquid；Separation structure is wanted
Prevent oozing of plumbing from turning over.Waterproof material is various in style on the market, and one type is asphalt water-proof coiled material, is mainly used for building
Body of wall, roofing and tunnel, highway, refuse landfill etc., play and resist extraneous rainwater, the one of subsoil water seepage can be rolled up
Bent become web-like flexible building material product, be connected as ne-leakage between engineering foundation with building, be the of whole engineering waterproofing
One barrier, plays vital effect to whole engineering, and it is all light poisonous substance that Colophonium is contained within anthracene, phenanthrene, pyridine etc., high temperature bar
Use under part, photochemical reaction can be caused under action of ultraviolet radiation, it is understood that there may be potential safety hazard, the high property of one that the present invention proposes
The problems referred to above can be can effectively solve the problem that by anticorrosion water-proof environmental protection new material.
Summary of the invention
The invention aims to solve shortcoming present in prior art, and a kind of high-performance anticorrosion proposed is waterproof
Environmental friendly material.
A kind of high-performance anticorrosion water-proof environmental protection new material, including following raw material: neoprene 20-45 part, polychlorostyrene
Vinyl 20-30 part, acrylonitrile-butadiene-styrene resin 10-15 part, zinc oxide 6-10 part, benzoic acid 3-8 part, Linesless charcoal
Black 10-15 part, dibenzylatiooluene 4-9 part, zinc soap 4-9 part, dihydropyridine 3-8 part, light stabilizer 2-8 part, Waterproof
Agent 8-15 part.
Preferably, described a kind of high-performance anticorrosion water-proof environmental protection new material, including following raw material: neoprene
24-42 part, Corvic 24-28 part, acrylonitrile-butadiene-styrene resin 12-14 part, zinc oxide 7-9 part, benzene first
Acid 4-6 part, white carbon 11-13 part, dibenzylatiooluene 5-8 part, zinc soap 5-7 part, dihydropyridine 4-6 part, light stabilizer 3-6
Part, watery water-proofing agent 9-13 part.
Preferably, described a kind of high-performance anticorrosion water-proof environmental protection new material, including following raw material: neoprene 32
Part, Corvic 28 parts, acrylonitrile-butadiene-styrene resin 14 parts, zinc oxide 8 parts, 5 parts of benzoic acid, white carbon 12
Part, dibenzylatiooluene 6 parts, zinc soap 7 parts, dihydropyridine 5 parts, light stabilizer 4 parts, watery water-proofing agent 12 parts.
Preferably, described neoprene, Corvic, the weight ratio of acrylonitrile-butadiene-styrene resin are 2-
3:2:1。
Preferably, described light stabilizer is carbon black.
Preferably, described watery water-proofing agent is PM-4700.
The preparation method of a kind of high-performance anticorrosion water-proof environmental protection new material, comprises the following steps:
S1, the neoprene of described proportion is joined in rubber vulcanizing tank, add the zinc oxide of described proportion, benzoic acid, high
Temperature 150-170 DEG C, vulcanizes 4-8h, standby；
S2, the acrylonitrile-butadiene-styrene resin of described proportion is joined in crucible melting stove, high temperature 230-260 DEG C,
Heating 1-2h, treats that it melts completely；
S3, by near for the temperature in step S2 170-190 DEG C, add the Corvic of described proportion, heated and stirred 1-2h,
Obtain hybrid resin A；
S4, will in step S1 sulfuration after rubber, hybrid resin A join in super mixer, be simultaneously introduced described proportion
White carbon, dibenzylatiooluene, zinc soap, dihydropyridine, light stabilizer, at 110-130 DEG C, mix 25-45min, obtain mixed
Compound B；
S5, joining in calender by mixture B, compacting extension becomes surface uniform, and thickness is the lamellar new material C of 3-6mm；
S6, watery water-proofing agent is uniformly sprayed on the two sides of new material C, naturally dry, to obtain final product.
A kind of high-performance anticorrosion water-proof environmental protection new material that the present invention proposes, it is main for selecting and using rubber and resin widely
Wanting raw material, composition is simple, raw material is easy to get, and the new material prepared has good anticorrosion, water resistance, has good simultaneously
Heat-resisting, fast light, ageing resistace, the anticorrosion water-proof environmental protection new material prepared can be widely applied in various adverse circumstances,
The invention allows for the preparation method of a kind of high-performance anticorrosion water-proof environmental protection new material, by after the vulcanization of rubber with resin high temperature
Addition auxiliary agent being blended be prepared, technological operation is simple, safe and environment-friendly, pollution-free, low cost, can obtain and extensively apply.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is explained orally further.
Embodiment one
A kind of high-performance anticorrosion water-proof environmental protection new material that the present invention proposes, including following raw material: neoprene 28 parts,
Corvic 20 parts, acrylonitrile-butadiene-styrene resin 10 parts, zinc oxide 7 parts, 5 parts of benzoic acid, white carbon 10 parts,
Dibenzylatiooluene 5 parts, zinc soap 4 parts, dihydropyridine 4 parts, light stabilizer 3 parts, watery water-proofing agent 8 parts.
Its preparation method, comprises the following steps:
S1, the neoprene of described proportion is joined in rubber vulcanizing tank, add the zinc oxide of described proportion, benzoic acid, high
Temperature 165 DEG C, vulcanizes 5h, standby；
S2, the acrylonitrile-butadiene-styrene resin of described proportion is joined in crucible melting stove, high temperature 245 DEG C, heating
1.5h, treats that it melts completely；
S3, by near for the temperature in step S2 180 DEG C, add the Corvic of described proportion, heated and stirred 1.5h, obtain mixed
Resin A；
S4, will in step S1 sulfuration after rubber, hybrid resin A join in super mixer, be simultaneously introduced described proportion
White carbon, dibenzylatiooluene, zinc soap, dihydropyridine, light stabilizer, at 120 DEG C, mix 35min, obtain mixture B；
S5, joining in calender by mixture B, compacting extension becomes surface uniform, and thickness is the lamellar new material C of 5mm；
S6, watery water-proofing agent is uniformly sprayed on the two sides of new material C, naturally dry, to obtain final product.
Embodiment two
A kind of high-performance anticorrosion water-proof environmental protection new material that the present invention proposes, including following raw material: neoprene 30 parts,
Corvic 24 parts, acrylonitrile-butadiene-styrene resin 12 parts, zinc oxide 6 parts, 4 parts of benzoic acid, white carbon 11 parts,
Dibenzylatiooluene 6 parts, zinc soap 5 parts, dihydropyridine 3 parts, light stabilizer 2 parts, watery water-proofing agent 10 parts.
Its preparation method, comprises the following steps:
S1, the neoprene of described proportion is joined in rubber vulcanizing tank, add the zinc oxide of described proportion, benzoic acid, high
Temperature 155 DEG C, vulcanizes 7h, standby；
S2, the acrylonitrile-butadiene-styrene resin of described proportion is joined in crucible melting stove, high temperature 250 DEG C, heating
1.2h, treats that it melts completely；
S3, by near for the temperature in step S2 190 DEG C, add the Corvic of described proportion, heated and stirred 1h, obtain mixing
Resin A；
S4, will in step S1 sulfuration after rubber, hybrid resin A join in super mixer, be simultaneously introduced described proportion
White carbon, dibenzylatiooluene, zinc soap, dihydropyridine, light stabilizer, at 115 DEG C, mix 40min, obtain mixture B；
S5, joining in calender by mixture B, compacting extension becomes surface uniform, and thickness is the lamellar new material C of 4mm；
S6, watery water-proofing agent is uniformly sprayed on the two sides of new material C, naturally dry, to obtain final product.
Embodiment three
A kind of high-performance anticorrosion water-proof environmental protection new material that the present invention proposes, including following raw material: neoprene 42 parts,
Corvic 30 parts, acrylonitrile-butadiene-styrene resin 15 parts, zinc oxide 10 parts, 8 parts of benzoic acid, white carbon 15
Part, dibenzylatiooluene 9 parts, zinc soap 8 parts, dihydropyridine 8 parts, light stabilizer 7 parts, watery water-proofing agent 15 parts.
Its preparation method, comprises the following steps:
S1, the neoprene of described proportion is joined in rubber vulcanizing tank, add the zinc oxide of described proportion, benzoic acid, high
Temperature 170 DEG C, vulcanizes 4h, standby；
S2, the acrylonitrile-butadiene-styrene resin of described proportion is joined in crucible melting stove, high temperature 230 DEG C, heating
2h, treats that it melts completely；
S3, by near for the temperature in step S2 185 DEG C, add the Corvic of described proportion, heated and stirred 1.2h, obtain mixed
Resin A；
S4, will in step S1 sulfuration after rubber, hybrid resin A join in super mixer, be simultaneously introduced described proportion
White carbon, dibenzylatiooluene, zinc soap, dihydropyridine, light stabilizer, at 125 DEG C, mix 30min, obtain mixture B；
S5, joining in calender by mixture B, compacting extension becomes surface uniform, and thickness is the lamellar new material C of 3mm；
S6, watery water-proofing agent is uniformly sprayed on the two sides of new material C, naturally dry, to obtain final product.
Embodiment four
A kind of high-performance anticorrosion water-proof environmental protection new material that the present invention proposes, including following raw material: neoprene 35 parts,
Corvic 26 parts, acrylonitrile-butadiene-styrene resin 13 parts, zinc oxide 8 parts, 6 parts of benzoic acid, white carbon 12 parts,
Dibenzylatiooluene 7 parts, zinc soap 6 parts, dihydropyridine 5 parts, light stabilizer 4 parts, watery water-proofing agent 11 parts.
Its preparation method, comprises the following steps:
S1, the neoprene of described proportion is joined in rubber vulcanizing tank, add the zinc oxide of described proportion, benzoic acid, high
Temperature 150 DEG C, vulcanizes 8h, standby；
S2, the acrylonitrile-butadiene-styrene resin of described proportion is joined in crucible melting stove, high temperature 260 DEG C, heating
1h, treats that it melts completely；
S3, by near for the temperature in step S2 170 DEG C, add the Corvic of described proportion, heated and stirred 2h, obtain mixing
Resin A；
S4, will in step S1 sulfuration after rubber, hybrid resin A join in super mixer, be simultaneously introduced described proportion
White carbon, dibenzylatiooluene, zinc soap, dihydropyridine, light stabilizer, at 130 DEG C, mix 25min, obtain mixture B；
S5, joining in calender by mixture B, compacting extension becomes surface uniform, and thickness is the lamellar new material C of 6mm；
S6, watery water-proofing agent is uniformly sprayed on the two sides of new material C, naturally dry, to obtain final product.
Embodiment five
A kind of high-performance anticorrosion water-proof environmental protection new material that the present invention proposes, including following raw material: neoprene 40 parts,
Corvic 28 parts, acrylonitrile-butadiene-styrene resin 14 parts, zinc oxide 9 parts, 7 parts of benzoic acid, white carbon 13 parts,
Dibenzylatiooluene 8 parts, zinc soap 7 parts, dihydropyridine 7 parts, light stabilizer 6 parts, watery water-proofing agent 13 parts.
Its preparation method, comprises the following steps:
S1, the neoprene of described proportion is joined in rubber vulcanizing tank, add the zinc oxide of described proportion, benzoic acid, high
Temperature 160 DEG C, vulcanizes 6h, standby；
S2, the acrylonitrile-butadiene-styrene resin of described proportion is joined in crucible melting stove, high temperature 240 DEG C, heating
1.8h, treats that it melts completely；
S3, by near for the temperature in step S2 175 DEG C, add the Corvic of described proportion, heated and stirred 1.8h, obtain mixed
Resin A；
S4, will in step S1 sulfuration after rubber, hybrid resin A join in super mixer, be simultaneously introduced described proportion
White carbon, dibenzylatiooluene, zinc soap, dihydropyridine, light stabilizer, at 110 DEG C, mix 45min, obtain mixture B；
S5, joining in calender by mixture B, compacting extension becomes surface uniform, and thickness is the lamellar new material C of 4.5mm；
S6, watery water-proofing agent is uniformly sprayed on the two sides of new material C, naturally dry, to obtain final product.
The following is after the anticorrosion water-proof environmental protection new material prepared in above-mentioned five groups of embodiments is carried out water resistance test
Result, water is sprinkled upon on obtained waterproof material, measures with waterproof tester after 3h, the following is measurement result:
| Embodiment | Embodiment one | Embodiment two | Embodiment three | Embodiment four | Embodiment five |
| Seepage rate | 0.8‰ | 0.55‰ | 0.73‰ | 1.1‰ | 0.68‰ |
From the above results, the new material water resistance that the present invention prepares is good, the new material prepared in embodiment two
Waterproof effect is optimal.Present component is simple, raw material is easy to get, and the new material prepared not only has good anticorrosion, waterproof
Performance, has good heat-resisting, fast light, ageing resistace simultaneously, can be widely applied in various adverse circumstances, and the present invention proposes
Preparation method, technological operation is simple, safe and environment-friendly, pollution-free, and low cost can obtain and extensively apply.
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto,
Any those familiar with the art in the technical scope that the invention discloses, according to technical scheme and
Inventive concept equivalent or change in addition, all should contain within protection scope of the present invention.
Claims (7)
1. a high-performance anticorrosion water-proof environmental protection new material, it is characterised in that include following raw material: neoprene 20-
45 parts, Corvic 20-30 part, acrylonitrile-butadiene-styrene resin 10-15 part, zinc oxide 6-10 part, benzoic acid
3-8 part, white carbon 10-15 part, dibenzylatiooluene 4-9 part, zinc soap 4-9 part, dihydropyridine 3-8 part, light stabilizer 2-8
Part, watery water-proofing agent 8-15 part.
A kind of high-performance anticorrosion water-proof environmental protection new material the most according to claim 1, it is characterised in that include following weight
Part raw material: neoprene 24-42 part, Corvic 24-28 part, acrylonitrile-butadiene-styrene resin 12-14 part, oxygen
Change zinc 7-9 part, benzoic acid 4-6 part, white carbon 11-13 part, dibenzylatiooluene 5-8 part, zinc soap 5-7 part, dihydropyridine 4-6
Part, light stabilizer 3-6 part, watery water-proofing agent 9-13 part.
A kind of high-performance anticorrosion water-proof environmental protection new material the most according to claim 1, it is characterised in that include following weight
Part raw material: neoprene 32 parts, Corvic 28 parts, acrylonitrile-butadiene-styrene resin 14 parts, zinc oxide 8 parts,
5 parts of benzoic acid, white carbon 12 parts, dibenzylatiooluene 6 parts, zinc soap 7 parts, dihydropyridine 5 parts, light stabilizer 4 parts, aqueous are anti-
12 parts of water preparation.
A kind of high-performance anticorrosion water-proof environmental protection new material the most according to claim 1, it is characterised in that described neoprene rubber
Glue, Corvic, the weight ratio of acrylonitrile-butadiene-styrene resin are 2-3:2:1.
A kind of high-performance anticorrosion water-proof environmental protection new material the most according to claim 1, it is characterised in that described light stabilizer
For carbon black.
A kind of high-performance anticorrosion water-proof environmental protection new material the most according to claim 1, it is characterised in that described Waterproof
Agent is PM-4700.
7. the preparation method of a high-performance anticorrosion water-proof environmental protection new material, it is characterised in that comprise the following steps:
S1, the neoprene of described proportion is joined in rubber vulcanizing tank, add the zinc oxide of described proportion, benzoic acid, high
Temperature 150-170 DEG C, vulcanizes 4-8h, standby；
S2, the acrylonitrile-butadiene-styrene resin of described proportion is joined in crucible melting stove, high temperature 230-260 DEG C,
Heating 1-2h, treats that it melts completely；
S3, by near for the temperature in step S2 170-190 DEG C, add the Corvic of described proportion, heated and stirred 1-2h,
Obtain hybrid resin A；
S4, will in step S1 sulfuration after rubber, hybrid resin A join in super mixer, be simultaneously introduced described proportion
White carbon, dibenzylatiooluene, zinc soap, dihydropyridine, light stabilizer, at 110-130 DEG C, mix 25-45min, obtain mixed
Compound B；
S5, joining in calender by mixture B, compacting extension becomes surface uniform, and thickness is the lamellar new material C of 3-6mm；
S6, watery water-proofing agent is uniformly sprayed on the two sides of new material C, naturally dry, to obtain final product.
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| CN106938569A (en) * | 2017-04-24 | 2017-07-11 | 张红星 | A kind of processing method of water-proof anti-corrosion coiled material |
| CN107793773A (en) * | 2017-11-07 | 2018-03-13 | 广西小草信息产业有限责任公司 | A kind of high-performance anti-corrosion water-proof environmental protection new material |
| WO2019214126A1 (en) * | 2018-05-08 | 2019-11-14 | 淄博鸣桐环保技术研发有限公司 | Novel high-performance anti-corrosion and waterproof environment-friendly material |
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Application publication date: 20170111 |