CN108328639A - 一种碳酸钙骨棒状纳米颗粒的制备方法 - Google Patents
一种碳酸钙骨棒状纳米颗粒的制备方法 Download PDFInfo
- Publication number
- CN108328639A CN108328639A CN201810116524.5A CN201810116524A CN108328639A CN 108328639 A CN108328639 A CN 108328639A CN 201810116524 A CN201810116524 A CN 201810116524A CN 108328639 A CN108328639 A CN 108328639A
- Authority
- CN
- China
- Prior art keywords
- feed liquid
- deionized water
- calcium oxide
- method described
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 42
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 19
- 210000000988 bone and bone Anatomy 0.000 title claims abstract description 15
- 239000002105 nanoparticle Substances 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims abstract description 6
- 239000007788 liquid Substances 0.000 claims abstract description 120
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 78
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims abstract description 53
- 239000000292 calcium oxide Substances 0.000 claims abstract description 53
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims abstract description 53
- 239000008367 deionised water Substances 0.000 claims abstract description 50
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 50
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 50
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 39
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 39
- 239000002245 particle Substances 0.000 claims abstract description 26
- 239000004094 surface-active agent Substances 0.000 claims abstract description 21
- 238000000703 high-speed centrifugation Methods 0.000 claims abstract description 19
- 239000007921 spray Substances 0.000 claims abstract description 17
- 238000003756 stirring Methods 0.000 claims abstract description 17
- 238000002604 ultrasonography Methods 0.000 claims abstract description 17
- JBIROUFYLSSYDX-UHFFFAOYSA-M benzododecinium chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 JBIROUFYLSSYDX-UHFFFAOYSA-M 0.000 claims description 18
- 238000005507 spraying Methods 0.000 claims description 18
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims description 16
- 238000005119 centrifugation Methods 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 13
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- FFDGPVCHZBVARC-UHFFFAOYSA-N N,N-dimethylglycine Chemical compound CN(C)CC(O)=O FFDGPVCHZBVARC-UHFFFAOYSA-N 0.000 description 28
- 239000007789 gas Substances 0.000 description 19
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 14
- 239000000463 material Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229910021532 Calcite Inorganic materials 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 2
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
- 239000000920 calcium hydroxide Substances 0.000 description 2
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 2
- 229910001424 calcium ion Inorganic materials 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- GHYMZHDODSTPJO-UHFFFAOYSA-N 2-(dodecylazaniumyl)-2-methylpropanoate Chemical group CCCCCCCCCCCCNC(C)(C)C(O)=O GHYMZHDODSTPJO-UHFFFAOYSA-N 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 238000005255 carburizing Methods 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 239000011258 core-shell material Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- -1 papermaking Substances 0.000 description 1
- 230000001869 rapid Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000000565 sealant Substances 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
- C01F11/181—Preparation of calcium carbonate by carbonation of aqueous solutions and characterised by control of the carbonation conditions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/002—Physical properties
- C08K2201/004—Additives being defined by their length
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Glanulating (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
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CN201810116524.5A CN108328639B (zh) | 2018-01-28 | 2018-01-28 | 一种碳酸钙骨棒状纳米颗粒的制备方法 |
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CN201810116524.5A CN108328639B (zh) | 2018-01-28 | 2018-01-28 | 一种碳酸钙骨棒状纳米颗粒的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN108328639A true CN108328639A (zh) | 2018-07-27 |
CN108328639B CN108328639B (zh) | 2020-04-28 |
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CN201810116524.5A Active CN108328639B (zh) | 2018-01-28 | 2018-01-28 | 一种碳酸钙骨棒状纳米颗粒的制备方法 |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101475199A (zh) * | 2009-01-21 | 2009-07-08 | 山东海泽纳米材料有限公司 | 一种碳酸钙纳米串珠的工业制备方法 |
CN102219250A (zh) * | 2011-03-28 | 2011-10-19 | 济南大学 | 一种纳米硫酸钡颗粒的制备方法 |
CN103351016A (zh) * | 2013-06-27 | 2013-10-16 | 浙江理工大学 | 一种制备球粒状多孔碳酸钙颗粒的方法 |
EP2796412A1 (en) * | 2013-04-24 | 2014-10-29 | Università Del Salento - Dipartimento Di Ingegneria Dell'Innovazione | Synthesis of nano-sized CaCO3 particles by spray dryer |
CN106587125A (zh) * | 2016-11-30 | 2017-04-26 | 华东理工大学 | 一种轻质碳酸钙的制备方法 |
-
2018
- 2018-01-28 CN CN201810116524.5A patent/CN108328639B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101475199A (zh) * | 2009-01-21 | 2009-07-08 | 山东海泽纳米材料有限公司 | 一种碳酸钙纳米串珠的工业制备方法 |
CN102219250A (zh) * | 2011-03-28 | 2011-10-19 | 济南大学 | 一种纳米硫酸钡颗粒的制备方法 |
EP2796412A1 (en) * | 2013-04-24 | 2014-10-29 | Università Del Salento - Dipartimento Di Ingegneria Dell'Innovazione | Synthesis of nano-sized CaCO3 particles by spray dryer |
CN103351016A (zh) * | 2013-06-27 | 2013-10-16 | 浙江理工大学 | 一种制备球粒状多孔碳酸钙颗粒的方法 |
CN106587125A (zh) * | 2016-11-30 | 2017-04-26 | 华东理工大学 | 一种轻质碳酸钙的制备方法 |
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CN108328639B (zh) | 2020-04-28 |
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PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
TA01 | Transfer of patent application right | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20200318 Address after: Yi Nong Zhen Dong Lian Cun (Dong Wan Cun), Xiaoshan District, Hangzhou City, Zhejiang Province Applicant after: HANGZHOU XIONGYING FINE CHEMICAL Co.,Ltd. Address before: 315400 room 1, 315, international business center, China Plastics City, Ningbo, Zhejiang, Yuyao Applicant before: NINGBO PLASTIC METAL PRODUCT Co.,Ltd. |
|
GR01 | Patent grant | ||
GR01 | Patent grant | ||
CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: Yi Nong Zhen Dong Lian Cun (Dong Wan Cun), Xiaoshan District, Hangzhou City, Zhejiang Province Patentee after: Hangzhou Eagle New Material Co.,Ltd. Address before: Yi Nong Zhen Dong Lian Cun (Dong Wan Cun), Xiaoshan District, Hangzhou City, Zhejiang Province Patentee before: Hangzhou Eagle New Material Co.,Ltd. Address after: Yi Nong Zhen Dong Lian Cun (Dong Wan Cun), Xiaoshan District, Hangzhou City, Zhejiang Province Patentee after: Hangzhou Eagle New Material Co.,Ltd. Address before: Yi Nong Zhen Dong Lian Cun (Dong Wan Cun), Xiaoshan District, Hangzhou City, Zhejiang Province Patentee before: HANGZHOU XIONGYING FINE CHEMICAL Co.,Ltd. |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method for calcium carbonate bone rod-shaped nanoparticles Effective date of registration: 20231231 Granted publication date: 20200428 Pledgee: Zhejiang Xiaoshan Rural Commercial Bank Co.,Ltd. Yinong Branch Pledgor: Hangzhou Eagle New Material Co.,Ltd. Registration number: Y2023330003162 |