CN108310024A - The preparation method of bouvardin tree plum acid and its application in treating disease - Google Patents
The preparation method of bouvardin tree plum acid and its application in treating disease Download PDFInfo
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- CN108310024A CN108310024A CN201810297956.0A CN201810297956A CN108310024A CN 108310024 A CN108310024 A CN 108310024A CN 201810297956 A CN201810297956 A CN 201810297956A CN 108310024 A CN108310024 A CN 108310024A
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
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- A61K9/00—Medicinal preparations characterised by special physical form
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- A61K9/0034—Urogenital system, e.g. vagina, uterus, cervix, penis, scrotum, urethra, bladder; Personal lubricants
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- A61K9/0046—Ear
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- A61K9/00—Medicinal preparations characterised by special physical form
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
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Abstract
The preparation method of bouvardin tree plum acid and its application in treating disease, by weight percentage, it is characterised in that：Include the following steps：1）Effective component extracting：2）Distillation separation：3）Make alum aqueous solution：4）Second distillation purifies：5）, stand purifying.Present invention tree plum acid has the function of the killing of strength to pathogenic microorganism, there is the effect of antibiotic, there is no the toxic side effect of antibiotic, there is no any injury to body tissue cell, especially to treating because of virus, germ, fungus-caused vaginitis, tympanitis, skin disease are significant in efficacy, safe and reliable, efficient and convenient, uneasy to recur.
Description
Technical field
The present invention relates to a kind of preparation methods of bouvardin tree plum acid, especially use red bayberry tree trunk, pass through heat of gasification
Effective component extracting is solved, is prepared into bouvardin tree plum acid, and be applied in the treatment of relevant disease.
Background technology
Microorganism is with mankind's symbiotic co-existence altogether according to only a few causes human health the microorganism of disease, and people are them
Referred to as harmful microorganism, including virus, germ, fungi etc..Human body has powerful immune system, innately has to harmful micro-
Function is blocked, inhibited and is killed in the invasion of biology, is escort for the health of itself.But because undesirable element makes human immunity
When hypofunction, harmful microorganism will take advantage of a weak point, corrode, injuring our body, cause various diseases,
At this moment artificial it must be just interfered, inhibited and killed, human body is enable to get well, and prevent further to infect,
The injury of bigger is caused to crowd, the birth of antibiotic is that human health makes tremendous contribution.
Antibiotic sterilization mainly by interfering the synthesis of bacteria cell wall, changes the modes such as bacterium inner metabolism to realize
, but this process also damages not guilty normal tissue cell simultaneously, and here it is so-called toxic side effects.Abuse of antibiotics causes
The damage of liver, kidney, heart also leads to the drug resistance of flora imbalance, antibiotic-associated diarrhea and bacterium, increases by two double infections
Dye or even delay treatment lead to the generation of the serious adverse reactions such as death.So the use to antibiotic is more careful.Therefore it studies
The anti-infection drug of novel non-toxic side effect is imperative, natural plants antibiotic be exactly extracted out of plant it is effective at
Point, including alkaloids, flavonoids, protein-based, organic acid and phenolic compound etc., mainly destruction germ cell film knot
Structure has the function that kill or inhibition, is not injured substantially to human tissue cell.
Invention content
In view of the foregoing drawbacks, it the purpose of the present invention is to provide a kind of raw material with red bayberry tree trunk, is carried using gasification and pyrolysis
The preparation method for taking tree plum acid and its otitis, vaginitis, the application on skin disease in the treatment.
The technical scheme is that be accomplished by the following way：The preparation method of bouvardin tree plum acid, with weight
Percentages are measured, are included the following steps：
1）, effective component extracting：Red bayberry tree trunk is ground into graininess, is carried out dehydrating with microwave drying equipment, makes particle
Water content control be placed in gasification and pyrolysis stove between 18%-32%, then by dewatered particle, heated sealed, when in stove
When particle temperature reaches 264 DEG C, in stove under conditions of anoxic particle start spontaneous combustion decomposition volatilize smog, by smog collect into
Row is cooling to obtain condensable liquid, when stove endoparticle temperature reaches 550 DEG C, stops collecting, that is, collects particle autoignition temperature and exist
Condensed fluid between 264-550 DEG C is tree plum acid stoste；The cooling temperature is controlled at 45 DEG C or less；
2）Distillation separation：Tree plum acid stoste is placed in distiller, air-distillation is carried out, when vapo(u)rizing temperature rises to 100 DEG C
Starting to collect distillate, the distillate of initial collection takes out, and takes out the 5-10% that fractional dose is total input amount, continues distillation and collects,
Stop heating when vapo(u)rizing temperature rises to 102 DEG C, distillation terminates, and the distillate that this section is collected into is effective distillate；
3）Make alum aqueous solution：Pure water 92%, alum 8% is taken to stir, dissolve fully becomes alum aqueous solution；
4）Second distillation purifies：It takes 80% effective distillate that 20% alum aqueous solution is added, is sufficiently stirred, it will be mixed after stirring
It closes in liquid merging container, is taken out after standing 48 hours of storage and carry out second distillation, collect tree plum acid and extract pure liquid；
5）Stand purifying：By in the distillate merging container through second distillation, purifying 180 days are stood under 26-45 DEG C of environment；I.e.
For bouvardin tree plum acid finished product material liquid.
A kind of application of bouvardin tree plum acid in treating vaginitis：By bouvardin tree plum acid finished product material liquid
With pure water dilute 6 times, i.e., 1:6 it is dilute match, be divided in dilute with long in spray boom vagina special-purpose sprayer with liquid, usage use
Amount：Spray lance is opened, vagina is inserted into, pressure spray makes liquid spray into vagina in misty, and once a day, every time under spray 20,3 days are one
The course for the treatment of, three course for the treatment of symptoms disappear.
A kind of application in otitis in the treatment of bouvardin tree plum acid：Tree plum acid is purified into stoste, 8% alum is added
The aqueous solution of content, additional proportion 1:1, the tree plum acid alum drops that will have been configured is divided in spare in trickle irrigation bottle, usage use
Amount, first fester in duct is sucked out with dry cotton swab, then tree plum acid alum drops is instilled, and daily drop 2-3 times drips 3-4 drops every time,
5 days courses for the treatment of, three course for the treatment of recoveries from illness.
A kind of application of bouvardin tree plum acid in treating skin disease：Tree plum acid purification stoste is dispensed into spray bottle
Interior, skin site of disease is wiped in spray for several times in one day, is gradually improved, and adheres to curing using one month.
Present invention tree plum acid has the function of the killing of strength to pathogenic microorganism, has the effect of antibiotic, without antibiosis
The toxic side effect of element does not have any injury, especially to treating because of virus, germ, fungus-caused vagina to body tissue cell
Inflammation, tympanitis, skin disease are significant in efficacy, safe and reliable, efficient and convenient, uneasy to recur.
Specific implementation mode
A kind of preparation method of bouvardin tree plum acid includes the following steps by weight percentage：
1, effective component extracting：Red bayberry tree trunk is ground into graininess, is carried out dehydrating with microwave drying equipment, makes particle
Water content control is placed between 18%-32%, then by dewatered particle in gasification and pyrolysis stove, heated sealed, when in stove
Grain temperature is when reaching 264 DEG C, and particle starts spontaneous combustion decomposition and volatilizes smog under conditions of anoxic in stove, and smog is collected and is carried out
It is cooling to obtain condensable liquid, when stove endoparticle temperature reaches 550 DEG C, stop collecting, that is, collects particle autoignition temperature and exist
Condensed fluid between 264-550 DEG C is tree plum acid stoste；The cooling temperature is controlled at 45 DEG C or less；
2, distillation separation：Tree plum acid stoste is placed in distiller, air-distillation is carried out, when vapo(u)rizing temperature rises to 100 DEG C
Starting to collect distillate, the distillate of initial collection takes out, and takes out the 5-10% that fractional dose is total input amount, continues distillation and collects,
Stop heating when vapo(u)rizing temperature rises to 102 DEG C, distillation terminates, and the distillate that this section is collected into is effective distillate；
3, alum aqueous solution is made：Pure water 92%, alum 8% is taken to stir, dissolve fully becomes alum aqueous solution；
4, second distillation purifies：It takes 80% effective distillate that 20% alum aqueous solution is added, is sufficiently stirred, it will be mixed after stirring
It closes in liquid merging container, is taken out after standing 48 hours of storage and carry out second distillation, collect tree plum acid and extract pure liquid；
5, purifying is stood：By in the distillate merging container through second distillation, purifying 180 days are stood under 26-45 DEG C of environment；I.e.
For bouvardin tree plum acid finished product material liquid.
Embodiment 1：
Application of the bouvardin tree plum acid in treating vaginitis liquid.
1, tree plum acid pure liquid pure water is diluted 6 times, i.e., 1:6 dilute match.
2, the tree plum acid of configuration is divided in long in spray boom vagina special-purpose sprayer.
3, accommodation：Bacterial vaginitis, monilial vaginitis, trichomonas vaginitis, senile vahinitis, leukorrhea
It is abnormal, pruritus vulvue etc..
4, usage and dosage：User makees supine posture, and padded buttocks opens spray lance, is inserted into vagina, and pressure spray makes liquid be in mist
Shape sprays into vagina.Once a day, every time under spray 20.
5, case 1：Mrs Cheng 69 years old, suffers from vaginitis half a year, and vaginal fluid is more, with shouting pain, pruritus vulvue unbearably,
It is unable to leave the bed, has eaten a period of time medicine and do not taken effect, using Shu Meisuan gynaecology spray, itch mitigation, was used in conjunction several days pain at that time
Symptom disappears, and secretion does not have yet, all restore normally, to get up and plant vegetables lowerly.
6, case 2：Miss Wu 35 years old, suffers from trichomonal vaginitis, and vaginal fluid increases, and is in purulence, and yellow green has stink,
Introitus and external genital itch, urinary tract have an infection, frequent micturition, urgent urination, odynuria, and vagina uses 0.75% Metrogel, takes first nitre
Azoles drug, unsatisfactory curative effect, and drug response is serious occur that flushing is red, and impatience of having palpitation, abdominal pain is perspired, use tree plum acid after drug withdrawal instead
Spray was mitigated using first day itch, and secretion gradually reduces after three days, and stink disappears, and vagina has the discharge of bean curd slag specimen foreign matter.
Half a month is used continuously, symptom completely disappears, not smelly, do not itch bitterly,, and urine is normal, dark and gloomy complexion switch to it is ruddy, it is long on the face
Small pox also Lock-out.
Embodiment 2：
The application in otitis drug in the treatment of bouvardin tree plum acid.
1, bouvardin tree plum acid purifies stoste, enters the aqueous solution of 8% alum content, additional proportion 1:1.
2, the tree plum acid alum drops configured, is divided in spare in trickle irrigation bottle.
3, first fester in duct is sucked out with dry cotton swab for dosage, then tree plum acid alum drops is instilled, daily drop 2-3 times,
Drop 3-4 drops every time.
4, case 1, Lee, man, 40 years old, main cause auris dextra was suppurated 10 years repeatedly, and once used a variety of auristilla are not cured, was checked left
Ear drum membrane is perforated, and external auditory canal has purulent secretion.It is diagnosed as otitis media purulenta chronica.It is fully recovered within 5 days with tree plum acid alum drops.
5, case 2, used as a personal name in ancient times, man, 47 years old, because swimming causes ear discomfort before 6 years, after gradually there is hydrops, suppurate, ear
Ring, Hearing, used antibiotic are showed no with the treatment of steroid hormone drug mixed aqueous solution.After use instead tree plum acid alum
Drops is fully recovered for 15 days, is never recurred over 5 years.
Embodiment 3：
Application of the bouvardin tree plum acid in treating skin disease.
1, in bouvardin tree plum acid stoste packing spray bottle.
2, application range：Tinea pedis, the tinea manuum, herpes zoster, wart, acne, dermapostasis, eczema of scrotum, pruitus, reproduction
Device bleb.It is clinical
3, clinical case 1：Chen, female, 44 years old, tinea pedis bacterium infection instep, redness, nigrescence, shinny, pain is incomparable, can not wear
Shoes take medicine and play antibiotic, lose recession.It is wiped afterwards with tree plum acid spray, one for several times, gradually improves, and adheres to using one month thoroughly
It cures, Chen does not take other any auxiliary treatments over the course for the treatment of.
4, clinical case 2；Jiang, man, 59 years old, suffer from eczema of scrotum it is more when, in Shanghai, Kan Liaojijia hospitals can not all eradicate,
Helpless Jiangsu Danyang of going back home looks for elder brother to treat, and brother is local famous physician, which has given him one bottle of tree plum acid spray, spray first
It is secondary just to feel very refreshing, it sprays several times, wet place's drying, scratchy disappearance is adhered to thoroughly curing using a period of time, in the past few years never
Recurrence.
5, clinical case 3：Certain, man 45 years old, suffers from the tinea manuum for many years, and itch decortication is continuous, is brought to life and is greatly not easy to hardship
It is angry, seek medical advice and medicine everywhere be exactly control it is bad, it is front and back to take more than 50,000 yuan, with thoroughly being cured after tree plum acid spray, restore as before.
Traditional Chinese Medicine, strawberry tree have antibacterial, anti-inflammatory, convergence and other effects, are widely used, and tree plum acid is to take heat of gasification
The process means such as solution, purifying, conversion effectively extract numerous active factors acidic aqueous solutions from red bayberry tree trunk, and the liquid is to harmful
Pathogenic microorganism has the killing function of strength, and without any side effects, especially in treatment because virus, germ, fungi cause
Various skin diseases, tympanitis, vaginitis it is significant in efficacy, it is securely and reliably, efficient and convenient.
Bouvardin tree plum acid has the effect of antibiotic, but the not harm of antibiotic on treatment relevant disease,
There is no any injury to body tissue cell while killing harmful bacteria.
Claims (4)
1. the preparation method of bouvardin tree plum acid, by weight percentage, it is characterised in that：Include the following steps：
1）, effective component extracting：Red bayberry tree trunk is ground into graininess, is carried out dehydrating with microwave drying equipment, makes particle
Water content control be placed in gasification and pyrolysis stove between 18%-32%, then by dewatered particle, heated sealed, when in stove
When particle temperature reaches 264 DEG C, in stove under conditions of anoxic particle start spontaneous combustion decomposition volatilize smog, by smog collect into
Row is cooling to obtain condensable liquid, when stove endoparticle temperature reaches 550 DEG C, stops collecting, that is, collects particle autoignition temperature and exist
Condensed fluid between 264-550 DEG C is tree plum acid stoste；The cooling temperature is controlled at 45 DEG C or less；
2）, distillation separation：Tree plum acid stoste is placed in distiller, air-distillation is carried out, when vapo(u)rizing temperature rises to 100 DEG C
Starting to collect distillate, the distillate of initial collection takes out, and takes out the 5-10% that fractional dose is total input amount, continues distillation and collects,
Stop heating when vapo(u)rizing temperature rises to 102 DEG C, distillation terminates, and the distillate that this section is collected into is effective distillate；
3）, make alum aqueous solution：Pure water 92%, alum 8% is taken to stir, dissolve fully becomes alum aqueous solution；
4）, second distillation purification：It takes 80% effective distillate that 20% alum aqueous solution is added, is sufficiently stirred, after stirring
Mixed liquor is placed in container, is taken out after standing 48 hours of storage and is carried out second distillation, is collected tree plum acid and is extracted pure liquid；
5）, stand purifying：By in the distillate merging container through second distillation, purifying 180 days are stood under 26-45 DEG C of environment；
As bouvardin tree plum acid finished product material liquid.
2. a kind of application of bouvardin tree plum acid according to claim 1 in treating vaginitis, it is characterised in that：
By bouvardin tree plum acid finished product material liquid with pure water dilute 6 times, i.e., 1:6 it is dilute match, be divided in dilute with long with liquid
In spray boom vagina special-purpose sprayer, usage and dosage：Spray lance is opened, vagina is inserted into, pressure spray makes liquid spray into vagina in misty, often
It is primary, and every time under spray 20,3 days as a treatment course, three course for the treatment of symptoms disappear.
3. a kind of application in otitis in the treatment of bouvardin tree plum acid according to claim 1, it is characterised in that：
Tree plum acid is purified into stoste, the aqueous solution of 8% alum content, additional proportion 1 is added:1, the tree plum acid alum configured is dripped
Agent is divided in spare in trickle irrigation bottle, usage and dosage, and first fester in duct is sucked out with dry cotton swab, then will set plum acid alum drops
It instills, daily drop 2-3 times, drips 3-4 drops, 5 days courses for the treatment of, three course for the treatment of recoveries from illness every time.
4. a kind of application of bouvardin tree plum acid according to claim 1 in treating skin disease：Tree plum acid is carried
In pure stoste packing spray bottle, skin site of disease is wiped in spray for several times in one day, is gradually improved, and adheres to curing using one month.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112426415A (en) * | 2020-10-29 | 2021-03-02 | 张士杰 | Production process of biological skin sterilizing and itching relieving repairing agent |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105131984A (en) * | 2015-07-07 | 2015-12-09 | 大连民族大学 | Continuous reproduction technology using biomass wastes and waste liquid |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105131984A (en) * | 2015-07-07 | 2015-12-09 | 大连民族大学 | Continuous reproduction technology using biomass wastes and waste liquid |
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| Title |
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| 卢辛成等: "木醋液的制备、精制与应用研究进展", 《林产化学与工业》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112426415A (en) * | 2020-10-29 | 2021-03-02 | 张士杰 | Production process of biological skin sterilizing and itching relieving repairing agent |
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Application publication date: 20180724 |