Chinese herbal medicine anticreep shampoo and preparation method thereof
Technical field
Present invention relates particularly to a kind of Chinese herbal medicine anticreep shampoo and preparation method thereof.
Background technology
Shampoo is essential hair shampoo article in life, and a good shampoo should at least meet claimed below:
(1) easy to use, it is easily spreadable, easy to rinse and do not stay adhesive residue;(2) good foaming, anti-dandruff performance, there is dandruff and dirt
When object, fine and close and abundant foam can be also generated;(3) wet comb resistance is small, and cardability is good after doing;(4) conditioning agent deposit appropriateness, no
It will produce visible residue;(5) safe, mild to hair, scalp, it is non-stimulated to eye;(6) fragrance is pure and fresh, happy, fragrance retention
It is good;(7) natural moist, hairy root nourishing, health are glossy;(8) it has good stability.Since modern society's life, work rhythm are fast, pressure
Power is big, and alopecia problem more becomes the big problem of puzzlement people, therefore consumer is when select shampoo, remove it is traditional it is anti-dandruff,
Moisturizing, treatment oil, profit are sent out, are disposable outer, and more people are inclined to use Anti-hair loss effect shampoo outstanding.Hair washing product currently on the market
Huge number, class difference are also bigger.If selection is improper, harmful substance can be caused to remain in head the excessive degreasing of scalp
Skin, and then scalp is caused to expand, irritation itch is generated, to aggravate alopecia, baldness and hair quality damage.
Chinese herbal medicine paste shampoo is the most prominent to Anti-hair loss effect, even if but most of brand shampoo contains in the market
Chinese herbal medicine, but it is limited to the extraction of active ingredient in Chinese herbal medicine, i.e., can only extract active ingredient 50-60% in Chinese herbal medicine, carry
Take rate low;Drug effect is caused to reduce, the waste of medicinal material.The present invention can reach carrying to 90% or more Chinese herbal medicine effective ingredients
It takes.The present invention selects ginger, Radix Astragali, Rhizoma Gastrodiae, Radix Salviae Miltiorrhizae, windproof tasteless Chinese medicine according to Chinese medicine combination principle, and it is anti-efficiently to extract Chinese medicine
De- ingredient, scalp absorptivity is high, has the function of Anti-hair loss, improves hair follicle, is strengthen the hair, hair tonic, moist, moisturizing, anti-dandruff.
Invention content
The present invention provides a kind of Chinese herbal medicine anticreep shampoo and preparation method thereof.The present invention adopts the following technical scheme that:
A kind of Chinese herbal medicine anticreep shampoo, including following raw materials are prepared:It is ginger, Radix Astragali, Rhizoma Gastrodiae, Radix Salviae Miltiorrhizae, windproof.
A kind of Chinese herbal medicine anticreep shampoo, including following weight parts raw material are prepared:0.2-0.8 parts of gingers, 0.5-1.5
Part Radix Astragali, 0.5-1.5 parts of Rhizoma Gastrodiaes, 0.3-0.9 parts of Radix Salviae Miltiorrhizaes, 0.4-1.2 parts windproof, 15-40 parts of surfactants, 3-10 parts of moisturizings
The dosage of agent, 0.5-1.5 parts of cationic conditioning agents, 0.6-1.8 parts of thickeners, water, the water is ginger, Radix Astragali, Rhizoma Gastrodiae, pellet
20-26 times of ginseng, windproof total weight.
A kind of Chinese herbal medicine anticreep shampoo, including following weight parts raw material are prepared:0.2-0.8 parts of gingers, 0.5-1.5
Part Radix Astragali, 0.5-1.5 parts of Rhizoma Gastrodiaes, 0.3-0.9 parts of Radix Salviae Miltiorrhizaes, 0.4-1.2 parts windproof, 15-40 parts of surfactants, 3-10 parts of moisturizings
Agent, 0.5-1.5 parts of cationic conditioning agents, 0.6-1.8 parts of thickeners, the 1-5 parts of hair care factors, the dosage of the water is ginger, Huang
20-26 times of stilbene, Rhizoma Gastrodiae, Radix Salviae Miltiorrhizae, windproof total weight.
Heretofore described cationic conditioning agent is dodecyl benzene sulfonic acid, Polyquaternium-10, polyquaternium -39, Guar
It is one or more in glue hydroxypropyl-trimethyl ammonium chloride.The cationic conditioning agent is preferably Polyquaternium-10 and guar gum
Hydroxypropyl-trimethyl ammonium chloride is (1-2) in mass ratio:The mixture of (1-2).
Heretofore described thickener is carbomer.The carbomer is preferably Acritamer 940.
Heretofore described surfactant is Cocoamidopropyl betaine, laureth sodium sulfovinate, PEG-150
Distearate, glycol distearate are (1-3) in mass ratio:(1-3):(2-4):1 mixture.
Heretofore described moisturizer is one kind in glycerine, panthenol, seed mucilage or the seed mucilage of modification.Described kind
The preparation method of sub- mucus is as follows:12- is added in 0.1-0.5kg S.Przewalskii Maxims grass seed, the small Chinese herbaceous peony grass seeds of 0.2-0.6kg
In 30kg water, it is warming up to 40-60 DEG C, is that 100-300 revs/min of condition stirs 3-6 hours in 40-60 DEG C, rotating speed, with 3000-
10000 revs/min of rotating speeds centrifuge 25-50 minutes, centrifuged supernatant are collected, by supernatant in 0.02-0.06MPa, 40-60 DEG C of items
Part is concentrated into 0.5-1kg, obtains seed mucilage.The preparation method of the modified seed mucilage is as follows:By the sweet western mouse of 0.1-0.5kg
The small Chinese herbaceous peony grass seed of tail grass seed, 0.2-0.6kg is added in 12-30kg water, is warming up to 40-60 DEG C, is in 40-60 DEG C, rotating speed
100-300 revs/min of condition stirs 3-6 hours, is centrifuged 25-50 minutes with 3000-10000 revs/min of rotating speed, collects in centrifugation
Clear liquid, into supernatant be added 0.02-2g phosphate, adjust pH to 4.7-5.2, be warming up to 65-75 DEG C, 65-75 DEG C, with
100-500 revs/min of rotating speed stirs 20-60 minutes, adjusts pH to 6.8-7.2, dense in 0.03-0.08MPa, 45-65 DEG C of conditions
It is reduced to 0.5-0.8kg, obtains modified seed mucilage;The phosphate is in sodium tripolyphosphate, sodium dihydrogen phosphate, sodium trimetaphosphate
One kind, preferably sodium tripolyphosphate.Plant forms in adapting to environmental process for a long time is wrapped in special viscous of the surface of the seed
Liquid matter, seed mucilage are to be wrapped in the special mucilaginous substance of the surface of the seed.Contain relatively rich sugar, amino acid, tool in seed mucilage
There is moisturizing, moisten, submissive effect.Polysaccharide structure after phosphate-modified changes, and can be generated to moisture retention, nourishing different degrees of
It influences.
The heretofore described hair care factor is silkworm chrysalis oil and/or forest frog's egg fat.The factor of taking care of hair is more preferably silkworm chrysalis oil
With the mixture of forest frog's egg fat, the mass ratio of the silkworm chrysalis oil and forest frog's egg fat is (1-3):(1-3).
The present invention also provides the preparation methods of Chinese herbal medicine anticreep shampoo, include the following steps, described part is parts by weight:
(1) extracts of Chinese herbal medicine is prepared:Ginger, Radix Astragali, Rhizoma Gastrodiae, Radix Salviae Miltiorrhizae, the windproof 10-20 mesh that smashes it through respectively are sieved, crushing is weighed
Afterwards by 0.2-0.8 parts of ginger, 0.5-1.5 parts of Radix Astragali, 0.5-1.5 parts of Rhizoma Gastrodiae, 0.3-0.9 parts of Radix Salviae Miltiorrhizae, windproof 0.4-1.2 parts it is mixed
It closes uniformly, obtains crude drug, crude drug is added in the water that quality is 8-10 times of crude drug quality, it is small that 12-24 is impregnated at 25-35 DEG C
When, it is heated to 95-100 DEG C, 2-4 hours are kept the temperature at 95-100 DEG C, crosses 50-100 mesh sieve, obtains an extracting solution and primary filter
Cake, the water that quality is 6-8 times of crude drug quality is added into a filter cake, is heated to 95-100 DEG C, and it is small that 1-3 is kept the temperature at 95-100 DEG C
When, 50-100 mesh sieve is crossed, secondary raffinate and secondary filter cake are obtained, it is 6-8 times of crude drug quality that quality is added into secondary filter cake
Water, be heated to 95-100 DEG C, 1-3 hours kept the temperature at 95-100 DEG C, cross 50-100 mesh sieve, obtain filtrate three times, merge primary
Filtrate, secondary filtrate and three times filtrate obtain mixing filtrate, will mixing filtrate cross 100-200 mesh sieve, obtain extracts of Chinese herbal medicine;
(2) extracts of Chinese herbal medicine of step (1) is heated to 65-75 DEG C, be added 15-40 parts of surfactants, 3-10 parts of moisturizer,
It is small to stir 1-3 at 65-75 DEG C, with 100-500 revs/min of rotating speed for 0.5-1.5 parts of cationic conditioning agents, 0.6-1.8 parts of thickeners
When, it is cooled to 25-30 DEG C, obtains Chinese herbal medicine anticreep shampoo.
The present invention also provides the preparation methods of Chinese herbal medicine anticreep shampoo, include the following steps, described part is parts by weight:
(1) extracts of Chinese herbal medicine is prepared:Ginger, Radix Astragali, Rhizoma Gastrodiae, Radix Salviae Miltiorrhizae, the windproof 10-20 mesh that smashes it through respectively are sieved, crushing is weighed
Afterwards by 0.2-0.8 parts of ginger, 0.5-1.5 parts of Radix Astragali, 0.5-1.5 parts of Rhizoma Gastrodiae, 0.3-0.9 parts of Radix Salviae Miltiorrhizae, windproof 0.4-1.2 parts it is mixed
It closes uniformly, obtains crude drug, crude drug is added in the water that quality is 8-10 times of crude drug quality, it is small that 12-24 is impregnated at 25-35 DEG C
When, it is heated to 95-100 DEG C, 2-4 hours are kept the temperature at 95-100 DEG C, crosses 50-100 mesh sieve, obtains an extracting solution and primary filter
Cake, the water that quality is 6-8 times of crude drug quality is added into a filter cake, is heated to 95-100 DEG C, and it is small that 1-3 is kept the temperature at 95-100 DEG C
When, 50-100 mesh sieve is crossed, secondary raffinate and secondary filter cake are obtained, it is 6-8 times of crude drug quality that quality is added into secondary filter cake
Water, be heated to 95-100 DEG C, 1-3 hours kept the temperature at 95-100 DEG C, cross 50-100 mesh sieve, obtain filtrate three times, merge primary
Filtrate, secondary filtrate and three times filtrate obtain mixing filtrate, will mixing filtrate cross 100-200 mesh sieve, obtain extracts of Chinese herbal medicine;
(2) extracts of Chinese herbal medicine of step (1) is heated to 65-75 DEG C, be added 15-40 parts of surfactants, 3-10 parts of moisturizer,
0.5-1.5 parts of cationic conditioning agents, 0.6-1.8 parts of thickeners, the 1-5 parts of hair care factors, at 65-75 DEG C, with 100-500 revs/min
Clock rotating speed stirs 1-3 hours, is cooled to 25-30 DEG C, obtains Chinese herbal medicine anticreep shampoo.
The Chinese herbal medicine anticreep shampoo of the present invention is selected ginger, Radix Astragali, Rhizoma Gastrodiae, Radix Salviae Miltiorrhizae, is prevented according to Chinese medicine combination principle
Wind traditional Chinese medicine of the five flavours, common conditioning human body scalp and hair follicle achieve, generating hair mild to scalp irritation in terms of Anti-hair loss
Effect is good, effect suitable for long-time service.Correspondingly, the present invention also provides the preparation method of Chinese herbal medicine anticreep shampoo, it should
Preparation method can extract medium-height grass the effective elements of the medicine to greatest extent, improve the Anti-hair loss of shampoo, hair tonic, educate hair effect.
On the basis of common knowledge of the art, above-mentioned each optimum condition, can be each preferably to get the present invention in any combination
Embodiment.
Specific implementation mode
It is further illustrated the present invention below by the mode of embodiment, but does not therefore limit the present invention to the reality
It applies among a range.In the following examples, the experimental methods for specific conditions are not specified, according to conventional methods and conditions, or according to quotient
Product specification selects.
In following embodiments, primary raw material and instrument used are as follows:
Ginger, the fresh rhizome of Zingiber herbaceos perennial ginger (Zingiber officinale Roscoe), has
The effect for inhibiting tumour, preventing dandruff, strengthen the hair.Place of production Shandong.
Radix Astragali, specifically used astragalus mongolicus (Classification system:Astragalus membranaceus(Fish)
Bungevar.Mongholicus (Bunge) Hsiao) dry root, control shortness of breath and palpitation, it is weak, collapse.The place of production Inner Mongol.
Rhizoma Gastrodiae, orchid Rhizoma Gastrodiae (Classification system:Gastrodia elata Bl.) stem tuber, the day that the present invention uses
Numb kind is gastrodia elata f. glauca (scientific name:Gastrodia elata f.glauca), the also known as dry Rhizoma Gastrodiae of iron is rare Chinese medicine.The place of production is lucky
Woods.
Radix Salviae Miltiorrhizae, the dry root of labiate Radix Salviae Miltiorrhizae Salvia miltiorrhiza Bge. have promoting blood circulation, promoting menstruation
The effect of analgesic, relieving restlessness that clears away heart-fire, cool blood to disappear carbuncle.Place of production Sichuan.
It is windproof, it is umbelliferae Saposhnikovia divaricata (Classification system:Saposhnikovia divaricata(Turcz.)
Schischk. dry root) has antipyretic, cooling;Ease pain, is calm and anticonvulsion;Enhance the effect of function of immune system.Production
Ground Hebei.
Cocoamidopropyl betaine, No. CAS:86438-79-1.
Laureth sodium sulfovinate, No. CAS:9004-82-4.
PEG-150 distearates, No. CAS:9005-08-7.
Glycol distearate, No. CAS:627-83-8.
Acritamer 940, brand:U.S. Lu Runbo.
Polyquaternium-10:That is chlorination -2- hydroxyls -3- (dimethylamino) propyl polyethylene oxide cellulose ether, No. CAS:
68610-92-4。
Guar hydroxypropyltrimonium ammonium chloride, the production of Guangzhou Ke You Chemical Industry Science Co., Ltd, model C-14S.
Sodium tripolyphosphate, No. CAS:7758-29-4.
Sodium dihydrogen phosphate, No. CAS:7758-80-7.
Sodium trimetaphosphate, No. CAS:7785-84-4.
S.Przewalskii Maxim grass seed, Salvia przewalskii Maxim (Classification system:Salvia przewalskii Maxim.) it is fresh at
Ripe seed.Place of production Gansu.
Small Chinese herbaceous peony grass seed, (Classification system Plantago minuta Pall., are called plantago lessingii, spire to small Asiatic plantain
Chinese herbaceous peony) fresh mature seed.The place of production Inner Mongol.
Silkworm chrysalis oil, can be by commercially available or be commercially available.The silkworm chrysalis oil used in the present invention according to application No. is
201010113528.1 patent of invention embodiment 1 be prepared.
Forest frog's egg fat, can by commercially available or be commercially available, the forest frog's egg fat that is used in the present invention according to application No. is
01113910.2 patent of invention embodiment 1 is prepared.
In following embodiments, used test method and key instrument are as follows:
Anti-hair loss measure of merit:Test object is 360 male pattern baldness patients, is divided into 8 groups, every group 45.8 groups of subjects
It is to use within every 3 days once to use the Chinese herbal medicine anticreep shampoo of 1-8 of the embodiment of the present invention, frequency of use respectively, is used every time
35mL, in addition to the present invention Chinese herbal medicine anticreep shampoo outside do not use other have one's hair wash, hair products, during test also without
The hairs beauty behaviors such as hair dyeing, hair-waving, evaluate Anti-hair loss curative effect using after 16 weeks.The standard of curative effect evaluation:It cures:Hair
Nothing falls off, or within alopecia 25 daily, and hair quality is soft, and combing is smooth, and color development blacks, and no bifurcated dries up, is sallow, and scalp is clear
Refreshing, brains is clear, and hair is moist;It is effective:Alopecia substantially reduces, or alopecia daily, between 25-50 roots, hair quality is soft, combs
Smooth, color development blacks, and substantially without bifurcated, withered, sallow, transdermal salubrious, brains is clear, and hair is moist;Effectively:Depilation phenomenon is still
Have, but alopecia daily, between 50-75 roots, hair quality is relatively soft, is easier to comb, color development blackening, substantially without bifurcated, it is withered,
Sallow, transdermal relatively salubrious, brains is more visible, and hair is relatively moist.In vain:Depilation phenomenon without change, or daily alopecia 75 with
On, hair is firmly crisp, it is difficult to comb, dry hair, color development is sallow.Test result is shown in Table 1.Each group result compares, P<0.05.
Carding property is tested:Using brand be DIA-STRON, the hair tester of model MTT175 carries out.Test bag
Dry cardability, the test of wet cardability are included, the wet cardability test is:0.3g topknots are cleaned, are 10% with 2g mass fractions
Laruyl alcohol sodium sulfovinate aqueous solution moisten 1min, then rinsed well with clear water, with comb comb it is once extra to remove
Moisture measures wet hair combing power W with hair tester1, repeat the above steps, measure 3 times, be averaged per a sample.Wet comb
Hair sample is placed on air drying 24 hours after the completion of rationality test, its hair drying comb reason work(is measured, repeats the above steps, often
A sample measures 3 times, is averaged W2.It is another to take 0.3g topknots, clean, 1min is moistened with 2g Chinese herbal medicine anticreep shampoo, then
It is rinsed well with clear water, is combed once to remove extra moisture with comb, wet hair combing power W is measured with hair tester1',
It repeats the above steps, measures 3 times, be averaged per a sample;Hair sample is placed on air after the completion of wet cardability is tested
Middle drying 24 hours measures its hair drying comb reason work(W2', it repeats the above steps, measures 3 times, be averaged per a sample.Calculate comb
Manage work(decreasing value.Wet hair combing power decreasing value=(W1-W1')/W1× 100%.Dry carding work(decreasing value=(W2-W2')/W2×
100%.Test result is shown in Table 2.
Anti-dandruff measure of merit:It is tested using dandruff point system, standards of grading are as follows:0 point indicates no dandruff, 0<Scoring
≤ 2 points:For the greyish white rough scales of small flakes, 2<Fen≤4 point Ping:For as low as median size chip, 4<Fen≤6 point Ping:For with
The loose connected big and thin chip of scalp, 6<Fen≤8 point Ping:For big tackness chip, 8<Fen≤10 point Ping:It is tight with scalp
Close attachment to yellow the thicker scales of skin that peel off.It is 6 to choose 80 dandruff scorings<The male subject of Fen≤8 point Ping is divided into 8 groups
Every group 10, it is every 3 angel that 8 groups of subjects use the Chinese herbal medicine anticreep shampoo of 1-8 of the embodiment of the present invention, frequency of use respectively
With primary, use 35mL every time, do not used outside the Chinese herbal medicine anticreep shampoo of the present invention other have one's hair wash, hair products,
Also anti-dandruff effect is evaluated using after four weeks without the hairs beauty behavior such as have hair dyed, perm during test.Evaluation side
Method:How much scored according to standards of grading with the scurf number adhered on hair in scalp and the above 4cm of root of hair, every group of scoring knot
Fruit takes the average value of 10 testers scoring in group.Test result is shown in Table 2, and each group result compares, P<0.05.
It is further illustrated the present invention below by the mode of embodiment.
Embodiment 1
A kind of Chinese herbal medicine anticreep shampoo, including the raw material of following weight parts are prepared:0.5 portion of ginger, 1.2 parts of Huangs
Stilbene, 0.8 part of Rhizoma Gastrodiae, 0.6 part of Radix Salviae Miltiorrhizae, 0.7 part windproof, 32 parts of surfactants, 5 parts of moisturizer, 1 part of cationic conditioning agent, 0.8
Part thickener, 76 parts of water.The cationic conditioning agent is that Polyquaternium-10 and guar hydroxypropyltrimonium ammonium chloride press quality
Than being 1:2 mixture.The thickener is Acritamer 940.The surfactant is Cocoamidopropyl betaine, bay
Alcohol polyethers sodium sulfovinate, PEG-150 distearates, glycol distearate are 1 in mass ratio:1:2:1 mixture.Institute
It is glycerine to state moisturizer.
The preparation method of Chinese herbal medicine anticreep shampoo includes the following steps that described part is parts by weight:(1) Chinese herbal medicine is prepared
Extracting solution:By ginger, Radix Astragali, Rhizoma Gastrodiae, Radix Salviae Miltiorrhizae, it is windproof smash it through respectively 10 mesh sieve, weigh crush after by 0.5 part of ginger,
1.2 parts of Radix Astragali, 0.8 part of Rhizoma Gastrodiae, 0.6 part of Radix Salviae Miltiorrhizae, it is windproof 0.7 part be uniformly mixed, obtain crude drug, crude drug, which is added to quality, makes a living
It in the water that 8 times of medicine quality, is impregnated 12 hours at 30 DEG C, is heated to 100 DEG C, 3 hours are kept the temperature at 100 DEG C, crossed 50 mesh sieve, obtain one
The water that quality is 6 times of crude drug quality is added into a filter cake, 100 DEG C are heated to, at 100 DEG C for secondary extracting solution and a filter cake
Heat preservation 2 hours, crosses 50 mesh sieve, obtains secondary raffinate and secondary filter cake, and it is 6 times of crude drug quality that quality is added into secondary filter cake
Water, be heated to 100 DEG C, 1.5 hours kept the temperature at 100 DEG C, cross 50 mesh sieve, obtain filtrate three times, merge first-time filtrate, secondary filter
Liquid and three times filtrate obtain mixing filtrate, and mixing filtrate is sieved with 100 mesh sieve, extracts of Chinese herbal medicine is obtained;(2) by step (1)
Extracts of Chinese herbal medicine is heated to 68 DEG C, and 32 parts of surfactants, 5 parts of moisturizer, 1 part of cationic conditioning agent, 0.8 part of thickening is added
Agent is stirred 2 hours at 68 DEG C, with 300 revs/min of rotating speeds, is cooled to 25 DEG C, obtains Chinese herbal medicine anticreep shampoo.
Embodiment 2
A kind of Chinese herbal medicine anticreep shampoo, including the raw material of following weight parts are prepared:0.5 portion of ginger, 1.2 parts of Huangs
Stilbene, 0.8 part of Rhizoma Gastrodiae, 0.6 part of Radix Salviae Miltiorrhizae, 0.7 part windproof, 32 parts of surfactants, 5 parts of moisturizer, 1 part of cationic conditioning agent, 0.8
Part thickener, 76 parts of water.The cationic conditioning agent is that Polyquaternium-10 and guar hydroxypropyltrimonium ammonium chloride press quality
Than being 1:2 mixture.The thickener is Acritamer 940.The surfactant is Cocoamidopropyl betaine, bay
Alcohol polyethers sodium sulfovinate, PEG-150 distearates, glycol distearate are 1 in mass ratio:1:2:1 mixture.Institute
It is seed mucilage to state moisturizer.The preparation method of seed mucilage is as follows:By 0.3kg S.Przewalskii Maxims grass seed, the small Asiatic plantains of 0.2kg
Seed is added in 15kg water, is warming up to 55 DEG C, is that 200 revs/min of conditions stir 5 hours in 55 DEG C, rotating speed, with 5000 revs/min
Clock rotating speed centrifuges 40 minutes, collects centrifuged supernatant, supernatant is concentrated into 0.6kg in 0.05MPa, 50 DEG C of conditions, is planted
Sub- mucus.
The preparation method is the same as that of Example 1 for Chinese herbal medicine anticreep shampoo.
Embodiment 3
A kind of Chinese herbal medicine anticreep shampoo, including the raw material of following weight parts are prepared:0.5 portion of ginger, 1.2 parts of Huangs
Stilbene, 0.8 part of Rhizoma Gastrodiae, 0.6 part of Radix Salviae Miltiorrhizae, 0.7 part windproof, 32 parts of surfactants, 5 parts of moisturizer, 1 part of cationic conditioning agent, 0.8
Part thickener, 76 parts of water.The cationic conditioning agent is that Polyquaternium-10 and guar hydroxypropyltrimonium ammonium chloride press quality
Than being 1:2 mixture.The thickener is Acritamer 940.The surfactant is Cocoamidopropyl betaine, bay
Alcohol polyethers sodium sulfovinate, PEG-150 distearates, glycol distearate are 1 in mass ratio:1:2:1 mixture.Institute
The moisturizer stated is modified seed mucilage.The preparation method of the modified seed mucilage is as follows:By 0.3kg S.Przewalskii Maxim grass seeds
The small Chinese herbaceous peony grass seed of son, 0.2kg is added in 15kg water, is warming up to 55 DEG C, is that 200 revs/min of conditions stir 5 in 55 DEG C, rotating speed
Hour, it is centrifuged 40 minutes with 5000 revs/min of rotating speeds, collects centrifuged supernatant, 0.05g phosphate is added into supernatant, adjusted
Save pH to 4.8, be warming up to 65 DEG C, stirred 40 minutes at 65 DEG C, with 200 revs/min of rotating speeds, adjust pH to 7.0,0.05MPa,
50 DEG C of conditions are concentrated into 0.6kg, obtain modified seed mucilage.The phosphate is sodium tripolyphosphate.It is used when adjusting pH value
2mol/L hydrochloric acid and 2mol/L sodium hydroxides are adjusted.
The preparation method is the same as that of Example 1 for Chinese herbal medicine anticreep shampoo.
Embodiment 4
It is substantially the same manner as Example 3, it differs only in:Phosphate described in the present embodiment 4 is sodium dihydrogen phosphate.
Embodiment 5
It is substantially the same manner as Example 3, it differs only in:Phosphate described in the present embodiment 5 is sodium trimetaphosphate.
Embodiment 6
A kind of Chinese herbal medicine anticreep shampoo, including the raw material of following weight parts are prepared:0.5 portion of ginger, 1.2 parts of Huangs
Stilbene, 0.8 part of Rhizoma Gastrodiae, 0.6 part of Radix Salviae Miltiorrhizae, 0.7 part windproof, 32 parts of surfactants, 5 parts of moisturizer, 1 part of cationic conditioning agent, 0.8
Part thickener, 3.5 parts of the hair care factors, 76 parts of water.The cationic conditioning agent is Polyquaternium-10 and guar gum hydroxypropyl trimethylammonium
Ammonium chloride is 1 in mass ratio:2 mixture.The thickener is Acritamer 940.The surfactant is coconut oleoyl amine
Propyl betaine, laureth sodium sulfovinate, PEG-150 distearates, glycol distearate are 1 in mass ratio:
1:2:1 mixture.The moisturizer is modified seed mucilage.The preparation method of the modified seed mucilage is the same as embodiment 3.
The hair care factor is silkworm chrysalis oil.
The preparation method of Chinese herbal medicine anticreep shampoo includes the following steps that described part is parts by weight:(1) Chinese herbal medicine is prepared
Extracting solution:By ginger, Radix Astragali, Rhizoma Gastrodiae, Radix Salviae Miltiorrhizae, it is windproof smash it through respectively 10 mesh sieve, weigh crush after by 0.5 part of ginger,
1.2 parts of Radix Astragali, 0.8 part of Rhizoma Gastrodiae, 0.6 part of Radix Salviae Miltiorrhizae, it is windproof 0.7 part be uniformly mixed, obtain crude drug, crude drug, which is added to quality, makes a living
It in the water that 8 times of medicine quality, is impregnated 12 hours at 30 DEG C, is heated to 100 DEG C, 3 hours are kept the temperature at 100 DEG C, crossed 50 mesh sieve, obtain one
The water that quality is 6 times of crude drug quality is added into a filter cake, 100 DEG C are heated to, at 100 DEG C for secondary extracting solution and a filter cake
Heat preservation 2 hours, crosses 50 mesh sieve, obtains secondary raffinate and secondary filter cake, and it is 6 times of crude drug quality that quality is added into secondary filter cake
Water, be heated to 100 DEG C, 1.5 hours kept the temperature at 100 DEG C, cross 50 mesh sieve, obtain filtrate three times, merge first-time filtrate, secondary filter
Liquid and three times filtrate obtain mixing filtrate, and mixing filtrate is sieved with 100 mesh sieve, extracts of Chinese herbal medicine is obtained;(2) by step (1)
Extracts of Chinese herbal medicine is heated to 68 DEG C, and 32 parts of surfactants, 5 parts of moisturizer, 1 part of cationic conditioning agent, 0.8 part of thickening is added
Agent, 3.5 parts of hair care factors, are stirred 2 hours at 68 DEG C, with 300 revs/min of rotating speeds, are cooled to 25 DEG C, obtain Chinese herbal medicine anticreep and wash
It becomes visible.
Embodiment 7
It is substantially the same manner as Example 6, it differs only in, the factor of taking care of hair described in the present embodiment 7 is forest frog's egg fat.
Embodiment 8
It is substantially the same manner as Example 6, it differs only in:The factor of taking care of hair described in the present embodiment 8 is silkworm chrysalis oil and wood frog ovum
The mass ratio of the mixture of oil, the silkworm chrysalis oil and forest frog's egg fat is 1:1.
Test case
Chinese herbal medicine anticreep shampoo of the present invention is subjected to Anti-hair loss measure of merit, test result is shown in Table 1.
Table 1:Anti-hair loss measure of merit result table
Invention Chinese herbal medicine anticreep shampoo is subjected to combing power test and anti-dandruff measure of merit, test result are shown in Table 2.
Table 2:Combing power is tested and anti-dandruff measure of merit result table
The Chinese herbal medicine anticreep shampoo of the present invention is selected ginger, Radix Astragali, Rhizoma Gastrodiae, Radix Salviae Miltiorrhizae, is prevented according to Chinese medicine combination principle
Wind traditional Chinese medicine of the five flavours efficiently extracts Chinese medicinal anti-hair loss ingredient, scalp absorptivity is high, with Anti-hair loss, improves hair follicle, strengthen the hair, hair tonic
Effect.The moisturizer contained in Chinese herbal medicine anticreep shampoo can moisten hair, improve hair difficult combing problem caused by withered.
Chinese herbal medicine anticreep shampoo also has good anti-dandruff effect.
The preferred embodiment of the present invention has been described in detail above.It should be appreciated that those skilled in the art without
It needs creative work according to the present invention can conceive and makes many modifications and variations.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical solution, all should be in the protection domain being defined in the patent claims.