CN108309841A - Skin care compositions based on China fir leaf caulerpa extract and its application - Google Patents
Skin care compositions based on China fir leaf caulerpa extract and its application Download PDFInfo
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- CN108309841A CN108309841A CN201810315672.XA CN201810315672A CN108309841A CN 108309841 A CN108309841 A CN 108309841A CN 201810315672 A CN201810315672 A CN 201810315672A CN 108309841 A CN108309841 A CN 108309841A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The present invention relates to a kind of skin care compositions based on China fir leaf caulerpa extract and its applications.The skin care compositions based on China fir leaf caulerpa extract includes 0.5 part~5 parts of China fir leaf caulerpa extract, 0.5 part~4 parts of milk thistle extract, 0.5 part~1 part of golden hairpin dendrobium extract, 0.1 part~0.5 part of lantern berry extract and 0.1 part~0.5 part of Tiannu Magnolia flower extract.The skin anti-aging effect of the above-mentioned skin care compositions based on China fir leaf caulerpa extract is preferable.
Description
Technical field
The present invention relates to daily chemical product technical field, more particularly to based on China fir leaf caulerpa extract skin care compositions and
It is applied.
Background technology
As being constantly progressive for social economy is abundant with material life, skin care item have come into ordinary citizen house as the popular vehicles.Skin care
Product are the substance or mixture of human skin surface to be imposed on, in a manner of smearing or spray etc. to reach cleaning, skin care or increasing
The product of strong skin elasticity.Wherein, facial mask is by covering or coated on face, contact of the barrier face skin with air, barrier
The evaporation of skin moisture, increases the humidity of cuticula, cutin-softening, and skin temperature increases to expand pore, is conducive to seek
It forms and point is smoothly absorbed.However, existing facial mask is preventing skin old mostly using moisturizing or cleaning skin as main effect
Effect in terms of change is poor, cannot meet consumer demand.
Invention content
Based on this, it is necessary to provide a kind of skin care of the anti-aging effect to skin preferably based on China fir leaf caulerpa extract
Composition and its application.
A kind of skin care compositions based on China fir leaf caulerpa extract includes 0.5 part~5 parts of China fir leaf in terms of mass fraction
Caulerpa extract, 0.5 part~4 parts of milk thistle extract, 0.5 part~1 part of golden hairpin dendrobium extract, 0.1 part~0.5 part
Lantern berry extract and 0.1 part~0.5 part of Tiannu Magnolia flower extract.
The above-mentioned skin care compositions based on China fir leaf caulerpa extract is by by China fir leaf caulerpa extract and other plant group
Divide synergistic effect, can not only have stronger inoxidizability and moisture retention, additionally it is possible to quickly make skin rich in moisture and bullet
Property, it is quick to the problem of skin water shortage and relaxation, it can more effectively resist skin aging, desalination microgroove, keep skin
Elasticity.Experiment proves that the inoxidizability of the above-mentioned skin care compositions based on China fir leaf caulerpa extract contains algae better than common
The inoxidizability of the skin care item of extract, such as spirulina, and China fir leaf caulerpa extract and golden hairpin dendrobium extract cooperate with work
With, can accelerate improve skin moisture and elasticity, while above-mentioned skin care compositions can a degree of reparations livid ring around eye with
The skin problems such as red blood silk, above-mentioned active component are vegetalitas component, safety, nonirritant.It is above-mentioned to be carried based on China fir leaf caulerpa
Take the skin care compositions of object preferable to the anti-aging effect of skin.
Further include 0.1 part~0.5 part of ginseng root extract in one of the embodiments, in terms of mass fraction.
In one of the embodiments, in terms of mass fraction, including 1 part~3 parts of China fir leaf caulerpa extract, 1 part~2 parts
Milk thistle extract, 0.6 part~0.8 part of golden hairpin dendrobium extract, 0.2 part~0.4 part of lantern berry extract, 0.2 part
~0.4 part of Tiannu Magnolia flower extract and 0.2 part~0.4 part of ginseng root extract.
Further include that 0.1 part~0.5 part of Ka Misong arnicas carry in one of the embodiments, in terms of mass fraction
Take object and 0.1 part~0.5 part of bignose rhinacanthus branchlet and leaf extract.
In one of the embodiments, in terms of mass fraction, further include 0.1 part~0.5 part ginger caul-fat and 0.05 part~
0.2 part of pot marigold seed oil.
Further include 1 part~5 parts of glycerine, the 1,2- of 0.5 part~4 parts in one of the embodiments, in terms of mass fraction
Pentanediol and 0.5 part~2 parts of glycine betaine.
In one of the embodiments, in terms of mass fraction, further include 0.5 part~2 parts tocopherol, 0.5 part~5 parts
Linseed oil, 0.5 part~5 parts of hydrogenated jojoba oil and 0.5 part~4 parts of white pond flower seed oil.
Further include 0.5 part~3 parts of polypropylene ester cross-linked polymer in one of the embodiments, in terms of mass fraction.
Further include 0.05 part~0.3 part of renovation agent, the reparation in one of the embodiments, in terms of mass fraction
Agent is selected from least one of epithelical cell growth factor, stem cell factor and vascular endothelial growth factor.
Application of the above-mentioned skin care compositions based on China fir leaf caulerpa extract in facial mask preparation.
Specific implementation mode
It to facilitate the understanding of the present invention, below will be to invention is more fully described.Give the preferable of the present invention
Embodiment.But the present invention can realize in many different forms, however it is not limited to embodiment described herein.Phase
Instead, purpose of providing these embodiments is makes the disclosure of the present invention more thorough and comprehensive.
Unless otherwise defined, all of technologies and scientific terms used here by the article and belong to the technical field of the present invention
The normally understood meaning of technical staff is identical.Used term is intended merely to description tool in the description of the invention herein
The purpose of the embodiment of body, it is not intended that in the limitation present invention.
The skin care compositions based on China fir leaf caulerpa extract of one embodiment, in terms of mass fraction, including：0.5 part~5
Part China fir leaf caulerpa extract, 0.5 part~4 parts of milk thistle extract, 0.5 part~1 part of golden hairpin dendrobium extract, 0.1 part
~0.5 part of lantern berry extract and 0.1 part~0.5 part of Tiannu Magnolia flower extract.
China fir leaf caulerpa belongs to Chlorophyta Caulerpaceae caulerpa category, and containing superoxide dismutase, and superoxide dismutase albumen contains
Amount and Rate activity are higher, have stronger antioxygenic property, meanwhile, China fir leaf caulerpa extract contains algal polysaccharides, mannitol
And fucoidin etc. counts various bioactivators, can improve the activity of peroxidase and superoxide dismutase, to
The antiradical activities for improving skin are anti-aging to achieve the effect that.
In a wherein embodiment, based on the skin care compositions of China fir leaf caulerpa extract, including 1 in terms of mass fraction
Part~4 parts of China fir leaf caulerpa extract.Further, China fir leaf caulerpa extract is 1 part~3 parts.In some embodiments, China fir leaf
Caulerpa extract is 0.5 part, 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts or 5 parts.
In a wherein embodiment, China fir leaf caulerpa extract is the water extract of China fir leaf caulerpa.An implementation wherein
In mode, the preparation method of China fir leaf caulerpa extract：China fir leaf caulerpa is crushed to and is crossed the mesh sieve of 60 mesh~100, according to pulverizing and sieving
The mass ratio of China fir leaf caulerpa powder and water afterwards is 1:20~1:30 be added water, in ultrasonic frequency 25kHz~35kHz, 110W~
160W, 40 DEG C~60 DEG C extract 30 minutes~80 minutes, separation of solid and liquid obtain extracting solution, after drying, obtain China fir leaf caulerpa and carry
Take object, wherein dry mode is drying or spray drying.Certainly, it should be noted that China fir leaf caulerpa extract may be
It is commercially available.
Contain silymarin in milk thistle extract, silymarin has stronger inoxidizability and removes the energy of free radical
Power can prevent the stimulation of the aging and extraneous radiation of skin to skin, and silymarin can inhibit the work of elastoser
Property, promote the generation for constituting the collagen and elastin of the extracellular matrix of corium, increases elasticity of skin, meanwhile, research
Show that silymarin has anti-inflammatory effect, the inflammation symptom of skin can be alleviated.In addition, milk thistle extract is skin-penetrating
It is relatively strong, be conducive to carry other nutriments and infiltrate through cell, especially milk thistle extract and cooperate with China fir leaf caulerpa extract energy
The enough metabolism for effectively releiving and accelerating skin.
In a wherein embodiment, in terms of mass fraction, milk thistle extract can also be 1 part~2 parts.At some
In embodiment, milk thistle extract can be 0.5 part, 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts or 4 parts.
In a wherein embodiment, milk thistle extract is the alcohol extract of milk thistle.An embodiment wherein
In, the preparation method of milk thistle extract：Milk thistle fruit is dry, crush and cross the mesh sieve of 30 mesh~80, volume basis is added
Content be 75%~95% ethyl alcohol aqueous solution in ultrasonic frequency 30kHz~40kHz, 400W~600W, 25 DEG C~40 DEG C
Extraction 15 minutes~30 minutes, separation of solid and liquid obtain extracting solution, after drying, obtain milk thistle extract, wherein pulverize and sieve
The quality of Herba Silybi mariani powder afterwards and the volumn concentration of addition are that the ratio between the volume of aqueous solution of 75%~95% ethyl alcohol is 1:
15~1:25, dry mode is vacuum drying or rotary evaporation drying.Certainly, it should be noted that milk thistle extract
Can be commercially available.
Golden hairpin dendrobium extract contains alkaloid and stem of noble dendrobium class polysaccharide, has scavenging effect, Neng Goukang to a variety of free radicals
It aoxidizes and anti-aging, and the blood flow of capillary can be increased, have the function of promoting blood circulation, meanwhile, golden hairpin dendrobium extract exists
There is the function of water suction under low humidity, there is moistening effect, in addition, golden hairpin dendrobium extract can be accelerated with China fir leaf caulerpa extract
Improve the moisture and elasticity of skin.In a wherein embodiment, golden hairpin dendrobium extract is 0.6 part~0.8 part.At some
In embodiment, golden hairpin dendrobium extract is 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1 part.
In a wherein embodiment, golden hairpin dendrobium extract is the water extract of the gold fork stem of noble dendrobium.An implementation wherein
In mode, the preparation method of golden hairpin dendrobium extract：By HERBA DENDROBII drying, it is ground into coarse powder, pure water is added in 50 DEG C~80
DEG C extraction 1h~3h, separation of solid and liquid obtain extracting solution, after drying, obtain golden hairpin dendrobium extract, wherein the Jin Chai after crushing
The ratio between the quality of the stem of noble dendrobium and the volume of pure water of addition are 1:10~1:25, dry mode is vacuum drying or spray drying.
Certainly, it should be noted that golden hairpin dendrobium extract may be commercially available.
Cape gooseberry is annual or perennial herbaceous plant, the vitamin C containing high-content, and contains a large amount of polyphenol
Class, flavonoids and organic acid active material have stronger inoxidizability, also have certain antiphlogistic effects.Wherein one
In a embodiment, lantern berry extract is solid extract.In a wherein embodiment, in terms of mass fraction, lantern
Berry extract can be 0.2 part~0.4 part.In some embodiments, lantern berry extract be 0.1 part, 0.2 part, 0.3 part,
0.4 part or 0.5 part.
Tiannu Magnolia flower extract can inhibit nitric oxide production generation, have certain anti-oxidation function, also contain phenol
Class and magnoflorine can inhibit collagenase activity, slow down the degradation of collagen fabric, and then maintain skin elasticity,
Prevent skin aging；Tiannu Magnolia flower extract can inhibit the generation of inflammatory factor 1L-1a simultaneously, have the function of it is anti-inflammatory,
Additionally it is possible to inhibit the transfer of melanosome, achieve the effect that whitening.In a wherein embodiment, in terms of mass fraction,
Tiannu Magnolia flower extract be include 0.2 part~0.4 part.In some embodiments, Tiannu Magnolia flower extract be 0.1 part, 0.2
Part, 0.3 part, 0.4 part or 0.5 part.
In a wherein embodiment, Tiannu Magnolia flower extract is the alcohol extract of Tiannu Magnolia flower.One wherein
In embodiment, the preparation method of Tiannu Magnolia flower extract：After Tiannu Magnolia is spent drying and crushed, volumn concentration is added
It for the aqueous solution of 70%~80% ethyl alcohol, is extracted 3 days~4 days at 23 DEG C~27 DEG C, separation of solid and liquid obtains extracting solution, through drying
Afterwards, Tiannu Magnolia flower extract is obtained, wherein the quality of Tiannu Magnolia flower and the volumn concentration of addition after crushing are
The ratio between volume of aqueous solution of 70%~80% ethyl alcohol is 1:8~1:12, dry mode is vacuum drying or spray drying.When
So, it should be noted that Tiannu Magnolia flower extract may be commercially available.
In a wherein embodiment, the skin care compositions based on China fir leaf caulerpa extract is also wrapped in terms of mass fraction
Include 0.1 part~0.5 part of ginseng root extract.Ginseng extract can activate catalase, be sent out with degrading hydrogen peroxide
The effect for removing free radical is waved, vascular endothelial cell proliferation, extension and growth can be promoted, red blood silk, while people can be prevented
Conopsea extraction has activation to luciferase, has anti-inflammatory effect.In a wherein embodiment, ginseng root extract is
Solid extract.Further, in terms of mass fraction, ginseng root extract can be 0.2 part~0.4 part.In some embodiments
In, in terms of mass fraction, ginseng root extract can be 0.1 part, 0.2 part, 0.3 part, 0.4 part or 0.5 part.
In a wherein embodiment, based on the skin care compositions of China fir leaf caulerpa extract, in terms of mass fraction, including
1 part~3 parts of China fir leaf caulerpa extract, 1 part~2 parts of milk thistle extract, 0.6 part~0.8 part of golden hairpin dendrobium extract,
0.2 part~0.4 part of lantern berry extract, 0.2 part~0.4 part of Tiannu Magnolia flower extract and 0.2 part~0.4 part of ginseng
Root extract.The skin care compositions of above-mentioned China fir leaf caulerpa extract coordinates other plants using China fir leaf caulerpa extract as primary raw material
Physical property raw material, formula are reasonable so that above-mentioned skin care compositions has stronger inoxidizability.
In a wherein embodiment, the skin care compositions based on China fir leaf caulerpa extract is also wrapped in terms of mass fraction
Include 0.1 part~0.5 part of Ka Misong Arnicas flower extract and 0.1 part~0.5 part of bignose rhinacanthus branchlet and leaf extract.One wherein
Further include 0.2 part~0.4 part of Ka Misong Arnicas flower extract and 0.2 part~0.4 in terms of mass fraction in embodiment
The bignose rhinacanthus branchlet and leaf extract of part.In some embodiments, further include 0.3 part of Ka Misong arnicas in terms of mass fraction
Extract and 0.3 part of bignose rhinacanthus branchlet and leaf extract.
Ka Misong Arnicas flower extract can improve cathepsin active, promote the proliferation of fiber sprout cell, can
Enhance cell metabolism.In a wherein embodiment, in terms of mass fraction, Ka Misong Arnica flower extracts are solid
Extract.In a wherein embodiment, in terms of mass fraction, Ka Misong Arnicas flower extract can be 0.2 part~0.4
Part.In some embodiments, in terms of mass fraction, Ka Misong Arnicas flower extract can be 0.1 part, 0.2 part, 0.3 part,
0.4 part or 0.5 part.
Bignose rhinacanthus branchlet and leaf extract can promote the generation of collagen and brain amide, to enhance skin cell metabolism,
It can also inhibit tyrosinase activity, and then have effects that whitening skin-active.In a wherein embodiment, with mass fraction
Meter, bignose rhinacanthus branchlet and leaf extract can be 0.2 part~0.4 part.In some embodiments, in terms of mass fraction, bignose rhinacanthus branchlet and leaf extraction
Object can be 0.1 part, 0.2 part, 0.3 part, 0.4 part or 0.5 part.
In a wherein embodiment, the skin care compositions based on China fir leaf caulerpa extract is also wrapped in terms of mass fraction
Include 0.1 part~0.5 part of ginger caul-fat and 0.05 part~0.2 part of pot marigold seed oil.In a wherein embodiment, with quality
Number meter further includes 0.2 part~0.4 part of ginger caul-fat and 0.1 part~0.15 part of pot marigold seed oil.
Ginger caul-fat has stronger inhibiting effect to the bacteriums such as staphylococcus aureus and Escherichia coli, can avoid skin
Due to microorganism infection the problems such as inflammation, long acne, additionally it is possible to avoid above-mentioned skin care compositions microbial contamination and go bad, simultaneously
Ginger caul-fat can also effectively inhibit the decomposition of hyaluronic acid, have the function of moisturizing and maintain skin quality healthy and stable.Wherein one
In a embodiment, in terms of mass fraction, ginger caul-fat can be 0.2 part~0.4 part.In some embodiments, with mass fraction
Meter, ginger caul-fat can be 0.1 part, 0.2 part, 0.3 part, 0.4 part or 0.5 part.
Pot marigold seed oil has stronger inhibiting effect to staphylococcus and streptococcus, can antibacterial anti-inflammatory, restrain wound,
Administer inflammation, the problems such as dark sore and pore are coarse；Can also calm skin, improve sensibility skin quality；Drying can also be moistened simultaneously
Skin promotes the metabolism of skin.In a wherein embodiment, in terms of mass fraction, pot marigold seed oil can be 0.1
Part~0.15 part.In some embodiments, in terms of mass fraction, pot marigold seed oil can be 0.05 part, 0.1 part, 0.15 part or
0.2 part.
In a wherein embodiment, the preparation method of pot marigold seed oil is：By the drying of pot marigold seed, it is crushed to 40
Pot marigold seed after crushing is added in extraction kettle, uses supercritical CO by mesh2In 30 DEG C~35 DEG C, extracting pressure be 25MPa~
It is extracted 2 hours~4 hours under 30MPa, obtains extract, as pot marigold seed oil, wherein CO2Flow be 3kg/h~4kg/
H, dry mode are drying.Certainly, it should be noted that in other embodiments, pot marigold seed oil may be commercially available
's.
In a wherein embodiment, in terms of mass fraction, the skin care compositions based on China fir leaf caulerpa extract also wraps
Include 1 part~5 parts of glycerine, 0.5 part~4 parts of 1,2- pentanediols and 0.5 part~2 parts of glycine betaine.Glycerine, 1,2- pentanediols and
Glycine betaine can have stronger hygroscopic effect, and the water of skin can be kept to moisten, and 1,2- pentanediol also has centainly antibacterial
Effect reduces allergic reaction caused by preservative, meanwhile, glycine betaine has excellent cleaning action, being capable of cleaning skin.Into one
Step ground, further includes 2 parts~4 parts of glycerine, 1 part~3 parts of 1,2- pentanediols and 1 part~1.5 parts of beet in terms of mass fraction
Alkali.Further, further include 3 parts of glycerine, 2 parts of 1,2- pentanediols and 1.2 parts of glycine betaine in terms of mass fraction.
In a wherein embodiment, in terms of mass fraction, the skin care compositions based on China fir leaf caulerpa extract also wraps
Include 0.5 part~2 parts of tocopherol, 0.5 part~5 parts of linseed oil, 0.5 part~5 parts of hydrogenated jojoba oil and 0.5 part~4
The white pond flower seed oil of part.Tocopherol can effectively antagonize free radical, and lipid peroxide is inhibited to generate, and eliminating chloasma inhibits junket
The activity of propylhomoserin enzyme, to reduce melanin production.Linseed oil, hydrogenated jojoba oil and white pond flower seed oil all have anti-oxidant
Property, it being capable of delaying skin aging.Further, in terms of mass fraction, further include 1 part~1.5 parts tocopherol, 2 parts~4 parts
Linseed oil, 2 parts~4 parts of hydrogenated jojoba oil and 1 part~3 parts of white pond flower seed oil.
In a wherein embodiment, in terms of mass fraction, the skin care compositions based on China fir leaf caulerpa extract also wraps
Include 0.5 part~3 parts of polypropylene ester cross-linked polymer.In some embodiments, in terms of mass fraction, polypropylene ester cross-linked polymeric
Object can be 0.5 part, 1 part, 1.5 parts, 2 parts, 2.5 parts or 3 parts.
In a wherein embodiment, in terms of mass fraction, the skin care compositions based on China fir leaf caulerpa extract also wraps
50 parts~90 parts of solvent is included, solvent is at least one of distilled water and deionized water.Certainly, it should be noted that solvent
It is not limited to above-mentioned point out that substance, solvent may be fruit juice, such as cider.
In a wherein embodiment, based on the skin care compositions of China fir leaf caulerpa extract, in terms of mass fraction including：
0.5 part~5 parts of China fir leaf caulerpa extract, 0.5 part~4 parts of milk thistle extract, the extraction of 0.5 part~1 part of HERBA DENDROBII
Object, 0.1 part~0.5 part of lantern berry extract, 0.1 part~0.5 part of Tiannu Magnolia flower extract, 0.1 part~0.5 part of people
Join root extract, 0.1 part~0.5 part of Ka Misong Arnicas flower extract, 0.1 part~0.5 part of bignose rhinacanthus branchlet and leaf extract,
0.1 part~0.5 part of ginger caul-fat, 0.05 part~0.2 part of pot marigold seed oil, 1 part~5 parts of glycerine, 0.5 part~4 parts
1,2- pentanediols, 0.5 part~2 parts of glycine betaine, 0.5 part~2 parts of tocopherol, 0.5 part~5 parts of linseed oil, 0.5 part~
5 parts of hydrogenated jojoba oil, 0.5 part~4 parts of white pond flower seed oil, 0.5 part~3 parts of polypropylene ester cross-linked polymer and 50 parts
~90 parts of solvent.
In a wherein embodiment, in terms of mass fraction, the skin care compositions based on China fir leaf caulerpa extract also wraps
Include 0.05 part~0.3 part of renovation agent.Further, in terms of mass fraction, the skin care compositions based on China fir leaf caulerpa extract
It further include 0.1 part~0.2 part of renovation agent.In some embodiments, renovation agent is 0.05 part, 0.1 part, 0.2 part or 0.3 part.
Renovation agent is selected from least one of epithelical cell growth factor, stem cell factor and vascular endothelial growth factor.
In a wherein embodiment, in terms of mass fraction, renovation agent includes 0.05 part~0.3 part of epithelical cell growth factor.
Further, in terms of mass fraction, renovation agent includes 0.1 part~0.2 part of epithelical cell growth factor.In some embodiments
In, epithelical cell growth factor is 0.05 part, 0.1 part, 0.2 part or 0.3 part.Epithelical cell growth factor being capable of inducing cell increasing
It grows, Differentiation, promotes body epidermal cell, epithelial cell, fibroblastic growth, division and metabolism, promote micro-
The growth of blood vessel improves the microenvironment of cell growth, can repair Local Damaged skin, improves the pigment situation of skin, adjusts
Collagenous fibres, enhance skin elasticity, reduces wrinkle of skin and prevent the effect of skin aging.Granulation tissue can also be stimulated
The epithelialization for forming and promoting granulation tissue is prevented and is protected to shorten the wound healing time and reduce the effect of scar formation
Manage sore of fullying recover from an illness.
In a wherein embodiment, in terms of mass fraction, renovation agent include 0.05 part~0.3 part stem cell because
Son.Further, in terms of mass fraction, renovation agent includes 0.1 part~0.2 part of stem cell factor.In some embodiments, it does
Cell factor is 0.05 part, 0.1 part, 0.2 part or 0.3 part.Stem cell factor is also known as mast cell growth factor, Kit ligands
(KL) or the Steel factors (SLF), it is a kind of acidoglycoprotein generated by the stroma cell in bone marrow microenvironment.Stem cell because
Son can repair tissue cell, promote the metabolism of skin, improve the microcirculation of skin, prevent and modification skin aging.
In a wherein embodiment, in terms of mass fraction, renovation agent includes 0.05 part~0.3 part of blood vessel endothelium life
The long factor.Further, in terms of mass fraction, renovation agent includes 0.1 part~0.2 part of vascular endothelial growth factor.At some
In embodiment, vascular endothelial growth factor is 0.05 part, 0.1 part, 0.2 part or 0.3 part.Vascular endothelial growth factor can have
Effect improves local vascular permeability, can provide sufficient nutriment and its for the synthesis of fibroblastic proliferation and collagen
His growth factor promotes division, the proliferation of cell, improves skin microcirculation, while can also effectively facilitate new capillary vessel
Generation, improve the metabolism of skin, play the role of anti-aging.
In a wherein embodiment, in terms of mass fraction, renovation agent includes 0.03 part~0.1 part of epidermal cell life
The long factor, 0.01 part~0.1 part of stem cell factor, 0.01 part~0.1 part of vascular endothelial growth factor.
The above-mentioned skin care compositions based on China fir leaf caulerpa extract is by by China fir leaf caulerpa extract and other plant group
Divide synergistic effect so that skin care compositions has stronger inoxidizability and moisture retention, and then can resist skin aging, desalination
Microgroove keeps elasticity of skin, meanwhile, above-mentioned active component is vegetalitas component, safety, nonirritant.In addition, above-mentioned skin care
Composition also contains renovation agent, can repair tissue cell, activate division and the proliferation of skin progenitor cell, accelerate collagen
Synthesis, the microcirculation for improving skin restore cell elasticity, calm down microgroove, additionally it is possible to slow down the apoptosis of skin function cell, enhance
The anti-interference ability of Skin Cell, and then prevent and change skin aging.
In a wherein embodiment, the above-mentioned skin care compositions based on China fir leaf caulerpa extract is in facial mask preparation
Using.
In wherein some embodiments, above-mentioned facial mask further includes the acceptable auxiliary material of skin care item.
In wherein some embodiments, the acceptable auxiliary material of skin care item is in pH adjusting agent, essence and chelating agent
It is at least one.
PH adjusting agent can be such that the pH value of above-mentioned facial mask adjusts to 6~7.In a wherein embodiment, pH adjusting agent
Selected from least one of citric acid and sodium citrate.Certainly, it should be noted that if the pH in above-mentioned face is 6~7, pH tune
Section agent can be omitted.
In a wherein embodiment, in terms of mass fraction, above-mentioned skin care item further include 0.1 part~0.3 part of essence.
In a wherein embodiment, essence is cream jasmin france or lavender oil.In some embodiments, essence be 0.1 part,
0.2 part or 0.3 part.
In a wherein embodiment, in terms of mass fraction, above-mentioned skin care item further include 0.1 part~0.3 part of chelating
Agent, chelating agent are selected from least one of disodium ethylene diamine tetraacetate and sodium versenate.In some embodiments, chela
Mixture is 0.1 part, 0.2 part or 0.3 part.
In addition, the present invention also provides the preparation method of the facial mask based on China fir leaf caulerpa extract of the above embodiment, packet
Include following steps：
S110, by tocopherol, linseed oil, hydrogenated jojoba oil, white pond flower seed oil, milk thistle extract, Tiannu Magnolia
Flower extract, ginger caul-fat and pot marigold seed the oil mixing at 50 DEG C~60 DEG C, obtain the first mixture.
In a wherein embodiment, the mode of mixing is stirring, and the rotating speed of stirring is 100rpm~300rpm.Into one
Step, the time of stirring is 0.2h~0.4h.
S120, glycerine, 1,2- pentanediols, polypropylene ester cross-linked polymer and water are put into emulsification pot, is heated to 80 DEG C
~85 DEG C, mixing simultaneously keeps the temperature 20 minutes~40 minutes.
S130,50 DEG C~60 DEG C are cooled to, the first mixture is added in emulsification pot, homogeneous 3 minutes~after ten minutes,
50 DEG C~60 DEG C are stirred 20 minutes~40 minutes, and the second mixture is obtained.
S140, the second mixture is cooled to 40 DEG C~45 DEG C, be added China fir leaf caulerpa extract, golden hairpin dendrobium extract,
Lantern berry extract, ginseng root extract, close loose Arnica flower extract, bignose rhinacanthus branchlet and leaf extract, renovation agent, chelating agent, chela
Mixture and essence, homogeneous 1 minute~5 minutes, stir evenly, obtain third mixture.
S150, pH adjusting agent is continuously added, adjusts pH to 6~7, obtains the facial mask based on China fir leaf caulerpa extract.
Certainly, it should be noted that can be omitted if the pH of third mixture is 6~7, S150, third mixture is
It can be based on the facial mask of China fir leaf caulerpa extract.
The preparation method of the above-mentioned facial mask based on China fir leaf caulerpa extract is simple for process, easily realizes industrialized production.
Here is the explanation of specific embodiment, and following embodiment unless otherwise specified, is not then contained except inevitably miscellaneous
The component pointed out is not known in other other than matter.
In following embodiment, unless otherwise specified, China fir leaf caulerpa extract is that China fir leaf caulerpa is crushed to and crossed 80 mesh sieve, is pressed
The mass ratio of quality and water according to the China fir leaf caulerpa powder after pulverizing and sieving is 1:25 be added water, in ultrasonic frequency 30kHz,
130W, 50 DEG C extract 60 minutes, separation of solid and liquid obtain extracting solution and obtained after drying, the water content of China fir leaf caulerpa extract is
5wt%.Milk thistle extract is that milk thistle fruit is dry, crushes and cross 50 mesh sieve, and it is 80% that volumn concentration, which is added,
The aqueous solution of ethyl alcohol extracts 20 minutes in ultrasonic frequency 40kHz, 500W, 30 DEG C, after separation of solid and liquid obtains extracting solution and dries
Obtain, the quality of the Herba Silybi mariani powder after pulverizing and sieving and the volumn concentration of addition be the aqueous solution of 85% ethyl alcohol volume it
Than being 1:20, the water content of milk thistle extract is 6wt%.
In following embodiment, unless otherwise specified, golden hairpin dendrobium extract is that HERBA DENDROBII is dry, is ground into coarse powder,
Heat pure water in 65 DEG C extract 2h, separation of solid and liquid obtain extracting solution and obtained after drying, the quality of the HERBA DENDROBII after crushing with
The ratio between volume of pure water of addition is 1:20, the water content of golden hairpin dendrobium extract is 5wt%.Tiannu Magnolia flower extract is day
After the drying of female's magnolia and crushing, the aqueous solution that volumn concentration is 75% ethyl alcohol is added, is extracted 4 days at 25 DEG C, solid-liquid
Isolated extracting solution simultaneously obtains after drying, and the quality of Tiannu Magnolia flower and the volumn concentration of addition after crushing are 70%
The ratio between volume of aqueous solution of~80% ethyl alcohol is 1:8~1:12, the water content of Tiannu Magnolia flower extract is 5wt%.Golden small cup
Flower seed oil is that pot marigold seed is dry, is crushed to 40 mesh, and the pot marigold seed after crushing is added in extraction kettle, supercritical CO is used2
It is to extract 3 hours to obtain under 28MPa in 33 DEG C, extracting pressure, CO2Flow be 3kg/h.
In following embodiment, unless otherwise specified, lantern berry extract is purchased from Xi'an Qing Zhi Bioisystech Co., Ltd, people
Ginseng root extract is purchased from the Xi'an bio tech ltd Rui Ying, and Ka Misong Arnica flower extracts are purchased from the bright biology in Baoji side
Development corporation, Ltd., bignose rhinacanthus branchlet and leaf extract are purchased from the Lanzhou bio tech ltd water Lai Si, and ginger caul-fat is purchased from Guang Zhouhan
One hundred this daily use chemicals development in science and technology Co., Ltd.
Embodiment 1
The skin care compositions of the present embodiment, according to the mass fraction including 0.5 part of China fir leaf caulerpa extract, 0.5 part of water
Fly Ji extract, 0.5 part of golden hairpin dendrobium extract, 0.1 part of lantern berry extract and the flower extraction of 0.1 part of Tiannu Magnolia
Object.
Embodiment 2
The skin care compositions of the present embodiment, according to the mass fraction including 5 parts of China fir leaf caulerpa extract, 4 parts of milk thistle
Extract, 1 part of golden hairpin dendrobium extract, 0.5 part of lantern berry extract and 0.5 part of Tiannu Magnolia flower extract.
Embodiment 3
The skin care compositions of the present embodiment, according to the mass fraction including 0.5 part of China fir leaf caulerpa extract, 0.5 part of water
Fly Ji extract, 0.5 part of golden hairpin dendrobium extract, 0.1 part of lantern berry extract, 0.1 part of Tiannu Magnolia flower extract
And 0.1 part of ginseng root extract.
Embodiment 4
The skin care compositions of the present embodiment includes 0.5 part of spirulina extract, 0.5 part of fine grinding according to the mass fraction
Ji extract, 0.5 part of golden hairpin dendrobium extract, 0.1 part of lantern berry extract and 0.1 part of Tiannu Magnolia flower extract.
Embodiment 5
The skin care compositions of the present embodiment, include according to the mass fraction 0.5 part China fir leaf caulerpa extract, 0.5 part anti-
Bad hematic acid, 0.1 part of lantern berry extract and 0.1 part of Tiannu Magnolia flower extract.
Embodiment 6
The skin care compositions of the present embodiment, according to the mass fraction including 0.5 part of China fir leaf caulerpa extract, 0.5 part of water
Fly Ji extract, 0.5 part of golden hairpin dendrobium extract, 0.1 part of lantern berry extract, 0.1 part of Tiannu Magnolia flower extract,
90 parts of distilled water, 1 part of glycerine, 0.5 part of 1,2- pentanediols, 0.5 part of glycine betaine, 0.5 part of tocopherol, 0.5 part
Linseed oil, 0.5 part of hydrogenated jojoba oil, 0.5 part of white pond flower seed oil, 0.5 part of polypropylene ester cross-linked polymer, 0.01
Part citric acid, 0.3 part of sodium citrate, 0.1 part of cream jasmin france, 0.1 part of ginger caul-fat, 0.05 part of pot marigold seed oil and
0.3 part of disodium ethylene diamine tetraacetate.
Embodiment 7
The skin care compositions of the present embodiment, according to the mass fraction including 0.5 part of China fir leaf caulerpa extract, 0.5 part of water
Fly Ji extract, 0.5 part of golden hairpin dendrobium extract, 0.1 part of lantern berry extract, 0.1 part of Tiannu Magnolia flower extract,
90 parts of distilled water, 1 part of glycerine, 0.5 part of 1,2- pentanediols, 0.5 part of glycine betaine, 0.5 part of tocopherol, 0.5 part
Linseed oil, 0.5 part of hydrogenated jojoba oil, 0.5 part of white pond flower seed oil, 0.5 part of polypropylene ester cross-linked polymer, 0.01
The citric acid, 0.3 part of sodium citrate, 0.1 part of cream jasmin france, 0.2 part of ethylparaben and 0.3 part of ethylenediamine tetraacetic of part
Acetic acid disodium.
Embodiment 8
The skin care compositions of the present embodiment, according to the mass fraction including 0.5 part of China fir leaf caulerpa extract, 0.5 part of water
Fly Ji extract, 0.5 part of golden hairpin dendrobium extract, 0.1 part of lantern berry extract, 0.1 part of Tiannu Magnolia flower extract,
0.1 part of Ka Misong Arnicas flower extract, 0.1 part of bignose rhinacanthus branchlet and leaf extract, 90 parts of distilled water, 1 part of glycerine, 0.5
The 1,2- pentanediols, 0.5 part of glycine betaine, 0.5 part of tocopherol, 0.5 part of linseed oil, 0.5 part of hydrogenation Jojoba of part
Oil, 0.5 part of white pond flower seed oil, 0.5 part of polypropylene ester cross-linked polymer, 0.01 part of citric acid, 0.3 part of citric acid
Sodium, 0.1 part of cream jasmin france, 0.1 part of ginger caul-fat, 0.05 part of pot marigold seed oil and 0.3 part of disodium ethylene diamine tetraacetate.
Embodiment 9
The skin care compositions of the present embodiment, according to the mass fraction including 5 parts of China fir leaf caulerpa extract, 4 parts of milk thistle
Extract, 1 part of golden hairpin dendrobium extract, 0.5 part of lantern berry extract, 0.5 part of Tiannu Magnolia flower extract, 0.5 part
Ginseng root extract, 0.5 part of Ka Misong Arnicas flower extract, 0.5 part of bignose rhinacanthus branchlet and leaf extract, 50 parts of distillation
Water, 5 parts of glycerine, 4 parts of 1,2- pentanediols, 2 parts of glycine betaine, 2 parts of tocopherol, 5 parts of linseed oil, 5 parts of hydrogenation
Jojoba oil, 4 parts of white pond flower seed oil, 3 parts of polypropylene ester cross-linked polymer, 0.03 part of citric acid, 1 part of citric acid
Sodium, 0.3 part of lavender oil, 0.5 part of ginger caul-fat, 0.2 part of pot marigold seed oil and 0.5 part of ethylenediamine tetra-acetic acid three
Sodium.
Embodiment 10
The skin care compositions of the present embodiment, according to the mass fraction including 0.5 part of China fir leaf caulerpa extract, 0.5 part of water
Fly Ji extract, 0.5 part of golden hairpin dendrobium extract, 0.1 part of lantern berry extract, 0.1 part of Tiannu Magnolia flower extract,
90 parts of distilled water, 1 part of glycerine, 0.5 part of 1,2- pentanediols, 0.5 part of glycine betaine, 0.5 part of tocopherol, 0.5 part
Linseed oil, 0.5 part of hydrogenated jojoba oil, 0.5 part of white pond flower seed oil, 0.5 part of polypropylene ester cross-linked polymer, 0.01
Part citric acid, 0.3 part of sodium citrate, 0.1 part of cream jasmin france, 0.1 part of ginger caul-fat, 0.05 part of pot marigold seed oil,
0.3 part of disodium ethylene diamine tetraacetate and 0.05 part of epithelical cell growth factor.
Embodiment 11
The skin care compositions of the present embodiment, according to the mass fraction including 0.5 part of China fir leaf caulerpa extract, 0.5 part of water
Fly Ji extract, 0.5 part of golden hairpin dendrobium extract, 0.1 part of lantern berry extract, 0.1 part of Tiannu Magnolia flower extract,
90 parts of distilled water, 1 part of glycerine, 0.5 part of 1,2- pentanediols, 0.5 part of glycine betaine, 0.5 part of tocopherol, 0.5 part
Linseed oil, 0.5 part of hydrogenated jojoba oil, 0.5 part of white pond flower seed oil, 0.5 part of polypropylene ester cross-linked polymer, 0.01
The citric acid of part, 0.3 part of sodium citrate, 0.1 part of cream jasmin france, 0.3 part of disodium ethylene diamine tetraacetate, 0.1 part of ginger
Caul-fat, 0.05 part of pot marigold seed oil and 0.05 part of vascular endothelial growth factor.
Embodiment 12
The skin care compositions of the present embodiment, according to the mass fraction including 5 parts of China fir leaf caulerpa extract, 4 parts of milk thistle
Extract, 1 part of golden hairpin dendrobium extract, 0.5 part of lantern berry extract, 0.5 part of Tiannu Magnolia flower extract, 0.5 part
Ginseng root extract, 0.5 part of Ka Misong Arnicas flower extract, 0.5 part of bignose rhinacanthus branchlet and leaf extract, 50 parts of distillation
Water, 5 parts of glycerine, 4 parts of 1,2- pentanediols, 2 parts of glycine betaine, 2 parts of tocopherol, 5 parts of linseed oil, 5 parts of hydrogenation
Jojoba oil, 4 parts of white pond flower seed oil, 3 parts of polypropylene ester cross-linked polymer, 0.03 part of citric acid, 1 part of citric acid
Sodium, 0.3 part of lavender oil, 0.5 part of sodium versenate, 0.5 part of ginger caul-fat, 0.2 part of pot marigold seed oil
And 0.3 part of stem cell factor.
Embodiment 13
The skin care compositions of the present embodiment, according to the mass fraction including 5 parts of China fir leaf caulerpa extract, 4 parts of milk thistle
Extract, 1 part of golden hairpin dendrobium extract, 0.5 part of lantern berry extract, 0.5 part of Tiannu Magnolia flower extract, 0.5 part
Ginseng root extract, 0.5 part of Ka Misong Arnicas flower extract, 0.5 part of bignose rhinacanthus branchlet and leaf extract, 50 parts of distillation
Water, 5 parts of glycerine, 4 parts of 1,2- pentanediols, 2 parts of glycine betaine, 2 parts of tocopherol, 5 parts of linseed oil, 5 parts of hydrogenation
Jojoba oil, 4 parts of white pond flower seed oil, 3 parts of polypropylene ester cross-linked polymer, 0.03 part of citric acid, 1 part of citric acid
Sodium, 0.3 part of lavender oil, 0.5 part of sodium versenate, 0.5 part of ginger caul-fat, 0.2 part of pot marigold seed oil,
0.1 part of epithelical cell growth factor, 0.1 part of stem cell factor and 0.1 part of vascular endothelial growth factor.
Embodiment 14
The skin care compositions of the present embodiment includes 0.5 part of spirulina extract, 0.5 part of fine grinding according to the mass fraction
Ji extract, 0.5 part of golden hairpin dendrobium extract, 0.1 part of lantern berry extract, 0.1 part of Tiannu Magnolia flower extract, 90
The distilled water of part, 1 part of glycerine, 0.5 part of 1,2- pentanediols, 0.5 part of glycine betaine, 0.5 part of tocopherol, 0.5 part of Asia
Flaxseed oil, 0.5 part of hydrogenated jojoba oil, 0.5 part of white pond flower seed oil, 0.5 part of polypropylene ester cross-linked polymer, 0.01 part
Citric acid, 0.3 part of sodium citrate, 0.1 part of cream jasmin france, 0.1 part of ginger caul-fat, 0.05 part of pot marigold seed oil and
0.3 part of disodium ethylene diamine tetraacetate.
Embodiment 15
The skin care compositions based on China fir leaf caulerpa extract of the present embodiment includes 0.5 part of China fir leaf according to the mass fraction
Caulerpa extract, 0.5 part of ascorbic acid, 0.1 part of lantern berry extract, 0.1 part of Tiannu Magnolia flower extract, 90 parts
Distilled water, 1 part of glycerine, 0.5 part of 1,2- pentanediols, 0.5 part of glycine betaine, 0.5 part of tocopherol, 0.5 part of linseed
Oil, 0.5 part of hydrogenated jojoba oil, 0.5 part of white pond flower seed oil, 0.5 part of polypropylene ester cross-linked polymer, 0.01 part of lemon
Lemon acid, 0.3 part of sodium citrate, 0.1 part of cream jasmin france, 0.1 part of ginger caul-fat, 0.05 part of pot marigold seed oil and 0.3 part
Disodium ethylene diamine tetraacetate.
Test：
1, organoleptic properties are tested
The skin care compositions of embodiment 6~15 is observed under room temperature and non-direct sunlight respectively, above-mentioned skin care compositions
It is fine and smooth, uniform color, pure in smell.
2, centrefuge experiment
It takes the skin care compositions of the embodiment 6~15 of 5g to be fitted into the centrifuge tube of 10mL respectively, 20 is centrifuged with 3000rpm
Minute, above-mentioned skin care compositions is without lamination.
3, heat-resisting, cold-resistant test
The skin care compositions of the embodiment of 20g 6~15 is positioned in 40 DEG C of insulating box, after 24 hours, is restored respectively
To room temperature, above-mentioned skin care compositions does not occur being layered or deposited phenomenon.
The skin care compositions of the embodiment of 20g 6~15 is positioned in -10 DEG C of insulating box respectively, after 24 hours, is restored
To room temperature, above-mentioned skin care compositions does not occur being layered or deposited phenomenon.
4, biological stability
The skin care compositions of Example 6~15 is placed in 25 DEG C and stores 30 days and 60 days respectively, and with reference to national standard
GB7918.1~5-1987 measures total number of bacterial colonies and mould yeast colony sum, assay method ginseng in above-mentioned skin care compositions
According to GB7918.1~5-1987.
After measured, total number of bacterial colonies of the skin care compositions of embodiment 6~15 the 30th day and the 60th day is respectively less than
10cfu/g, and mould yeast colony sum is respectively less than 10cfu/g, illustrates that ginger caul-fat can make skin care with the addition of pot marigold seed oil
Composition has preferably bacteriostasis property, suitable with the antiseptic property of ethylparaben, is not necessarily to other additional preservatives, can keep away
Exempt from stimulation and damage of the chemical preservative to skin.
5, inoxidizability is tested
The skin care compositions of Examples 1 to 5 is diluted with distilled water, obtaining the mass concentration containing skin care compositions is
The sample solution of 0.05g/L carries out anti-oxidant test.
The skin care compositions of embodiment 6~15 is diluted with distilled water, obtaining the mass concentration containing skin care compositions is
The sample solution of 5.0g/L carries out anti-oxidant test.
(1) to the clearance rate of DPPH
Taking the above-mentioned each sample solution of 3mL, the ethanol solution with 3mL 0.2mol/mL DPPH, mixing are protected from light and put respectively
It sets 30 minutes, absorbance A is measured at 517nm1, while the above-mentioned each sample for measuring 3mL mixed with the absolute ethyl alcohol of 3mL after
Absorbance B at 517nm1, measure 3mL absolute ethyl alcohol mixed with the ethanol solution of 3mL 0.2mol/mL DPPH after
Absorbance C at 517nm1, and calculate DPPH elimination factors according to following formula (1-1).The sample test three of each embodiment
Group, calculates the average value of three groups of results, and measurement result refers to table 1.Formula (1-1) is as follows：
In formula, A1- each sample reacted with DPPH after absorbance, B1- each sample and the mixed extinction of absolute ethyl alcohol
Degree, C1The mixed absorbance of the ethanol solution of-absolute ethyl alcohol and DPPH.
(2) to the clearance rate of OH
The above-mentioned each sample solution for taking 2mL respectively, with the salicylic acid solution of 2mL, 10mmol/L, the sulphur of 2mL, 10mmol/L
Sour ferrous solution mixing, is added the hydrogenperoxide steam generator of 2mL, 88mmol/L, after being reacted 30 minutes in 37 DEG C of water-baths after mixing, in
Absorbance A is measured at 510nm2, replace hydrogenperoxide steam generator to measure absorbance B with the distilled water of 2mL2, with the distilled water generation of 2mL
Absorbance C is measured for sample solution2, and according to the clearance rate of following formula (1-2) calculating OH.The sample of each embodiment is surveyed
Three groups are tried, the average value of three groups of results is calculated, measurement result refers to table 1.Formula (1-2) is as follows：
In formula, A2- sample and the absorbance after hydroperoxidation, B2- molten instead of hydrogen peroxide with the distilled water of 2mL
Liquid measures absorbance, C2- with the distilled water of 2mL replace sample solution measure absorbance.
(3) to O2Clearance rate
By the Tris-HCl buffer solutions containing 5mL, pH8.2 in 25 DEG C of water-baths 20 minutes, the sample solution of 2mL is sequentially added
With the pyrogallol hydrochloric acid solution of 0.5mL, 5mmol/L, mixing, reacts 4 minutes in 25 DEG C of water-baths, immediately in 230nm immediately
Place measures its absorbance A3, pyrogallol hydrochloric acid solution is replaced with the hydrochloric acid solution of 0.5mL, 0.1mol/L, measures and is surveyed at 230nm
Fixed its absorbance B3, replace sample solution with the distilled water of 2mL and measure to measure its absorbance C at 230nm3, and according to following public affairs
Formula (1-3) calculates O2Clearance rate.Three groups of the sample test of each embodiment, calculates the average value of three groups of results, measurement result
Refer to table 1.Formula (1-3) is as follows：
In formula, A3- sample reacted with pyrogallol hydrochloric acid solution after absorbance, B3- with the salt of 0.5mL, 0.1mol/L
Acid solution replaces pyrogallol hydrochloric acid solution to measure absorbance, C3- with the distilled water of 2mL replace sample solution measure absorbance.
The inoxidizability of the skin care compositions of 1 embodiment 1~15 of table
| DPPH free radical scavenging activities | OH free radical scavenging activities | ·O2Clearance rate | |
| Embodiment 1 | 65.1% | 70.2% | 75.6% |
| Embodiment 2 | 66.4% | 71.3% | 75.8% |
| Embodiment 3 | 68.7% | 75.1% | 74.9% |
| Embodiment 4 | 60.9% | 67.6% | 68.2% |
| Embodiment 5 | 61.9% | 68.8% | 70.8% |
| Embodiment 6 | 76.3% | 79.6% | 80.1% |
| Embodiment 7 | 68.1% | 71.5% | 81.4% |
| Embodiment 8 | 78.5% | 80.4% | 80.8% |
| Embodiment 9 | 89.1% | 92.2% | 90.7% |
| Embodiment 10 | 75.8% | 78.7% | 80.7% |
| Embodiment 11 | 76.9% | 79.1% | 79.8% |
| Embodiment 12 | 89.4% | 92.8% | 90.9% |
| Embodiment 13 | 90.2% | 93.9% | 91.1% |
| Embodiment 14 | 71.1% | 75.8% | 72.5% |
| Embodiment 15 | 72.5% | 76.1% | 74.1% |
As can be seen from Table 1, the DPPH free radical scavenging activities of the skin care compositions of Examples 1 to 3 are not less than 65.1%,
OH free radical scavenging activities are not less than 70.2%, O2Clearance rate is not less than 75.6%, the skin care compositions of embodiment 6~14
DPPH free radical scavenging activities be not less than 68.1%, and OH free radical scavenging activities be not less than 71.5%, O2Clearance rate is equal
Not less than 80.1%, illustrate that the above-mentioned skin care compositions based on China fir leaf caulerpa extract has stronger inoxidizability, Neng Gouqing
Except the free radical of skin, damage of the free radical to skin, delay skin aging are prevented.The skin care compositions of embodiment 1 it is above-mentioned
The clearance rate of three kinds of free radicals is better than above-mentioned three kinds of free radical scavenging activities of the skin care compositions of embodiment 4~5, and embodiment 6
Skin care compositions above-mentioned three kinds of free radicals clearance rate better than above-mentioned three kinds of skin care compositions of embodiment 14~15 from
By the clearance rate of base, illustrate that China fir leaf caulerpa extract and the synergistic effect of gold fork Herba Dendrobii extract can further increase skin care group
Close the inoxidizability of object.
6, skin proof test
(1) volunteer that the age is 28 years old~36 years old is laggard in daily face cleaning using the skin care compositions of embodiment 6~15
Row skin care, usage time are 60 days, and volunteer's every morning and evening carry out skin care using the skin care compositions of the present invention respectively,
Application method is specially：It takes the composition 2mL of the present invention to be uniformly applied to skin of face, smears 5 minutes.Wherein, each to implement
Example has 20 volunteers to use.It should be noted that other skin nursing situations of above-mentioned all volunteers are consistent.
Above-mentioned volunteer states progress skin index test in the 30th day and the 60th day of skin care compositions in use, random to take out
It takes 5 volunteers therein to test, and calculates the average value of parameters, test result is as shown in table 2.Skin is carried out to refer to
When number test, tested using moisture of skin index tester (Fes Kai Er).The ideal value of moisture be 40%~
60%, the ideal value of oil content is 15%~20%, and the ideal value of coefficient of elasticity is 0.45~0.55.
The skin of the skin care compositions of 2 embodiment 6~15 of table tries out test result
From table 2 it can be seen that after skin care compositions using embodiment 6~13, the moisture of the face of volunteer and
Coefficient of elasticity is improved, and oil content declines, and face lacks moisture and the phenomenon of elasticity is significantly improved, and illustrates above-mentioned
Skin care compositions based on China fir leaf caulerpa extract has the effect of preferable moisturizing, can alleviate cutis laxa, reduces skin
Microgroove and wrinkle；Secondly, above-mentioned all volunteers do not occur the reaction of the irritability such as skin allergy, skin pimples, long acne, say
Bright above-mentioned skin care compositions is safe and free of toxic and side effects.
The skin care compositions of embodiment 6 to face moisture and coefficient of elasticity improvement be superior to embodiment 14~
The effect of 15 skin care compositions illustrates the synergistic effect of China fir leaf caulerpa extract and golden hairpin dendrobium extract, is more advantageous to guarantor
Hold the water profit and elasticity of skin.Simultaneously using the volunteer of the skin care compositions of embodiment 6, the moisture before use in the 60th day contains
15% and 11.1% is respectively increased with coefficient of elasticity in moisture before amount use in than the 30th day, uses the skin care group of embodiment 14
The volunteer of object is closed, the moisture before moisture use in than the 30th day before use in the 60th day carries respectively with coefficient of elasticity
High 7.3% and 6.8%, using the volunteer of the skin care compositions of embodiment 15, the moisture before use in the 60th day is than
12.5% and 4.7% is respectively increased with coefficient of elasticity in moisture before use in 30 days, illustrates the skin care compositions energy of embodiment 6
Enough moistures and elasticity for quickly improving skin further relate to cooperateing with for China fir leaf caulerpa extract and golden hairpin dendrobium extract
Effect, can quickly improve the moisture and elasticity of skin.
The skin care compositions of embodiment 10 is better than the improvement of the coefficient of elasticity of face the effect of the skin care compositions of embodiment 6
Fruit, illustrate the addition of renovation agent be conducive to improve skin elasticity keep the younger state of skin to desalinate microgroove and wrinkle.
The skin care compositions of embodiment 13 is better than the improvement of the coefficient of elasticity of face the effect of the skin care compositions of embodiment 12, explanation
A variety of renovation agent synergistic effects, can further increase the elasticity of skin.
(2) age is 28 years old~36 years old often stays up late, the apparent volunteer of livid ring around eye is as subject, using implementation
The skin care compositions of example 6~15 carries out skin care after daily face cleaning, and usage time is 60 days, volunteer's every morning and evening point
Skin care compositions that Shi Yong be not of the invention carries out skin care, and application method is specially：The composition 2mL of the present invention is taken uniformly to be applied to
Skin of face is smeared 5 minutes.Wherein, each embodiment has 20 volunteers to use.It should be noted that above-mentioned institute
There are other skin nursing situations of volunteer consistent.Above-mentioned volunteer states the 30th day and the 60th day of skin care compositions in use
Observe trial effect, trial effect index：Black circle does not improve>Black circle improves>Black circle is obviously improved, and is calculated and reached each
The number of index, test result are as shown in table 3.
(3) the apparent volunteer of red blood silk that the age is 28 years old~36 years old is as subject, using embodiment 6~15
Skin care compositions carries out skin care after daily face cleaning, and usage time is 60 days, and volunteer's every morning and evening use this respectively
The composition of invention carries out skin care, and application method is specially：It takes the composition 2mL of the present invention to be uniformly applied to skin of face, applies
It smears 5 minutes.Wherein, each embodiment has 20 volunteers to use.It should be noted that its of above-mentioned all volunteers
His skin nursing situation is consistent.Above-mentioned volunteer states the effect on probation of observation in the 30th day and the 60th day of skin care compositions in use
Fruit, trial effect index：Red blood silk does not change>Red blood silk is desalinated>Red blood silk is obviously desalinated, and calculates the people for reaching each index
Number, test result are as shown in table 3.
The skin repair test result for the skin care compositions that 3 embodiment 6~15 of table is prepared
From table 3 it can be seen that volunteer is after the skin care compositions using embodiment 6~13, livid ring around eye have improvement, red
The trace of blood also has desalination, illustrates that the above-mentioned skin care compositions based on China fir leaf caulerpa extract can repair damaged skin, promotes skin
Skin cell neogenesis repairs livid ring around eye, desalinates red blood silk.Wherein, obviously changed using black circle after the skin care compositions of embodiment 10
The number that kind number and red blood silk is obviously desalinated is significantly more than embodiment 6, illustrates that the addition of renovation agent being capable of apparent black eye
The skin problems such as circle and red blood silk；The repairing effect of the skin care compositions of embodiment 13 is better than the repairing effect of embodiment 12, says
The synergistic effect of bright a variety of renovation agents can improve the repairing performance of skin care compositions.
The repairing effect of the skin care compositions of embodiment 6 is better than the repairing effect of the skin care compositions of embodiment 14~15,
Illustrate that the synergistic effect of China fir leaf caulerpa extract and golden hairpin dendrobium extract is more advantageous to the repairing effect for improving skin care compositions,
Improve the skin problems such as black circle and red blood silk.
Each technical characteristic of embodiment described above can be combined arbitrarily, to keep description succinct, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, it is all considered to be the range of this specification record.
Several embodiments of the invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the protection of the present invention
Range.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (10)
1. a kind of skin care compositions based on China fir leaf caulerpa extract, which is characterized in that in terms of mass fraction, including 0.5 part~5
Part China fir leaf caulerpa extract, 0.5 part~4 parts of milk thistle extract, 0.5 part~1 part of golden hairpin dendrobium extract, 0.1 part
~0.5 part of lantern berry extract and 0.1 part~0.5 part of Tiannu Magnolia flower extract.
2. the skin care compositions according to claim 1 based on China fir leaf caulerpa extract, which is characterized in that with mass fraction
Meter, further includes 0.1 part~0.5 part of ginseng root extract.
3. the skin care compositions according to claim 2 based on China fir leaf caulerpa extract, which is characterized in that with mass fraction
Meter, including 1 part~3 parts of China fir leaf caulerpa extract, 1 part~2 parts of milk thistle extract, 0.6 part~0.8 part of HERBA DENDROBII
Extract, 0.2 part~0.4 part of lantern berry extract, 0.2 part~0.4 part of Tiannu Magnolia flower extract and 0.2 part~0.4
The ginseng root extract of part.
4. the skin care compositions according to claim 1 based on China fir leaf caulerpa extract, which is characterized in that with mass fraction
Meter, further includes 0.1 part~0.5 part of Ka Misong Arnicas flower extract and 0.1 part~0.5 part of bignose rhinacanthus branchlet and leaf extract.
5. the skin care compositions according to claim 1 based on China fir leaf caulerpa extract, which is characterized in that with mass fraction
Meter further includes 0.1 part~0.5 part of ginger caul-fat and 0.05 part~0.2 part of pot marigold seed oil.
6. the skin care compositions according to claim 1 based on China fir leaf caulerpa extract, which is characterized in that with mass fraction
Meter, further includes 1 part~5 parts of glycerine, 0.5 part~4 parts of 1,2- pentanediols and 0.5 part~2 parts of glycine betaine.
7. the skin care compositions according to claim 1 based on China fir leaf caulerpa extract, which is characterized in that with mass fraction
Meter, further include 0.5 part~2 parts of tocopherol, 0.5 part~5 parts of linseed oil, 0.5 part~5 parts of hydrogenated jojoba oil and
0.5 part~4 parts of white pond flower seed oil.
8. the skin care compositions according to claim 1 based on China fir leaf caulerpa extract, which is characterized in that with mass fraction
Meter, further includes 0.5 part~3 parts of polypropylene ester cross-linked polymer.
9. the skin care compositions according to claim 1 based on China fir leaf caulerpa extract, which is characterized in that with mass fraction
Meter, further includes 0.05 part~0.3 part of renovation agent, and the renovation agent is selected from epithelical cell growth factor, stem cell factor and blood
At least one of endothelial tube growth factor.
10. skin care compositions the answering in facial mask according to any one of claims 1 to 9 based on China fir leaf caulerpa extract
With.
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| CN201810315672.XA CN108309841A (en) | 2018-04-10 | 2018-04-10 | Skin care compositions based on China fir leaf caulerpa extract and its application |
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| CN201810315672.XA CN108309841A (en) | 2018-04-10 | 2018-04-10 | Skin care compositions based on China fir leaf caulerpa extract and its application |
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| CN110051605A (en) * | 2019-05-25 | 2019-07-26 | 广东大鹏医药科技有限公司 | A kind of oral cleaning anti-inflammation liquid of the ingredient containing trollflower and preparation method thereof |
| CN111700829A (en) * | 2020-05-29 | 2020-09-25 | 四川万物本草健康科技有限公司 | Persimmon leaf-containing product composition and application thereof in skin care products |
| CN113876668A (en) * | 2021-11-16 | 2022-01-04 | 北京青颜博识健康管理有限公司 | Anti-saccharification plant-derived composition, preparation method thereof and application thereof in beauty products |
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| CN105899186A (en) * | 2014-01-10 | 2016-08-24 | 科思摩国际成分公司 | Plant extract comprising sucrose esters as an active agent for use in a cosmetic, dermatological or nutricosmetic composition |
| CN106236676A (en) * | 2016-10-23 | 2016-12-21 | 广东轻工职业技术学院 | A kind of vegetable composition with senile-resistant efficacy and application thereof |
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| CN105899186A (en) * | 2014-01-10 | 2016-08-24 | 科思摩国际成分公司 | Plant extract comprising sucrose esters as an active agent for use in a cosmetic, dermatological or nutricosmetic composition |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110051605A (en) * | 2019-05-25 | 2019-07-26 | 广东大鹏医药科技有限公司 | A kind of oral cleaning anti-inflammation liquid of the ingredient containing trollflower and preparation method thereof |
| CN111700829A (en) * | 2020-05-29 | 2020-09-25 | 四川万物本草健康科技有限公司 | Persimmon leaf-containing product composition and application thereof in skin care products |
| CN113876668A (en) * | 2021-11-16 | 2022-01-04 | 北京青颜博识健康管理有限公司 | Anti-saccharification plant-derived composition, preparation method thereof and application thereof in beauty products |
| CN113876668B (en) * | 2021-11-16 | 2023-11-03 | 上海青颜博识生物技术有限公司 | Anti-saccharification plant source composition, preparation method thereof and application thereof in cosmetic product |
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Application publication date: 20180724 |