CN108281243B - Device and method for treating surface of micro-stack structure insulating material by discharge plasma - Google Patents

Device and method for treating surface of micro-stack structure insulating material by discharge plasma Download PDF

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CN108281243B
CN108281243B CN201810085786.XA CN201810085786A CN108281243B CN 108281243 B CN108281243 B CN 108281243B CN 201810085786 A CN201810085786 A CN 201810085786A CN 108281243 B CN108281243 B CN 108281243B
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王珏
严萍
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Abstract

本发明公开了一种放电等离子体处理微堆层结构绝缘材料表面的装置,该装置包括:高压引入极一端通过电源高压输出端子与脉冲电源连接,另一端通过高压导电杆与高压电极连接;接地电极设于高压电极的正下方,接地电极通过接地导电杆与底座连接并接地;被处理试样固定于高压电极和接地电极之间,且被处理试样与高压电极和接地电极紧密贴合无间隙。本发明还公开了一种放电等离子体处理微堆层结构绝缘材料表面的方法,包括:步骤1、根据各设备的连接组装处理装置;步骤2、放置被处理试样使其固定于高压电极与接地电极之间且不存在间隙;步骤3、打开脉冲电源形成均匀的辉光放电;步骤4、辉光放电产生的低温等离子体对被处理试样表面进行融蚀处理。

Figure 201810085786

The invention discloses a device for treating the surface of insulating material of a micro-stack structure by discharge plasma. The device comprises: one end of a high-voltage introduction electrode is connected to a pulse power supply through a high-voltage output terminal of a power supply, and the other end is connected to a high-voltage electrode through a high-voltage conductive rod; The electrode is set directly under the high-voltage electrode, and the ground electrode is connected to the base and grounded through the grounding conductive rod; the sample to be processed is fixed between the high-voltage electrode and the ground electrode, and the sample to be processed is closely attached to the high-voltage electrode and the ground electrode without any damage. gap. The invention also discloses a method for treating the surface of an insulating material of a micro-stack layer structure by discharge plasma, comprising: step 1, assembling a processing device according to the connection of each equipment; step 2, placing the sample to be processed to fix it on the high-voltage electrode and the There is no gap between the ground electrodes; step 3, turn on the pulse power supply to form a uniform glow discharge; step 4, the low-temperature plasma generated by the glow discharge performs ablation treatment on the surface of the treated sample.

Figure 201810085786

Description

放电等离子体处理微堆层结构绝缘材料表面的装置及方法Apparatus and method for treating surface of insulating material of micro-stack structure by discharge plasma

技术领域technical field

本发明涉及绝缘子技术领域,具体而言,涉及放电等离子体处理微堆层结构绝缘材料表面的装置及方法。The present invention relates to the technical field of insulators, and in particular, to a device and method for treating the surface of an insulating material of a micro-stack structure with discharge plasma.

背景技术Background technique

微堆层结构绝缘材料,即微米到毫米级厚度的金属和绝缘层叠式复合绝缘结构,在直流、交流和脉冲高电压都显示出了优秀的沿面绝缘强度,大大提高了绝缘效率和质量,为大型脉冲功率设备、电力设备的关键功能实现及小型化、高效化提供途径。The micro-stacked insulating material, that is, the metal and insulating laminated composite insulating structure with a thickness of micrometers to millimeters, shows excellent creeping dielectric strength in DC, AC and pulsed high voltage, which greatly improves the insulation efficiency and quality. The realization of key functions of large-scale pulse power equipment and power equipment, as well as the way to miniaturize and improve efficiency.

微堆层绝缘材料的表面加工和处理工艺是保证其性能实现的关键技术。微堆层绝缘制备工艺复杂,采用机械加工、精细抛光和超声清洗的方法进行形状加工和表面处理。从目前的使用效果来看,采用这种工艺加工出的微堆层绝缘材料,它的闪络特性一致性很难保证,这主要是由于绝缘子表面处理工艺造成的。可见,微堆层绝缘要达到优秀的沿面闪络强度其表面处理工艺是关键技术,也是它广泛应用必须解决的问题。微堆层绝缘子的形状需要经过机械加工获得,虽然目前的加工精度已经很高,其表面似乎十分光滑,但由于金属与绝缘材料的机械特性的巨大差别,从微观看,金属层表面存在微凸起和毛刺是必然的。金属凸起的强场效应将会显著作用于两者界面上的不均匀处,使金属层电子发射、电子电荷运动及相互碰撞特性发生剧烈变化,造成局部电场集中,从而导致更快的绝缘破坏,所以要实现微堆层绝缘的优秀绝缘性能,必须有良好的表面处理工艺保证。The surface processing and treatment technology of micro-stacked insulating materials are the key technologies to ensure the realization of their performance. The micro-stack insulation preparation process is complicated, and the shape processing and surface treatment are carried out by means of mechanical processing, fine polishing and ultrasonic cleaning. Judging from the current use effect, it is difficult to guarantee the consistency of the flashover characteristics of the micro-stacked insulating material processed by this process, which is mainly caused by the surface treatment process of the insulator. It can be seen that the surface treatment process is the key technology for micro-stack insulation to achieve excellent flashover strength along the surface, and it is also a problem that must be solved in its wide application. The shape of the micro-stacked insulator needs to be obtained by mechanical processing. Although the current processing accuracy is very high, the surface seems to be very smooth, but due to the huge difference in the mechanical properties of metal and insulating materials, microscopically, there are micro-convexities on the surface of the metal layer. Raises and glitches are inevitable. The strong field effect of the metal protrusion will significantly affect the unevenness of the interface between the two, causing the metal layer electron emission, electron charge movement and mutual collision characteristics to change drastically, resulting in local electric field concentration, resulting in faster insulation damage. , so to achieve the excellent insulation performance of the micro-stack insulation, there must be a good surface treatment process guarantee.

等离子体表面处理技术是在材料表面处理科学领域出现的一种高科技环保新技术。采用低温等离子体表面处理技术可以有效去除绝缘材料表面的金属凸起和污染物,研磨金属层,可以利用等离子体技术对微堆层绝缘进行表面处理,消除微堆层绝缘材料表面的金属凸起、毛刺、绝缘凸起,保证其表面的均匀一致,降低材料绝缘性能的分散性,整体提高材料的沿面绝缘强度。Plasma surface treatment technology is a high-tech environmental protection new technology in the field of material surface treatment science. The use of low-temperature plasma surface treatment technology can effectively remove the metal protrusions and contaminants on the surface of the insulating material, grind the metal layer, and use the plasma technology to perform surface treatment on the insulation of the micro-stack layer to eliminate the metal protrusion on the surface of the insulation material of the micro-stack layer. , burrs, insulation protrusions, to ensure the uniformity of the surface, reduce the dispersion of the insulation properties of the material, and improve the overall insulation strength of the material along the surface.

发明内容SUMMARY OF THE INVENTION

为解决上述问题,本发明的目的在于提供一种放电等离子体处理微堆层结构绝缘材料表面的装置及方法,消除微堆层绝缘材料表面的金属、绝缘的凸起、毛刺,保证其表面的均匀一致,降低材料绝缘性能的分散性,整体提高材料的沿面绝缘强度。In order to solve the above-mentioned problems, the purpose of the present invention is to provide a device and method for treating the surface of the insulating material of the micro-stacked layer structure by discharge plasma, so as to eliminate the metal, insulating protrusions and burrs on the surface of the insulating material of the micro-stacked layer, and ensure the surface of the insulating material. Uniform and consistent, reducing the dispersion of the insulation properties of the material, and improving the overall insulation strength of the material along the surface.

本发明提供了一种放电等离子体处理微堆层结构绝缘材料表面的装置,该装置包括:The invention provides a device for treating the surface of an insulating material of a micro-stack structure with discharge plasma, the device comprising:

高压引入极,其一端通过电源高压输出端子与脉冲电源连接,所述高压引入极另一端通过高压导电杆与高压电极连接;a high-voltage lead-in pole, one end of which is connected to the pulse power supply through a high-voltage output terminal of the power supply, and the other end of the high-voltage lead-in pole is connected to the high-voltage electrode through a high-voltage conductive rod;

接地电极,其设于所述高压电极的正下方,所述接地电极通过接地导电杆与底座连接并接地;a grounding electrode, which is arranged directly below the high-voltage electrode, and the grounding electrode is connected to the base through a grounding conductive rod and grounded;

被处理试样,其固定于所述高压电极和所述接地电极之间,且所述被处理试样与所述高压电极和所述接地电极紧密贴合无间隙。The sample to be processed is fixed between the high-voltage electrode and the ground electrode, and the sample to be processed is in close contact with the high-voltage electrode and the ground electrode without a gap.

作为本发明的进一步改进,所述高压引入极外部套有一个输入绝缘子。As a further improvement of the present invention, an input insulator is sheathed outside the high-voltage lead-in pole.

作为本发明的进一步改进,所述高压导电杆、所述高压电极、所述被处理试样、所述接地电极和所述接地导电杆均处于放电处理室外壳与所述底座形成的密闭空间中。As a further improvement of the present invention, the high-voltage conductive rod, the high-voltage electrode, the sample to be processed, the ground electrode and the grounded conductive rod are all located in a closed space formed by the discharge processing chamber shell and the base .

作为本发明的进一步改进,所述放电处理室外壳的两侧分别设有进气接口和出气接口,且所述进气接口与气瓶连接,所述出气接口与真空泵连接。As a further improvement of the present invention, an air inlet port and an air outlet port are respectively provided on both sides of the housing of the discharge treatment chamber, and the air inlet port is connected to a gas cylinder, and the air outlet port is connected to a vacuum pump.

作为本发明的进一步改进,所述脉冲电源输出为纳秒级重复频率的高压脉冲,其脉冲宽度为20ns~200ns,脉冲放电频率为200Hz~10k Hz,电压幅值为5kV~50kV,功率为200W~2000W。As a further improvement of the present invention, the pulse power output is a high-voltage pulse with a nanosecond repetition frequency, the pulse width is 20ns-200ns, the pulse discharge frequency is 200Hz-10k Hz, the voltage amplitude is 5kV-50kV, and the power is 200W ~2000W.

作为本发明的进一步改进,所述高压电极与所述接地电极之间的竖直距离为2mm~30mm。As a further improvement of the present invention, the vertical distance between the high voltage electrode and the ground electrode is 2 mm˜30 mm.

作为本发明的进一步改进,所述被处理试样为圆柱体、椭圆柱体或平板型。As a further improvement of the present invention, the sample to be processed is a cylinder, an elliptical cylinder or a flat plate.

作为本发明的进一步改进,当所述被处理试样为圆柱体、椭圆柱体时,所述高压电极与所述接地电极为圆形平板状,且所述高压电极与所述接地电极的直径为其二者与所述被处理试样接触面上最长方向距离的2倍以上且不能小于20mm;当所述被处理试样平板型时,所述高压电极与所述接地电极为指状或条状,所述高压电极与所述接地电极的长度为其二者间距离的5倍以上,且所述高压电极与所述接地电极的长度与所述被处理试样的长度或所述被处理试样需处理区域的长度相同。As a further improvement of the present invention, when the sample to be processed is a cylinder or an elliptical cylinder, the high-voltage electrode and the ground electrode are circular flat plates, and the diameters of the high-voltage electrode and the ground electrode are It is more than 2 times the longest direction distance between the two and the contact surface of the sample to be processed and cannot be less than 20mm; when the sample to be processed is flat, the high-voltage electrode and the ground electrode are finger-shaped or strip, the length of the high voltage electrode and the ground electrode is more than 5 times the distance between them, and the length of the high voltage electrode and the ground electrode is the same as the length of the sample to be processed or the The length of the treated area of the sample to be treated is the same.

作为本发明的进一步改进,所述接地电极为位置固定的电极,所述高压电极为位置可调节的电极。As a further improvement of the present invention, the ground electrode is an electrode whose position is fixed, and the high-voltage electrode is an electrode whose position can be adjusted.

本发明还提供了一种等放电离子体处理微堆层结构绝缘材料表面的方法,该方法包括以下步骤:The present invention also provides a method for plasma treatment of the surface of the insulating material of the micro-stack structure, the method comprising the following steps:

步骤1、组装放电等离子体处理微堆层结构绝缘材料表面的装置;Step 1. Assemble a device for treating the surface of the insulating material of the micro-stack structure with discharge plasma;

步骤2、将被处理试样放置于接地电极上,并调节高压电极的位置,使被处理试样固定于高压电极与接地电极之间且不存在间隙;Step 2. Place the sample to be processed on the ground electrode, and adjust the position of the high-voltage electrode so that the sample to be processed is fixed between the high-voltage electrode and the ground electrode without a gap;

步骤3、打开脉冲电源,通过高压电极和接地电极在被处理试样的两端施加高压脉冲,并在被处理试样的表面形成均匀的辉光放电;Step 3. Turn on the pulse power supply, apply a high-voltage pulse to both ends of the sample to be processed through the high-voltage electrode and the ground electrode, and form a uniform glow discharge on the surface of the sample to be processed;

步骤4、步骤3中辉光放电产生的低温等离子体对被处理试样表面的金属、绝缘的凸起或毛刺等进行融蚀处理;In step 4 and step 3, the low-temperature plasma generated by the glow discharge performs ablation treatment on the metal, insulating protrusions or burrs on the surface of the sample to be treated;

步骤5、待被处理试样处理完成,对其表面形貌进行检测。Step 5. After the processing of the sample to be processed is completed, its surface morphology is detected.

本发明的有益效果为:第一,本发明所述的低温放电等离子体处理金属与绝缘层叠复合材料表面的方法,可使金属绝缘层叠复合材料表面更加光滑,减小材料在电场下的电场畸变,有利于提高其沿面闪络特性;第二,本发明提供的方法能够解决一般机械加工、打磨和抛光无法消除对金属绝缘层叠结构材料金属绝缘交界面的破坏,同时也可应用于纯金属材料和绝缘材料的表面处理,消除材料表面的毛刺和凸起。The beneficial effects of the present invention are as follows: First, the method for treating the surface of a metal-insulating laminated composite material by low-temperature discharge plasma according to the present invention can make the surface of the metal-insulating laminated composite material smoother and reduce the electric field distortion of the material under an electric field. , which is beneficial to improve its flashover characteristics along the surface; secondly, the method provided by the present invention can solve the problem that general machining, grinding and polishing cannot eliminate the damage to the metal-insulating interface of the metal-insulating laminated structure material, and can also be applied to pure metal materials. And the surface treatment of insulating materials to eliminate burrs and protrusions on the surface of the material.

附图说明Description of drawings

图1为本发明实施例所述的一种放电等离子体处理微堆层结构绝缘材料表面的方法流程图;FIG. 1 is a flowchart of a method for treating the surface of an insulating material of a micro-stack layer structure with discharge plasma according to an embodiment of the present invention;

图2为本发明实施例所述的一种放电等离子体处理微堆层结构绝缘材料表面的装置处理平板型被处理样品的结构示意图;2 is a schematic structural diagram of a device for treating a flat-type treated sample by a device for treating the surface of an insulating material of a micro-stack structure with discharge plasma according to an embodiment of the present invention;

图3为本发明实施例所述的平板型被处理样品与高压电极、接地电极连接方式侧视图;3 is a side view of the connection mode of the flat-plate type processed sample, the high-voltage electrode and the ground electrode according to the embodiment of the present invention;

图4为本发明实施例所述的平板型被处理样品与高压电极、接地电极连接方式俯视图;FIG. 4 is a top view of the connection mode of the flat-plate processed sample, the high-voltage electrode and the ground electrode according to the embodiment of the present invention;

图5为本发明实施例所述的一种放电等离子体处理微堆层结构绝缘材料表面的装置处理圆柱形被处理样品的结构示意图。FIG. 5 is a schematic structural diagram of a device for treating the surface of an insulating material of a micro-stack structure with discharge plasma according to an embodiment of the present invention, and a schematic structural diagram of a cylindrical sample to be treated.

图中,In the figure,

1、高压引入极;2输入绝缘子;3、放电处理室外壳;4、高压导电杆;5、高压电极;6、被处理试样;7、接地电极;8、接地导电杆;9、进气接口;10、抽气接口;11、底座;12、脉冲电源;13、电源高压输出端子;14、真空泵;15、气瓶。1. High voltage lead-in pole; 2. Input insulator; 3. Discharge treatment chamber shell; 4. High-voltage conductive rod; 5. High-voltage electrode; 6. Processed sample; 7. Grounding electrode; 8. Grounding conductive rod; Interface; 10, pumping interface; 11, base; 12, pulse power supply; 13, high voltage output terminal of power supply; 14, vacuum pump; 15, gas cylinder.

具体实施方式Detailed ways

下面通过具体的实施例并结合附图对本发明做进一步的详细描述。The present invention will be further described in detail below through specific embodiments and in conjunction with the accompanying drawings.

实施例1Example 1

如图2所示,本发明实施例1所述的是一种放电等离子体处理微堆层结构绝缘材料表面的装置处理平板型被处理样品,该装置包括:As shown in FIG. 2, Embodiment 1 of the present invention describes a device for treating the surface of insulating material of a micro-stack structure with discharge plasma to treat a flat-type processed sample, and the device includes:

高压引入极1,其一端通过电源高压输出端子13与脉冲电源12连接,高压引入极1另一端通过高压导电杆4与高压电极5连接;The high-voltage lead-in pole 1 has one end connected to the pulse power supply 12 through the power supply high-voltage output terminal 13, and the other end of the high-voltage lead-in pole 1 is connected to the high-voltage electrode 5 through the high-voltage conductive rod 4;

接地电极7,其设于高压电极5的正下方,接地电极7通过接地导电杆8与底座11连接并接地;The ground electrode 7 is arranged directly below the high voltage electrode 5, and the ground electrode 7 is connected to the base 11 through the grounding conductive rod 8 and grounded;

被处理试样6,其固定于高压电极5和接地电极7之间,且被处理试样6与高压电极5和接地电极7紧密贴合无间隙。The sample 6 to be processed is fixed between the high voltage electrode 5 and the ground electrode 7 , and the sample 6 to be processed is closely attached to the high voltage electrode 5 and the ground electrode 7 without a gap.

进一步的,高压引入极1外部套有若干个输入绝缘子2。Further, a plurality of input insulators 2 are sheathed outside the high voltage lead-in pole 1 .

进一步的,高压导电杆4、高压电极5、被处理试样6、接地电极7和接地导电杆8均处于放电处理室外壳3与底座11形成的密闭空间中。Further, the high-voltage conductive rod 4 , the high-voltage electrode 5 , the processed sample 6 , the ground electrode 7 and the grounded conductive rod 8 are all located in the closed space formed by the discharge processing chamber shell 3 and the base 11 .

进一步的,放电处理室外壳3的两侧分别设有进气接口9和出气接口10,且进气接口9与气瓶15连接,出气接口10与真空泵14连接。Further, an air inlet port 9 and an air outlet port 10 are respectively provided on both sides of the discharge processing chamber shell 3 , and the air inlet port 9 is connected with the gas cylinder 15 , and the air outlet port 10 is connected with the vacuum pump 14 .

放电等离子体处理微堆层结构绝缘材料表面的装置包括一套电源系统、一套电极系统以及一个用于处理试样的放电处理室:电源系统由脉冲电源12和电源高压输出端子13组成;电极系统由高压引入极1、高压导电杆4、高压电极5、接地电极7和接地导电杆8组成;放电处理室由输入绝缘子2、放电处理室外壳3、进气接口9、出气接口10和底座组成。脉冲电源12高压极通过放电处理室高压引入极1、高压导杆4输入到高压电极5,脉冲电源12的低压极和放电处理室底座11共同接地,组成放电回路。放电处理室的底座11通过接地导杆8与接地电极7连接。被处理试样6是金属绝缘层式复合材料,其固定在高压电极5和接地电极7之间,两个电极与被处理试样6紧密贴合,不存在任何间隙,高压电极5和接地电极7之间电场均匀。The device for treating the surface of the insulating material of the microstack structure by discharge plasma includes a power supply system, an electrode system and a discharge processing chamber for processing samples: the power supply system consists of a pulse power supply 12 and a high voltage output terminal 13 of the power supply; the electrodes The system consists of high-voltage introduction pole 1, high-voltage conductive rod 4, high-voltage electrode 5, grounding electrode 7 and grounding conductive rod 8; the discharge processing chamber is composed of input insulator 2, discharge processing chamber shell 3, inlet port 9, outlet port 10 and base composition. The high voltage electrode of the pulse power supply 12 is input to the high voltage electrode 5 through the high voltage introduction electrode 1 and the high voltage guide rod 4 of the discharge processing chamber. The base 11 of the discharge processing chamber is connected to the ground electrode 7 through the ground rod 8 . The sample 6 to be treated is a metal insulating layer type composite material, which is fixed between the high-voltage electrode 5 and the ground electrode 7. The two electrodes are closely attached to the sample 6 to be treated without any gap. The high-voltage electrode 5 and the ground electrode The electric field between 7 is uniform.

进一步的,脉冲电源12输出为纳秒级重复频率的高压脉冲,其脉冲宽度为20ns~200ns,脉冲放电频率为200Hz~10k Hz,电压幅值为5kV~50kV,功率为200W~2000W。脉冲电源12的参数选择需要根据被处理试样6的形状、高度和直径以及放电处理室内的气压和气体种类来决定。被处理试样6的高度越高,电源放电的电压幅值越高,频率越快;放电处理室内的气压越低电源放电的电压幅值越低,频率越慢。电源放电参数电压幅值、频率、脉冲宽度之间的关系为电压幅值升高,频率和脉冲宽度降低;频率升高,电压幅值和脉冲宽度降低,脉冲宽度升高,电压幅值和频率降低。脉冲电源12的参数选择要保证脉冲放电在被处理试样6表面产生均匀的辉光放电并形成一定浓度的等离子体。为保证在被处理试样6表面产生均匀的辉光放电,在1个大气压下空气中,被处理试样6的宽度(即高压电极5和接地电极7间距离)在5mm以内时,脉冲场强的设计可参考25kV/cm,脉冲频率1kHz,脉冲宽度100ns;被处理试样6的宽度(即高压电极5和接地电极7间距离)在5mm到15mm之间时,脉冲电源的放电参数设计可参考脉冲场强20kV/cm,脉冲频率2kHz,脉冲宽度100ns;被处理试样6的宽度(即高压电极5和接地电极7间距离)在15mm到30mm之间时,脉冲电源的放电参数设计可参考脉冲场强18kV/cm,脉冲频率1kHz,脉冲宽度100ns。形成的等离子体密度在1013-1014个/cm3之间。本实施例中的放电处理室内的气体可以为氮气、空气也可以是氩气或其他气体,放电处理室可以承受一个大气压的内外压力,一般为几十到几千帕。且放电处理室的高压输入端和放电处理室外壳3之间最高可耐受重复频率为10kHz、30kV的纳秒级脉冲电压。Further, the output of the pulse power supply 12 is a high-voltage pulse with a nanosecond repetition frequency, the pulse width is 20ns-200ns, the pulse discharge frequency is 200Hz-10k Hz, the voltage amplitude is 5kV-50kV, and the power is 200W-2000W. The parameter selection of the pulse power supply 12 needs to be determined according to the shape, height and diameter of the sample 6 to be processed, as well as the gas pressure and gas type in the discharge processing chamber. The higher the height of the sample 6 to be treated, the higher the voltage amplitude of the power supply discharge and the faster the frequency; the lower the air pressure in the discharge processing chamber, the lower the voltage amplitude of the power supply discharge and the slower the frequency. The relationship between the voltage amplitude, frequency and pulse width of the power supply discharge parameters is that the voltage amplitude increases, the frequency and pulse width decrease; the frequency increases, the voltage amplitude and pulse width decrease, the pulse width increases, the voltage amplitude and frequency decrease reduce. The parameters of the pulse power supply 12 are selected to ensure that the pulse discharge generates a uniform glow discharge on the surface of the sample 6 to be processed and forms plasma with a certain concentration. In order to ensure a uniform glow discharge on the surface of the sample 6 to be treated, in the air at 1 atmosphere, when the width of the sample 6 to be treated (ie the distance between the high voltage electrode 5 and the ground electrode 7) is within 5 mm, the pulse field The strong design can refer to 25kV/cm, pulse frequency 1kHz, pulse width 100ns; when the width of the sample 6 to be processed (ie the distance between the high voltage electrode 5 and the ground electrode 7) is between 5mm and 15mm, the discharge parameters of the pulse power supply are designed. For reference, the pulse field strength is 20kV/cm, the pulse frequency is 2kHz, and the pulse width is 100ns; when the width of the sample 6 to be processed (ie the distance between the high voltage electrode 5 and the ground electrode 7) is between 15mm and 30mm, the discharge parameters of the pulse power supply are designed The reference pulse field strength is 18kV/cm, the pulse frequency is 1kHz, and the pulse width is 100ns. The density of the formed plasma is between 10 13 -10 14 /cm 3 . In this embodiment, the gas in the discharge processing chamber can be nitrogen, air, or argon or other gases, and the discharge processing chamber can withstand an internal and external pressure of one atmosphere, generally tens to several thousand Pa. Moreover, the high-voltage input end of the discharge processing chamber and the outer shell 3 of the discharge processing chamber can withstand a nanosecond pulse voltage with a repetition frequency of 10 kHz and 30 kV at the highest.

进一步的,高压电极5与接地电极7之间的竖直距离为2mm~30mm。Further, the vertical distance between the high voltage electrode 5 and the ground electrode 7 is 2 mm˜30 mm.

进一步的,当被处理试样6为平板型时,高压电极5与接地电极7为指状或条状,高压电极5与接地电极7的长度为其二者间距离的5倍以上,且高压电极5与接地电极7的长度与被处理试样6的长度或被处理试样6需处理区域的长度相同。高压电极5与接地电极7间的电场方向与其二者的长度方向相互垂直。Further, when the sample 6 to be processed is a flat plate type, the high voltage electrode 5 and the ground electrode 7 are in the shape of fingers or strips, the length of the high voltage electrode 5 and the ground electrode 7 is more than 5 times the distance between them, and the high voltage The lengths of the electrode 5 and the ground electrode 7 are the same as the length of the sample 6 to be processed or the length of the area to be processed of the sample 6 to be processed. The direction of the electric field between the high-voltage electrode 5 and the ground electrode 7 is perpendicular to the longitudinal directions of the two.

进一步的,接地电极7为位置固定的电极,高压电极5为位置可调节的电极。在放置被处理试样6时,先将被处理试样6放置于接地电极7上,在通过调节高压电极5的位置来调整高压电极5与接地电极7间的距离,最终使被处理试样6固定于两个电极的中心并与两个电极紧密贴合。Further, the ground electrode 7 is an electrode with a fixed position, and the high-voltage electrode 5 is an electrode with an adjustable position. When placing the sample 6 to be processed, first place the sample 6 to be processed on the ground electrode 7, and then adjust the distance between the high voltage electrode 5 and the ground electrode 7 by adjusting the position of the high voltage electrode 5, and finally make the sample to be processed 6 is fixed in the center of the two electrodes and closely fits with the two electrodes.

本实施例以长度为20mm、宽度为10mm的处理区域为里说明。如图2所示,放电处理室高压引入极1固定于高压导电杆4一端,另一端与高压电极5连接,电源低压极和放电处理室金属底座11共同接地,组成放电回路。放电处理室底座11通过接地导电杆8与接地电极7连接。This embodiment is described with a processing area having a length of 20 mm and a width of 10 mm. As shown in Figure 2, the high voltage lead-in electrode 1 of the discharge processing chamber is fixed on one end of the high voltage conductive rod 4, and the other end is connected to the high voltage electrode 5. The low voltage electrode of the power supply and the metal base 11 of the discharge processing chamber are grounded together to form a discharge circuit. The discharge processing chamber base 11 is connected to the ground electrode 7 through the ground conductive rod 8 .

如图3所示,高压电极5和接地电极7分别压紧在被处理试样6上,高压电极5和接地电极7与被处理试样6紧密接触,无缝隙。被处理试样6在高压电极5和接地电极7之间的区域是被处理试样6的放电处理区域。如图4所示,为了保证放电处理区域的电场基本均匀,高压电极5和接地电极7的两边圆滑过渡。高压电极5和接地电极7与被处理试样6的长度相同,为20mm。高压电极5和接地电极7间的距离与被处理试样6的被处理区域宽度相同,为10mm。As shown in FIG. 3 , the high voltage electrode 5 and the ground electrode 7 are respectively pressed on the sample 6 to be processed, and the high voltage electrode 5 and the ground electrode 7 are in close contact with the sample 6 to be processed without any gap. The region of the sample to be treated 6 between the high voltage electrode 5 and the ground electrode 7 is the discharge treatment region of the sample to be treated 6 . As shown in FIG. 4 , in order to ensure that the electric field in the discharge treatment area is basically uniform, the two sides of the high voltage electrode 5 and the ground electrode 7 transition smoothly. The high-voltage electrode 5 and the ground electrode 7 have the same length as the sample 6 to be processed, which is 20 mm. The distance between the high voltage electrode 5 and the ground electrode 7 was the same as the width of the treated area of the treated sample 6, and was 10 mm.

如图2所示,脉冲电源12输出高压通过高压引入极1、高压导电杆4、高压电极5、接地电极7、接地导电杆8施加到被处理试样6两端。脉冲电源12输出电压幅值为18kV,频率5kHz,脉冲宽度70ns。连续的放电产生密度约1013个/cm3的较为均匀放电等离子体持续作用在被处理试样6表面,融蚀被处理试样6表面金属、绝缘的凸起和毛刺,使被处理试样6的表面更加光滑,金属与绝缘的交界面更加清晰,提高被处理试样6的沿面绝缘强度。As shown in FIG. 2 , the high voltage output from the pulse power supply 12 is applied to both ends of the sample 6 to be processed through the high voltage introduction electrode 1 , the high voltage conductive rod 4 , the high voltage electrode 5 , the ground electrode 7 , and the ground conductive rod 8 . The output voltage amplitude of the pulse power supply 12 is 18kV, the frequency is 5kHz, and the pulse width is 70ns. The continuous discharge produces a relatively uniform discharge plasma with a density of about 10 13 /cm 3 , which continuously acts on the surface of the sample 6 to be treated, and erodes the metal, insulating protrusions and burrs on the surface of the sample 6 to be treated. The surface of 6 is smoother, the interface between the metal and the insulation is clearer, and the creeping dielectric strength of the treated sample 6 is improved.

实施例2Example 2

如图5所示,本发明实施例2所述的是一种放电等离子体处理微堆层结构绝缘材料表面的装置处理圆柱形被处理样品:As shown in FIG. 5 , the second embodiment of the present invention is a device for treating the surface of insulating material of a micro-stack structure with discharge plasma to treat a cylindrical sample to be processed:

本实施例与实施例1的区别之处在于,当所述被处理试样为圆柱体、椭圆柱体时,所述高压电极与所述接地电极为圆形平板状,且所述高压电极与所述接地电极的直径为其二者与所述被处理试样接触面上最长方向距离的2倍以上且不能小于20mm。本实施例以低气压氩气作为环境气体,以直径为15mm、高度为20mm的被处理试样6为例说明。The difference between this embodiment and Embodiment 1 is that when the sample to be processed is a cylinder or an elliptical cylinder, the high-voltage electrode and the ground electrode are circular plates, and the high-voltage electrode and the The diameter of the ground electrode is more than 2 times the longest direction distance between the two and the contact surface of the sample to be processed and cannot be less than 20 mm. In this embodiment, low-pressure argon gas is used as the ambient gas, and a sample 6 to be processed having a diameter of 15 mm and a height of 20 mm is used as an example for description.

如图5所示,放电处理室高压引入极1固定于高压导电杆4一端,另一端与高压电极5连接,电源低压极和放电处理室金属底座11共同接地,组成放电回路。放电处理室底座11通过接地导电杆8与接地电极7连接。高压电极5压紧放置在接地电极7中心的被处理试样6上,高压电极5、接地电极7与被处理试样6紧密接触,无缝隙。被处理试样6的圆柱侧面是放电处理区域。为了保证放电处理区域的电场基本均匀,高压电极5和接地电极7的边缘圆滑过渡。高压电极5和接地电极7直径为40mm,厚度为15mm。As shown in Figure 5, the high voltage lead-in electrode 1 of the discharge processing chamber is fixed on one end of the high voltage conductive rod 4, and the other end is connected to the high voltage electrode 5. The low voltage electrode of the power supply and the metal base 11 of the discharge processing chamber are grounded together to form a discharge circuit. The discharge processing chamber base 11 is connected to the ground electrode 7 through the ground conductive rod 8 . The high voltage electrode 5 is pressed and placed on the processed sample 6 in the center of the ground electrode 7, and the high voltage electrode 5 and the ground electrode 7 are in close contact with the processed sample 6 without any gap. The cylindrical side surface of the sample 6 to be treated is an electric discharge treatment area. In order to ensure that the electric field in the discharge treatment area is substantially uniform, the edges of the high voltage electrode 5 and the ground electrode 7 transition smoothly. The high-voltage electrode 5 and the ground electrode 7 are 40 mm in diameter and 15 mm in thickness.

如图5所示,真空泵14为放电处理室抽气,放电处理室内的真空度达到10-4Pa,真空泵14停止抽气,关闭出气接口10。气瓶15向放电处理室内通入氩气,放电处理室内真空度达到10Pa时,停止输入氩气,关闭进气接口9。As shown in FIG. 5 , the vacuum pump 14 evacuates the discharge processing chamber, and the vacuum degree in the discharge processing chamber reaches 10 −4 Pa, the vacuum pump 14 stops pumping, and the air outlet 10 is closed. The gas cylinder 15 is fed with argon gas into the discharge processing chamber. When the vacuum degree in the discharge processing chamber reaches 10Pa, the input of argon gas is stopped, and the inlet port 9 is closed.

如图5所示,脉冲电源12输出高压通过高压引入极1、高压导电杆4、高压电极5、接地电极7、接地导电杆8施加到被处理试样6两端。脉冲电源12输出电压幅值为3.5kV,频率1kHz,脉冲宽度70ns。连续的放电产生密度约1013个/cm3的较为均匀放电等离子体持续作用在被处理试样6表面,融蚀被处理试样6表面金属、绝缘的凸起和毛刺,使被处理试样6的表面更加光滑,金属与绝缘的交界面更加清晰,提高被处理试样6的沿面绝缘强度。As shown in FIG. 5 , the high voltage output from the pulse power supply 12 is applied to both ends of the sample 6 to be processed through the high voltage introduction electrode 1 , the high voltage conductive rod 4 , the high voltage electrode 5 , the ground electrode 7 , and the ground conductive rod 8 . The output voltage amplitude of the pulse power supply 12 is 3.5kV, the frequency is 1kHz, and the pulse width is 70ns. The continuous discharge produces a relatively uniform discharge plasma with a density of about 10 13 /cm 3 , which continuously acts on the surface of the sample 6 to be treated, and erodes the metal, insulating protrusions and burrs on the surface of the sample 6 to be treated. The surface of 6 is smoother, the interface between the metal and the insulation is clearer, and the creeping dielectric strength of the treated sample 6 is improved.

实施例3Example 3

如图1所示,本发明实施例2所述的是一种放电等离子体处理微堆层结构绝缘材料表面的方法,该方法包括以下步骤:As shown in FIG. 1 , Embodiment 2 of the present invention is a method for treating the surface of an insulating material of a micro-stack structure with discharge plasma, and the method includes the following steps:

步骤1、根据权利要求1-9中任意一项所述的放电等离子体处理微堆层结构绝缘材料表面装置中各个设备间的连接关系,组装放电等离子体处理微堆层结构绝缘材料表面的装置:放电处理室高压引入极1固定于高压导电杆4一端,另一端与高压电极5连接,电源低压极和放电处理室金属底座11共同接地,组成放电回路。放电处理室底座11通过接地导电杆8与接地电极7连接。高压电极5压紧放置在接地电极7中心的被处理试样6上,高压电极5、接地电极7与被处理试样6紧密接触,无缝隙。Step 1. According to the connection relationship between the various devices in the device for treating the surface of the insulating material of the micro-stack layer structure according to any one of claims 1-9, assemble the device for treating the surface of the insulating material of the micro-stack layer structure by the discharge plasma : The high voltage introduction electrode 1 of the discharge treatment chamber is fixed on one end of the high voltage conductive rod 4, and the other end is connected to the high voltage electrode 5. The low voltage electrode of the power supply and the metal base 11 of the discharge treatment chamber are grounded together to form a discharge circuit. The discharge processing chamber base 11 is connected to the ground electrode 7 through the ground conductive rod 8 . The high voltage electrode 5 is pressed and placed on the processed sample 6 in the center of the ground electrode 7, and the high voltage electrode 5 and the ground electrode 7 are in close contact with the processed sample 6 without any gap.

步骤2、将被处理试样6放置于接地电极7上,并调节高压电极5的位置,使被处理试样6固定于高压电极5与接地电极7之间且不存在间隙;Step 2. Place the processed sample 6 on the ground electrode 7, and adjust the position of the high-voltage electrode 5 so that the processed sample 6 is fixed between the high-voltage electrode 5 and the ground electrode 7 and there is no gap;

步骤3、打开脉冲电源12,通过高压电极5和接地电极7在被处理试样6的两端施加高压脉冲,并在被处理试样6的表面形成均匀的辉光放电;Step 3. Turn on the pulse power supply 12, apply a high-voltage pulse to both ends of the sample 6 to be processed through the high-voltage electrode 5 and the ground electrode 7, and form a uniform glow discharge on the surface of the sample 6 to be processed;

步骤4、步骤3中辉光放电产生的低温等离子体对被处理试样6表面的绝缘凸起或毛刺等进行融蚀处理;In step 4 and step 3, the low-temperature plasma generated by the glow discharge performs ablation treatment on the insulating protrusions or burrs on the surface of the sample 6 to be treated;

步骤5、待被处理试样6处理完成,对其表面形貌进行检测。Step 5. After the processing of the sample 6 to be processed is completed, its surface morphology is detected.

脉冲电源12通过高压电极5和接地电极7在被处理样品6两端施加重复频率纳秒级高压脉冲,在被处理样品6表面形成较为均匀的辉光放电,辉光放电产生一定浓度低温等离子体将被处理样品6表面的金属、绝缘凸起、毛刺等融蚀,使微堆层结构绝缘材料的表面更加光滑,金属与绝缘的交界面更加清晰,从而提高被处理样品6的沿面绝缘强度。The pulse power supply 12 applies a high-voltage pulse with a repetition rate of nanoseconds at both ends of the sample 6 to be processed through the high-voltage electrode 5 and the ground electrode 7, and a relatively uniform glow discharge is formed on the surface of the sample 6 to be processed, and the glow discharge generates a certain concentration of low-temperature plasma The metal, insulating protrusions, burrs, etc. on the surface of the sample 6 to be processed are melted, so that the surface of the insulating material of the micro-stack structure is smoother, and the interface between the metal and the insulation is clearer, thereby improving the insulation strength of the sample 6 along the surface.

以上所述仅为本发明的优选实施例而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention. For those skilled in the art, the present invention may have various modifications and changes. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included within the protection scope of the present invention.

Claims (8)

1. An apparatus for treating the surface of an insulating material with a micro-stack structure by discharge plasma, comprising:
one end of the high-voltage leading-in pole (1) is connected with a pulse power supply (12) through a power supply high-voltage output terminal (13), the other end of the high-voltage leading-in pole (1) is connected with a high-voltage electrode (5) through a high-voltage conducting rod (4), the pulse power supply (12) outputs high-voltage pulses with nanosecond repetition frequency, the pulse width of the high-voltage pulses is 20 ns-200 ns, the pulse discharge frequency is 200 Hz-10 kHz, the voltage amplitude is 5 kV-50 kV, and the power is 200W-2000W;
the grounding electrode (7) is arranged right below the high-voltage electrode (5), and the grounding electrode (7) is connected with the base (11) through a grounding conducting rod (8) and is grounded;
a sample (6) to be processed fixed between the high voltage electrode (5) and the ground electrode (7), wherein the sample (6) to be processed is in close contact with the high voltage electrode (5) and the ground electrode (7) without a gap;
when the sample (6) to be processed is a cylinder or an elliptic cylinder, the high-voltage electrode (5) and the grounding electrode (7) are in a circular flat plate shape, and the diameters of the high-voltage electrode (5) and the grounding electrode (7) are more than 2 times of the longest direction distance on the contact surface of the high-voltage electrode and the grounding electrode and the sample (6) to be processed and cannot be less than 20 mm; when the sample (6) to be processed is in a flat plate shape, the high-voltage electrode (5) and the grounding electrode (7) are in a finger shape or a strip shape, the length of the high-voltage electrode (5) and the length of the grounding electrode (7) are more than 5 times of the distance between the high-voltage electrode and the grounding electrode, and the length of the high-voltage electrode (5) and the length of the grounding electrode (7) are the same as the length of the sample (6) to be processed or the length of an area of the sample (6) to be processed.
2. The apparatus for treating the surface of an insulating material of a micro-stack structure by discharge plasma according to claim 1, wherein an input insulator (2) is externally sleeved on the high voltage leading-in electrode (1).
3. The apparatus for treating the surface of the insulation material with micro-stack structure by discharge plasma according to claim 1, wherein the high voltage conducting rod (4), the high voltage electrode (5), the sample to be treated (6), the grounding electrode (7) and the grounding conducting rod (8) are all in the closed space formed by the discharge treatment chamber shell (3) and the base (11).
4. The apparatus for treating the surface of the insulation material with the micro-stack structure by discharge plasma according to claim 3, wherein the discharge treatment chamber shell (3) is provided with an air inlet interface (9) and an air outlet interface (10) on two sides respectively, the air inlet interface (9) is connected with an air bottle (15), and the air outlet interface (10) is connected with a vacuum pump (14).
5. The apparatus for discharge plasma treatment of the surface of insulation material of micro-stack structure according to claim 1, characterized in that the vertical distance between the high voltage electrode (5) and the ground electrode (7) is 2mm to 30 mm.
6. The apparatus for treating the surface of an insulating material of a micro-stack structure by discharge plasma according to claim 1, wherein the sample (6) to be treated is a cylindrical, elliptical or flat plate.
7. The apparatus for discharge plasma treatment of the surface of insulation material of micro-stack structure according to claim 1, characterized in that the ground electrode (7) is a fixed electrode and the high voltage electrode (5) is an adjustable electrode.
8. A method for treating a surface of a micro-stack structured insulating material using the apparatus for treating a surface of a micro-stack structured insulating material by discharge plasma according to any one of claims 1 to 7, comprising the steps of:
step 1, assembling a device for treating the surface of an insulating material with a micro-stack structure by using discharge plasma;
step 2, placing the sample (6) to be processed on the grounding electrode (7), and adjusting the position of the high-voltage electrode (5) to ensure that no gap exists between the high-voltage electrode (5) and the grounding electrode (7) when the sample (6) to be processed is fixed;
step 3, turning on a pulse power supply (12), applying high-voltage pulses to two ends of the sample (6) to be processed through a high-voltage electrode (5) and a grounding electrode (7), and forming uniform glow discharge on the surface of the sample (6) to be processed;
4, carrying out ablation treatment on the metal, the insulated bulges or burrs on the surface of the sample (6) to be treated by the low-temperature plasma generated by glow discharge in the step 3;
and 5, finishing the treatment of the sample (6) to be treated, and detecting the surface appearance of the sample.
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CN110739109A (en) * 2019-10-10 2020-01-31 华北电力大学 System and method for improving surface electrical strength of insulators in C4F7N gas
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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1029702A2 (en) * 1999-02-15 2000-08-23 Konica Corporation Surface treatment method, production method for ink jet recording medium, and ink jet recording medium
JP3393444B2 (en) * 1993-04-05 2003-04-07 株式会社ダイオー Atmospheric pressure glow discharge plasma treatment method
CN2930194Y (en) * 2006-07-18 2007-08-01 万京林 Glow discharge low temperature plasma device
CN105913984A (en) * 2016-05-17 2016-08-31 西安交通大学 Device and method for processing surface of basin-type insulator by means of glow discharge fluorination
CN106312215A (en) * 2016-09-09 2017-01-11 清华大学 Method and device for removing metal burs
CN107466150A (en) * 2017-09-19 2017-12-12 南京工业大学 Three-dimensional low-temperature plasma processing device

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3393444B2 (en) * 1993-04-05 2003-04-07 株式会社ダイオー Atmospheric pressure glow discharge plasma treatment method
EP1029702A2 (en) * 1999-02-15 2000-08-23 Konica Corporation Surface treatment method, production method for ink jet recording medium, and ink jet recording medium
CN2930194Y (en) * 2006-07-18 2007-08-01 万京林 Glow discharge low temperature plasma device
CN105913984A (en) * 2016-05-17 2016-08-31 西安交通大学 Device and method for processing surface of basin-type insulator by means of glow discharge fluorination
CN106312215A (en) * 2016-09-09 2017-01-11 清华大学 Method and device for removing metal burs
CN107466150A (en) * 2017-09-19 2017-12-12 南京工业大学 Three-dimensional low-temperature plasma processing device

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
大气压脉冲放电等离子体的研究现状与展望;卢新培,严萍,任春生,邵涛;《中国科学:物理学 力学 天文学》;20110720;全文 *

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