CN108272834A - A kind of Processing methods technique of resina liquidamberis medicinal material - Google Patents
A kind of Processing methods technique of resina liquidamberis medicinal material Download PDFInfo
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- CN108272834A CN108272834A CN201710066571.9A CN201710066571A CN108272834A CN 108272834 A CN108272834 A CN 108272834A CN 201710066571 A CN201710066571 A CN 201710066571A CN 108272834 A CN108272834 A CN 108272834A
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- raw material
- water
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- resina liquidamberis
- medicinal material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Alternative & Traditional Medicine (AREA)
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- Botany (AREA)
- Medical Informatics (AREA)
- Medicinal Chemistry (AREA)
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- General Health & Medical Sciences (AREA)
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- Extraction Or Liquid Replacement (AREA)
Abstract
The present invention relates to a kind of Processing methods techniques of resina liquidamberis medicinal material.Including using liquid resina liquidamberis as raw material, liquid resina liquidamberis being heated to filter while hot after 100 110 DEG C, remove the impurity in raw material, filtrate using distilling with water, be dried under reduced pressure collection heavy constituent, be cooled to room temperature and obtain resina liquidamberis medicinal material product.This technological process is easy to operate, and high income, safety are good, at low cost.
Description
Technical field
The present invention relates to a kind of Processing methods techniques of resina liquidamberis medicinal material, especially a kind of to use heat filtering, distilling with water
Method.
Background technology
Resina liquidamberis medicinal material is liquid resina liquidamberis resin in the present invention.Resina liquidamberis is traditional Chinese medicine, and source is gold thread
The resin of plum section plant Chinese sweet gum.Resina liquidamberis medicinal material also known as beautiful sweetgum resin, rue, RESINA LIQUIDAMBARIS FORMOSANAE have promoting blood circulation and stopping pain, solve taking poison and growing muscle due,
Cooling blood and hemostasis acts on, and is used for injury from falling down, and ulcer sore pain is spitted blood, bleeding from five sense organs or subcutaneous tissue, traumatic hemorrhage etc..In addition to clinical formulation application, and
The raw material of Moschus traumatic injury and rheumatism cream etc..
Resina liquidamberis sterling is irregular blocky, or is in similar round graininess, is differed in size, diameter mostly between 0.5-1cm,
A small number of reachable 3cm.Surface is faint yellow to yellowish-brown, translucent or opaque.Matter is crisp frangible, is crushed mask hyaloid gloss.Gas
Faint scent, fragrance is denseer when burning, lightly seasoned.
Liquidambar resinoid ketone acid containing A Mubu, Ah nurse's butolic acid, bis- alkyd of A Mubu, Fructus Liquidambaris ketone acid, two alkyd of Fructus Liquidambaris,
Resina liquidamberis ursolic acid, resina liquidamberis novic acid.This product is dissolved in ethyl alcohol.
Current existing production technology is dissolved using high concentration ethanol, and the method that precipitated impurities refilter needs to use
To a large amount of alcohol solvent, technique is more complex, cost is higher and there are some potential safety problemss.
Invention content
The present invention relates to a kind of Processing methods techniques of resina liquidamberis medicinal material.Including using liquid resina liquidamberis as raw material, by liquid
Resina liquidamberis filters while hot after being heated to 100-110 DEG C, remove raw material in impurity, filtrate using distilling with water, be dried under reduced pressure
Heavy constituent is collected, room temperature is cooled to and obtains resina liquidamberis medicinal material product.This technological process is easy to operate, and high income, safety be good, cost
It is low.
The present invention relates to a kind of Processing methods techniques of resina liquidamberis medicinal material, which is characterized in that includes the following steps：
1）Raw material heats：Raw material is heated to 100-110 DEG C,
2）Heat filtering cleans：The raw material of heating is filtered while hot, removes impurity,
3）Distilling with water：Raw material after removing impurity is subjected to distilling with water, so that heavy constituent is separated with light component, is dried under reduced pressure,
Heavy constituent is collected,
4）Cooling condensation：The heavy constituent of collection is cooled to room temperature, condenses into product.
1, preferably, step 1）The heating temperature is that raw material is heated to 100-110 using water-bath or oil bath mode
℃。
2, preferably, step 3）The distillation pressure of the distilling with water is no more than 0.2MPa（Interlayer heat supply）, vacuum degree
0.09-0.1MPa。
3, preferably, step 3）The limit that light component is detached when the distilling with water is the 17%-20% of inventory.
4, there are following advantages by the present invention：Heat filtering removal of impurities is more safe with ethyl alcohol dissolving removing impurity by means of precipitation than traditional handicraft,
It is at low cost, it is simple for process, solve the difficult disadvantage of resinae medicinal material removal of impurities, meanwhile, it is dried under reduced pressure technique letter using distilling with water
Single, equipment requirement is low.
Specific implementation mode
The present invention is further illustrated for following embodiment, but the scope of protection of present invention is not limited to down
Row embodiment.
Example 1：
Take sweetgum fat raw material（The place of production：Guangxi）100kg is heated to 100 DEG C of temperature of charge, is filtered to remove impurity, material is added
Equipment is concentrated under reduced pressure and carries out distilling with water, isolated light component is the 17% of raw material, collects heavy constituent, obtains product 80.9kg, is received
Rate 80.9%.
Example 2：
Take sweetgum fat raw material（The place of production：Guangxi）100kg is heated to 105 DEG C of temperature of charge, is filtered to remove impurity, material is added
Reduced pressure equipment carries out distilling with water, isolated light component is the 17% of raw material, collects heavy constituent, obtains product 79.8kg, receives
Rate 79.8%.
Example 3：
Take sweetgum fat raw material（The place of production：Guangxi）100kg is heated to 110 DEG C of temperature of charge, is filtered to remove impurity, material is added
Reduced pressure equipment carries out distilling with water, isolated light component is the 18% of raw material, collects heavy constituent, obtains product 78.9kg, receives
Rate 78.9%.
Example 4：
Take sweetgum fat raw material（The place of production：Guangxi）100kg is heated to 110 DEG C of temperature of charge, is filtered to remove impurity, material is added
Reduced pressure equipment carries out distilling with water, isolated light component is the 20% of raw material, collects heavy constituent, obtains product 76.5kg, receives
Rate 76.5%.
Claims (4)
1. a kind of Processing methods technique of resina liquidamberis medicinal material, it is characterised in that include the following steps：
1）Raw material heats：Raw material is heated to 100-110 DEG C,
2）Heat filtering cleans：The raw material of heating is filtered while hot, removes impurity,
3）Distilling with water：Raw material after removing impurity is subjected to distilling with water, so that heavy constituent is separated with light component, is dried under reduced pressure,
Heavy constituent is collected,
4）Cooling condensation：The heavy constituent of collection is cooled to room temperature, condenses into product.
2. step 1 as described in claim 1）, it is characterised in that raw material is heated to 100-110 using water-bath or oil bath mode
℃。
3. step 3 as described in claim 1）, it is characterised in that the distillation pressure of distilling with water is no more than 0.2MPa（Interlayer supplies
Heat）, vacuum degree 0.09-0.1MPa.
4. step 3 as described in claim 1）, it is characterised in that the limit that light component is detached when distilling with water is inventory
17%-20%。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710066571.9A CN108272834A (en) | 2017-02-07 | 2017-02-07 | A kind of Processing methods technique of resina liquidamberis medicinal material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710066571.9A CN108272834A (en) | 2017-02-07 | 2017-02-07 | A kind of Processing methods technique of resina liquidamberis medicinal material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108272834A true CN108272834A (en) | 2018-07-13 |
Family
ID=62801120
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710066571.9A Pending CN108272834A (en) | 2017-02-07 | 2017-02-07 | A kind of Processing methods technique of resina liquidamberis medicinal material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108272834A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108338998A (en) * | 2018-04-18 | 2018-07-31 | 福建中益制药有限公司 | A kind of curing of resina liquidamberis |
| CN109010392A (en) * | 2018-09-17 | 2018-12-18 | 健民药业集团股份有限公司 | A kind of resina liquidamberis medicinal material fast processing method |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104327739A (en) * | 2014-10-28 | 2015-02-04 | 南京林业大学 | Liquidambar taiwaniana resin distillation processing method by nitrogen desorption |
-
2017
- 2017-02-07 CN CN201710066571.9A patent/CN108272834A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104327739A (en) * | 2014-10-28 | 2015-02-04 | 南京林业大学 | Liquidambar taiwaniana resin distillation processing method by nitrogen desorption |
Non-Patent Citations (1)
| Title |
|---|
| 宋晓: "枫脂水蒸气蒸馏工艺的研究", 《生物质化学工程》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108338998A (en) * | 2018-04-18 | 2018-07-31 | 福建中益制药有限公司 | A kind of curing of resina liquidamberis |
| CN109010392A (en) * | 2018-09-17 | 2018-12-18 | 健民药业集团股份有限公司 | A kind of resina liquidamberis medicinal material fast processing method |
| CN109010392B (en) * | 2018-09-17 | 2021-05-04 | 健民药业集团股份有限公司 | Rapid processing method of liquidambar formosana medicine |
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Application publication date: 20180713 |
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