CN108264398A - A kind of preparation method of bagasse base Slow release organic fertilizer - Google Patents

A kind of preparation method of bagasse base Slow release organic fertilizer Download PDF

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Publication number
CN108264398A
CN108264398A CN201810112008.5A CN201810112008A CN108264398A CN 108264398 A CN108264398 A CN 108264398A CN 201810112008 A CN201810112008 A CN 201810112008A CN 108264398 A CN108264398 A CN 108264398A
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bagasse
slow release
preparation
fertilizer
organic fertilizer
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陆登俊
梁欣泉
杨晓光
李坚斌
邓立高
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Guangxi University
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Guangxi University
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D1/00Fertilisers containing potassium
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/30Layered or coated, e.g. dust-preventing coatings

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The present invention provides a kind of preparation method of bagasse base Slow release organic fertilizer, is related to agricultural fertilizer preparation field.Include the following steps:Prepared by bagasse pretreatment, water-absorbing resin, prepared by fertile core and coating, simple for process, pollution-free, is easy to industrialized production.Using bagasse water-absorbing resin as membrane material, using organic fertilizer as fertile core, the Slow release organic fertilizer of preparation has high-hydroscopicity and the slow release dual function to fertilizer simultaneously.Water-absorbing resin is prepared using bagasse, cost is not only reduced, and soil physico-chemical property can be improved after degrading, soil density can be reduced, improve soil permeability.With water conservation, fertilizer conservation, section fertilizer, significantly improvement soil, volume increase, low efficient multi-efficiency.

Description

A kind of preparation method of bagasse base Slow release organic fertilizer
Technical field
The present invention relates to agricultural fertilizer preparation fields, and in particular to a kind of preparation method of bagasse base Slow release organic fertilizer.
Background technology
China is large agricultural country, but is had a large population and a few land, and cultivated area is only the soil gross area 10% or so, and per capita cultivated land is average Only 0.08 hectare.Chemical fertilizer plays obvious action as a kind of important agricultural material product to improving crop yield, is Modern Agriculture The indispensable production factors of industry.According to national chemical fertilizer net statistics, external nitrogenous fertilizer in this season utilization rate 60%-70%, and I State's nitrogenous fertilizer this season utilization rate is 30%-35%, phosphate fertilizer 10%-25%, potash fertilizer 35%-50%, but wherein with the volatilization of nitrogen Loss is the most serious.The utilization rate of nitrogenous fertilizer is low, hinders China's Agriculture Production.
For people for a long time largely using inorganic fertilizer, in addition occupation mode is improper, fertilizer interest rate use is not high, causes fertilizer a large amount of Loss, soil and water body are polluted, crops resistance decline, it is serious threatened agricultural sustainable development.Have Machine fertilizer can not only provide full nutrition for crops, and fertilizer efficiency is long, can increase and update the soil organism, promote microorganism numerous It grows, improves the physicochemical property and bioactivity of soil, be the Main Nutrients of pollution-free food production.Meanwhile by adding in fertilizer Add long-acting sustained-release agent, inhibit the activity of certain enzymes in soil to slow down the decomposition and inversion of nitrogen be also improve utilization rate of fertilizer one Effective way.
Representative of the coated slow release fertilizer as fertilizer product of new generation, by adding long-acting sustained-release agent in fertilizer, inhibits In soil the activity of certain enzymes come slow down the decomposition and inversion of nitrogen be improve utilization rate of fertilizer an effective way.Many people are slow The basic theories (selection and development of such as slow/controlled release mechanism, influence factor and slow-release material etc.) of release fertilizer, the life of slow release fertilizer Production manufacture etc. has done many work, and make great progress.However, the production cost of coated fertilizer is higher, Price can't be widely accepted, and be limited its scope of application.It is currently used primarily in lawn, golf course, fruit tree, flowers seedling Garden, vegetables etc., only 7% is used for crops market, and it is imperative to seek a kind of new slow-release compound fertilizer carrier.
Sugarcane Industry is the pillar industry in the main industrial crops in Guangxi and Guangxi, is the main economic source of peasant. Sugarcane is one of primary raw material of sugaring.The remaining bagasse after squeezing sugar, account for about sugarcane 24%~27% (wherein contain About 50%) moisture, often produces one ton of sucrose, will generate 2~3 tons of bagasse.For a long time, large batch of bagasse master It to be burnt up in itself as fuel for sugar refinery or discarded, it is this very low using the economic value of method.Bagasse resource is developed and used, The economic benefit in sugar refinery can not only be improved, a large amount of resource can be also provided for other industry, this to the economic development in Guangxi and Resource reutilization is respectively provided with important meaning.Therefore, a kind of preparation side of the efficient bagasse base Slow release organic fertilizer of low cost is developed Method has higher market value.
Invention content
The goal of the invention of the present invention is, in view of the above-mentioned problems, providing a kind of preparation method of bagasse base Slow release organic fertilizer, no Soil moisture loss can be only significantly reduced, water storage, water retention property are excellent, can also improve soil texture and provided for plant growth must The nutrient and trace element wanted.With water conservation, fertilizer conservation, section fertilizer, significantly improvement soil, volume increase, low efficient multi-efficiency.
In order to achieve the above objectives, the technical solution adopted in the present invention is:
A kind of preparation method of bagasse base Slow release organic fertilizer, includes the following steps:
S1. bagasse pre-processes
1) bagasse is weighed, is then crushed, 80~100 mesh excessively sieve to obtain bagasse powder;
2) H is added in the bagasse powder2O2With the mixed liquor of NaOH, 3~5h is stirred to react at 80~88 DEG C, is then taken out Filter, it is dry;
3) CH is added in into the bagasse powder by 2) handling3COOH and NaCLO2Mixed liquor is stirred to react at 70~80 DEG C 0.5~2h, distillation water washing to neutrality, drying obtain sugarcane fiber.
S2. prepared by water-absorbing resin
1) it by the NaOH solution that mass fraction is 15%, is slowly added into acrylic acid, stirring is allowed to neutralize, and cooling is standby With;
2) to step S1 prepare sugarcane fiber sequentially add neutralize after acrylic acid, kaolin, initiator, crosslinking agent and Polyvinyl alcohol is stirred to react 2~4h in 60~70 DEG C of waters bath with thermostatic control, is then washed successively with distilled water, ethyl alcohol, and drying obtains To bagasse water-absorbing resin.
S3. prepared by fertile core
Bagasse charcoal, biogas residue, nitrogenous fertilizer, phosphate fertilizer, potash fertilizer and complex micro organism fungicide are uniformly mixed, then cross 50~80 Mesh sieves, and obtains fertile core.
S4. coating
The fertile core is heated to 65~75 DEG C, preheats 15~25min, then add in shared by fertile core mass fraction 1%~ Temperature is reduced to 55~60 DEG C of 20~40min of stirring, is formed by 2% polyvinyl alcohol and 5%~10% bagasse water-absorbing resin Single-size cools down up to bagasse base Slow release organic fertilizer finished product.
Preferably, in step S1,0.5%~0.8%H is added in the bagasse powder2O2With the mixing of 3%~5%NaOH The liquid ratio 25~30 of liquid, the mixed liquor and bagasse:1.
Preferably, in step S1,30~35ml/LCH is added in into the bagasse powder by 2) handling3COOH and 9~10g/ LNaCLO2Mixed liquor, the solid-liquid ratio of the mixed liquor and bagasse is 25~30:1.
Preferably, in step S2, NaOH add in acrylic acid in degree of neutralization be 60%~70%.
Preferably, in step S2, sugarcane fiber, acrylic acid, kaolin, initiator, crosslinking agent and the poly- second of the addition The weight ratio of enol is 1:9~12:0.5~1:0.1~0.2:0.02~0.05:1~2.
Preferably, in step S3, the preparation method of the bagasse charcoal is:Bagasse is dried, is crushed, Ran Hou 2~4h is carbonized at 400~600 DEG C, is cooled to room temperature obtained.
Preferably, the carbonization process is first warming up to 400~450 using segmentation heat preserving mode with the rate of 5 DEG C/min DEG C, 30~60min is kept the temperature, is then warming up to 500~600 DEG C again with the rate of 1 DEG C/min, 1.5~3h is kept the temperature, is finally cooled to Room temperature.
Preferably, in step S3, the fertilizer core includes following components according to parts by weight:20~30 parts of bagasse charcoal, natural pond 0.3~1 part of 20~50 parts of slag, 3~7 parts of nitrogenous fertilizer, 2~3 parts of phosphate fertilizer, 1~4 part of potash fertilizer and complex micro organism fungicide.
Preferably, in step S3, the complex micro organism fungicide is EM complex micro organism fungicides.
Preferably, in step S4, the crosslinking agent is N, and N'- methylene-bisacrylamides, the initiator is persulfuric acid Ammonium or potassium peroxydisulfate.
Due to the adoption of the above technical scheme, the invention has the advantages that:
1. the preparation method of the bagasse base Slow release organic fertilizer of the present invention, using bagasse water-absorbing resin as membrane material, with organic fertilizer For fertile core, the Slow release organic fertilizer of preparation has high-hydroscopicity and the slow release dual function to fertilizer simultaneously.It is prepared using bagasse Water-absorbing resin not only reduces cost, and can improve soil physico-chemical property after degrading, and can reduce soil density, improves soil Earth permeability.With water conservation, fertilizer conservation, section fertilizer, significantly improvement soil, volume increase, low efficient multi-efficiency.
The bagasse water-absorbing resin is after bagasse is pre-processed, using kaolin, acrylic acid as starting monomer, with N, N Di-2-ethylhexylphosphine oxide propyl amides (MBA) are crosslinking agent, and ammonium persulfate and aqueous solution of sodium bisulfite are reduction initiator, using solution Polymerization is prepared, and has half interpenetrating network structure.It had not only maintained the water suction of water-absorbing resin and water retention property, but also can profit With water-absorbing resin to fertilizer slow release, the utilization rate of fertilizer is improved, and price is relatively low, economic benefit is all with environmental-protection function It is good.
Kaolin has excellent microorganism decomposition performance, and free from environmental pollution and cheap, product is easy to spread.
2. the preparation method of the bagasse base Slow release organic fertilizer of the present invention, using deriving from a wealth of sources, cheap biological can drop The bagasse of solution effectively reduces the cost of organic fertilizer, a new approach has been sought in the application for bagasse as raw material.It is sweet Bagasse first passes through pretreatment, can reduce lignin and hemicellulose, effectively enhances the activity of sugarcane fiber, so as to preferably With kaolin, acroleic acid polymerization, reaction efficiency is high, forms reticular structure, the water-absorbing resin of preparation, water suction and had good sustained release effect.
3. the bagasse base Slow release organic fertilizer preparation method of the present invention contains bagasse charcoal, biogas residue, nitrogenous fertilizer, phosphorus in fertile core Fertilizer, potash fertilizer and complex micro organism fungicide, disclosure satisfy that the different nutritional need of plant, and can improve soil texture and enhancing soil The ability of water conservation, fertilizer conservation.Bagasse biomass carbon has stronger adsorption capacity, so as to act synergistically with bagasse water-absorbing resin, carries The slow-release capability of high fertilizer reduces fertilizer loss, increases operation rate;On the other hand, also one has been sought for the application of bagasse New approach improves the utilization rate of bagasse.Biogas residue is a kind of spy containing fertilizer, biological pesticide and feed addictive function Different substance containing many nutritional ingredients and bioactive substance, can not only improve soil physical and chemical property, increase fertility, moreover it is possible to Crop yield is significantly improved, so as to improve the fertility of bagasse base Slow release organic fertilizer.
4. the preparation method of the preparation method of bagasse base Slow release organic fertilizer of the present invention, simple for process, with obvious effects, it is easy to work Industry metaplasia is produced, and has good market prospects.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to Limit the present invention.
Embodiment 1
A kind of preparation method of bagasse base Slow release organic fertilizer, includes the following steps:
S1. bagasse pre-processes
1) bagasse is weighed, then crushes, sieve with 100 mesh sieve to obtain bagasse powder;
2) 0.7%H is added in the bagasse powder2O2With the mixed liquor of 4%NaOH (H in mixed liquor2O2Mass concentration be 0.7%th, the mass concentration of NaOH is the 4%) liquid ratio 30 of the mixed liquor and bagasse:1,4h is stirred to react at 86 DEG C, so After filter, it is dry;
3) 31ml/LCH is added in into the bagasse powder by 2) handling3COOH and 9.5g/LNaCLO2Mixed liquor (mixed liquor Middle CH3A concentration of 31ml/L, NaCLO of COOH2A concentration of 9.5g/L), the solid-liquid ratio of the mixed liquor and bagasse is 30:1, 1h, distillation water washing to neutrality are stirred to react at 75 DEG C, drying obtains sugarcane fiber.
S2. prepared by water-absorbing resin
1) it by the NaOH solution that mass fraction is 15%, is slowly added into acrylic acid, stirring is allowed to neutralize, and degree of neutralization is 65% cooling is spare;
The sugarcane fiber prepared to step S1 sequentially adds the acrylic acid after neutralizing, kaolin, initiator, crosslinking agent and gathers Vinyl alcohol is stirred to react 3h in 65 DEG C of waters bath with thermostatic control, is then washed successively with distilled water, ethyl alcohol, drying, obtains bagasse water suction Resin.The sugarcane fiber, acrylic acid, kaolin, initiator, crosslinking agent and polyvinyl alcohol weight ratio be 1:10:6:0.2: 0.03:2。
The crosslinking agent is N, and N'- methylene-bisacrylamides, the initiator is ammonium persulfate or potassium peroxydisulfate.
S3. prepared by fertile core
Bagasse charcoal, biogas residue, nitrogenous fertilizer, phosphate fertilizer, potash fertilizer and complex micro organism fungicide are uniformly mixed, then cross 60 mesh Sieve, obtains fertile core.
The fertilizer core includes following components according to parts by weight:25 parts of bagasse charcoal, 30 parts of biogas residue, 5 parts of nitrogenous fertilizer, phosphate fertilizer 2 0.5 part of part, 2 parts of potash fertilizer and complex micro organism fungicide.
The complex micro organism fungicide is EM complex micro organism fungicides.
The preparation method of the bagasse charcoal is:Bagasse is dried, is crushed, is then being carbonized, is cooled to room temperature system .The carbonization process is first warming up to 450 DEG C with the rate of 5 DEG C/min, is kept the temperature 30min, Ran Houzai using segmentation heat preserving mode 550 DEG C are warming up to the rate of 1 DEG C/min, 1.5h is kept the temperature, is finally cooled to room temperature.
S4. coating
The fertile core is heated to 70 DEG C, preheats 20min, then the polyethylene of fertile core mass fraction 1.5% shared by addition Temperature is reduced to 60 DEG C of stirring 20min, forms single-size, cool down up to bagasse by alcohol and 5~10% bagasse water-absorbing resin Base Slow release organic fertilizer finished product.
Embodiment 2
A kind of preparation method of bagasse base Slow release organic fertilizer, includes the following steps:
S1. bagasse pre-processes
1) bagasse is weighed, is then crushed, 80 mesh excessively sieve to obtain bagasse powder;
2) 0.8%H is added in the bagasse powder2O2With the mixed liquor of 5%NaOH, the liquid ratio of the mixed liquor and bagasse 25:1,5h is stirred to react at 80 DEG C, is then filtered, it is dry;
3) 30ml/LCH is added in into the bagasse powder by 2) handling3COOH and 9g/LNaCLO2Mixed liquor, the mixing The solid-liquid ratio of liquid and bagasse is 25:1,0.5h, distillation water washing to neutrality are stirred to react at 80 DEG C, drying obtains bagasse fibre Dimension.
S2. prepared by water-absorbing resin
1) it by the NaOH solution that mass fraction is 15%, is slowly added into acrylic acid, stirring is allowed to neutralize, and degree of neutralization is 70% cooling is spare;
2) to step S1 prepare sugarcane fiber sequentially add neutralize after acrylic acid, kaolin, initiator, crosslinking agent and Polyvinyl alcohol is stirred to react 4h in 60 DEG C of waters bath with thermostatic control, is then washed successively with distilled water, ethyl alcohol, drying, obtains bagasse suction Water-resin.The sugarcane fiber of the addition, acrylic acid, kaolin, initiator, crosslinking agent and polyvinyl alcohol weight ratio be 1: 12:1:0.2:0.05:2。
The crosslinking agent is N, and N'- methylene-bisacrylamides, the initiator is ammonium persulfate or potassium peroxydisulfate.
S3. prepared by fertile core
Bagasse charcoal, biogas residue, nitrogenous fertilizer, phosphate fertilizer, potash fertilizer and complex micro organism fungicide are uniformly mixed, then cross 50~80 Mesh sieves, and obtains fertile core.
The fertilizer core includes following components according to parts by weight:30 parts of bagasse charcoal, 40 parts of biogas residue, 7 parts of nitrogenous fertilizer, phosphate fertilizer 3 1 part of part, 1 part of potash fertilizer and complex micro organism fungicide.
The complex micro organism fungicide is EM complex micro organism fungicides.
The preparation method of the bagasse charcoal is:Bagasse is dried, is crushed, then carbonizes 4h, is cooled to room temperature system .The carbonization process is first warming up to 400 DEG C with the rate of 5 DEG C/min, is kept the temperature 60min, Ran Houzai using segmentation heat preserving mode 500 DEG C are warming up to the rate of 1 DEG C/min, 3h is kept the temperature, is finally cooled to room temperature.
S4. coating
The fertile core is heated to 75 DEG C, preheats 15min, then the polyvinyl alcohol of fertile core mass fraction 2% shared by addition Bagasse water-absorbing resin with 5~10%, is reduced to 55 DEG C of stirring 40min by temperature, forms single-size, cool down up to bagasse base Slow release organic fertilizer finished product.
Embodiment 3
In prepared by a kind of preparation method of bagasse base Slow release organic fertilizer, wherein step S3. fertilizer core, by bagasse charcoal, natural pond Slag, nitrogenous fertilizer, phosphate fertilizer, potash fertilizer and complex micro organism fungicide are uniformly mixed, and are then crossed 50 mesh sieve, are obtained fertile core.It is described fertilizer core according to Parts by weight include following components:20 parts of bagasse charcoal, 50 parts of biogas residue, 5 parts of nitrogenous fertilizer, 2 parts of phosphate fertilizer, 1 part of potash fertilizer and composite microbial 1 part of object microbial inoculum.The complex micro organism fungicide is EM complex micro organism fungicides.
Other steps are the same as embodiment 1.
For planting capsicum, 4 pieces 1 mu of experimental plot plantation capsicum is chosen, experimental plot 1-3 applies embodiment 1-3 respectively Bagasse base Slow release organic fertilizer, experimental plot 4 do not apply common organic fertilizer, and dose is identical with fertilization time, mode, other plantations Mode all same.The growth period to harvest time from detects 20d plant heights, good harvest time, good harvest yield respectively.Such as the following table 1 It is shown.
1 test result of table compares
It can be seen that from the data of embodiment 1-3 data combinations table 1 with the experimental plot 4 of common organic fertilizer is used to compare, Using bagasse base Slow release organic fertilizer, porosity of soil, the organic matter content in soil of experimental field 1-3 improve;Meanwhile the plant of capsicum Height is increased, and harvest time shifts to an earlier date, output increased.Illustrate that Slow release organic fertilizer prepared by the present invention can not only improve fertilizer profit With rate, crop yield is improved, and soil physico-chemical property can be improved after degrading, reduces soil density, improve soil permeability, With water conservation, fertilizer conservation, section fertilizer, significantly improvement soil, volume increase, low efficient multi-efficiency.
Above description is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair Bright patent claim.The equal variation or modification change completed under technical concept suggested by all present invention, should all belong to Cover the scope of the claims in the present invention.

Claims (10)

1. a kind of preparation method of bagasse base Slow release organic fertilizer, which is characterized in that include the following steps:
S1. bagasse pre-processes
1) bagasse is weighed, is then crushed, 80~100 mesh excessively sieve to obtain bagasse powder;
2) H is added in the bagasse powder2O2With the mixed liquor of NaOH, 3~5h is stirred to react at 80~88 DEG C, is then filtered, done It is dry;
3) CH is added in into the bagasse powder by 2) handling3COOH and NaCLO2Mixed liquor is stirred to react 0.5 at 70~80 DEG C ~2h, distillation water washing to neutrality, drying obtain sugarcane fiber;
S2. prepared by water-absorbing resin
1) it by the NaOH solution that mass fraction is 15%, is slowly added into acrylic acid, stirring is allowed to neutralize, and cooling is spare;
2) acrylic acid, kaolin, initiator, crosslinking agent and poly- second after neutralizing are sequentially added to the step S1 sugarcane fibers prepared Enol is stirred to react 2~4h in 60~70 DEG C of waters bath with thermostatic control, is then washed successively with distilled water, ethyl alcohol, and drying obtains sugarcane Slag water-absorbing resin;
S3. prepared by fertile core
Bagasse charcoal, biogas residue, nitrogenous fertilizer, phosphate fertilizer, potash fertilizer and complex micro organism fungicide are uniformly mixed, then cross 50~80 mesh Sieve, obtains fertile core;
S4. coating
The fertile core is heated to 65~75 DEG C, preheats 15~25min, then fertile core mass fraction 1%~2% shared by addition Temperature is reduced to 55~60 DEG C of 20~40min of stirring, is formed uniform by polyvinyl alcohol and 5%~10% bagasse water-absorbing resin Particle cools down up to bagasse base Slow release organic fertilizer finished product.
2. the preparation method of bagasse base Slow release organic fertilizer according to claim 1, which is characterized in that in step S1, to institute It states bagasse powder and adds in 0.5%~0.8%H2O2With the mixed liquor of 3%~5%NaOH, the liquid ratio 25 of the mixed liquor and bagasse ~30:1.
3. the preparation method of bagasse base Slow release organic fertilizer according to claim 1, which is characterized in that in step S1, Xiang Jing It crosses in 2) the bagasse powder of processing and adds in 30~35ml/LCH3COOH and 9~10g/LNaCLO2Mixed liquor, the mixed liquor and sugarcane The solid-liquid ratio of slag is 25~30:1.
4. the preparation method of bagasse base Slow release organic fertilizer according to claim 1, which is characterized in that in step S2, NaOH Add in acrylic acid in degree of neutralization be 60%~70%.
5. the preparation method of bagasse base Slow release organic fertilizer according to claim 1, which is characterized in that described in step S2 The sugarcane fiber of addition, acrylic acid, kaolin, initiator, crosslinking agent and polyvinyl alcohol weight ratio be 1:9~12:0.5~1: 0.1~0.2:0.02~0.05:1~2.
6. the preparation method of bagasse base Slow release organic fertilizer according to claim 1, which is characterized in that described in step S3 The preparation method of bagasse charcoal is:Bagasse is dried, is crushed, 2~4h is then carbonized at 400~600 DEG C, is cooled to room Temperature is made.
7. the preparation method of bagasse base Slow release organic fertilizer according to claim 6, which is characterized in that the carbonization process is adopted With segmentation heat preserving mode, be first warming up to 400~450 DEG C with the rate of 5 DEG C/min, keep the temperature 30~60min, then again with 1 DEG C/ The rate of min is warming up to 500~600 DEG C, keeps the temperature 1.5~3h, is finally cooled to room temperature.
8. the preparation method of bagasse base Slow release organic fertilizer according to claim 1, which is characterized in that described in step S3 Fertile core includes following components according to parts by weight:20~30 parts of bagasse charcoal, 20~50 parts of biogas residue, 3~7 parts of nitrogenous fertilizer, phosphate fertilizer 2~ 0.3~1 part of 3 parts, 1~4 part of potash fertilizer and complex micro organism fungicide.
9. the preparation method of bagasse base Slow release organic fertilizer according to claim 1, which is characterized in that described in step S3 Complex micro organism fungicide is EM complex micro organism fungicides.
10. the preparation method of bagasse base Slow release organic fertilizer according to claim 1, which is characterized in that described in step S4 Crosslinking agent is N, and N'- methylene-bisacrylamides, the initiator is ammonium persulfate or potassium peroxydisulfate.
CN201810112008.5A 2018-02-05 2018-02-05 A kind of preparation method of bagasse base Slow release organic fertilizer Pending CN108264398A (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
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CN108794190A (en) * 2018-07-26 2018-11-13 广西田阳县创新农业综合开发有限公司 A kind of insect prevention fertilizer of mango and preparation method thereof
CN108863623A (en) * 2018-09-21 2018-11-23 广东省生物工程研究所(广州甘蔗糖业研究所) A kind of charcoal base medicine fertilizer of clothianidin-containing and preparation method thereof
CN108911877A (en) * 2018-08-27 2018-11-30 广西大学 A kind of method of filter mud of sugar refinery charing production sugarcane charcoal slow-release fertilizer
CN109503269A (en) * 2018-12-29 2019-03-22 成都云图控股股份有限公司 A kind of coated slow-release material and preparation method thereof and film-coated and slow release fertilizer as made from it
CN109864983A (en) * 2019-04-16 2019-06-11 广西大学 It is a kind of using bagasse as essential oil sustained-release antibacterial capsule of wall material and preparation method thereof
CN109937836A (en) * 2019-03-27 2019-06-28 六安初心生物科技有限公司 A kind of growing dendrobium matrix and preparation method thereof increasing dendrobium polysaccharide content
CN111440013A (en) * 2020-05-29 2020-07-24 天津大学 Potassium-rich slow-release biochar and preparation method and application thereof
CN114031457A (en) * 2021-11-12 2022-02-11 绥化学院 Long-acting slow-release compound fertilizer and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104072686A (en) * 2014-06-30 2014-10-01 山东大学 Preparation method of straw-based super absorbent resin with nitrogen phosphorus fertilizer slow-release function
CN104388096A (en) * 2014-09-25 2015-03-04 广西大学 Bagasse composite soil conditioner preparation method
CN105085074A (en) * 2015-09-10 2015-11-25 青岛伟源达技术服务有限公司 Water retention agent coating-type high-water-retentivity slow-release fertilizer and preparation method thereof
CN105859416A (en) * 2016-04-15 2016-08-17 陕西科技大学 Water-retaining controlled-release phosphate fertilizer and preparation method thereof
CN106748577A (en) * 2016-11-25 2017-05-31 福建农林大学 A kind of nanometre glue sugarcane leaf/composite coated slow-released nitrogenous fertilizer of bagasse and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104072686A (en) * 2014-06-30 2014-10-01 山东大学 Preparation method of straw-based super absorbent resin with nitrogen phosphorus fertilizer slow-release function
CN104388096A (en) * 2014-09-25 2015-03-04 广西大学 Bagasse composite soil conditioner preparation method
CN105085074A (en) * 2015-09-10 2015-11-25 青岛伟源达技术服务有限公司 Water retention agent coating-type high-water-retentivity slow-release fertilizer and preparation method thereof
CN105859416A (en) * 2016-04-15 2016-08-17 陕西科技大学 Water-retaining controlled-release phosphate fertilizer and preparation method thereof
CN106748577A (en) * 2016-11-25 2017-05-31 福建农林大学 A kind of nanometre glue sugarcane leaf/composite coated slow-released nitrogenous fertilizer of bagasse and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
马红梅: "蔗渣纤维/高岭土/丙烯酸复合高吸水树脂的制备及性能研究", 《中国优秀硕士学位论文全文数据库工程科技I辑》 *

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108794190A (en) * 2018-07-26 2018-11-13 广西田阳县创新农业综合开发有限公司 A kind of insect prevention fertilizer of mango and preparation method thereof
CN108911877A (en) * 2018-08-27 2018-11-30 广西大学 A kind of method of filter mud of sugar refinery charing production sugarcane charcoal slow-release fertilizer
CN108863623A (en) * 2018-09-21 2018-11-23 广东省生物工程研究所(广州甘蔗糖业研究所) A kind of charcoal base medicine fertilizer of clothianidin-containing and preparation method thereof
CN109503269A (en) * 2018-12-29 2019-03-22 成都云图控股股份有限公司 A kind of coated slow-release material and preparation method thereof and film-coated and slow release fertilizer as made from it
CN109937836A (en) * 2019-03-27 2019-06-28 六安初心生物科技有限公司 A kind of growing dendrobium matrix and preparation method thereof increasing dendrobium polysaccharide content
CN109864983A (en) * 2019-04-16 2019-06-11 广西大学 It is a kind of using bagasse as essential oil sustained-release antibacterial capsule of wall material and preparation method thereof
CN109864983B (en) * 2019-04-16 2021-04-23 广西大学 Essential oil slow-release antibacterial capsule taking bagasse as wall material and preparation method thereof
CN111440013A (en) * 2020-05-29 2020-07-24 天津大学 Potassium-rich slow-release biochar and preparation method and application thereof
CN114031457A (en) * 2021-11-12 2022-02-11 绥化学院 Long-acting slow-release compound fertilizer and preparation method thereof

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Application publication date: 20180710