CN108261434A - Sanchi flower, stem-leaf extract, the instant tea containing sanchi flower, stem-leaf extract, and preparation method thereof - Google Patents
Sanchi flower, stem-leaf extract, the instant tea containing sanchi flower, stem-leaf extract, and preparation method thereof Download PDFInfo
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- CN108261434A CN108261434A CN201810195484.8A CN201810195484A CN108261434A CN 108261434 A CN108261434 A CN 108261434A CN 201810195484 A CN201810195484 A CN 201810195484A CN 108261434 A CN108261434 A CN 108261434A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/34—Tea substitutes, e.g. matè; Extracts or infusions thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/55—Liquid-liquid separation; Phase separation
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- Food Science & Technology (AREA)
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- Preparation Of Fruits And Vegetables (AREA)
Abstract
The present invention relates to extracted form natural plant field and field of food, and in particular to a kind of sanchi flower, stem-leaf extract, preparation method and its instant tea and preparation method.The sanchi flower, stem-leaf extract are using weight ratio as 1:1 sanchi flower and notoginseng haulm is raw material, is extracted by water, prepared by alcohol precipitation and concentrate drying.The sanchi flower, stem-leaf extract preparation method include dispensing, extraction concentration, alcohol precipitation, concentration and etc..The preparation method containing sanchi flower, the instant tea of stem-leaf extract includes weighing raw material in proportion and mixes, by mixture successively softwood processed, granulation and drying, whole grain, total mixed and etc..The present invention proportions sanchi flower and notoginseng haulm use, ensure that the extract not only active ingredient comprising sanchi flower and notoginseng haulm, but also will not introduce excessive additional impurities.The extracting method can effectively extract the active ingredient of sanchi flower and notoginseng haulm, small to the destruction of active ingredient, and the using effect of extract improves.
Description
Technical field
The present invention relates to extracted form natural plant field and field of food, and in particular to a kind of sanchi flower, stem-leaf extract, its
Preparation method and the instant tea and preparation method thereof containing the sanchi flower, stem-leaf extract.
Background technology
Radix Notoginseng is one of China's traditional Chinese medicine, mainly originates in Yunnan Province.《Compendium of Materia Medica》In about Radix Notoginseng the effect of, just like
Lower record：Styptic powder blood analgesic therapy, golden sword arrow wound, fall flutter cane sore, blood goes out more than person, chews rotten painting or mixes it for end, blood is i.e. only.
Also main hematemesis and epistaxis, lower blood bloody flux, metrorrhagia incessant menorrhea, postpartum extravesated blood not under, blood fortune blood pain, Akamu carbuncle swells, it is all that tiger stings snakebite
Disease.
Radix Notoginseng belongs to the plant variety of food and medicine consangunity, and with the development of extractive technique, Radix Notoginseng mostly is taken various hands at present
Section, extracts its active ingredient, to improve the bioavilability of active ingredient, avoid drug side-effect etc..As Chinese medicine
One common knowledge in field, the different parts of same plant often have different drug effects.For Radix Notoginseng, according to the modern times
Medical chemistry from the viewpoint of, the type and content of active ingredient contained by different parts difference is needed according to reality
Situation is treated with a certain discrimination.Traditional extracting method is concerned only with extraction process in itself, without recognizing foregoing problems.
Invention content
It is a discovery of the invention that according to sanchi flower and the difference of notoginseng haulm active ingredient, it should be by sanchi flower and notoginseng haulm
Raw material after proportionally arranging in pairs or groups as extraction can obtain the extract that active constituent content is high, type is balanced, impurity is few.
On the basis of aforementioned discovery, on the one hand, a kind of sanchi flower, stem-leaf extract are provided；It is carried in another aspect, providing this
Take the preparation method of object；In another aspect, provide the instant tea containing the sanchi flower, stem-leaf extract；In another aspect, provide the speed
The preparation method of molten tea.
On the one hand, a kind of sanchi flower, stem-leaf extract are provided, which is characterized in that the extract is using weight ratio as 1:1
Sanchi flower and notoginseng haulm are raw material, are extracted by water, alcohol precipitation and concentrate drying are prepared.
On the other hand, the preparation method of aforementioned sanchi flower, stem-leaf extract is provided, the described method comprises the following steps：
S01, dispensing：According to weight ratio 1:1 ratio, weighs sanchi flower and notoginseng haulm, obtains extraction raw material；
S02, extraction concentration：Using water as extracting solution, the extraction raw material of S01 is extracted, and crude extract is concentrated
To obtain thick extracted extract；
S03, alcohol precipitation：Ethyl alcohol is added in into the thick extracted extract of S02, is filtered after standing, collects filtrate；
S04, concentration：The filtrate of S04 is concentrated under reduced pressure, obtains concentrated extract；
S05, drying：The concentrated extract of S04 is dried, obtains sanchi flower, stem-leaf extract.
The sanchi flower and notoginseng haulm, which are positioned over after arrival initial test in medicinal material library, to be stored, and is selected before use through choosing
Use high-quality feedstocks.Further, in step S01, the notoginseng haulm mixes after crushed with the sanchi flower as extraction
Raw material.
Further, in step S02,2 extractions is carried out to extraction raw material, are included the following steps：
S02-1, it boils to extract the reflux of the water of 8-10 times of volume of raw material first and carries 2h, filter and collect filtrate；
S02-2, it then boils to extract the reflux of the water of 6-8 times of raw material and carries 1h, filter and collect filtrate；
S02-3, merge filtrate twice, obtain crude extract.
Further, in step S02, crude extract is concentrated at 50-60 DEG C, until crude extract is in opposite proportion
1.02-1.25 paste, obtain thick extracted extract.
Further, in step S03, ethyl alcohol is added in into the thick extracted extract of S02, until ethanol content is 50-
70wt.% is filtered after standing.
Further, in step S04, filtrate is concentrated under reduced pressure at 50-60 DEG C, until the opposite proportion of concentrated extract
For 1.15-1.30.
Further, it in step S05, is dried in D grades of clean areas.
Further, the preparation method of the Notogineng Extract further include packaging, product inspection, enter in library storage a step or
The step of multistep.
On the other hand, the instant tea containing aforementioned sanchi flower, stem-leaf extract is provided, including
600 parts of sanchi flower, stem-leaf extract
2000-3000 parts of auxiliary material.
On the other hand, provide aforementioned sanchi flower, stem-leaf extract instant tea preparation method, include the following steps：
S11, raw material is weighed in proportion and is mixed；
S12, by the mixture of S11 successively softwood processed, granulation；
S13, the pellet of S12 is dried；
S14, by the dried feed whole grain of S13, total mixed.
Further, the mixing of the S11 is to mix 30min under the rotating speed of 30rpm.
Further, the granulation of the S12 uses 30 mesh screens.
Further, the drying of the S13 is the dry 2h at 80 DEG C.
Further, the whole grain of the S14 is to be sieved respectively with the sieve of 20 mesh and 60 mesh, and 20 mesh cannot be crossed by discarding
The particle of sieve and the fine powder that 60 mesh sieve can be crossed；Total mix is to mix 30min under the rotating speed of 30rpm.
Further, the preparation method of the instant tea further includes packaging, product inspection, enters one or multi-step in library storage
The step of.
One or more of above-mentioned technical proposal technical solution has the advantages that：
1st, the present invention proportions sanchi flower and notoginseng haulm uses, ensure that extract both comprising sanchi flower and three
The active ingredient of seven cauline leafs, and excessive additional impurities will not be introduced.
2nd, the extracting method can effectively extract sanchi flower and notoginseng haulm active ingredient, the destruction to the active ingredient
Small, the using effect of extract improves.
Description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below to embodiment or existing
Attached drawing is briefly described needed in technology.It should be evident that the accompanying drawings in the following description is only the present invention's
Some embodiments, for those of ordinary skill in the art, without creative efforts, can also be according to this
A little attached drawings obtain other attached drawings.
Fig. 1 be sanchi flower, stem-leaf extract preparation method one embodiment flow chart.
Fig. 2 is the flow chart of one embodiment of the preparation method of the instant tea containing sanchi flower, stem-leaf extract.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme of the present invention is clearly and completely described.Based on this
Embodiment in invention, the every other reality that those of ordinary skill in the art are obtained without creative efforts
Example is applied, shall fall within the protection scope of the present invention.
Embodiment 1：The preparation method of sanchi flower, stem-leaf extract
According to weight ratio 1:1 ratio weighs sanchi flower and each 1kg of notoginseng haulm, after notoginseng haulm is crushed, by the two
Mixing.
Aforementioned sanchi flower cauline leaf mixture is put into the 50L extraction kettles with heating and condensing unit, input 20kg is pure
Change water, be heated to the 2h that flows back and extract, release extracting solution, then 12kg purified waters are added in into kettle, be heated to the 1h that flows back and extract,
Extracting solution is released, two parts of extracting solutions are merged, obtain crude extract.Crude extract is put into the 50L concentration kettles with heating unit,
Temperature is maintained at 55 DEG C or so, and is stirred continuously, until crude extract is in the paste that opposite proportion is 1.15, obtains thick extracted extract.
Ethyl alcohol is added in into thick extracted extract under stiring, ethanol content is made to reach 65wt.%, stands filtering；Filtrate is existed
It is concentrated under reduced pressure at 55 DEG C, until the opposite proportion of residual solids is 1.20, obtains concentrated extract.
Concentrated extract is transferred to D grades of clean areas, is dried to obtain sanchi flower, stem-leaf extract.
Embodiment 2：Preparation method containing sanchi flower, the instant tea of stem-leaf extract
Raw material is weighed according to following proportioning：
Material is mixed into 30min under 30rpm rotating speeds, the granulation of 30 mesh screens is crossed after softwood is made.
It then by particle drying 2h at 80 DEG C, then is sieved successively with the sieve of 20 mesh and 60 mesh, discarding cannot mistake
The particle of 20 mesh sieve and the fine powder that can cross 60 mesh sieve, 30min is always mixed under the rotating speed of 30rpm, obtains sanchi flower, cauline leaf carries later
Take the instant tea product of object.
By sanchi flower, stem-leaf extract instant tea product packaging after, through product inspection, certified products move into storehouse storage.
The above description is merely a specific embodiment, but protection scope of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can readily occur in change or replacement, should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. sanchi flower, stem-leaf extract, which is characterized in that the extract is using weight ratio as 1:1 sanchi flower and notoginseng haulm
For raw material, extracted by water, alcohol precipitation and concentrate drying are prepared.
2. the preparation method of sanchi flower, stem-leaf extract, which is characterized in that the described method comprises the following steps：
S01, dispensing：According to weight ratio 1:1 ratio, weighs sanchi flower and notoginseng haulm, obtains extraction raw material；
S02, extraction concentration：Using water as extracting solution, the extraction raw material of S01 is extracted, and crude extract is concentrated to obtain
Obtain thick extracted extract；
S03, alcohol precipitation：Ethyl alcohol is added in into the thick extracted extract of S02, is filtered after standing, collects filtrate；
S04, concentration：The filtrate of S03 is concentrated under reduced pressure, obtains concentrated extract；
S05, drying：The concentrated extract of S04 is dried, obtains sanchi flower, stem-leaf extract.
3. the preparation method of sanchi flower according to claim 2, stem-leaf extract, which is characterized in that in step S01, institute
Notoginseng haulm is stated to be mixed with the sanchi flower after crushed as extraction raw material.
4. the preparation method of sanchi flower according to claim 2, stem-leaf extract, which is characterized in that right in step S02
It extracts raw material and carries out 2 extractions, include the following steps：
S02-1, it boils to extract the reflux of the water of 8-10 times of volume of raw material first and carries 2h, filter and collect filtrate；
S02-2, it then boils to extract the reflux of the water of 6-8 times of raw material and carries 1h, filter and collect filtrate；
S02-3, merge filtrate twice, obtain crude extract.
5. the preparation method of the sanchi flower, stem-leaf extract according to claim 2 or 4, which is characterized in that in step S02,
Crude extract is concentrated at 50-60 DEG C, until crude extract is in the paste that opposite proportion is 1.02-1.25, obtains thick extracted extract.
6. the preparation method of sanchi flower according to claim 2, stem-leaf extract, which is characterized in that in step S03, to
Ethyl alcohol is added in the thick extracted extract of S02, until ethanol content is 50-70wt.%, is filtered after standing.
7. the preparation method of sanchi flower according to claim 2, stem-leaf extract, which is characterized in that in step S04, filter
Liquid is concentrated under reduced pressure at 50-60 DEG C, until the opposite proportion of concentrated extract is 1.15-1.30.
8. the instant tea containing sanchi flower, stem-leaf extract, which is characterized in that the instant tea includes
600 parts of sanchi flower, stem-leaf extract
2000-3000 parts of auxiliary material；
The sanchi flower, stem-leaf extract are sanchi flower described in claim 1, stem-leaf extract or according to claim 2-6
The preparation-obtained sanchi flower of preparation method, the stem-leaf extract of any one of them sanchi flower, stem-leaf extract.
9. the preparation method according to claim 8 containing sanchi flower, the instant tea of stem-leaf extract, which is characterized in that
Include the following steps：
S11, raw material is weighed in proportion and is mixed；
S12, by the mixture of S11 successively softwood processed, granulation；
S13, the pellet of S12 is dried；
S14, by the dried feed whole grain of S13, total mixed.
10. the preparation method of instant tea according to claim 9, which is characterized in that the whole grain of the S14 is respectively with 20
The sieve of mesh and 60 mesh is sieved, and discards the particle that cannot cross 20 mesh sieve and the fine powder that can cross 60 mesh sieve；It is described it is total mixed be
30min is mixed under the rotating speed of 30rpm.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810195484.8A CN108261434A (en) | 2018-03-09 | 2018-03-09 | Sanchi flower, stem-leaf extract, the instant tea containing sanchi flower, stem-leaf extract, and preparation method thereof |
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| CN201810195484.8A CN108261434A (en) | 2018-03-09 | 2018-03-09 | Sanchi flower, stem-leaf extract, the instant tea containing sanchi flower, stem-leaf extract, and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108835639A (en) * | 2018-08-07 | 2018-11-20 | 玉溪市维和维生堂保健食品有限公司 | A kind of Radix Notoginseng spray composition and the preparation method and application thereof |
| CN110974859A (en) * | 2019-12-31 | 2020-04-10 | 普洱淞茂滇草六味制药股份有限公司 | Notoginseng tea and its preparation method |
| WO2020087537A1 (en) * | 2018-11-02 | 2020-05-07 | 王志钢 | Panax notoginseng health food, preparation method and application thereof |
| CN111513329A (en) * | 2020-05-18 | 2020-08-11 | 云南农业大学 | Preparation process and application of pseudo-ginseng flower stem and leaf extract |
| CN113995075A (en) * | 2021-11-22 | 2022-02-01 | 金七药业股份有限公司 | Pseudo-ginseng solid beverage and preparation method thereof |
| CN114177210A (en) * | 2021-10-09 | 2022-03-15 | 金七药业股份有限公司 | Formula and preparation process of whole panax notoginseng |
| CN114748525A (en) * | 2022-04-26 | 2022-07-15 | 云南七丹药业股份有限公司 | Preparation method of oral liquid containing pseudo-ginseng and product thereof |
| CN114773158A (en) * | 2022-04-26 | 2022-07-22 | 云南七丹药业股份有限公司 | Extraction process and production method of effective components of fresh pseudo-ginseng flower |
| CN115005306A (en) * | 2022-07-14 | 2022-09-06 | 云南农业大学 | Preparation process and application of pseudo-ginseng stem leaf-mulberry leaf extract |
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| CN101390546A (en) * | 2007-09-22 | 2009-03-25 | 杨光孝 | Notoginseng puer bagged tea |
| CN102057999A (en) * | 2009-11-17 | 2011-05-18 | 天津天士力制药股份有限公司 | Health care instant tea |
| CN106720745A (en) * | 2016-12-01 | 2017-05-31 | 昆明理工大学 | A kind of notoginseng flower for improving the health care of sleep and preparation method thereof |
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2018
- 2018-03-09 CN CN201810195484.8A patent/CN108261434A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101390546A (en) * | 2007-09-22 | 2009-03-25 | 杨光孝 | Notoginseng puer bagged tea |
| CN102057999A (en) * | 2009-11-17 | 2011-05-18 | 天津天士力制药股份有限公司 | Health care instant tea |
| CN106720745A (en) * | 2016-12-01 | 2017-05-31 | 昆明理工大学 | A kind of notoginseng flower for improving the health care of sleep and preparation method thereof |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108835639A (en) * | 2018-08-07 | 2018-11-20 | 玉溪市维和维生堂保健食品有限公司 | A kind of Radix Notoginseng spray composition and the preparation method and application thereof |
| WO2020087537A1 (en) * | 2018-11-02 | 2020-05-07 | 王志钢 | Panax notoginseng health food, preparation method and application thereof |
| CN110974859A (en) * | 2019-12-31 | 2020-04-10 | 普洱淞茂滇草六味制药股份有限公司 | Notoginseng tea and its preparation method |
| CN111513329A (en) * | 2020-05-18 | 2020-08-11 | 云南农业大学 | Preparation process and application of pseudo-ginseng flower stem and leaf extract |
| CN114177210A (en) * | 2021-10-09 | 2022-03-15 | 金七药业股份有限公司 | Formula and preparation process of whole panax notoginseng |
| CN113995075A (en) * | 2021-11-22 | 2022-02-01 | 金七药业股份有限公司 | Pseudo-ginseng solid beverage and preparation method thereof |
| CN114748525A (en) * | 2022-04-26 | 2022-07-15 | 云南七丹药业股份有限公司 | Preparation method of oral liquid containing pseudo-ginseng and product thereof |
| CN114773158A (en) * | 2022-04-26 | 2022-07-22 | 云南七丹药业股份有限公司 | Extraction process and production method of effective components of fresh pseudo-ginseng flower |
| CN115005306A (en) * | 2022-07-14 | 2022-09-06 | 云南农业大学 | Preparation process and application of pseudo-ginseng stem leaf-mulberry leaf extract |
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Application publication date: 20180710 |