CN108239290A - The process units of visbreaking agent sodium humate - Google Patents
The process units of visbreaking agent sodium humate Download PDFInfo
- Publication number
- CN108239290A CN108239290A CN201711445817.XA CN201711445817A CN108239290A CN 108239290 A CN108239290 A CN 108239290A CN 201711445817 A CN201711445817 A CN 201711445817A CN 108239290 A CN108239290 A CN 108239290A
- Authority
- CN
- China
- Prior art keywords
- reaction kettle
- process units
- sodium humate
- inspissator
- agent sodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H6/00—Macromolecular compounds derived from lignin, e.g. tannins, humic acids
Abstract
The process units of visbreaking agent sodium humate, mainly includes：Reaction kettle (D101), inspissator (L101), drier (L102), pulverizer (L103), wherein, inspissator (L101) is connected with reaction kettle (D101), drier (L102) is connected respectively with inspissator (L101), pulverizer (L103), wherein, 210 230L of reaction kettle (D101) nominal volume.
Description
Technical field
The present invention relates to compound synthesis device more particularly to the process units of visbreaking agent sodium humate.
Background technology
Sodium humate has drop to stick, drops dehydration, is anti-collapse, resistance to for drilling mud, fresh-water drilling fluid high temperature resistant fluid loss additive
The effects that temperature, anti-pollution, it is also possible to make cement water reducing agent.It can be used as fertilizer and plant growth substance in agriculturally sodium humate,
Crop growth can be stimulated, improves soil texture, improves crop drought resistance ability, promotes nitrogen-fixing bacteria activation, industrially
Sodium humate can be used for increasing yeast ability, improve ethanol production, it is also possible to make lubricant etc..Existing process units compares mostly
More complicated, sodium humate is as visbreaking agent, and for process units quality for improving product quality, reducing by-products content has weight
Want economic implications.
Invention content
The purpose of the present invention is to provide the process units of visbreaking agent sodium humate, mainly include：It is reaction kettle (D101), dense
Contracting device (L101), drier (L102), pulverizer (L103), wherein, inspissator (L101) is connected with reaction kettle (D101), does
Dry device (L102) is connected respectively with inspissator (L101), pulverizer (L103), wherein, reaction kettle (D101) nominal volume 210-
230L, reaction kettle (D101) chuck capacity 90-95L, reaction kettle (D101) outer pot diameter 600-620mm.
The process units of visbreaking agent sodium humate, production procedure are：High quality brown coal is put into reaction kettle D101, is controlled
Temperature reacts 1-2h to 50-57 DEG C, and product is passed sequentially through inspissator L101 concentrates 3-5 times, drier L102 dryings 90-
120min, disintegrating machine L103 crush 30-50min to get finished product.The invention has the advantages that：Reduce reaction intermediate link, reduce
Reaction temperature and reaction time, improve reaction yield.
Description of the drawings
Fig. 1 is the process units of visbreaking agent sodium humate, is mainly included：Reaction kettle (D101), inspissator (L101), drying
Device (L102), pulverizer (L103).
Specific embodiment
With reference to specific implementation example, the invention will be further described：
Example 1：
Raw materials for production and dosage
| Lignite | Technical grade | 200 | Caustic soda | Technical grade | 40 |
The process units of visbreaking agent sodium humate, mainly includes：Reaction kettle (D101), inspissator (L101), drier
(L102), pulverizer (L103), wherein, inspissator (L101) is connected with reaction kettle (D101), drier (L102) respectively with
Inspissator (L101), pulverizer (L103) are connected, wherein, reaction kettle (D101) nominal volume 210L, reaction kettle (D101) folder
Cover capacity 90L, reaction kettle (D101) outer pot diameter 600mm.
The process units of visbreaking agent sodium humate, production procedure are：High quality brown coal is put into reaction kettle D101, is controlled
Temperature reacts 1h to 50 DEG C, and product is passed sequentially through inspissator L101 concentrations 3 times, drier L102 dryings 90min, disintegrating machine
L103 crushes 30min to get finished product.
Product quality
| Water-soluble content of humic acid/% | 53 |
| Moisture/% | ≤10 |
| Fineness (crossing 40 mesh sieve)/% | 100 |
| PH value | 9.2 |
| Appearance | Black powder |
Example 2：
Raw materials for production and dosage
| Lignite | Technical grade | 260 | Caustic soda | Technical grade | 50 |
The process units of visbreaking agent sodium humate, mainly includes：Reaction kettle (D101), inspissator (L101), drier
(L102), pulverizer (L103), wherein, inspissator (L101) is connected with reaction kettle (D101), drier (L102) respectively with
Inspissator (L101), pulverizer (L103) are connected, wherein, reaction kettle (D101) nominal volume 230L, reaction kettle (D101) folder
Cover capacity 95L, reaction kettle (D101) outer pot diameter 620mm.
The process units of visbreaking agent sodium humate, production procedure are：High quality brown coal is put into reaction kettle D101, is controlled
Temperature reacts 2h to 57 DEG C, and product is passed sequentially through inspissator L101 concentrations 5 times, drier L102 dryings 120min, disintegrating machine
L103 crushes 50min to get finished product.
Product quality
| Water-soluble content of humic acid/% | 55 |
| Moisture/% | ≤11 |
| Fineness (crossing 40 mesh sieve)/% | 100 |
| PH value | 9.5 |
| Appearance | Black powder |
It described in above example, is merely preferred embodiments of the present invention, but protection scope of the present invention not office
Be limited to this, any one skilled in the art in the technical scope disclosed by the present invention, the technique according to the invention
Scheme and its inventive concept are subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (3)
1. the process units of visbreaking agent sodium humate, which is characterized in that mainly include：Reaction kettle (D101), inspissator (L101),
Drier (L102), pulverizer (L103), wherein, inspissator (L101) is connected with reaction kettle (D101), drier (L102)
It is connected respectively with inspissator (L101), pulverizer (L103), wherein, reaction kettle (D101) nominal volume 210-230L.
2. the process units of visbreaking agent sodium humate according to claim 1, which is characterized in that the reaction kettle (D101)
Chuck capacity 90-95L.
3. the process units of visbreaking agent sodium humate according to claim 1, which is characterized in that the reaction kettle (D101)
Outer pot diameter 600-620mm.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711445817.XA CN108239290A (en) | 2017-12-27 | 2017-12-27 | The process units of visbreaking agent sodium humate |
| AU2018101966A AU2018101966A4 (en) | 2017-12-27 | 2018-12-05 | Viscosity reducer sodium humate production plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711445817.XA CN108239290A (en) | 2017-12-27 | 2017-12-27 | The process units of visbreaking agent sodium humate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108239290A true CN108239290A (en) | 2018-07-03 |
Family
ID=62701286
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711445817.XA Withdrawn CN108239290A (en) | 2017-12-27 | 2017-12-27 | The process units of visbreaking agent sodium humate |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN108239290A (en) |
| AU (1) | AU2018101966A4 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110041904A (en) * | 2019-04-23 | 2019-07-23 | 中国海洋石油集团有限公司 | Humic acid and alkylamine Compositional type heavy crude thinner and the preparation method and application thereof |
-
2017
- 2017-12-27 CN CN201711445817.XA patent/CN108239290A/en not_active Withdrawn
-
2018
- 2018-12-05 AU AU2018101966A patent/AU2018101966A4/en not_active Ceased
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110041904A (en) * | 2019-04-23 | 2019-07-23 | 中国海洋石油集团有限公司 | Humic acid and alkylamine Compositional type heavy crude thinner and the preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| AU2018101966A4 (en) | 2019-01-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180703 |
|
| WW01 | Invention patent application withdrawn after publication |