CN108219534A - A kind of bright blue disperse dye composition - Google Patents
A kind of bright blue disperse dye composition Download PDFInfo
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- CN108219534A CN108219534A CN201711489702.0A CN201711489702A CN108219534A CN 108219534 A CN108219534 A CN 108219534A CN 201711489702 A CN201711489702 A CN 201711489702A CN 108219534 A CN108219534 A CN 108219534A
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- China
- Prior art keywords
- bright blue
- pud
- dye composition
- disperse dye
- blue disperse
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of bright blue disperse dye composition, including following components by percentage to the quality:Gorgeous indigo plant PUD B:10 20%;Bright blue PUD:1 10%;Light yellow PUD SD:0.001 1%;Dispersant Reax85A:5 20%;Dispersing agent MF:50 80%.The bright blue disperse dye composition of the present invention can substitute the bright blue S GL of dispersion and use, and coloring and fastness are attained by the requirement of dyestuff, more gorgeous on color than disperseing bright blue S GL on the basis of fastness is ensured, and greatly reduce cost.
Description
Technical field
The present invention relates to textile field more particularly to a kind of bright blue disperse dye compositions.
Background technology
It is a kind of single compound dyestuff to disperse bright blue S-GL, is mainly used for the dyeing of polyester fiber.In national standard HG/T
Defined in 4023-2008 disperse bright blue S-GL molecular formula be C20H17N3O5, relative molecular mass 379.37.Due to raw material
Pressure, disperse bright blue S-GL price soar to again and again about 150-200 member/kilogram, it is out of stock in spite of rising price, can not meet the need of production
It asks, therefore is badly in need of a kind of substitute for disperseing bright blue S-GL, easily prepare, it is at low cost.According to general color theory, with three
Primary colors can compound out a variety of colors.But the usual vividness of dyestuff for conventionally compounding out is relatively low.Vividness is high
Dyestuff vividness can be reduced to the degree of needs by allotment, but the low dyestuff of vividness but allocate in any case how
Also it cannot be higher than the dyestuff of initial vividness.Therefore it is extremely difficult for reaching certain vividness.Furthermore as dyestuff
It uses, the fastness of dyestuff is needed to reach certain standard, in general fastness should reach more than 4.Conventional preparation method, though
The color that can be so needed with several primary colors, but fastness is usually relatively low, it is impossible to it is perfectly adhered on textile, passes through
After washing or solarization, easily fade.Therefore color needs can be met and meet vividness and fastness need by wanting to obtain one kind
The dyestuff wanted is extremely difficult.
Invention content
Technical problem solved by the invention is, in order to overcome the existing bright blue S-GL prices of dispersion high, to be not easy to prepare
Defect provides a kind of bright blue disperse dye composition.It is bright blue that the bright blue disperse dye composition of the present invention can substitute dispersion
S-GL is used, and greatly reduces cost.
The present invention is to solve above-mentioned technical problem by the following technical programs:
The present invention provides a kind of bright blue disperse dye composition, including following components by percentage to the quality:
Gorgeous indigo plant PUD-B:10%-20%;
Bright blue PUD:1%-10%;
Light yellow PUD-SD:0.001%-1%;
Dispersant Reax85A:5%-20%;
Dispersing agent MF:50%-80%.
Preferably, the content of the gorgeous indigo plant PUD-B is 15%-18%.
Preferably, the content of the bright blue PUD is 1%-5%.
Preferably, the content of the light yellow PUD-SD is 0.1%-0.5%.
Preferably, the content of the dispersant Reax85A is 10%-20%.
Preferably, the content of the dispersing agent MF is 50%-70%.
Preferably, the bright blue disperse dye composition includes following components by percentage to the quality:
Gorgeous indigo plant PUD-B:15.6%;
Bright blue PUD:4%;
Light yellow PUD-SD:0.4%;
Dispersant Reax85A:20%;
Dispersing agent MF:60%.
Preferably, the preparation method of the bright blue disperse dye composition is by gorgeous indigo plant PUD-B, bright blue PUD and light yellow
PUD-SD adds in dispersant Reax85A and dispersing agent MF, levigate by zirconium pearl or quartz sand, is uniformly mixed, upper spray drying tower
Spray drying.
On the basis of common knowledge of the art, above-mentioned each optimum condition can be combined arbitrarily to get each preferable reality of the present invention
Example.
The reagents and materials used in the present invention are commercially available.
The positive effect of the present invention is:The bright blue disperse dye composition of the present invention can substitute the bright blue S- of dispersion
GL is used, and coloring and fastness are attained by the requirement of dyestuff, on the basis of fastness is ensured, than disperseing bright blue S-GL on color
It is more gorgeous, and greatly reduce cost.
Specific embodiment
It is further illustrated the present invention below by the mode of embodiment, but does not therefore limit the present invention to the reality
It applies among a range.Test method without specific conditions in the following example, according to conventional methods and conditions or according to quotient
Product specification selects.
The Component Source of various embodiments of the present invention is described as follows:
Gorgeous indigo plant PUD-B:Purchased from its Group Plc of Town in Shanghai promise, product typeGorgeous indigo plant PUD;
Bright blue PUD:Purchased from its Group Plc of Town in Shanghai promise, product typeBright blue PUD;
Light yellow PUD-SD:Purchased from its Group Plc of Town in Shanghai promise, product type Light yellow PUD-
SD;
Dispersant Reax85A:It is that alkaline pulp waste liquid (kraft pulp waste liquid) is concentrated and chemically treated and obtain, purchases
In Westvaco companies of the U.S.;
Dispersing agent MF:Purchased from its Group Plc of Town in Shanghai promise, also known as dispersing agent MF, molecule
Formula is C23H18O6S2Na2, molecular weight 500.49.
This hair embodiment 1-4 uses following preparation method:
Gorgeous indigo plant PUD-B filter cakes, bright blue PUD filter cakes and light yellow PUD-SD filter cakes are added in into dispersant Reax85A and diffusant
MF, it is levigate by zirconium pearl or quartz sand, it is uniformly mixed, upper spray drying tower spray drying.
Embodiment 1
The bright blue disperse dye composition of embodiment 1 includes following components by percentage to the quality:
Gorgeous indigo plant PUD-B:15.6%;
Bright blue PUD:3.9%;
Light yellow PUD-SD:0.4%;
Dispersant Reax85A:20%;
Dispersing agent MF:60.1%.
The dye uptake of dyestuff is measured according to GBT 23976.1-2009, the results are shown in Table 1:
The dye uptake measurement result of 1 embodiment 1 of table
Embodiment 2
The bright blue disperse dye composition of embodiment 2 includes following components by percentage to the quality:
Gorgeous indigo plant PUD-B:19.6%;
Bright blue PUD:3.9%;
Light yellow PUD-SD:0.4%;
Dispersant Reax85A:20%;
Dispersing agent MF:56%.
The dye uptake of dyestuff is measured according to GBT 23976.1-2009, the results are shown in Table 2:
The dye uptake measurement result of 2 embodiment 2 of table
Embodiment 3
The bright blue disperse dye composition of embodiment 3 includes following components by percentage to the quality:
Gorgeous indigo plant PUD-B:15.7%;
Bright blue PUD:4%;
Light yellow PUD-SD:0.4%;
Dispersant Reax85A:20%;
Dispersing agent MF:59.9%.
The dye uptake of dyestuff is measured according to GBT 23976.1-2009, the results are shown in Table 3:
The dye uptake measurement result of 3 embodiment 3 of table
Embodiment 4
The bright blue disperse dye composition of embodiment 4 includes following components by percentage to the quality:
Gorgeous indigo plant PUD-B:16%;
Bright blue PUD:4.05%;
Light yellow PUD-SD:0.41%;
Dispersant Reax85A:20%;
Dispersing agent MF:59.54%.
The dye uptake of dyestuff is measured according to GBT 23976.1-2009, the results are shown in Table 4:
The dye uptake measurement result of 4 embodiment 4 of table
Embodiment 5
The bright blue disperse dye composition of embodiment 5 includes following components by percentage to the quality:
Gorgeous indigo plant PUD-B:16%;
Bright blue PUD:4.02%;
Light yellow PUD-SD:0.4%;
Dispersant Reax85A:20%;
Dispersing agent MF:59.58%.
The dye uptake of dyestuff is measured according to GBT 23976.1-2009, the results are shown in Table 5:
The dye uptake measurement result of 5 embodiment 5 of table
Embodiment 6
The bright blue disperse dye composition of embodiment 6 includes following components by percentage to the quality:
Gorgeous indigo plant PUD-B:15.9%;
Bright blue PUD:4%;
Light yellow PUD-SD:0.4%;
Dispersant Reax85A:20%;
Dispersing agent MF:59.7%.
The dye uptake of dyestuff is measured according to GBT 23976.1-2009, the results are shown in Table 6:
The dye uptake measurement result of 6 embodiment 6 of table
Comparative example 1
The bright blue disperse dye composition of comparative example 1 includes following components by percentage to the quality:
Gorgeous indigo plant PUD-B:6%;
Bright blue PUD:4%;
Dispersant Reax85A:20%;
Dispersing agent MF:60%.
The dye uptake of dyestuff is measured according to GBT 23976.1-2009, the results are shown in Table 7:
The dye uptake measurement result of 7 embodiment 7 of table
Comparative example 2
The bright blue disperse dye composition of comparative example 2 includes following components by percentage to the quality:
Gorgeous indigo plant PUD-B:15.5%;
Bright blue PUD:4%;
Light yellow PUD-SD:0.5%;
Dispersant Reax85A:60%;
Dispersing agent MF:20%.
The dye uptake of dyestuff is measured according to GBT 23976.1-2009, the results are shown in Table 8:
The dye uptake measurement result of 8 embodiment 8 of table
Bright blue dispersion is measured to embodiment 1-6 and comparative example 1-2 according to the bioassay standard of ISO 105C06C2S respectively to contaminate
The feed composition washing fastness on vinegar fibre, cotton, nylon, terylene, acrylic fibers and wool respectively is tested bright blue according to ISO105B02
The light fastness of disperse dye composition measures bright-colored degree according to GBT 2394-2013, and vividness is divided into darker, equivalent
More gorgeous three kinds of grades, index DL, Da, Db and DEcmc associated with vividness are also listed in wherein, and measurement result is shown in Table 9:
The measurement result of table 9 embodiment 1-6 and comparative example 1-2
Embodiment | Washing fastness | Light fastness | Vividness | DL | Da | Db | DEcmc |
Embodiment 1 | 4.5 | 6 | It is equivalent | -0.11 | 0.66 | -0.73 | 0.62 |
Embodiment 2 | 4.5 | 6 | It is equivalent | 0.2 | 0.16 | -0.2 | 0.18 |
Embodiment 3 | 4.5 | 6 | It is more gorgeous | 0.14 | 0.33 | -0.18 | 0.25 |
Embodiment 4 | 4.5 | 6 | It is more gorgeous | -0.06 | 0 | 0.42 | 0.21 |
Embodiment 5 | 4.5 | 6 | It is more gorgeous | -0.02 | 0.06 | 0.14 | 0.07 |
Embodiment 6 | 4.5 | 6 | It is more gorgeous | -0.12 | 0.22 | -0.18 | 0.19 |
Comparative example 1 | 4 | 6 | It is darker | -0.05 | 0.15 | -0.4 | 0.25 |
Comparative example 2 | 4 | 6 | It is darker | 0.15 | 0.13 | -0.29 | 0.62 |
Disperse bright blue S-GL | 4 | 6 | / | -0.12 | 0.06 | 0.21 | / |
The bright blue disperse dye composition of the present invention can substitute the bright blue S-GL of dispersion and use, and coloring and fastness are attained by
The requirement of dyestuff, it is more gorgeous on color than disperseing bright blue S-GL on the basis of fastness is ensured, and greatly reduce cost.
Although specific embodiments of the present invention have been described above, it will be appreciated by those of skill in the art that this is only
For example, protection scope of the present invention is to be defined by the appended claims.Those skilled in the art without departing substantially from
Under the premise of the principle and substance of the present invention, many changes and modifications may be made, but these change and
Modification each falls within protection scope of the present invention.
Claims (8)
1. a kind of bright blue disperse dye composition, including following components by percentage to the quality:
Gorgeous indigo plant PUD-B:10%-20%;
Bright blue PUD:1%-10%;
Light yellow PUD-SD:0.001%-1%;
Dispersant Reax85A:5%-20%;
Dispersing agent MF:50%-80%.
2. bright blue disperse dye composition as described in claim 1, which is characterized in that the content of the gorgeous indigo plant PUD-B is
15%-18%.
3. bright blue disperse dye composition as described in claim 1, which is characterized in that the content of the bright blue PUD is 1%-
5%.
4. bright blue disperse dye composition as described in claim 1, which is characterized in that the content of the light yellow PUD-SD is
0.1%-0.5%.
5. bright blue disperse dye composition as described in claim 1, which is characterized in that the content of the dispersant Reax85A
For 10%-20%.
6. bright blue disperse dye composition as described in claim 1, which is characterized in that the content of the dispersing agent MF is
50%-70%.
7. bright blue disperse dye composition as described in claim 1, which is characterized in that the bright blue disperse dye composition packet
Include following components by percentage to the quality:
Gorgeous indigo plant PUD-B:15.6%;
Bright blue PUD:4%;
Light yellow PUD-SD:0.4%;
Dispersant Reax85A:20%;
Dispersing agent MF:60%.
8. the bright blue disperse dye composition as described in claim 1 to 7 any one, which is characterized in that the bright blue dispersion
The preparation method of dye composite is that gorgeous indigo plant PUD-B, bright blue PUD and light yellow PUD-SD are added in dispersant Reax85A and diffusion
Agent MF, it is levigate by zirconium pearl or quartz sand, it is uniformly mixed, upper spray drying tower spray drying.
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CN201711489702.0A CN108219534A (en) | 2017-12-29 | 2017-12-29 | A kind of bright blue disperse dye composition |
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CN201711489702.0A CN108219534A (en) | 2017-12-29 | 2017-12-29 | A kind of bright blue disperse dye composition |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110373045A (en) * | 2019-07-23 | 2019-10-25 | 孚美科(绍兴)染料科技有限公司 | It is a kind of to disperse bright blue S-GB200% dye composite and its application |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101768820A (en) * | 2010-01-26 | 2010-07-07 | 白宏栋 | Manufacturing method of woven high and low wool printed carpets |
CN106192454A (en) * | 2016-07-13 | 2016-12-07 | 浙江亿得化工有限公司 | The intaglio plate of a kind of dacron directly prints or soft version directly prints printing technology and dispersion Weak solvent ink application in the process |
-
2017
- 2017-12-29 CN CN201711489702.0A patent/CN108219534A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101768820A (en) * | 2010-01-26 | 2010-07-07 | 白宏栋 | Manufacturing method of woven high and low wool printed carpets |
CN106192454A (en) * | 2016-07-13 | 2016-12-07 | 浙江亿得化工有限公司 | The intaglio plate of a kind of dacron directly prints or soft version directly prints printing technology and dispersion Weak solvent ink application in the process |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110373045A (en) * | 2019-07-23 | 2019-10-25 | 孚美科(绍兴)染料科技有限公司 | It is a kind of to disperse bright blue S-GB200% dye composite and its application |
CN110373045B (en) * | 2019-07-23 | 2023-11-10 | 孚美科(绍兴)染料科技有限公司 | Disperse turquoise blue S-GB200% dye composition and application thereof |
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