CN107974102A - A kind of composite disperse orange dye - Google Patents
A kind of composite disperse orange dye Download PDFInfo
- Publication number
- CN107974102A CN107974102A CN201711036851.1A CN201711036851A CN107974102A CN 107974102 A CN107974102 A CN 107974102A CN 201711036851 A CN201711036851 A CN 201711036851A CN 107974102 A CN107974102 A CN 107974102A
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- CN
- China
- Prior art keywords
- disperse orange
- agent
- dispersant
- composite
- auxiliary agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0046—Mixtures of two or more azo dyes
- C09B67/0051—Mixtures of two or more azo dyes mixture of two or more monoazo dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
Abstract
The present invention proposes a kind of composite disperse orange dye, including following percentage composition raw material：Disperse orange 73 15 23%, disperse orange 56 10%, disperse orange 25 12 14%, disperse orange 37 0 11%, disperse orange 44 0 6%, adjuncts Balance, the present invention is compounded by rational raw material, effectively increase dyeing performance, color fastness to washing, colour fastness to perspiration, colour fastness to rubbing, color fastness to hot pressing are respectively provided with obvious raising, and dye-uptake is more than 85%.
Description
Technical field
The present invention relates to technical field of dye, and in particular to a kind of composite disperse orange dye.
Background technology
Disperse dyes are a kind of starting stages in dyeing course, in dispersity to hydrophobic under the action of dispersant
A kind of nonionic dye that property fiber is dyed.Disperse dyes have complete chromatography, bright in colour, and coloring intensity is high,
And there is good economy.Counted according to dyestuff Industry in China association, China's disperse dyes consumption arranges the head for occupying various dyestuffs
Position, the usage amount 60% of whole world disperse dyes is produced by China to be exported.
Wherein, orange disperse dye can be with disperse dark blue colour system and dispersed ruby colour system and scattered black mutual colorant match, application
Property good but presently commercially available orange disperse dye be mostly one-component, for colorant match when can not only influence dye-uptake, uniformly
Degree, and it is difficult to transition of the shallow orange of control to deep orange, comprehensive color fastness for textile is poor.At present, with the improvement of people's life quality, people
To textile dyeing requirement constantly lifting, solarization to dyestuff, soap, wash, hot pressing, friction, the requirement such as fastness to perspiration carry
New requirement is gone out, therefore, developing the disperse dyes of compounding, dyeability is most important to improve, in addition, in dyestuff compounding
During, the reasonable selection of auxiliary agent is also very important, and ensures the dispersion stabilization of suspended substance as far as possible, improves product pad dyeing
Dye uptake.
The content of the invention
For above-mentioned problem, the present invention proposes a kind of composite disperse orange dye, is compounded by rational raw material,
Dyeing performance is effectively increased, color fastness to washing, colour fastness to perspiration, colour fastness to rubbing, color fastness to hot pressing have
It is significantly improved, dye-uptake is more than 85%.
In order to realize above-mentioned purpose, the present invention uses following technical solution：
A kind of composite disperse orange dye, including following percentage composition raw material：Disperse orange 7315-23%, disperse orange 56-
10%th, disperse orange 25 12-14%, disperse orange 370-11%, disperse orange 440-6%, adjuncts Balance.
Preferably, composite disperse orange dye, including following percentage composition raw material：Disperse orange 7320-23%, disperse orange 56-
8%th, disperse orange 25 12-13%, disperse orange 375-7%, disperse orange 442-3%, adjuncts Balance.
Preferably, auxiliary agent includes levelling agent, color fixing agent, dispersant, and wherein levelling agent accounts for the 2-10% of auxiliary agent gross mass, consolidates
Toner accounts for the 2-9% of auxiliary agent gross mass, dispersant is surplus.
Preferably, auxiliary agent further includes the PEG-1000 for accounting for auxiliary agent gross mass 0-8% and accounts for the poly- of auxiliary agent gross mass 0-5%
Vinyl acetate.
Preferably, auxiliary agent includes the component of following percentage composition：It is levelling agent 7%, color fixing agent 5%, PEG-10007%, poly-
Vinyl acetate 4.5%, dispersant surplus.
Preferably, for levelling agent using levelling agent BOF and the mixture of AEO-9, both mass ratioes are 1：0.6-1.
Preferably, color fixing agent uses polyethyleneimine.
Preferably, dispersant uses one kind in Dispersant MF, dispersant NNO, dispersing agent C NF and sodium lignin sulfonate
Or numerous compositions.
Preferably, dispersant is the composition of Dispersant MF, dispersant NNO and sodium lignin sulfonate, and three's mass ratio is
2：1：1.5.
Due to using above-mentioned technical solution, the beneficial effects of the invention are as follows：The present invention is compounded by rational raw material and (used
Dyed in high temperature), easy to adjust different orange system coloured light, and hue shift is weak, effectively increases dyeing performance, resistance to
Wash color fastness, colour fastness to perspiration, colour fastness to rubbing, color fastness to hot pressing etc. and be respectively provided with obvious raising, dye-uptake is more than
85%.
Color fastness to washing is 4-5 grades, 4-5 grades of colour fastness to perspiration, 3-5 grades of colour fastness to rubbing, color fastness to hot pressing 4-5
Level, 4-5 grades of sublimation reliability (180 DEG C).
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention,
Technical solution in the embodiment of the present invention is clearly and completely described.Based on the embodiment of the present invention, the common skill in this area
Art personnel all other embodiments obtained without creative efforts, belong to the model that the present invention protects
Enclose.
Embodiment 1：
A kind of composite disperse orange dye, it is characterised in that including following percentage composition raw material：Disperse orange 7318%, disperse
Orange 58%, disperse orange 25 12%, disperse orange 370%, disperse orange 442%, adjuncts Balance.
Auxiliary agent includes levelling agent, color fixing agent, dispersant, and wherein levelling agent accounts for the 8% of auxiliary agent gross mass, color fixing agent and accounts for auxiliary agent
Gross mass 4%, dispersant be surplus.
Wherein, for levelling agent using levelling agent BOF and the mixture of AEO-9, both mass ratioes are 1：0.7, color fixing agent uses
Polyethyleneimine, dispersant are mass ratio 2：1：1.5 Dispersant MF, dispersant NNO, the composition of sodium lignin sulfonate.
Embodiment 2：
A kind of composite disperse orange dye, it is characterised in that including following percentage composition raw material：Disperse orange 7315%, disperse
Orange 510%, disperse orange 25 12%, disperse orange 375%, disperse orange 440%, adjuncts Balance.
Auxiliary agent includes levelling agent, color fixing agent, dispersant, and wherein levelling agent accounts for the 4% of auxiliary agent gross mass, color fixing agent and accounts for auxiliary agent
Gross mass 6%, dispersant be surplus.
Wherein, for levelling agent using levelling agent BOF and the mixture of AEO-9, both mass ratioes are 1：0.9, color fixing agent uses
Polyethyleneimine, dispersant are mass ratio 2：1：1.5 Dispersant MF, dispersant NNO, the composition of sodium lignin sulfonate.
Embodiment 3：
A kind of composite disperse orange dye, it is characterised in that including following percentage composition raw material：Disperse orange 7322%, disperse
Orange 58%, disperse orange 25 14%, disperse orange 3711%, disperse orange 446%, adjuncts Balance.
Auxiliary agent includes levelling agent, color fixing agent, dispersant, and wherein levelling agent accounts for the 7% of auxiliary agent gross mass, color fixing agent and accounts for auxiliary agent
Gross mass 5%, dispersant be surplus；Further include the PEG-1000 for accounting for auxiliary agent gross mass 8% and account for auxiliary agent gross mass 0%
Polyvinyl acetate.
Wherein, for levelling agent using levelling agent BOF and the mixture of AEO-9, both mass ratioes are 1：1, color fixing agent is using poly-
Aziridine, dispersant are mass ratio 1：1 Dispersant MF, the composition of dispersant NNO.
Embodiment 4：
A kind of composite disperse orange dye, it is characterised in that including following percentage composition raw material：Disperse orange 7323%, disperse
Orange 56%, disperse orange 25 12%, disperse orange 370%, disperse orange 440%, adjuncts Balance.
Auxiliary agent includes levelling agent, color fixing agent, dispersant, and wherein levelling agent accounts for the 10% of auxiliary agent gross mass, color fixing agent and accounts for and help
Agent gross mass 9%, dispersant be surplus；Further include the PEG-1000 for accounting for auxiliary agent gross mass 7% and account for auxiliary agent gross mass
4.5% polyvinyl acetate.
Wherein, for levelling agent using levelling agent BOF and the mixture of AEO-9, both mass ratioes are 1：0.8, color fixing agent uses
Polyethyleneimine, dispersant are mass ratio 2：1：1.5 Dispersant MF, dispersant NNO, the composition of sodium lignin sulfonate.
Embodiment 5：
A kind of composite disperse orange dye, it is characterised in that including following percentage composition raw material：Disperse orange 7320%, disperse
Orange 57%, disperse orange 25 13%, disperse orange 377%, disperse orange 443%, adjuncts Balance.
Auxiliary agent includes levelling agent, color fixing agent, dispersant, and wherein levelling agent accounts for the 2% of auxiliary agent gross mass, color fixing agent and accounts for auxiliary agent
Gross mass 2%, dispersant be surplus；Further include the PEG-1000 for accounting for auxiliary agent gross mass 0% and account for auxiliary agent gross mass 5%
Polyvinyl acetate.
Wherein, for levelling agent using levelling agent BOF and the mixture of AEO-9, both mass ratioes are 1：0.7, color fixing agent uses
Polyethyleneimine, dispersant use sodium lignin sulfonate.
The composite disperse orange dye preparation process of above-described embodiment 1-5 is as follows：First disperse orange is weighed by mass percentage
Each dye content (is scaled former dyestuff wet cake weight to stock up) by raw material filter cake by formula, is placed in grinder, with 500-
600rpm grinds 10-12h, obtains dyestuff powder, then adds auxiliary agent thereto and suitable water (or wetting agent) is beaten
Slurry is obtained, slurry is placed in liquid honing machine 4-6h is ground with 550rpm, then stir 30- under 50-55 DEG C of constant temperature
60min, is immediately sent into drying in microwave drying room, while sprays into a small amount of dust-proofing agent and carry out dust-proof handle up to composite diffusion
Orange dyestuff.
Composite disperse orange dye made from embodiment 1-5 is subjected to every fastness properties test, as a result such as following table：
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
The present invention is described in detail, it will be understood by those of ordinary skill in the art that：It still can be to foregoing each implementation
Technical solution described in example is modified, or carries out equivalent substitution to which part technical characteristic；And these modification or
Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical solution.
Claims (9)
1. a kind of composite disperse orange dye, it is characterised in that including following percentage composition raw material：Disperse orange 7315-23%, disperse
Orange 56-10%, disperse orange 25 12-14%, disperse orange 370-11%, disperse orange 440-6%, adjuncts Balance.
2. composite disperse orange dye according to claim 1, it is characterised in that including following percentage composition raw material：It is scattered
Orange 7320-23%, disperse orange 56-8%, disperse orange 25 12-13%, disperse orange 375-7%, disperse orange 442-3%, more than auxiliary agent
Amount.
3. composite disperse orange dye according to claim 1 or 2, it is characterised in that：The auxiliary agent includes levelling agent, fixation
Agent, dispersant, wherein levelling agent account for the 2-10% of auxiliary agent gross mass, color fixing agent accounts for the 2-9% of auxiliary agent gross mass, dispersant is remaining
Amount.
4. composite disperse orange dye according to claim 3, it is characterised in that：The auxiliary agent, which further includes, accounts for auxiliary agent gross mass
The PEG-1000 of 0-8% and the polyvinyl acetate for accounting for auxiliary agent gross mass 0-5%.
5. composite disperse orange dye according to claim 4, it is characterised in that the auxiliary agent includes following percentage composition
Component：Levelling agent 7%, color fixing agent 5%, PEG-10007%, polyvinyl acetate 4.5%, dispersant surplus.
6. according to 4 or 5 any one of them composite disperse orange dye of claim, it is characterised in that：The levelling agent is using even
The mixture of stain BOF and AEO-9, both mass ratioes are 1：0.6-1.
7. according to 4 or 5 any one of them composite disperse orange dye of claim, it is characterised in that：The color fixing agent is using poly-
Aziridine.
8. according to 4 or 5 any one of them composite disperse orange dye of claim, it is characterised in that：The dispersant, which uses, to be divided
One or more compositions in powder MF, dispersant NNO, dispersing agent C NF and sodium lignin sulfonate.
9. composite disperse orange dye according to claim 8, it is characterised in that：The dispersant is Dispersant MF, disperses
The composition of agent NNO and sodium lignin sulfonate, three's mass ratio are 2：1：1.5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711036851.1A CN107974102A (en) | 2017-10-30 | 2017-10-30 | A kind of composite disperse orange dye |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711036851.1A CN107974102A (en) | 2017-10-30 | 2017-10-30 | A kind of composite disperse orange dye |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107974102A true CN107974102A (en) | 2018-05-01 |
Family
ID=62012854
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711036851.1A Pending CN107974102A (en) | 2017-10-30 | 2017-10-30 | A kind of composite disperse orange dye |
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| Country | Link |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113462195A (en) * | 2021-07-06 | 2021-10-01 | 浙江捷发科技股份有限公司 | Preparation method of modified sodium lignosulfonate dye dispersing agent |
| CN113874444A (en) * | 2019-05-23 | 2021-12-31 | 日本化药株式会社 | Coloring dispersion liquid, recording medium, and method for printing hydrophobic fiber |
| CN114989634A (en) * | 2022-07-05 | 2022-09-02 | 绍兴金绿洲新材料科技有限公司 | Disperse orange dye mixture |
Citations (7)
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|---|---|---|---|---|
| CN1631989A (en) * | 2004-11-10 | 2005-06-29 | 浙江龙盛集团股份有限公司 | Composite disperse orange dye |
| CN1995154A (en) * | 2006-12-21 | 2007-07-11 | 浙江龙盛集团股份有限公司 | Dispersing orange dye composition and dispersing dye |
| CN101654566A (en) * | 2009-09-10 | 2010-02-24 | 董源 | Monoazo type composition dye |
| CN102634233A (en) * | 2012-03-27 | 2012-08-15 | 江苏之江化工有限公司 | Orange mix |
| CN104356688A (en) * | 2014-09-16 | 2015-02-18 | 绍兴县精细化工有限公司 | Yellow disperse dyes composition and preparation method and application thereof |
| CN105970671A (en) * | 2016-07-22 | 2016-09-28 | 沈阳化工研究院有限公司 | Dyeing and coating integrated dye dyeing and printing paste-shaped compound and application thereof |
| CN106221380A (en) * | 2016-08-19 | 2016-12-14 | 常州江昇化工有限公司 | A kind of environmental-protection water-based pigment mill base and preparation method thereof |
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2017
- 2017-10-30 CN CN201711036851.1A patent/CN107974102A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1631989A (en) * | 2004-11-10 | 2005-06-29 | 浙江龙盛集团股份有限公司 | Composite disperse orange dye |
| CN1995154A (en) * | 2006-12-21 | 2007-07-11 | 浙江龙盛集团股份有限公司 | Dispersing orange dye composition and dispersing dye |
| CN101654566A (en) * | 2009-09-10 | 2010-02-24 | 董源 | Monoazo type composition dye |
| CN102634233A (en) * | 2012-03-27 | 2012-08-15 | 江苏之江化工有限公司 | Orange mix |
| CN104356688A (en) * | 2014-09-16 | 2015-02-18 | 绍兴县精细化工有限公司 | Yellow disperse dyes composition and preparation method and application thereof |
| CN105970671A (en) * | 2016-07-22 | 2016-09-28 | 沈阳化工研究院有限公司 | Dyeing and coating integrated dye dyeing and printing paste-shaped compound and application thereof |
| CN106221380A (en) * | 2016-08-19 | 2016-12-14 | 常州江昇化工有限公司 | A kind of environmental-protection water-based pigment mill base and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113874444A (en) * | 2019-05-23 | 2021-12-31 | 日本化药株式会社 | Coloring dispersion liquid, recording medium, and method for printing hydrophobic fiber |
| EP3988619A4 (en) * | 2019-05-23 | 2023-08-09 | Nippon Kayaku Kabushiki Kaisha | Colored dispersion, recording medium, and textile printing method for hydrophobic fibers |
| CN113462195A (en) * | 2021-07-06 | 2021-10-01 | 浙江捷发科技股份有限公司 | Preparation method of modified sodium lignosulfonate dye dispersing agent |
| CN114989634A (en) * | 2022-07-05 | 2022-09-02 | 绍兴金绿洲新材料科技有限公司 | Disperse orange dye mixture |
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| PB01 | Publication | ||
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Application publication date: 20180501 |