CN102634233A - Orange mix - Google Patents
Orange mix Download PDFInfo
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- CN102634233A CN102634233A CN2012100828713A CN201210082871A CN102634233A CN 102634233 A CN102634233 A CN 102634233A CN 2012100828713 A CN2012100828713 A CN 2012100828713A CN 201210082871 A CN201210082871 A CN 201210082871A CN 102634233 A CN102634233 A CN 102634233A
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Abstract
The invention discloses orange mix and production method thereof. The orange mix is mainly produced by mixing disperse yellow 163 shown in a structural formula (I), disperse orange 61 shown in a structural formula (II) and disperse orange 73 shown in a structural formula (III). When the organ dye is used to print and dye superfine fiber materials, dyed fabrics with good properties such as bright color, vivid print profile, fine pattern washing fastness, sun-drying resistance, sweat resistance and the like can be obtained by adjusting proportions of the different components.
Description
One technical field
The present invention relates to a kind of orange mixture and preparation method thereof, belong to the chemical material preparing technical field.
Two background technologies
Azoic dyestuff (azo dyes; The azo-group two ends connect one type of organic cpds of aryl) be fabric clothing most widely used one type of synthetic dyestuff in dyeing and printing process; Advantage such as that azoic dyestuff has is bright-colored, fastness is good, color and luster is various in style; The dyeing and the stamp that are used for multiple natural and synthon, also be used to paint, plastics, rubber etc. painted.Ultra-fine fibre is one type of novel synthon, have soft, ventilative moisture absorption; Advantage such as comfortable and easy to wear, because its monfil is thin, specific fiber surface is long-pending big; Colouring speed is fast, be difficult for dying even, dye dark, in reality dyeing; Several kinds of composite solving of dyestuff commonly used, but monomer dye colouring Harmony becomes a difficult problem again.
Three summary of the invention
The object of the present invention is to provide a kind of excellent a kind of orange mixture dyestuff of coordination performance that has.
The technical solution that realizes the object of the invention is: a kind of orange mixture dyestuff, and mainly be component A, a kind of structural formula suc as formula the DISPERSE YELLOW 163 shown in (I) and do B component and a kind of structural formula suc as formula the DISPERSE ORANGE 30 200 61 shown in (II) and be component C suc as formula the DISPERSE ORANGE 30 200 73 shown in (III) and mix by a kind of structural formula; Wherein the quality percentage composition of component A is 10-60%, and the quality percentage composition of B component is 10-55%, and the quality percentage composition of component C is 5-40%;
All the other are auxiliary agent.
As to further qualification of the present invention, based on described component A, B component and component C, wherein the quality percentage composition of component A is 15-40%, and the quality percentage composition of B component is 15-45%, and the quality percentage composition of component C is 7.5-30%.
Described auxiliary agent comprises one of following or its mixture, sodium lignosulfonate (xylogen 85A, 83A) and condensation compound of methyl naphthalene sulfonic acid and formaldehyde (Dispersant MF).
A kind of orange mixture dyestuff of the present invention can prepare by following method: will press above-mentioned proportioning after pre-dispersed pulverizing like the represented azo cpd of structural formula (I), structural formula (II) and structural formula (III); Add the dissolving of auxiliary agent and warm water dispersed with stirring, through sand mill continuously grinding and filtration; Sand milling to terminal after, spraying drying evenly sprays into simultaneously dust laying oil and dispersion agent, finished product packing.
Component A of the present invention, B component and component C all can purchase the commercial goods.
According to a kind of orange mixture dyestuff of the present invention, can adopt common dip method to dye, also can be used for direct printing.Wherein, direct printing is as dying pre-treatment with fabric, and oven dry is finalized the design, and seal dispersed dye mill base evaporates again on printing machine, vapour steaming colour fixing, washing at last, stentering forming.During with a kind of orange mixture dye printing and dyeing super-fine fiber material of the present invention,, can obtain to have the dyeing and weaving thing of premium propertiess such as beautiful in colour, stamp clear-cut, decorative pattern washing fastness are good, sun-proof, perspiration resistance through the adjustment proportion among different.
Four description of drawings
Accompanying drawing is the schema of a kind of orange mixture preparation of the present invention.
Five embodiments
Below in conjunction with specific embodiment the present invention is further described, these embodiment only are clear open the present invention, but protection scope of the present invention is not limited in this.
Embodiment 1
With the xylogen 85A of 10 gram component A, 55 gram B component, 35 gram component C, 100 grams, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.This dyestuff can provide fabric each item fastness ability good orange.
Embodiment 2
With the xylogen 83A of 15 gram component A, 45 gram B component, 40 gram component C, 100 grams, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.This dyestuff can provide fabric each item fastness ability good orange.
Embodiment 3
With the Dispersant MF of 60 gram component A, 35 gram B component, 5 gram component C, 100 grams, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.
Embodiment 4
With the xylogen 85A of 55 gram component A, 10 gram B component, 35 gram component C, 100 grams, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.
Embodiment 5
With 47.5 gram component A, 45 gram B component, 7.5 gram component C, the xylogen 85A of 50 grams, 55 gram Dispersant MFs, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.
Embodiment 6
With the Dispersant MF of 40 gram component A, 30 gram B component, 30 gram component C, 100 grams, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.
Embodiment 7
With the Dispersant MF of 36 gram component A, 44 gram B component, 20 gram component C, 110 grams, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.
Embodiment 8
With 35 gram component A, 40 gram B component, 25 gram component C, the xylogen 83A of 28 grams, 70 gram Dispersant MFs, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.
Embodiment 9
With 55 gram component A, 15 gram B component, 30 gram component C, the xylogen 83A of 60 grams, 40 gram Dispersant MFs, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.
Embodiment 10
With 38 gram component A, 42 gram B component, 20 gram component C, the xylogen 85A of 45 grams, 55 gram Dispersant MFs, after adding water and mixing, to grind with shredder and to disperse, spraying drying gets product.
Embodiment 11
Respectively get 1.0 grams and implement a kind of orange mixture that row 1-10 make and be dispersed in 500 ml waters, mix with 80 milliliters water after drawing 20 milliliters, use acetate accent dye bath PH to be 4.5-5.5; Putting into 2 gram ultra-fine fibres when being warming up to 60 ℃ respectively dyes; In 35 minutes, be warming up to 130 ℃, be incubated 30 minutes, take out when dyeing finishes to be cooled to 80 ℃ and dye appearance; Cold water cleans and reduction clearing, oven dry.Observe appearance cloth coloured light, adopt GB GB/T3920-1997, GB/T3921-1997, GB/T5718-1997 to test dyefastness respectively, the result is: fastness to rubbing is that 4-5 level, soaping fastness are 4-5 level, perspiration fastness 3.5-4 level, light fastness 5-6 level.
Embodiment 12
Earlier polyester piece good is dyed pre-treatment, remove the finish and the slurry that add in the weaving process, and carry out heat setting type; Seal dispersed dye mill base on printing machine; Control PH4-6.5, temperature 160-185 ℃ direct printing 4-15 minute is steamed fixation with High Temperature Gas, washes at last, oven dry, stentering forming.Wherein, dye paste 100 grams are formed by the sodium alginate paste modulation of above-mentioned orange mixture 6 grams, urea 1 gram, nitrobenzene sodium sulfonate 0.5 gram, SODIUM PHOSPHATE, MONOBASIC 0.5 gram, p-phenyl phenol 2 grams and 90 grams.According to its each item colour fastness excellent property of the test of method described in the embodiment 11.
Claims (3)
1. orange mixture; It is characterized in that this dyestuff is made up of following component: a kind of structural formula is component A, a kind of structural formula suc as formula the DISPERSE YELLOW 163 shown in (I) and is done B component and a kind of structural formula suc as formula the DISPERSE ORANGE 30 200 61 shown in (II) and be component C suc as formula the DISPERSE ORANGE 30 200 73 shown in (III) and mix wherein that the quality percentage composition of component A is 10-60%; The quality percentage composition of B component is 10-55%, and the quality percentage composition of component C is 5-40%;
All the other are auxiliary agent.
2. a kind of stamp according to claim 1 is deceived dispersed dye; It is characterized in that: based on described component A, B component and component C; Wherein the quality percentage composition of component A is 15-40%, and the quality percentage composition of B component is 15-45%, and the quality percentage composition of component C is 7.5-30%.
3. a kind of stamp according to claim 1 is deceived dispersed dye, it is characterized in that: described auxiliary agent comprises one of following or its mixture, sodium lignosulfonate and condensation compound of methyl naphthalene sulfonic acid and formaldehyde.
Priority Applications (1)
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CN2012100828713A CN102634233A (en) | 2012-03-27 | 2012-03-27 | Orange mix |
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CN2012100828713A CN102634233A (en) | 2012-03-27 | 2012-03-27 | Orange mix |
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CN2012100828713A Pending CN102634233A (en) | 2012-03-27 | 2012-03-27 | Orange mix |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103450708A (en) * | 2013-09-10 | 2013-12-18 | 江苏亚邦染料股份有限公司 | Environment-friendly orange disperse dye mixture |
CN103740135A (en) * | 2013-12-16 | 2014-04-23 | 浙江龙盛集团股份有限公司 | Low-temperature and environment-friendly disperse yellow dye composition |
CN107974102A (en) * | 2017-10-30 | 2018-05-01 | 安徽凯奇化工科技股份有限公司 | A kind of composite disperse orange dye |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0491386A1 (en) * | 1990-12-18 | 1992-06-24 | DyStar Japan Ltd. | Disperse dye mixture and dyeing method employing it |
JP3310470B2 (en) * | 1994-02-04 | 2002-08-05 | 日本化薬株式会社 | Red disperse dye composition and method for dyeing hydrophobic fiber material using the same |
CN101020789A (en) * | 2007-02-14 | 2007-08-22 | 浙江龙盛染料化工有限公司 | Azo disperse dye composition |
JP4278197B2 (en) * | 1998-04-20 | 2009-06-10 | ダイスタージャパン株式会社 | Disperse dye mixture |
CN101979442A (en) * | 2010-07-30 | 2011-02-23 | 江苏亚邦染料股份有限公司 | Golden yellow disperse dye for direct printing on polyester fibers |
-
2012
- 2012-03-27 CN CN2012100828713A patent/CN102634233A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0491386A1 (en) * | 1990-12-18 | 1992-06-24 | DyStar Japan Ltd. | Disperse dye mixture and dyeing method employing it |
JP3310470B2 (en) * | 1994-02-04 | 2002-08-05 | 日本化薬株式会社 | Red disperse dye composition and method for dyeing hydrophobic fiber material using the same |
JP4278197B2 (en) * | 1998-04-20 | 2009-06-10 | ダイスタージャパン株式会社 | Disperse dye mixture |
CN101020789A (en) * | 2007-02-14 | 2007-08-22 | 浙江龙盛染料化工有限公司 | Azo disperse dye composition |
CN101979442A (en) * | 2010-07-30 | 2011-02-23 | 江苏亚邦染料股份有限公司 | Golden yellow disperse dye for direct printing on polyester fibers |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103450708A (en) * | 2013-09-10 | 2013-12-18 | 江苏亚邦染料股份有限公司 | Environment-friendly orange disperse dye mixture |
CN103740135A (en) * | 2013-12-16 | 2014-04-23 | 浙江龙盛集团股份有限公司 | Low-temperature and environment-friendly disperse yellow dye composition |
CN103740135B (en) * | 2013-12-16 | 2016-05-04 | 浙江龙盛集团股份有限公司 | A kind of low-temperature environment-friendly type disperse yellow dye composition |
CN107974102A (en) * | 2017-10-30 | 2018-05-01 | 安徽凯奇化工科技股份有限公司 | A kind of composite disperse orange dye |
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Application publication date: 20120815 |