CN108218390B - For storing sth. in a cellar the material and preparation method of wine jar sealing - Google Patents
For storing sth. in a cellar the material and preparation method of wine jar sealing Download PDFInfo
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- CN108218390B CN108218390B CN201711497733.0A CN201711497733A CN108218390B CN 108218390 B CN108218390 B CN 108218390B CN 201711497733 A CN201711497733 A CN 201711497733A CN 108218390 B CN108218390 B CN 108218390B
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D51/00—Closures not otherwise provided for
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1305—Organic additives
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
- C04B35/632—Organic additives
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
- C04B35/632—Organic additives
- C04B35/636—Polysaccharides or derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/10—Materials in mouldable or extrudable form for sealing or packing joints or covers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
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- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
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Abstract
The invention discloses a kind of wine jar sealing materials, which is characterized in that the joint filling material includes material of main part, chitosan and Geniposide；The material of main part includes yellow soil, tealeaf residue powder, husk powder；Wherein by mass, based on the additive amount of chitosan quality of materials 1%-10%, the 0.1%-1% of quality of materials based on the additive amount of Geniposide, yellow soil: husk: the mass ratio of tealeaf residue is 5-10: 2-1: 1.The joint filling material of preparation of the invention has good air-tightness, antibiotic property, while also ensuring the microcirculation inside wine jar, and the time for the preservation wine that can be enhanced and flavor are suitble to commercialization and large-scale use.
Description
Technical field
The present invention relates to a kind of for storing sth. in a cellar the material and preparation method of wine jar sealing.
Background technique
Wine jar, is the container for containing wine, and the wine of the most frequently used wine jar includes white wine and yellow rice wine.It is well known that wine is old
Perfume (or spice), high-quality brewed wine must have Storage period appropriate.Brewed wine is during very long storage, the envelope altar material of wine jar altar
It is most important, play the role of to the preservation of brewed wine very important.Yellow soil is called dead loess, bitter yellow mud.The viscous weight of soil property, is ploughed
Make difficulty, corrodes seriously, topsoil is shallow.The masses describe: " one knife when dry, mess of raining." in this kind of grown on soil
Crops, fertilizer deficiency and water shortage low output.The reason of low yield: heavy in texture, structural difference, topsoil is shallow, easily drought easily flood；Effectively
Fertility is low, and permeability is poor, and nutrients release is slow；Bad tilth difficulty is ploughed and difficult rake, and soil aciditiy is higher, and available phosphorus content is low, easily
Make rice anisopliae.
Currently known includes three categories, first is that composite soil, i.e., using yellow soil or cement concrete and some additives
Altar lid is sealed after mixing, the fume generated in kiln altar, native absorption can be mixed, the time has grown cocktail party in altar and therefore reduced；Two
It is that plastics fabric width altar moves in circles again and again although can block the absorption of fume with plastic cloth, the time has grown generation plasticizing
Substance, harmful substance, and influence vinosity；Third is that wine container sealing material is made using some animal visceras, such as application No. is
201010552801 Chinese patent application discloses a kind of wine container sealing material and preparation method thereof, and this method is with animal blood
Primary raw material, fresh animal blood: water: the weight ratio of white lime is 1:1:0.005, and fermented formation wine container sealing material solves
Common plastics film seals the problems such as toxic altar, generation side effect；Application No. is 201310031376.4 Chinese patent applications to disclose
A kind of wine container sealing material and its preparation and application, pass through sorting cleaning, preservative treatment, bactericidal and air drying processing for porcine bladder
Wine container sealing material is obtained, but such methods need certain preservative treatment, and some couples of people can be more or less introduced in preservation process
The harmful ingredient of body, and there are certain peculiar smell for animal viscera, influence the mouthfeel of wine to a certain extent, and there is also productions
The disadvantages of higher cost, complex manufacturing technology, long production cycle.CN106479829A is disclosed mainly by multilayer rice-pudding leaf layer and ox
Mulberry paper layer is successively alternately formed by stacking from bottom to up；The envelope altar soil is done by a certain proportion of yellow soil, white lime, water
Straw, husk system are prepared.But the sealing method is excessively cumbersome, and is easy dry and cracked.
Common environment darkness of storing sth. in a cellar is clammy, many moulds easy to breed, therefore many common joint filling materials are when long
Between in the environment of be easy moldy metamorphism, to influence the quality of cellar.
Summary of the invention
In view of the above technical problems, the present invention provides a kind of wine jar sealing materials, which is characterized in that the joint filling material
Including material of main part, chitosan and Geniposide；The material of main part includes yellow soil, tealeaf residue powder, husk powder；Wherein press
Quality meter, the 1%-10% of quality of materials based on the additive amount of chitosan, quality of materials based on the additive amount of Geniposide
0.1%-1%, yellow soil: husk: the mass ratio of tealeaf residue is 5-10:2-1:1.
Further, the yellow soil selection clayey soil is biased to loamy texture soil, and clay is between 30~20%.
Further, the tealeaf residue powder, husk powder are the residue and common husk after common tealeaves use,
By drying and crushing to partial size 1mm or less.
Further, based on the additive amount of chitosan quality of materials 5%.
Further, based on the additive amount of Geniposide quality of materials 0.5%.
Further, yellow soil: husk: the mass ratio 8:1:1 of tealeaf residue.
Further, the partial size of chitosan is 200nm hereinafter, preferably 100nm or less.
The present invention also provides a kind of preparation methods of wine jar sealing material, characterized by the following steps:
(1) ingredient: ratio according to claim 1 weighs following raw material, yellow soil, tealeaf residue powder, husk respectively
Powder, chitosan and Geniposide；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Russian system is twin-stage classification, i.e., by physical sand (>0.01mm) and physical clay (<0.01mm)
Soil is divided into sand, loam and nine grades of clay three classes by mass fraction.The present invention is preferably loam, and clay is 30~20%
Between, because it, which has, is suitble to viscosity and voidage.
The present invention has one by the way that tealeaf residue powder, auxiliary material of the husk powder as sealing mud, the sealing mud of formation is added
Fixed high viscosity makes the wine in wine jar be difficult to volatilize away to realize stronger airtightness.It can also be formed simultaneously certain micro-
Duct makes fume form microcirculation in altar, promotes the formation of lipid.And tealeaf residue and the distinctive fragrance of husk are utilized, into
The flavor of one step improvement wine.Yellow soil: husk: the mass ratio of tealeaf residue is 5-10:2-1:1, further, yellow soil: husk:
The mass ratio 8:1:1 of tealeaf residue.The above two auxiliary material of too small addition, cannot sufficiently realize technical effect of the invention, and mistake
The above two auxiliary material of big addition causes sealing mud excessively loose frangible.Wherein, tealeaf residue powder, husk powder are common
Residue and common husk after tealeaves use, by drying and crushing to partial size 1mm or less.Excessive partial size leads to particle mistake
Slightly, it forms macropore and is unfavorable for airtightness.Husk is rice shell in invention, one layer of shell outside paddy.
Chitosan and Geniposide are as additive.The chitosan of Nano grade has stronger viscosity and bactericidal properties.As
Additive can further increase the viscosity of sealing mud, guarantee obturation effect, while chitosan has certain bactericidal properties, can be with
Prevent the moldy metamorphism of the sealing part under dark clammy environment.In order to preferably realize technical effect of the invention, examine simultaneously
Consider cost, the 1%-10% of quality of materials based on the additive amount of chitosan, further, based on the additive amount of chitosan is preferred
The 5% of body quality of materials, the partial size of further chitosan are preferably 100nm or less.Geniposide is a kind of natural biological crosslinking
Agent, with chitosan, rice husk powder etc. is used cooperatively, and can further increase airtightness, quality of materials based on the additive amount of Geniposide
0.1%-1%, further, the additive amount of Geniposide is preferably the 0.5% of material of main part quality.
Under given conditions, hydrolysis, alkylation, acylation, carboxy methylation, sulfonation, nitrification, halogen can occur for chitosan
Change, oxidation, reduction, condensation and complexing etc. chemically react, and the various chitosan derivatives with different performance are produced, to expand
The big application range of chitosan.
There are active hydroxyl and amino in chitosan macromolecular, they have stronger chemical reaction ability.In alkaline item
Hydroxyl under part on C-6 can occur to react as follows: hydroxyethylation --- chitosan is reacted with ethylene oxide, can obtain hydroxyl second
The derivative of base.Carboxy methylation --- chitosan and chloroacetate reaction just carboxymethylated derivative.Sulfonic acid esterification ---
Chitin and chitosan generates sulphonic acid ester as cellulose, with that can react with carbon disulfide after alkali process.Cyanoethylation ---
Addition reaction can occur for acrylonitrile and chitosan, generate the derivative of cyanoethylation.
Geniposide (Genipin) is product of the Gardenoside after beta-glucosidase enzyme hydrolysis, is a kind of excellent natural life
Object crosslinking agent can make biomaterial with crosslinkings such as protein, collagen, gelatin and chitosans.The preparation method one of Geniposide
As using extracting geniposide from cape jasmine, then use beta-glucosidase enzyme hydrolysis, then with ether extraction, be concentrated in vacuo, tie again
It is brilliant and be made, it can also be using microbe transformation method preparation.Geniposide content in Cortex Eucommiae and cape jasmine is higher, reaches 3-
8% or so, but since cape jasmine cultivation is easy, yield is big, the production of Geniposide is mainly using cape jasmine as raw material.It is comforted according to Jiangxi Province
Agricultural sector of state city statistics, the per mu yield of cape jasmine fresh fruit is up to very heavy, the special characteristic of acid red soil in the particularly suitable hilly country Gan Dong of cape jasmine
Soil and warm humid climate, are largely planted in Fuzhou Shi Linchuan District, Jinxi County etc. in recent years.Due to technical problem, cape jasmine at present
It is the low value-added product such as cape jasmine dry fruit and Gardenia Yellow crude product that product, which is mainly sold, and therefore, there is an urgent need to study cape jasmine
Synthetical development technology, especially Gardenia Yellow waste liquid recycling technology.
The joint filling material of preparation of the invention has good air-tightness, antibiotic property, while also ensuring inside wine jar
Microcirculation, the time for the preservation wine that can be enhanced and flavor, are suitble to commercialization and large-scale use.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained, shall fall within the protection scope of the present invention.In order to which the present invention may be better understood,
Below with reference to embodiment, the invention will be further described:
According to the formula of embodiment and comparative example, sequentially include the following steps:
(1) ingredient: following raw material, yellow soil, tealeaf residue powder, husk powder, chitosan are weighed respectively in the ratio of table 1
And Geniposide；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Embodiment 1
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 5 mass parts 100nm evaluate the chitosan and 0.5 mass parts Geniposide of partial size；The grain of tealeaf residue powder and husk powder
Diameter is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Embodiment 2
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 10 mass parts 100nm evaluate the chitosan and 0.5 mass parts Geniposide of partial size；Tealeaf residue powder and husk powder
Partial size is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Embodiment 3
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 1 mass parts 100nm evaluate the chitosan and 0.5 mass parts Geniposide of partial size；The grain of tealeaf residue powder and husk powder
Diameter is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Embodiment 4
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 5 mass parts 100nm evaluate the chitosan and 0.1 mass parts Geniposide of partial size；The grain of tealeaf residue powder and husk powder
Diameter is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Embodiment 5
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 5 mass parts 100nm evaluate the chitosan and 1 mass parts Geniposide of partial size；The partial size of tealeaf residue powder and husk powder
It is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Embodiment 6
(1) ingredient: following raw material, 73 mass parts yellow soils, 18 mass parts husk powders, 9 mass parts tealeaves are weighed respectively
Ground-slag body, 5 mass parts 100nm evaluate the chitosan and 0.5 mass parts Geniposide of partial size；The grain of tealeaf residue powder and husk powder
Diameter is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Embodiment 7
(1) ingredient: following raw material, 84 mass parts yellow soils, 8 mass parts tealeaf residue powders, 8 mass parts husks are weighed respectively
Powder, 5 mass parts 100nm evaluate the chitosan and 0.5 mass parts Geniposide of partial size；The partial size of tealeaf residue powder and husk powder
It is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Comparative example 1
(1) ingredient: following raw material, 89 mass parts yellow soils, 11 mass parts tealeaf residue powders, 5 mass parts are weighed respectively
The chitosan and 0.5 mass parts Geniposide of 100nm evaluation partial size；The partial size of husk powder is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Comparative example 2
(1) ingredient: following raw material, 89 mass parts yellow soils, 11 mass parts husk powders, 5 mass parts 100nm are weighed respectively
Evaluate the chitosan and 0.5 mass parts Geniposide of partial size；The partial size of tealeaf residue powder and husk powder is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Comparative example 3
(1) ingredient: weighing following raw material, 100 mass parts yellow soils respectively, and 5 mass parts 100nm evaluate the chitosan of partial size
With 0.5 mass parts Geniposide；The partial size of tealeaf residue powder and husk powder is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Comparative example 4
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder and 0.5 mass parts Geniposide；The partial size of tealeaf residue powder and husk powder is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder be sufficiently mixed uniformly after, etc. weight be added water after stir evenly, be added
The yellow soil that drying and grinding is crossed, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Comparative example 5
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 15 mass parts 100nm evaluate the chitosan and 0.5 mass parts Geniposide of partial size；Tealeaf residue powder and husk powder
Partial size is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Comparative example 6
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 5 mass parts 100nm evaluate the chitosan of partial size；The partial size of tealeaf residue powder and husk powder is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) it is sufficiently stirred 2-6 hours.
Comparative example 7
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 5 mass parts 100nm evaluate the chitosan and 2 mass parts Geniposides of partial size；The partial size of tealeaf residue powder and husk powder
It is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Comparative example 8
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 5 mass parts 100nm evaluate the chitosan and 0.5 mass parts Geniposide of partial size；The grain of tealeaf residue powder and husk powder
Diameter is crushed to 5mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Comparative example 9
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
Shell powder, 5 mass parts 500nm evaluate the chitosan and 0.5 mass parts Geniposide of partial size；The grain of tealeaf residue powder and husk powder
Diameter is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder, after chitosan is sufficiently mixed uniformly, etc. weight be added after water stir it is equal
It is even, the yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
Comparative example 10
(1) ingredient: following raw material, 80 mass parts yellow soils, 10 mass parts tealeaf residue powders, 10 mass parts paddy are weighed respectively
The partial size of shell powder, tealeaf residue powder and husk powder is crushed to 1mm；
(2) stir: tealeaf residue powder, husk powder after mixing, etc. weight be added water after stir evenly, be added
The yellow soil that drying and grinding is crossed, stirs into fluid state；
(3) it is sufficiently stirred 2-6 hours.
The formula of table 1 each embodiment and comparative example
Sealing mud prepared by above-described embodiment and comparative example just seals the white wine of same batch and same volume
Processing, and save store sth. in a cellar save one-year age after, volatility is calculated after taking-up.And by 10 professional tasters, to preservation
Fragrance, mouthfeel gives a mark respectively in the range of 0-10 point, calculates overall average, be calculated as flavour mark, as a result as follows.
The test result of table 2 each embodiment and comparative example
According to the experimental result of upper table it is found that comparative example 1,2 and comparative example 4,5 are it is found that the amount of chitosan is excessive,
It cannot realize better effect, cause cost excessively high instead, too small amount causes volatility excessive and influences flavor, to comparison
Ratio 9 is it is found that the partial size of chitosan needs to control otherwise to cause volatility excessive in a certain range.Comparative example 3,4 and right
The amount of ratio 6,7, Geniposide is excessive, cannot also realize better effect, causes cost excessively high instead, and too small amount causes to volatilize
Rate is excessive and influences flavor.Embodiment 6,7 and comparative example 1,2,3 compare, it is known that tealeaf residue and rice husk powder is added, can increase
Flavor and volatility is reduced, and compare comparative example 8, it is known that needed to control its partial size in a certain range, otherwise cause to wave
Hair rate is excessive.Comparative example 10,4,6 and embodiment 1 are compared, comparative example 4,6 is individually added into chitosan and Geniposide, to volatility
It reduces and flavor promotion has certain effect, but be added simultaneously in embodiment 1, synergistic effect can be played and further increase effect.
The joint filling material of preparation of the invention has good air-tightness, antibiotic property, while also ensuring inside wine jar
Microcirculation, the time for the preservation wine that can be enhanced and flavor, are suitble to commercialization and large-scale use.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (9)
1. a kind of wine jar sealing material, which is characterized in that the joint filling material includes material of main part, chitosan and Geniposide；Institute
Stating material of main part includes yellow soil, tealeaf residue powder, husk powder；Wherein by mass, material based on the additive amount of chitosan
Expect the 1%-10% of quality, the 0.1%-1% of quality of materials, yellow soil: husk powder: tealeaves based on the additive amount of Geniposide
The mass ratio of ground-slag body is 5-10: 2-1: 1.
2. wine jar sealing material according to claim 1, it is characterised in that: the yellow soil selection clayey soil is biased to earth
Matter soil, clay is between 30~20%.
3. wine jar sealing material according to claim 1, it is characterised in that: the tealeaf residue powder, husk powder are normal
Residue and common husk after the tealeaves use seen, by drying and crushing to partial size 1mm or less.
4. wine jar sealing material according to claim 1, it is characterised in that: quality of materials based on the additive amount of chitosan
5%.
5. wine jar sealing material according to claim 1, it is characterised in that: quality of materials based on the additive amount of Geniposide
0.5%.
6. wine jar sealing material according to claim 1, it is characterised in that: yellow soil: husk powder: tealeaf residue powder
Mass ratio 8: 1: 1.
7. wine jar sealing material according to claim 1, it is characterised in that: the partial size of the chitosan is 200nm or less.
8. wine jar sealing material according to claim 1, it is characterised in that: the partial size of the chitosan is 100nm or less.
9. a kind of preparation method of wine jar sealing material, characterized by the following steps:
(1) ingredient: ratio according to claim 1 weighs following raw material respectively, yellow soil, tealeaf residue powder, husk powder,
Chitosan and Geniposide；
(2) stir: tealeaf residue powder, husk powder, chitosan be sufficiently mixed uniformly after, etc. weight be added water after stir evenly,
The yellow soil that drying and grinding is crossed is added, stirs into fluid state；
(3) Geniposide is added to be sufficiently stirred 2-6 hours.
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| CN201711497733.0A CN108218390B (en) | 2017-12-29 | 2017-12-29 | For storing sth. in a cellar the material and preparation method of wine jar sealing |
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| CN108218390B true CN108218390B (en) | 2019-02-15 |
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| CN110304340A (en) * | 2019-07-05 | 2019-10-08 | 林海 | A kind of wine container sealing method |
| CN110734267A (en) * | 2019-11-19 | 2020-01-31 | 怀化市德宏酒业有限公司 | wine jar sealing material and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1600654A (en) * | 2003-09-27 | 2005-03-30 | 蒋天祥 | Technique for fabricating wine jar containing high-grade Shaoxing wine and special equipment |
| CN101671175A (en) * | 2009-09-14 | 2010-03-17 | 宜兴市昊源陶瓷厂 | Ceramic wine-bottle and preparation method thereof |
| CN102060508A (en) * | 2010-11-22 | 2011-05-18 | 南通白蒲黄酒有限公司 | Wine container sealing material and manufacture method thereof |
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2017
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1600654A (en) * | 2003-09-27 | 2005-03-30 | 蒋天祥 | Technique for fabricating wine jar containing high-grade Shaoxing wine and special equipment |
| CN101671175A (en) * | 2009-09-14 | 2010-03-17 | 宜兴市昊源陶瓷厂 | Ceramic wine-bottle and preparation method thereof |
| CN102060508A (en) * | 2010-11-22 | 2011-05-18 | 南通白蒲黄酒有限公司 | Wine container sealing material and manufacture method thereof |
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