CN108193546A - A kind of preparation method and the paper filter stick of Chinese alpine rush fiber papery cigarette filter stick - Google Patents
A kind of preparation method and the paper filter stick of Chinese alpine rush fiber papery cigarette filter stick Download PDFInfo
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- CN108193546A CN108193546A CN201810027286.0A CN201810027286A CN108193546A CN 108193546 A CN108193546 A CN 108193546A CN 201810027286 A CN201810027286 A CN 201810027286A CN 108193546 A CN108193546 A CN 108193546A
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- China
- Prior art keywords
- filter stick
- paper
- preparation
- alpine rush
- chinese alpine
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
- D21F11/00—Processes for making continuous lengths of paper, or of cardboard, or of wet web for fibre board production, on paper-making machines
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B31—MAKING ARTICLES OF PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER; WORKING PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER
- B31F—MECHANICAL WORKING OR DEFORMATION OF PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER
- B31F1/00—Mechanical deformation without removing material, e.g. in combination with laminating
- B31F1/07—Embossing, i.e. producing impressions formed by locally deep-drawing, e.g. using rolls provided with complementary profiles
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
- D21H19/34—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising cellulose or derivatives thereof
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Paper (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The present invention relates to a kind of preparation method and the paper filter stick of Chinese alpine rush fiber papery cigarette filter stick, which includes the following steps：Step（1）, paper substrate preparation；Step（2）, body paper preparation；Step（3）, paper filter stick preparation.The paper filter stick of the present invention has preferable tar reduction effect, cigarette hay perfume (or spice) and faint scent note can be assigned when cigarette is aspirated, wooden miscellaneous gas and irritation decrease, aroma quality is promoted, oral cavity comfort improves, pleasant impression is sour-sweet, while the cost for the paper filter stick that can also turn waste into wealth, reduce, and opens up the new way of Chinese alpine rush recycling.
Description
Technical field
The present invention relates to a kind of preparation method of papery cigarette filter stick, especially a kind of Chinese alpine rush fiber papery cigarette filter stick
Preparation method, further relate to the paper filter stick that this method obtains, belong to cigarette filter rod new material development field.
Background technology
Cigarette filter is the main cigarette supplementary of tobacco business, the selection of cigarette filter rod material to the suction quality of cigarette and
Lowering harm and decreasing coking has significant impact.Compared with the cellulose acetate filter rod being commonly used, paper filter stick tar reduction, cost and
There is apparent advantage, but there are flue gas is dry, irritation is big, has apparent wood when cigarette is aspirated for paper filter stick cigarette in environmental protection
Matter gas, the shortcomings of pleasant impression is bitter, it is difficult to it commonly used in cigarette.The research being modified both at home and abroad about paper filter stick at present
For report still using pure wood pulp cellulose paper or bamboo pulp fiber paper as carrier, the defects of paper filter stick, does not obtain the improvement of essence.Therefore,
Seek and develop Novel plant fiber paper to have become one of the new tool for improving paper filter stick quality.
Chinese alpine rush (Eulaliopsis binata) also known as Chinese alpine rush intend Jin Mao or sheep palpus grass, intend Jin Mao for grass family
Belong to, be grass family perennial root fibre plant for many years.Chinese alpine rush is a kind of high-quality paper making raw material, is known as " hat of group's grass ", " in grass
Treasured ", have that lignin content is low, content of cellulose is high, and the features such as fiber is elongated, matter is tough, easily slurry, easy bleaching.Chinese alpine rush
Fiber is mainly characterized by thin and grows, average fiber length 2.10mm, only 10.4 μm or so of mean fibre width, length-width ratio
202, heteroproteose cell content is 29.4%, lower 5%-8% than other grass fibers, and wall chamber ratio is 2.13, is a kind of excellent medium-length fibre
Raw material and more good paper making pulp and it is currently the only can be all instead of the herbaceous plant of trees papermaking.What Chinese alpine rush was made
Paper, paper is uniform, fine and smooth, and elasticity is good, and pulling force is strong.At present, Chinese alpine rush is mainly used to produce cultural paper, high-grade paper etc..
In recent years, domestic scholars open the new way that Chinese alpine rush utilizes in production of cigarettes field.CN104273648A is public
A kind of cigarette filter using Chinese alpine rush has been opened, broken dragon grass particle is made an addition into segmented after flavoring is handled
In the cavity of composite filter tip, which assigns cigarette abundant fragrance while reducing tar and reducing harm, but cavity composite filter tip plus
Work difficulty is larger, quality stability is difficult to control.CN102488316A discloses a kind of cigarette for improving reconstituted tobacoo aesthetic quality
With additive and preparation method and application, dragon straw pulp replacement wood pulp is prepared into reconstituted tobacoo, although it, which has, reduces cigarette
Careless thin slice irritation reduces wooden miscellaneous gas so that this perfume (or spice) of tobacco is able to the effect promoted, but the Chinese alpine rush reconstituted tobacoo of the invention
Other miscellaneous gas can be introduced in burning.CN101665992A discloses a kind of plant tow filter fiber and preparation method thereof,
It is fibre bundle that a variety of slurry Solid contents such as Chinese alpine rush are sprayed wire drawing through pressure after solving thin, boiling, grinding, by bundles of filament
Tobacco smoke filter element fiber stick is made in beam, and the plant tow filter fiber manufacture craft of the invention is more complicated, and does not have flavoring in technique
Process section makes it be difficult to apply in cigarette, and cost is higher compared with traditionally on paper filter stick.
Particularity based on Chinese alpine rush, the present invention attempt to explore the production technology of the paper filter stick based on Chinese alpine rush, at present
Have no the open report identical with the present invention.
Invention content
To solve the above-mentioned problems, the purpose of the present invention is to provide the preparation sides of Chinese alpine rush fiber papery cigarette filter stick
Dragon grass fiber is individually manufactured paper with pulp into paper filter stick body paper paper substrate by method, and paper substrate is made after fragrant bamboo and the coating of green plum extracting solution, drying
Paper filter stick body paper is obtained, body paper rolls into Chinese alpine rush paper filter stick through conventional molding processes.Common paper filter stick can be improved to inhale
The defects of taste is poor, organoleptic quality are preferable.
The purpose of the present invention is achieved through the following technical solutions：
A kind of preparation method of Chinese alpine rush fiber papery cigarette filter stick, it is characterised in that：It is made by the steps：
Step（1）, paper substrate preparation：Commercially available Chinese alpine rush true qualities pulpboard is taken to carry out hydraulic pulping, discongest after carried out with disc mill
Defibrination process, refining concentration are mass fraction 6-11%, and beating interstice is 0.1-0.3 mm, and beating degree is controlled in 30-45 oSR,
Obtained paper filter stick is former after carrying out handsheet, squeezing, drying, winding, cutting by wet papermaking process after the conventional paper making additive of addition
Paper paper substrate；
Step（2）, body paper preparation：Fresh fragrant bamboo bamboo chip and green plum are taken according to mass ratio 3:7-7:After 3 mixing are broken with water into
Row circumfluence distillation obtains extracting solution, and solid-liquid ratio during extraction is 1:25-1:40, Extracting temperature is 60-80 DEG C, time 1.5-
3h is concentrated under reduced pressure after extracting solution is filtered, and obtains concentrate, then adds in and is carried out with 95% isometric ethyl alcohol of concentrate
Alcohol precipitation takes supernatant liquor as coating fluid after centrifugation；By coating solution in step（1）On the paper substrate of preparation after drying to get
To body paper；
Step（3）, paper filter stick preparation：Using paper filter stick conventional molding processes, by step（2）Body paper through press U-shaped line,
Paper filter stick is rolled into after molding, controls hardness >=82% of paper filter stick, resistance to suction is 27Pa≤every millimeter of filter stick≤35Pa.
The Chinese alpine rush paper filter stick of the present invention has hay note when being not added with any extracting solution, reduces wooden miscellaneous gas etc.,
But other defect is had on aesthetic quality, after being coated with fragrant bamboo and plum extracting solution, the irritation of flue gas can be reduced, improve mouth
The comfort of chamber, while increase the sour-sweet sense of faint scent note and pleasant impression.Fragrant bamboo and green plum extracting solution are effectively increased as material perfume (or spice)
Integrated sensory's mass of Chinese alpine rush fiber paper filter stick as cigarette filter rod so that it can use, while fine with traditional wood pulp
Dimension paper filter stick is compared, also better tar reduction effect.
Further, step（2）In, it carries out being concentrated under reduced pressure into the 1/4 of original volume after filtering.
Further, step（2）In, additive amount of the coating fluid on paper substrate is 0.5%-2%.
The Chinese alpine rush fiber papery cigarette filter stick that above-mentioned preparation method of the present invention obtains.
Compared with prior art, the advantage of the invention is that：
Cigarette hay perfume (or spice) and faint scent note can be assigned when cigarette is aspirated, wooden miscellaneous gas and irritation decrease, aroma quality
It being promoted, oral cavity comfort improves, and pleasant impression is sour-sweet, compared with traditional wood pulp cellulose paper filter stick, also better tar reduction
Effect.Can also turn waste into wealth, reduce simultaneously the cost of paper filter stick, open up the new way of Chinese alpine rush recycling.
Specific embodiment
The present invention is clearly and completely described with reference to the technical solution in embodiment, it is clear that described reality
It is only part of the embodiment of the present invention to apply example, instead of all the embodiments.Those skilled in the art are not paying creation
Property labour under the premise of all other embodiments obtained, shall fall within the protection scope of the present invention.
Embodiment 1
The preparation method of the Chinese alpine rush fiber papery cigarette filter stick of the present embodiment, is made by the steps：
Step（1）, paper substrate preparation：Commercially available Chinese alpine rush true qualities pulpboard is taken to carry out hydraulic pulping, discongest after carried out with disc mill
Defibrination process, refining concentration are mass fraction 6%, and beating interstice is 0.2 mm, and beating degree is 30 oSR, adds conventional papermaking and helps
Paper filter stick body paper paper substrate is made after carrying out handsheet, squeezing, drying, winding, cutting by wet papermaking process after agent；
Step（2）, body paper preparation：Fresh fragrant bamboo bamboo chip and green plum are taken according to mass ratio 3:After 7 mixing are broken heat is carried out with water
Refluxing extraction obtains extracting solution, solid-liquid ratio during extraction（w/v）It is 1:25, Extracting temperature be 65 DEG C, time 3h, by extracting solution into
Row is concentrated under reduced pressure into the 1/4 of original volume, obtains concentrate, then adds in and carries out alcohol precipitation with 95% isometric ethyl alcohol of concentrate,
Supernatant liquor is taken after centrifugation as coating fluid, by coating solution in step（1）Paper substrate on after drying to get to body paper,
Additive amount of the middle coating fluid on paper substrate is 0.5%；
Step（3）, paper filter stick preparation：Using paper filter stick conventional molding processes, by step（2）Body paper through press U-shaped line,
Paper filter stick is rolled into after molding, the hardness of paper filter stick is 83%, and the resistance to suction of 120mm paper filter sticks rolled is 3261 Pa.
Embodiment 2
The preparation method of the Chinese alpine rush fiber papery cigarette filter stick of the present embodiment, is made by the steps：
Step（1）, paper substrate preparation：Commercially available Chinese alpine rush true qualities pulpboard is taken to carry out hydraulic pulping, discongest after carried out with disc mill
Defibrination process, refining concentration are mass fraction 11%, and beating interstice 0.1mm, beating degree control is 45 oSR, and addition is conventional to make
Paper filter stick body paper paper substrate is made after carrying out handsheet, squeezing, drying, winding, cutting by wet papermaking process after paper auxiliary agent；
Step（2）, body paper preparation：Fresh fragrant bamboo bamboo chip and green plum are taken according to mass ratio 7:After 3 mixing are broken heat is carried out with water
Refluxing extraction obtains extracting solution, solid-liquid ratio during extraction（w/v）It is 1:40, Extracting temperature is 80 DEG C, and the time is 2 h, by extracting solution
It carries out being concentrated under reduced pressure into the 1/4 of original volume, obtains concentrate, then add in and carry out alcohol with 95% isometric ethyl alcohol of concentrate
It is heavy, supernatant liquor is taken after centrifugation as coating fluid, by coating solution in step（1）It is dried after on the paper substrate of preparation, wherein, it applies
Additive amount of the cloth liquid on paper substrate is 2%；
Step（3）, paper filter stick preparation：Using paper filter stick conventional molding processes, body paper rolls after pressing U-shaped line, molding
Into paper filter stick, the hardness of paper filter stick is 88%, and the resistance to suction of 120mm paper filter sticks rolled is 4161 Pa.
Embodiment 3
The preparation method of the Chinese alpine rush fiber papery cigarette filter stick of the present embodiment, is made by the steps：
Step（1）, paper substrate preparation：Commercially available Chinese alpine rush true qualities pulpboard is taken to carry out hydraulic pulping, discongest after carried out with disc mill
Defibrination process, refining concentration are mass fraction 9%, and beating interstice is 0.3 mm, and beating degree is 35 oSR, adds conventional papermaking and helps
Paper filter stick body paper paper substrate is made after carrying out handsheet, squeezing, drying, winding, cutting by wet papermaking process after agent；
Step（2）, body paper preparation：Fresh fragrant bamboo bamboo chip and green plum are taken according to mass ratio 6:After 4 mixing are broken heat is carried out with water
Refluxing extraction obtains extracting solution, solid-liquid ratio during extraction（w/v）It is 1:30, Extracting temperature is 60 DEG C, time 1.5h, by extracting solution
It carries out being concentrated under reduced pressure into the 1/4 of original volume, obtains concentrate, then add in and carry out alcohol with 95% isometric ethyl alcohol of concentrate
It is heavy, supernatant liquor is taken after centrifugation as coating fluid, by coating solution in step（1）Paper substrate on after dry, wherein, coating fluid
Additive amount on paper substrate is 1%；
Step（3）, paper filter stick preparation：Using paper filter stick conventional molding processes, body paper rolls after pressing U-shaped line, molding
Into paper filter stick, the hardness of paper filter stick is 86%, and the resistance to suction of 120mm paper filter sticks rolled is 3853 Pa.
By Chinese alpine rush paper filter stick prepared by embodiment 1-3 respectively with vinegar fibre filter stick equal length it is compound after prepare composite filter and sample
Product cigarette, respectively using the identical wood pulp cellulose paper filter stick of resistance to suction as control, to Chinese alpine rush papery composite filter and wood pulp cellulose
Papery composite filter cigarette sample respectively according to《Cigarette conventional analysis measures total granules and tar with smoking machine》（GB/T
19609-2004）Standard method carries out the measure of tarry matters in smoke, and carries out aesthetic quality comparative evaluation to cigarette sample, as a result such as
Shown in table 1-2：
1 cigarette sample tarry matters in smoke amount testing result of table
From the point of view of the testing result of the cigarette sample tarry matters in smoke amount of table 1, compared with wood pulp cellulose paper filter stick, identical resistance to suction
Chinese alpine rush paper filter stick has better tar reduction effect.
2 cigarette sample aesthetic quality's comparative evaluation's result of table
From the point of view of the sensory quality assessment result of table 2, in all three groups of cigarette samples, using Chinese alpine rush paper filter stick cigarette sample
The aesthetic quality of product is above the cigarette sample using wood pulp cellulose paper filter stick, compared with wood pulp cellulose paper filter stick, dragon
Cigarette hay perfume (or spice) and faint scent note can be assigned during careless paper filter stick suction, wooden miscellaneous gas and irritation decrease, aroma quality
It is promoted, oral cavity comfort improves, and pleasant impression is sour-sweet.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (4)
1. a kind of preparation method of Chinese alpine rush fiber papery cigarette filter stick, it is characterised in that：It is made by the steps：
Step（1）, paper substrate preparation：Commercially available Chinese alpine rush true qualities pulpboard is taken to carry out hydraulic pulping, discongest after carried out with disc mill
Defibrination process, refining concentration are mass fraction 6-11%, beating interstice 0.1-0.3mm, and beating degree control adds in 30-45oSR
Add and paper filter stick body paper is made after carrying out handsheet, squeezing, drying, winding, cutting by wet papermaking process after conventional paper making additive
Paper substrate；
Step（2）, body paper preparation：Fresh fragrant bamboo bamboo chip and green plum are taken according to mass ratio 3:7-7:After 3 mixing are broken with water into
Row circumfluence distillation obtains extracting solution, and solid-liquid ratio during extraction is 1:25-1:40, Extracting temperature is 60-80 DEG C, time 1.5-
3h carries out being concentrated under reduced pressure to give concentrate after extracting solution is filtered, and then adds in and carries out alcohol with 95% isometric ethyl alcohol of concentrate
It is heavy, supernatant liquor is taken after centrifugation as coating fluid；By coating solution in step（1）On the paper substrate of preparation after drying to get to
Body paper；
Step（3）, paper filter stick preparation：Using paper filter stick conventional molding processes, by step（2）Body paper through press U-shaped line,
Paper filter stick is rolled into after molding, controls hardness >=82% of paper filter stick, resistance to suction is 27Pa≤every millimeter of filter stick≤35Pa.
2. the preparation method of Chinese alpine rush fiber papery cigarette filter stick according to claim 1, it is characterised in that：Step（2）
In, it carries out being concentrated under reduced pressure into the 1/4 of original volume after filtering.
3. the preparation method of Chinese alpine rush fiber papery cigarette filter stick according to claim 1, it is characterised in that：Step（2）
In, additive amount of the coating fluid on paper substrate is 0.5%-2%.
4. the Chinese alpine rush fiber papery cigarette filter stick obtained using the preparation method described in one of claim 1-3.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810027286.0A CN108193546B (en) | 2018-01-11 | 2018-01-11 | Preparation method of Chinese alpine rush fiber cigarette paper filter stick and paper filter stick |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810027286.0A CN108193546B (en) | 2018-01-11 | 2018-01-11 | Preparation method of Chinese alpine rush fiber cigarette paper filter stick and paper filter stick |
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| Publication Number | Publication Date |
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| CN108193546A true CN108193546A (en) | 2018-06-22 |
| CN108193546B CN108193546B (en) | 2021-05-25 |
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| CN201810027286.0A Active CN108193546B (en) | 2018-01-11 | 2018-01-11 | Preparation method of Chinese alpine rush fiber cigarette paper filter stick and paper filter stick |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101665992A (en) * | 2009-09-18 | 2010-03-10 | 汕头市中烟包装有限公司 | Plant tow filter fiber and preparation method thereof |
| CN102488316A (en) * | 2011-12-08 | 2012-06-13 | 上海烟草集团有限责任公司 | Tobacco additive for improving sensory quality of tobacco sheet and preparation method as well as application thereof |
| CN102987558A (en) * | 2012-11-28 | 2013-03-27 | 红塔烟草(集团)有限责任公司 | Cigarette paper filter material containing fructus momordicae extract |
| CN104172472A (en) * | 2014-07-31 | 2014-12-03 | 云南中烟工业有限责任公司 | Paper filter stick of bagasse fiber cigarette |
-
2018
- 2018-01-11 CN CN201810027286.0A patent/CN108193546B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101665992A (en) * | 2009-09-18 | 2010-03-10 | 汕头市中烟包装有限公司 | Plant tow filter fiber and preparation method thereof |
| CN102488316A (en) * | 2011-12-08 | 2012-06-13 | 上海烟草集团有限责任公司 | Tobacco additive for improving sensory quality of tobacco sheet and preparation method as well as application thereof |
| CN102987558A (en) * | 2012-11-28 | 2013-03-27 | 红塔烟草(集团)有限责任公司 | Cigarette paper filter material containing fructus momordicae extract |
| CN104172472A (en) * | 2014-07-31 | 2014-12-03 | 云南中烟工业有限责任公司 | Paper filter stick of bagasse fiber cigarette |
Non-Patent Citations (1)
| Title |
|---|
| 贺玮静等: ""用100%龙须草生产卷烟纸"", 《天津造纸》 * |
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