CN108192779A - A kind of skin care scented soap and preparation method thereof - Google Patents
A kind of skin care scented soap and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
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Abstract
The invention belongs to skin care industries, and in particular to a kind of skin care scented soap and preparation method thereof.The present invention extracts active material from nostoc, predominantly polysaccharose substance, contain a large amount of protein, amino acid, vitamin etc., skin can be met normally to be metabolized, wherein a large amount of amino acid substance can play skin water retention, the rear tight, drying of alleviation, and vitamins ingredient can play uvioresistant, sun-proof effect.The present invention, which solves the perfumed soap majority with certain bactericidal effect currently on the market, can add strong alkaline substance, can generally larger stimulation be generated to skin, and peculiar smell is larger, can give people a kind of dry and astringent, tight feeling after use, long-time service can make skin become the problem of dry rough.
Description
Technical field
The invention belongs to skin care industries, and in particular to a kind of skin care scented soap and preparation method thereof.
Background technology
Perfumed soap is a kind of traditional articles for washing that each family generally uses, generally solid block product.Perfumed soap
Using object be different from laundry soap, it is to be directed to human skin, such as washes one's hands, washes one's face and has a bath.In recent years, as people give birth to
The flat raising of running water, not requiring nothing more than it has the function of clean skin, and to have the function of skin care, beauty and sterilization etc., and perfumed soap is
Through the necessary article for becoming people's daily life.
With the continuous improvement of people's living standards, product category is on the increase, and progressively towards environmentally protective, function
Change, specialized and seriation direction are developed, and modern product is incorporated for different consumer demands on the basis of traditional perfumed soap
Some additional functions, such as antibacterial, submissive, moisturizing, anti-acne, skin toner, whitening and lasting lasting, consumer obtain when in use
The multiple experience such as clean skin, comfortable, salubrious meets the rhythm of life of modern.Therefore, such product is constantly by the warm of consumer
Inner feelings becomes the first choice that family's perfumed soap class washes shield product.At present, skin-protection type perfumed soap and health care/disinfection sterilizing type perfumed soap are still leading
The trend in China perfumed soap market, it is certainly exquisite pack, the composite fragrant of beautiful soap type, high quality and top grade is still excellent
The necessary requirement of matter perfumed soap, but consumer notices some other additional functions of perfumed soap more and more, such as refreshes oneself, goes fatigue
Body cleaning and health soap, old man's soap promoting blood circulation and removing obstruction in channels, preventing chapped skin with nourishes rough skin, the perfumed soap with preserving moisture and protecting skin type and
Cooling type toilet soap.With the influence of green consumption trend, perfumed soap kind increasingly tends to superior, from human body and environment dual safety
From the point of view of property, people can increasingly tend to use Natural toilet soap.The trend of perfumed soap product is to top grade, functionally develops.
" safe and healthy, economic, efficient, environmentally friendly, benefit " is the development trend in perfumed soap future.
Current perfumed soap is mainly using sodium soap and other surfaces activating agent as primary raw material, addition activating agent, anti-corrosion
Manufactured product after the machine-shapings such as agent, foaming agent, fluorescer.Existing perfumed soap generally existing sterilizing ability in use is not strong
The shortcomings that, the perfumed soap majority with certain bactericidal effect can add strong alkaline substance currently on the market, and generally skin can be generated
Larger stimulation, and peculiar smell is larger, and a kind of dry and astringent, tight feeling of people can be also given after use, long-time service can make skin become dry
It is dry rough.Therefore, produce after a kind of use has the very big market demand to skin-friendly and the strong perfumed soap of sterilizing ability.
Invention content
The technical problems to be solved by the invention：For current perfumed soap generally existing sterilizing ability it is not strong the shortcomings that, at present
The perfumed soap majority with certain bactericidal effect can add strong alkaline substance in the market, and larger stimulation can be generally generated to skin, and
Peculiar smell is larger, can give people a kind of dry and astringent, tight feeling after use, and long-time service can make skin become the problem of dry rough,
A kind of skin care scented soap and preparation method thereof is provided.
In order to solve the above technical problems, the present invention is using technical solution as described below：
A kind of skin care scented soap, which is characterized in that according to the mass fraction, including 3 ~ 5 parts of moisturizer, 8 ~ 10 parts of skin care scented soap soap agents,
15 ~ 20 parts of grease additives, 8 ~ 12 parts of skin antioxidants.
The moisturizer is that nostoc is taken to crushed 50 mesh sieve, collects sieving particle A, and sieving particle A is taken to be placed in anhydrous second
15 ~ 20min of decoloration is impregnated in alcohol, filtering takes filter residue in mass ratio 1：90 add in water, and 6 ~ 7h is extracted in 90 ~ 95 DEG C, and filtering takes
Filtrate, rotary evaporation, concentration in being freeze-dried 12 ~ 15h, obtain moisturizer.
The preparation method of the skin care scented soap soap agent is：
（1）Chinese yam is taken to crush to sieve with 100 mesh sieve, collects sieving particle B in mass ratio 2：9 add in deionized waters, in 55 ~ 60 DEG C,
Supernatant A is collected in 150r/min 4 ~ 5h of mechanical shaking extraction, centrifugation, pH to 4.8 ~ 5.0 is adjusted, by supernatant A in mass ratio 10：1：1
Cellobiose enzyme and zytase are added in, in 45 ~ 48 DEG C, 180r/min 4 ~ 5h of saccharification, pH to 7 ~ 7.2 is adjusted, obtains saccharified liquid；
（2）Picking Lactobacillus casei, Lactobacillus kefir are seeded to respectively in MRS fluid nutrient mediums, 25 ~ 28 DEG C of activation trainings
2 ~ 3d is supported, obtains Lactobacillus casei activation culture liquid and Lactobacillus kefir activation culture liquid, according to the mass fraction, take 40 ~
50 parts of saccharified liquids, 100 ~ 150 parts of fermentation mediums, 1 ~ 2 part of Lactobacillus casei activation culture liquid, 0.5 ~ 0.7 part of kefir
Lactobacillus activation culture liquid, 1 ~ 2 part of CaCO3Mixing, in 38 ~ 42 DEG C, 130r/min 6 ~ 7d of fermentation obtain zymotic fluid, centrifuge, take
Clear liquid B obtains skin-protection soap soap agent.
The formula of the fermentation medium is：According to the mass fraction, 0.5 ~ 0.8 part of MgSO is taken4·7H2O, 0.5 ~ 0.7 part
KH2PO3, 0.1 ~ 0.2 part of NaCl, 5 ~ 10 parts of yeast extracts, 30 ~ 40 portions of skimmed milk powers, 1000 parts of water, 115 DEG C of sterilizing 20min.
The grease additive is that the hard English walnut seeds of Bai Er is taken to peel off shell to take benevolence, grinds, crosses 80 mesh sieve, collect
Be sieved particle C, and in mass ratio 1：10 add in petroleum ether mixing, extract 1 ~ 1.5h in 75 ~ 85 DEG C, repeat extraction 2 ~ 3 times, merge extraction
Liquid is taken, extraction slag is spare, takes extract liquor rotary evaporation, adds the anhydrous sodium sulfate of sieving particle C mass 25 ~ 30%, stands 12
~ 15h, centrifugation, takes supernatant B, as grease additive.
The skin antioxidant is to take spare extraction slag rotary evaporation, and slag in mass ratio 1 is extracted after taking rotary evaporation：
It is mixed in 3 addition hexanes, mixed solution is obtained, in 50 ~ 55 DEG C, into mixed solution in mass ratio 1：10, which add in mass fractions, is
60% methanol solution extracts 5 ~ 6h, takes extracting solution rotary evaporation, dry, obtains skin antioxidant.
The preparation method is to take grease additive in mass ratio 1：6 ~ 8 add in sodium hydroxide, and 1 ~ 2h of saponification obtains saponification
Reactant takes saponification object, the mixing of skin care scented soap soap agent, the water of skin care scented soap soap agent 80 ~ 90% is added, in 60 ~ 75 DEG C
It is stirred, obtains mixture, take mixture in mass ratio 5：2 add in skin care scented soap additive, after being warming up to 75 ~ 80 DEG C, mixing
20 ~ 30 min, molding, after cooling, by mold be placed in -20 DEG C freezing 18 ~ for 24 hours, thaw, obtain skin care scented soap.
The skin care scented soap additive be according to the mass fraction, take 2 ~ 3 parts of lauryl sodium sulfate, 1 ~ 2 part of titanium dioxide,
20 ~ 30 parts of mass fractions are 70% white sugar aqueous solution, 5 ~ 7 parts of glycerine, 0.8 ~ 1.2 part of cream jasmin france, 20 ~ 30 parts of absolute ethyl alcohols
Mixing to get.
Compared with other methods, advantageous effects are the present invention：
（1）The present invention extracts active material, predominantly polysaccharose substance from nostoc, containing a large amount of protein, amino acid,
Vitamin etc. can meet skin and normally be metabolized, wherein a large amount of amino acid substance can play skin water retention, alleviate and use
It is tight afterwards, dry, and vitamins ingredient can play uvioresistant, sun-proof effect；
（2）The present invention extracts a kind of saponin from Chinese yam, is a kind of natural nonionic surface active agent, has the table for reducing water
The ability of face tension, and with good dirt-removing power and foaming characteristic and harmless to the human body, and by adding lactobacillus-fermented,
Carbohydrate fermentation generates lactic acid in saponin, obtains the compound of saponin and lactic acid, has both two kinds of functions, a variety of work in newborn acid
Property enzyme can increase skin activity, accelerate cell division, enhance skin oxidation resistance, and more effectively can strengthen absorbing and increase
The moisture and nutrient of strong skin cell, the whitening cell activity of quick activating skin and the old skin cell of precipitation that faster subsides
Interior melanocyte, reaches skin effect, on the other hand neutralizes a part of alkaline matter in saponin, using will not be dry and astringent, tight
It is taut, there is certain moisture-keeping efficacy；
（3）The present invention extracts grease from the hard English walnut seeds of Bai Er, then extracts polyphenoils with oil meal, contains in the grease of extraction
The activity of aliphatic acid, squalene, Flavonoid substances, wherein squalene and superoxide dismutase in human body, the enhancing of immunity
Related, also with different physiological roles such as antibiosis rationality agings, the grease of extraction is and non-also rich in multivitamin and minerals
Chang Rongyi is absorbed by the skin, and salubrious non-greasy has splendid moistening effect, moisturize the skin while, also inside skin and
Subcutaneous fat combines, and forms deep layer water lock oil film, and Flavonoid substances therein have effects that antibacterial bacteriostatic；It on the other hand will extraction
Grease is added to as auxiliary material in perfumed soap manufacturing process, can play solvent action, dissolves skin surface grease, also functions to friction effect
Fruit is formed simultaneously hydrophobic film, plays protection skin, and can prevent external harmful substance invasion；
（4）Antioxidant in the present invention extraction hard English walnut seed oil meals of Bai Er, predominantly polyphenolic substance, on the one hand can
A variety of free radicals are effectively removed, on the other hand the fat of addition and grease can be protected not oxidized as natural, subtracted
The formation of few nitrous oxide extends the delivery date of perfumed soap, and the present invention makees surfactant by preparing skin care scented soap soap agent, promotes
It preferably being emulsified in skin care scented soap manufacturing process, another addition extraction grease plays solvent action, active ingredient is made preferably to dissolve,
Skin surface grease can also be dissolved, reaches cleaning action, addition moisturizer increases skin water conservation sense, increases antioxidant, leads to
Water-In-Oil structure is crossed, protection active ingredient is not oxidized.
Specific embodiment
Skimmed milk powder：It is purchased from Australian De Yun companies.
Fermentation medium：According to the mass fraction, 0.5 ~ 0.8 part of MgSO is taken4·7H2O, 0.5 ~ 0.7 part of KH2PO3, 0.1 ~ 0.2
Part NaCl, 5 ~ 10 parts of yeast extracts, 30 ~ 40 portions of skimmed milk powers, 1000 parts of water, 115 DEG C of sterilizing 20min.
Lactobacillus casei, Lactobacillus kefir：Inclined-plane is stored refrigerated.
Moisturizer：Nostoc is taken to crushed 50 mesh sieve, collects sieving particle A, sieving particle A is taken to be placed in absolute ethyl alcohol and is soaked
Bubble 15 ~ 20min of decoloration, filtering take filter residue in mass ratio 1：90 add in water, and 6 ~ 7h is extracted in 90 ~ 95 DEG C, and filtering takes filtrate to revolve
Turn evaporation, concentration is freeze-dried 12 ~ 15h, obtains moisturizer.
Skin care scented soap soap agent：（1）Chinese yam is taken to crush to sieve with 100 mesh sieve, collects sieving particle B in mass ratio 2：9 add in go from
Sub- water, in 55 ~ 60 DEG C, 150r/min 4 ~ 5h of mechanical shaking extraction, supernatant A is collected in centrifugation, adjusts pH to 4.8 ~ 5.0, supernatant A
In mass ratio 10：1：1 adds in cellobiose enzyme and zytase, in 45 ~ 48 DEG C, 180r/min 4 ~ 5h of saccharification, adjusts pH to 7
~ 7.2, obtain saccharified liquid；
（2）Picking Lactobacillus casei, Lactobacillus kefir are seeded to respectively in MRS fluid nutrient mediums, 25 ~ 28 DEG C of activation trainings
2 ~ 3d is supported, obtains Lactobacillus casei activation culture liquid and Lactobacillus kefir activation culture liquid, according to the mass fraction, take 40 ~
50 parts of saccharified liquids, 100 ~ 150 parts of fermentation mediums, 1 ~ 2 part of Lactobacillus casei activation culture liquid, 0.5 ~ 0.7 part of kefir
Lactobacillus activation culture liquid, 1 ~ 2 part of CaCO3Mixing, in 38 ~ 42 DEG C, 130r/min 6 ~ 7d of fermentation obtain zymotic fluid, centrifuge, take
Clear liquid B obtains skin-protection soap soap agent.
Grease additive：The hard English walnut seeds of Bai Er are taken, shell is peeled off and takes benevolence, grind, 80 mesh sieve is crossed, collects sieving
Particle C, in mass ratio 1：10 add in petroleum ether mixing, are placed in soxhlet's extractor, and 1 ~ 1.5h is extracted in 75 ~ 85 DEG C, repeat to extract
It takes 2 ~ 3 times, combining extraction liquid, extraction slag is spare, takes extract liquor rotary evaporation, adds the nothing of sieving particle C mass 25 ~ 30%
Aqueous sodium persulfate, stands 12 ~ 15h, and centrifugation takes supernatant B, as grease additive.
Skin antioxidant：Take extraction slag rotary evaporation spare in grease additive, take after rotary evaporation extraction slag by
Mass ratio 1：It is mixed in 3 addition hexanes, mixed solution is obtained, in 50 ~ 55 DEG C, into mixed solution in mass ratio 1：10 add in quality
Score is 60% methanol solution, extracts 5 ~ 6h, takes extracting solution rotary evaporation, dry, obtains skin antioxidant.
A kind of preparation method of skin care scented soap takes grease additive in mass ratio 1：6 ~ 8 add in sodium hydroxide, saponification
1 ~ 2h obtains saponification object, takes saponification object, the mixing of skin care scented soap soap agent, adds the water of skin care scented soap soap agent 80 ~ 90%,
It is stirred in 60 ~ 75 DEG C, obtains mixture, take mixture in mass ratio 5：2 add in skin care scented soap additive, are warming up to 75 ~ 80
After DEG C, 20 ~ 30min of mixing, molding, after cooling, by mold be placed in -20 DEG C freezing 18 ~ for 24 hours, thaw, obtain skin care scented soap.
Embodiment 1
Skimmed milk powder：It is purchased from Australian De Yun companies.
Fermentation medium：According to the mass fraction, 0.5 part of MgSO is taken4·7H2O, 0.5 part of KH2PO3, 0.1 part of NaCl, 5 parts of ferment
Female cream, 30 portions of skimmed milk powers, 1000 parts of water, 115 DEG C of sterilizing 20min.
Lactobacillus casei, Lactobacillus kefir：Inclined-plane is stored refrigerated.
Moisturizer：Nostoc is taken to crushed 50 mesh sieve, collects sieving particle A, sieving particle A is taken to be placed in absolute ethyl alcohol and is soaked
Bubble decoloration 15min, filtering take filter residue in mass ratio 1：90 add in water, and 6h is extracted in 90 DEG C, and filtering takes filtrate rotary evaporation, dense
Contracting is freeze-dried 12h, obtains moisturizer.
Skin care scented soap soap agent：（1）Chinese yam is taken to crush to sieve with 100 mesh sieve, collects sieving particle B in mass ratio 2：9 add in go from
Sub- water, in 55 DEG C, 150r/min mechanical shaking extraction 4h, supernatant A is collected in centrifugation, adjusts pH to 4.8, supernatant A is in mass ratio
10：1：1 adds in cellobiose enzyme and zytase, in 45 DEG C, 180r/min saccharification 4h, adjusts pH to 7, obtains saccharified liquid；
（2）Picking Lactobacillus casei, Lactobacillus kefir are seeded to respectively in MRS fluid nutrient mediums, 25 DEG C of activation cultures
2d obtains Lactobacillus casei activation culture liquid and Lactobacillus kefir activation culture liquid, according to the mass fraction, takes 40 parts of saccharification
Liquid, 100 parts of fermentation mediums, 1 part of Lactobacillus casei activation culture liquid, 0.5 part of Lactobacillus kefir activation culture liquid, 1
Part CaCO3Mixing, in 38 DEG C, 130r/min fermentation 6d obtain zymotic fluid, centrifuge, take supernatant B, obtain skin-protection soap soap agent.
Grease additive：The hard English walnut seeds of Bai Er are taken, shell is peeled off and takes benevolence, grind, 80 mesh sieve is crossed, collects sieving
Particle C, in mass ratio 1：10 add in petroleum ether mixing, are placed in soxhlet's extractor, extract 1h in 75 DEG C, repeat extraction 2 times, close
And extract liquor, extraction slag is spare, takes extract liquor rotary evaporation, adds the anhydrous sodium sulfate of sieving particle C mass 25%, stands
12h, centrifugation, takes supernatant B, as grease additive.
Skin antioxidant：Take extraction slag rotary evaporation spare in grease additive, take after rotary evaporation extraction slag by
Mass ratio 1：It is mixed in 3 addition hexanes, mixed solution is obtained, in 50 DEG C, into mixed solution in mass ratio 1：10 add in quality point
Number is 60% methanol solution, extracts 5h, takes extracting solution rotary evaporation, dry, obtains skin antioxidant.
A kind of preparation method of skin care scented soap takes grease additive in mass ratio 1：6 add in sodium hydroxide, saponification
1h obtains saponification object, takes saponification object, the mixing of skin care scented soap soap agent, the water of skin care scented soap soap agent 80% is added, in 60
It DEG C is stirred, obtains mixture, take mixture in mass ratio 5：2 add in skin care scented soap additive, after being warming up to 75 DEG C, mixing
Mold after cooling, is placed in -20 DEG C of freezing 18h, thaws, obtain skin care scented soap by 20min, molding.
Embodiment 2
Skimmed milk powder：It is purchased from Australian De Yun companies.
Fermentation medium：According to the mass fraction, 0.8 part of MgSO is taken4·7H2O, 0.7 part of KH2PO3, 0.2 part of NaCl, 10 parts
Yeast extract, 40 portions of skimmed milk powers, 1000 parts of water, 115 DEG C of sterilizing 20min.
Lactobacillus casei, Lactobacillus kefir：Inclined-plane is stored refrigerated.
Moisturizer：Nostoc is taken to crushed 50 mesh sieve, collects sieving particle A, sieving particle A is taken to be placed in absolute ethyl alcohol and is soaked
Bubble decoloration 20min, filtering take filter residue in mass ratio 1：90 add in water, and 7h is extracted in 95 DEG C, and filtering takes filtrate rotary evaporation, dense
Contracting is freeze-dried 15h, obtains moisturizer.
Skin care scented soap soap agent：（1）Chinese yam is taken to crush to sieve with 100 mesh sieve, collects sieving particle B in mass ratio 2：9 add in go from
Sub- water, in 60 DEG C, 150r/min mechanical shaking extraction 5h, supernatant A is collected in centrifugation, adjusts pH to 5.0, supernatant A is in mass ratio
10：1：1 adds in cellobiose enzyme and zytase, in 48 DEG C, 180r/min saccharification 5h, adjusts pH to 7.2, obtains saccharified liquid；
（2）Picking Lactobacillus casei, Lactobacillus kefir are seeded to respectively in MRS fluid nutrient mediums, 28 DEG C of activation cultures
3d obtains Lactobacillus casei activation culture liquid and Lactobacillus kefir activation culture liquid, according to the mass fraction, takes 50 parts of saccharification
Liquid, 150 parts of fermentation mediums, 2 parts of Lactobacillus casei activation culture liquid, 0.7 part of Lactobacillus kefir activation culture liquid, 2
Part CaCO3Mixing, in 42 DEG C, 130r/min fermentation 7d obtain zymotic fluid, centrifuge, take supernatant B, obtain skin-protection soap soap agent.
Grease additive：The hard English walnut seeds of Bai Er are taken, shell is peeled off and takes benevolence, grind, 80 mesh sieve is crossed, collects sieving
Particle C, in mass ratio 1：10 add in petroleum ether mixing, are placed in soxhlet's extractor, extract 1.5h in 85 DEG C, repeat extraction 3 times,
Combining extraction liquid, extraction slag is spare, takes extract liquor rotary evaporation, adds the anhydrous sodium sulfate of sieving particle C mass 30%, quiet
15h is put, centrifuges, takes supernatant B, as grease additive.
Skin antioxidant：Take extraction slag rotary evaporation spare in grease additive, take after rotary evaporation extraction slag by
Mass ratio 1：It is mixed in 3 addition hexanes, mixed solution is obtained, in 55 DEG C, into mixed solution in mass ratio 1：10 add in quality point
Number is 60% methanol solution, extracts 6h, takes extracting solution rotary evaporation, dry, obtains skin antioxidant.
A kind of preparation method of skin care scented soap takes grease additive in mass ratio 1：8 add in sodium hydroxide, saponification
2h obtains saponification object, takes saponification object, the mixing of skin care scented soap soap agent, the water of skin care scented soap soap agent 90% is added, in 75
It DEG C is stirred, obtains mixture, take mixture in mass ratio 5：2 add in skin care scented soap additive, after being warming up to 80 DEG C, mixing
Mold after cooling, is placed in -20 DEG C of freezings for 24 hours, thaws, obtain skin care scented soap by 30min, molding.
Embodiment 3
Skimmed milk powder：It is purchased from Australian De Yun companies.
Fermentation medium：According to the mass fraction, 0.65 part of MgSO is taken4·7H2O, 0.6 part of KH2PO3, 0.15 part of NaCl, 7.5
Part yeast extract, 35 portions of skimmed milk powers, 1000 parts of water, 115 DEG C of sterilizing 20min.
Lactobacillus casei, Lactobacillus kefir：Inclined-plane is stored refrigerated.
Moisturizer：Nostoc is taken to crushed 50 mesh sieve, collects sieving particle A, sieving particle A is taken to be placed in absolute ethyl alcohol and is soaked
Bubble decoloration 17.5min, filtering take filter residue in mass ratio 1：90 add in water, and 6.5h is extracted in 93 DEG C, and filtering takes filtrate rotation to steam
Hair, concentration are freeze-dried 13.5h, obtain moisturizer.
Skin care scented soap soap agent：（1）Chinese yam is taken to crush to sieve with 100 mesh sieve, collects sieving particle B in mass ratio 2：9 add in go from
Sub- water, in 57 DEG C, 150r/min mechanical shaking extraction 4.5h, supernatant A is collected in centrifugation, adjusts pH to 4.9, supernatant A is in mass ratio
10：1：1 adds in cellobiose enzyme and zytase, in 47 DEG C, 180r/min saccharification 4.5h, adjusts pH to 7.1, must be saccharified
Liquid；
（2）Picking Lactobacillus casei, Lactobacillus kefir are seeded to respectively in MRS fluid nutrient mediums, 27 DEG C of activation cultures
2.5d obtains Lactobacillus casei activation culture liquid and Lactobacillus kefir activation culture liquid, according to the mass fraction, takes 45 portions of sugar
Change liquid, 125 parts of fermentation mediums, 1.5 parts of Lactobacillus casei activation culture liquid, 0.6 part of Lactobacillus kefir activation culture
Liquid, 1.5 parts of CaCO3Mixing, in 40 DEG C, 130r/min fermentation 6.5d obtain zymotic fluid, centrifuge, take supernatant B, obtain skin-protection soap soap
Agent.
Grease additive：The hard English walnut seeds of Bai Er are taken, shell is peeled off and takes benevolence, grind, 80 mesh sieve is crossed, collects sieving
Particle C, in mass ratio 1：10 add in petroleum ether mixing, are placed in soxhlet's extractor, extract 1.3h in 80 DEG C, repeat extraction 2 times,
Combining extraction liquid, extraction slag is spare, takes extract liquor rotary evaporation, adds the anhydrous sodium sulfate of sieving particle C mass 27%, quiet
13.5h is put, centrifuges, takes supernatant B, as grease additive.
Skin antioxidant：Take extraction slag rotary evaporation spare in grease additive, take after rotary evaporation extraction slag by
Mass ratio 1：It is mixed in 3 addition hexanes, mixed solution is obtained, in 53 DEG C, into mixed solution in mass ratio 1：10 add in quality point
Number is 60% methanol solution, extracts 5.5h, takes extracting solution rotary evaporation, dry, obtains skin antioxidant.
A kind of preparation method of skin care scented soap takes grease additive in mass ratio 1：7 add in sodium hydroxide, saponification
1.5h obtains saponification object, takes saponification object, the mixing of skin care scented soap soap agent, adds the water of skin care scented soap soap agent 85%, in
67 DEG C are stirred, and obtain mixture, take mixture in mass ratio 5：2 add in skin care scented soap additive, after being warming up to 77 DEG C, mixing
Mold after cooling, is placed in -20 DEG C of freezing 21h, thaws, obtain skin care scented soap by 25min, molding.
Comparative example 1
It is essentially identical with the preparation process of embodiment 2, it has only the difference is that lacking skin care scented soap soap agent.
Comparative example 2
It is essentially identical with the preparation process of embodiment 2, it has only the difference is that lacking grease additive.
Comparative example 3
It is essentially identical with the preparation process of embodiment 2, it has only the difference is that lacking moisturizer.
Comparative example 4
It is essentially identical with the preparation process of embodiment 2, it has only the difference is that lacking antioxidant.
Comparative example 5
The perfumed soap of Jinhua company production.
The perfumed soap of the present invention and the perfumed soap of reference examples are subjected to antibacterial, anti-oxidant test.It is wherein measured using DPPH methods clear
Except DPPH free radicals ability measures with this antioxygenic property of product, DPPH clearance rate calculation formula are as follows：DPPH clearance rates
（%）=（1-A samples/A controls）×100.A is that absorbance is measured at 520nm.Color is more shallow, and DPPH clearance rates are higher, resists
Oxidisability is also stronger.100 subjects are randomly selected, indices are provided with 0 ~ 10 point, 10 points of representatives are most satisfied, 0 point of representative
Dissatisfied, test result is shown in Table 1.
Table 1：
| Test event | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 |
| DPPH is removed Rate % | 92.1 | 93.4 | 90.4 | 89.8 | 88.7 | 89.2 | 61.3 | 42.3~ 45.6 |
| Bacteriostasis rate % | 98.2 | 99.1 | 97.4 | 95.2 | 93.6 | 93.7 | 94.8 | 63.2~ 69.4 |
| Moisture retention | 8 | 10 | 9 | 8 | 9 | 7 | 9 | 5~6 |
| Fragrance | 10 | 10 | 10 | 7 | 9 | 9 | 9 | 6~7 |
| Sense organ compares | Skin lubrication, carefully It is greasy | Skin lubrication, carefully It is greasy | Skin lubrication, carefully It is greasy | Skin lubrication is fine and smooth | Skin is slightly It is dry | Skin lubrication, carefully It is greasy | Skin lubrication, carefully It is greasy | Chapped skin It is coarse |
Embodiment 2 is can be seen that as optimum embodiment by the data of embodiment 1 ~ 3, preparation-obtained skin care scented soap effect is best,
And substance prepared by the present invention has synergistic effect.Summary, skin care scented soap effect of the invention is good, is worth of widely use.
Claims (8)
1. a kind of skin care scented soap, which is characterized in that according to the mass fraction, including 3 ~ 5 parts of moisturizer, 8 ~ 10 parts of skin care scented soap soaps
Agent, 15 ~ 20 parts of grease additives, 8 ~ 12 parts of skin antioxidants.
2. skin care scented soap according to claim 1, which is characterized in that the moisturizer is that nostoc is taken to crushed 50 mesh
Sieve collects sieving particle A, and sieving particle A is taken to be placed in absolute ethyl alcohol and impregnates 15 ~ 20min of decoloration, filtering takes filter residue by quality
Than 1：90 add in water, and 6 ~ 7h is extracted in 90 ~ 95 DEG C, and filtering takes filtrate, rotary evaporation, and concentration in being freeze-dried 12 ~ 15h, obtains
Moisturizer.
3. skin care scented soap according to claim 1, which is characterized in that the preparation method of the skin care scented soap soap agent is：
（1）Chinese yam is taken to crush to sieve with 100 mesh sieve, collects sieving particle B in mass ratio 2：9 add in deionized waters, in 55 ~ 60 DEG C,
Supernatant A is collected in 150r/min 4 ~ 5h of mechanical shaking extraction, centrifugation, pH to 4.8 ~ 5.0 is adjusted, by supernatant A in mass ratio 10：1：1
Cellobiose enzyme and zytase are added in, in 45 ~ 48 DEG C, 180r/min 4 ~ 5h of saccharification, pH to 7 ~ 7.2 is adjusted, obtains saccharified liquid；
（2）Picking Lactobacillus casei, Lactobacillus kefir are seeded to respectively in MRS fluid nutrient mediums, 25 ~ 28 DEG C of activation trainings
2 ~ 3d is supported, obtains Lactobacillus casei activation culture liquid and Lactobacillus kefir activation culture liquid, according to the mass fraction, take 40 ~
50 parts of saccharified liquids, 100 ~ 150 parts of fermentation mediums, 1 ~ 2 part of Lactobacillus casei activation culture liquid, 0.5 ~ 0.7 part of kefir
Lactobacillus activation culture liquid, 1 ~ 2 part of CaCO3Mixing, in 38 ~ 42 DEG C, 130r/min 6 ~ 7d of fermentation obtain zymotic fluid, centrifuge, take
Clear liquid B obtains skin-protection soap soap agent.
4. the preparation method of skin care scented soap soap agent according to claim 3, which is characterized in that the fermentation medium is matched
Fang Wei：According to the mass fraction, 0.5 ~ 0.8 part of MgSO is taken4·7H2O, 0.5 ~ 0.7 part of KH2PO3, 0.1 ~ 0.2 part of NaCl, 5 ~ 10 parts
Yeast extract, 30 ~ 40 portions of skimmed milk powers, 1000 parts of water, 115 DEG C of sterilizing 20min.
5. skin care scented soap according to claim 1, which is characterized in that the grease additive is to take the hard English walnut seeds of Bai Er
Peel off shell take benevolence, grind, cross 80 mesh sieve, collect sieving particle C, in mass ratio 1：10 add in petroleum ether mixing, in
75 ~ 85 DEG C of 1 ~ 1.5h of extraction, repeat extraction 2 ~ 3 times, combining extraction liquid, extraction slag is spare, takes extract liquor rotary evaporation, adds
The anhydrous sodium sulfate for particle C mass 25 ~ 30% of being sieved, stands 12 ~ 15h, and centrifugation takes supernatant B, as grease additive.
6. skin care scented soap according to claim 1, which is characterized in that the skin antioxidant is to take spare extraction slag
Rotary evaporation extracts slag in mass ratio 1 after taking rotary evaporation：It is mixed in 3 addition hexanes, obtains mixed solution, in 50 ~ 55 DEG C, to
In mass ratio 1 in mixed solution：10 add in the methanol solution that mass fraction is 60%, extract 5 ~ 6h, take extracting solution rotary evaporation,
It is dry, obtain skin antioxidant.
7. a kind of preparation method of skin care scented soap as described in claim 1, which is characterized in that the preparation method is that grease is taken to add
Add agent in mass ratio 1：6 ~ 8 add in sodium hydroxide, and 1 ~ 2h of saponification obtains saponification object, takes saponification object, skin care scented soap
Soap agent mix, add the water of skin care scented soap soap agent 80 ~ 90%, be stirred in 60 ~ 75 DEG C, obtain mixture, take mixture by
Mass ratio 5：2 add in skin care scented soap additive, after being warming up to 75 ~ 80 DEG C, 20 ~ 30 min of mixing, and molding, after cooling, by mold
Be placed in -20 DEG C freezing 18 ~ for 24 hours, thaw, obtain skin care scented soap.
8. the preparation method of skin care scented soap according to claim 7, which is characterized in that the skin care scented soap additive be by
Mass fraction meter takes the white sugar that 2 ~ 3 parts of lauryl sodium sulfate, 1 ~ 2 part of titanium dioxide, 20 ~ 30 parts of mass fractions are 70% water-soluble
Liquid, 5 ~ 7 parts of glycerine, 0.8 ~ 1.2 part of cream jasmin france, the mixing of 20 ~ 30 parts of absolute ethyl alcohols to get.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108753498A (en) * | 2018-07-04 | 2018-11-06 | 长春金荷药业有限公司 | A kind of washing perfumed soap and production technology containing deer oil badger seed oil |
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| CN1239735A (en) * | 1999-05-14 | 1999-12-29 | 石家庄光明日用化学股份有限公司 | High-activity natural skin care scented soap |
| CN1528913A (en) * | 2003-10-20 | 2004-09-15 | 武汉泰古投资有限公司 | Method for extracting diosgenin for joint production of starch suger by prehy drolysis of yellow ginger by multienzyme process |
| CN1544649A (en) * | 2003-11-11 | 2004-11-10 | 姜中兴 | Process for extracting saponin |
| CN106755131A (en) * | 2017-01-18 | 2017-05-31 | 华南理工大学 | A kind of method that industrial waste sugarcane marrow high efficiency synchronous saccharification common fermentation produces ethanol |
| CN106727263A (en) * | 2016-11-22 | 2017-05-31 | 深圳弘睿康生物科技有限公司 | Skin Tiny ecosystem improves preparation and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1239735A (en) * | 1999-05-14 | 1999-12-29 | 石家庄光明日用化学股份有限公司 | High-activity natural skin care scented soap |
| CN1528913A (en) * | 2003-10-20 | 2004-09-15 | 武汉泰古投资有限公司 | Method for extracting diosgenin for joint production of starch suger by prehy drolysis of yellow ginger by multienzyme process |
| CN1544649A (en) * | 2003-11-11 | 2004-11-10 | 姜中兴 | Process for extracting saponin |
| CN106727263A (en) * | 2016-11-22 | 2017-05-31 | 深圳弘睿康生物科技有限公司 | Skin Tiny ecosystem improves preparation and preparation method thereof |
| CN106755131A (en) * | 2017-01-18 | 2017-05-31 | 华南理工大学 | A kind of method that industrial waste sugarcane marrow high efficiency synchronous saccharification common fermentation produces ethanol |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108753498A (en) * | 2018-07-04 | 2018-11-06 | 长春金荷药业有限公司 | A kind of washing perfumed soap and production technology containing deer oil badger seed oil |
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