CN108192534A - A kind of novel Self-leveling adhesive material - Google Patents
A kind of novel Self-leveling adhesive material Download PDFInfo
- Publication number
- CN108192534A CN108192534A CN201711479320.XA CN201711479320A CN108192534A CN 108192534 A CN108192534 A CN 108192534A CN 201711479320 A CN201711479320 A CN 201711479320A CN 108192534 A CN108192534 A CN 108192534A
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- China
- Prior art keywords
- parts
- adhesive material
- novel self
- water
- leveling
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/02—Homopolymers or copolymers of acids; Metal or ammonium salts thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J167/00—Adhesives based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Adhesives based on derivatives of such polymers
- C09J167/04—Polyesters derived from hydroxycarboxylic acids, e.g. lactones
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/38—Boron-containing compounds
- C08K2003/387—Borates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/06—Biodegradable
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/10—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet
- C09J2301/12—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers
- C09J2301/122—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers the adhesive layer being present only on one side of the carrier, e.g. single-sided adhesive tape
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
A kind of novel Self-leveling adhesive material of the present invention, including adhesive layer, the adhesive layer contains the component of following parts by weight：10 30 parts of 80 110 parts of water, 10 20 parts of starch, 20 30 parts of polyhydroxyalkanoate, acrylic acid and/or its ester copolymer, 48 parts of alkaline matter, 12 parts of water-proofing agent, 0.5 2 parts of crosslinking agent, 0.2 1.5 parts of antiseptic, 13 parts of levelling agent.The present invention has the characteristics that self-leveling energy, good holding power, environmentally safe, production cost is low.
Description
Technical field
The present invention relates to adhesive material technical field, more particularly to a kind of novel Self-leveling adhesive material.
Background technology
Adhesive sticker is also self-adhesive label material, is using paper, film or special material as fabric, and the back side is coated with adhesive,
To apply a kind of composite material of the silicon protection sheet as base stock.Adhesive sticker originates from the thirties in last century, because it has without brush coating, no
With paste, without dip in water, it is pollution-free, save labeling the time the advantages that, be widely used in all trades and professions industry.It does not do
The adhesive layer of glue is the very important component part of adhesive label.Adhesive material often has corrugation, alice, comes off etc. existing
As, this is all related with the performance quality of adhesive layer, particularly by adhesive be coated on facial tissue layer bottom surface process, due to glue
Glutinous agent can differ larger with the surface of facial tissue, be easy to cause adhesive and coated in facial tissue layer bottom surface uneven, some places are thick, have
A little places are thin, need to be repeated as many times operation and can be only achieved the effect uniformly coated.
In addition, traditional adhesive material is difficult to degrade, difficult recycling, immense pressure is caused to environment.As the whole world is to ring
The requirement in border is higher and higher, and environmentally safe adhesive layer has become the emphasis and hot spot of research, and it is therefore necessary to existing
The adhesive layer of some adhesive materials is improved.
Invention content
The object of the present invention is to provide one kind have self-leveling energy, good holding power, it is environmentally safe, be produced into
This low adhesive material.
In order to achieve the above objectives, the present invention provides a kind of novel Self-leveling adhesive materials, special including adhesive layer
Sign is that the adhesive layer contains the component of following parts by weight：80-110 parts of water, 10-20 parts of starch, polyhydroxyalkanoate
10-30 parts of 20-30 parts, acrylic acid and/or its ester copolymer, 4-8 parts of alkaline matter, 1-2 parts of water-proofing agent, 0.5-2 parts of crosslinking agent,
0.2-1.5 parts of antiseptic, 1-3 parts of levelling agent.
Preferably, in the novel Self-leveling adhesive material of the present invention, the adhesive layer contains the component of following parts by weight：
95-105 parts of water, 15-20 parts of starch, 22-28 parts of polyhydroxyalkanoate, acrylic acid and/or 15-25 parts of its ester copolymer, alkali
5-7 parts of substance of property, 1.2-1.8 parts of water-proofing agent, 0.8-1.8 parts of crosslinking agent, 0.5-1.2 parts of antiseptic, 1.2-2.5 parts of levelling agent.
It is highly preferred that the adhesive layer contains the component of following parts by weight：100 parts of water, 18 parts of starch, poly- hydroxy aliphatic
22 parts of 25 parts of acid esters, acrylic acid and/or its ester copolymer, 6 parts of alkaline matter, 1.5 parts of water-proofing agent, 1.5 parts of crosslinking agent, antiseptic
0.6 part, 2 parts of levelling agent.
Preferably, in the novel Self-leveling adhesive material of the present invention, the starch is natural plant starch.
Preferably, in the novel Self-leveling adhesive material of the present invention, the acrylic acid and/or its ester copolymer are acrylic acid
N-butyl, Isooctyl acrylate monomer, isodecyl acrylate, methyl methacrylate, acrylic acid, two kinds of methacrylic acid or two kinds
Above copolymer.
Preferably, in the novel Self-leveling adhesive material of the present invention, the alkaline matter is calcium hydroxide, sodium hydroxide and
One or both of potassium hydroxide.
Preferably, in the novel Self-leveling adhesive material of the present invention, the water-proofing agent is potassium zirconium carbonate.
Preferably, in the novel Self-leveling adhesive material of the present invention, the crosslinking agent is borax or boric acid.
Preferably, in the novel Self-leveling adhesive material of the present invention, the antiseptic is cationic chitosan quaternary ammonium salt, ten
One or both of dialkyl dimethyl Benzylphosphonium Bromide ammonium, dodecyl trimethyl ammonium chloride.
Preferably, in the novel Self-leveling adhesive material of the present invention, the levelling agent is trisiloxane surfactant.
Trisiloxane surfactant is applied to adhesive material field by the present invention so that adhesive layer
Performance with Self-leveling so as to improve the uniformity that adhesive is coated in facial tissue layer bottom surface, and then improves adhesive sticker material
The performance of material；The degradable biologicals such as polyhydroxyalkanoate material is applied to adhesive material field, reduces adhesive sticker material
Expect the influence to environment, can realize the complete biodegradable of adhesive material；In addition, the present invention has, preparation method is simple,
Production cost is low, it is environmentally safe the advantages of.
Specific embodiment
The novel Self-leveling adhesive material of the present invention, including adhesive layer, wherein adhesive layer is located at adhesive material
Between facial tissue layer and ground paper layer.
In specific embodiment 1, the adhesive layer contains the component of following parts by weight：80-110 parts of water, starch 10-20
Part, 20-30 parts of polyhydroxyalkanoate, acrylic acid and/or 10-30 parts of its ester copolymer, 4-8 parts of alkaline matter, water-proofing agent 1-2
Part, 0.5-2 parts of crosslinking agent, 0.2-1.5 parts of antiseptic, 1-3 parts of levelling agent.
In specific embodiment 2, the adhesive layer contains the component of following parts by weight：95-105 parts of water, starch 15-20
Part, 22-28 parts of polyhydroxyalkanoate, acrylic acid and/or 15-25 parts of its ester copolymer, 5-7 parts of alkaline matter, water-proofing agent
1.2-1.8 parts, 0.8-1.8 parts of crosslinking agent, 0.5-1.2 parts of antiseptic, 1.2-2.5 parts of levelling agent.
In specific embodiment 3, the adhesive layer contains the component of following parts by weight：100 parts of water, gathers 18 parts of starch
22 parts of 25 parts of hydroxy fatty acid, acrylic acid and/or its ester copolymer, 6 parts of alkaline matter, 1.5 parts of water-proofing agent, crosslinking agent 1.5
Part, 0.6 part of antiseptic, 2 parts of levelling agent.
In comparing embodiment, the adhesive layer contains the component of following parts by weight：80-110 parts of water, 10-20 parts of starch,
10-30 parts of 20-30 parts of polyhydroxyalkanoate, acrylic acid and/or its ester copolymer, 4-8 parts of alkaline matter, 1-2 parts of water-proofing agent,
0.5-2 parts of crosslinking agent, 0.2-1.5 parts of antiseptic.
The starch is natural plant starch.The acrylic acid and/or its ester copolymer are n-butyl acrylate, acrylic acid
Different monooctyl ester, isodecyl acrylate, methyl methacrylate, acrylic acid, methacrylic acid two or more copolymer.
The alkaline matter is one or both of calcium hydroxide, sodium hydroxide and potassium hydroxide.The water-proofing agent is potassium zirconium carbonate.
The crosslinking agent is borax or boric acid.The antiseptic is cationic chitosan quaternary ammonium salt, dodecyl dimethyl benzyl bromide
Change one or both of ammonium, dodecyl trimethyl ammonium chloride.The levelling agent is trisiloxane surfactant.
The degradation rate of the adhesive layer of above-mentioned specific embodiment 1-3, adhesion strength, can load force, extensibility, coating it is uniform
The experimental data comparison of required number of operations is as follows：
The preparation method of the novel Self-leveling adhesive material label of the present invention：
Embodiment 1
Weigh water 80g, starch 10g, polyhydroxyalkanoate 20g, acrylic acid and methylmethacrylate copolymer 10g,
Sodium hydroxide 4g, potassium zirconium carbonate 1g, borax 0.5g, dodecyl trimethyl ammonium chloride 0.2g, trisiloxane surfactant 1g.
Starch is soluble in water, sodium hydroxide is added in after stirring 15min, continues to stir 20min, adds in polyhydroxyalkanoate, propylene
Acid and methylmethacrylate copolymer continue to stir 30min, are eventually adding potassium zirconium carbonate, borax, trimethyl chlorine
Change ammonium and trisiloxane surfactant, continue stirring up to sample is uniform and tacky flowing, standing naturally cools to room temperature
After save backup.
Embodiment 2
Weigh water 110g, starch 20g, polyhydroxyalkanoate 30g, acrylic acid and n-butyl acrylate copolymers 30g, hydrogen
Potassium oxide 8g, potassium zirconium carbonate 1g, boric acid 2g, dodecyl dimethyl benzyl ammonium bromide 1.5g, trisiloxane surfactant 3g.
Starch is soluble in water, potassium hydroxide is added in after stirring 15min, continues to stir 20min, adds in polyhydroxyalkanoate, propylene
Acid and n-butyl acrylate copolymers continue to stir 30min, are eventually adding potassium zirconium carbonate, boric acid, dodecyl dimethyl benzyl
Ammonium bromide and trisiloxane surfactant continue stirring up to sample is uniform and tacky flowing, and standing naturally cools to room
It is saved backup after temperature.
Embodiment 3
Weigh water 100g, starch 18g, polyhydroxyalkanoate 25g, acrylic acid and Isooctyl acrylate monomer copolymer 30g, hydrogen
Calcium oxide 6g, potassium zirconium carbonate 1.5g, boric acid 1.5g, dodecyl dimethyl benzyl ammonium bromide 0.6g, trisiloxanes surface-active
Agent 2g.Starch is soluble in water, stir 15min after add in calcium hydroxide, continue stir 20min, add in polyhydroxyalkanoate,
Acrylic acid and Isooctyl acrylate monomer copolymer continue to stir 30min, are eventually adding potassium zirconium carbonate, boric acid, dodecyl dimethyl
Benzylphosphonium Bromide ammonium and trisiloxane surfactant continue stirring until sample is uniform and tacky flowing, stand, natural cooling
It is saved backup after to room temperature.
Use the adhesive layer prepare the method for novel Self-leveling adhesive material label for：By gluing obtained above
Agent is evenly coated on the facial tissue prepared, is subsequently placed in baking oven drying, is obtained coating the plane materiel of adhesive, will coat adhesive
The pressing that passes through rubber rollers and roller of plane materiel and base stock, you can obtain adhesive label.
Above-described is only some embodiments of the present invention.For those of ordinary skill in the art, not
Under the premise of being detached from the invention design, various modifications and improvements can be made, these belong to the protection model of the present invention
It encloses.
Claims (10)
1. a kind of novel Self-leveling adhesive material, including adhesive layer, which is characterized in that the adhesive layer contains following heavy
Measure the component of part：80-110 parts of water, 10-20 parts of starch, 20-30 parts of polyhydroxyalkanoate, acrylic acid and/or its ester copolymer
10-30 parts, 4-8 parts of alkaline matter, 1-2 parts of water-proofing agent, 0.5-2 parts of crosslinking agent, 0.2-1.5 parts of antiseptic, 1-3 parts of levelling agent.
2. novel Self-leveling adhesive material according to claim 1, which is characterized in that the adhesive layer contains following
The component of parts by weight：95-105 parts of water, 15-20 parts of starch, 22-28 parts of polyhydroxyalkanoate, acrylic acid and/or the copolymerization of its ester
15-25 parts of object, 5-7 parts of alkaline matter, 1.2-1.8 parts of water-proofing agent, 0.8-1.8 parts of crosslinking agent, 0.5-1.2 parts of antiseptic, levelling
1.2-2.5 parts of agent.
3. novel Self-leveling adhesive material according to claim 1, which is characterized in that the adhesive layer contains following
The component of parts by weight：100 parts of water, 18 parts of starch, 25 parts of polyhydroxyalkanoate, acrylic acid and/or 22 parts of its ester copolymer, alkali
6 parts of substance of property, 1.5 parts of water-proofing agent, 1.5 parts of crosslinking agent, 0.6 part of antiseptic, 2 parts of levelling agent.
4. novel Self-leveling adhesive material according to any one of claim 1-3, which is characterized in that the starch is
Natural plant starch.
5. novel Self-leveling adhesive material according to any one of claim 1-3, which is characterized in that the acrylic acid
And/or its ester copolymer is n-butyl acrylate, Isooctyl acrylate monomer, isodecyl acrylate, methyl methacrylate, propylene
Two or more copolymer of acid, methacrylic acid.
6. novel Self-leveling adhesive material according to any one of claim 1-3, which is characterized in that the basic species
Matter is one or both of calcium hydroxide, sodium hydroxide and potassium hydroxide.
7. novel Self-leveling adhesive material according to any one of claim 1-3, which is characterized in that the water-proofing agent
For potassium zirconium carbonate.
8. novel Self-leveling adhesive material according to any one of claim 1-3, which is characterized in that the crosslinking agent
For borax or boric acid.
9. novel Self-leveling adhesive material according to any one of claim 1-3, which is characterized in that the antiseptic
For one kind in cationic chitosan quaternary ammonium salt, dodecyl dimethyl benzyl ammonium bromide, dodecyl trimethyl ammonium chloride or
Two kinds.
10. novel Self-leveling adhesive material according to any one of claim 1-3, which is characterized in that the levelling
Agent is trisiloxane surfactant.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711479320.XA CN108192534A (en) | 2017-12-29 | 2017-12-29 | A kind of novel Self-leveling adhesive material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711479320.XA CN108192534A (en) | 2017-12-29 | 2017-12-29 | A kind of novel Self-leveling adhesive material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108192534A true CN108192534A (en) | 2018-06-22 |
Family
ID=62586643
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711479320.XA Pending CN108192534A (en) | 2017-12-29 | 2017-12-29 | A kind of novel Self-leveling adhesive material |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102867459A (en) * | 2011-11-07 | 2013-01-09 | 中国印刷科学技术研究所 | Biodegradable adhesive sticker label |
| CN104263275A (en) * | 2014-09-10 | 2015-01-07 | 上海金大塑胶有限公司 | Environment-friendly self-adhesive label material |
| CN105602487A (en) * | 2015-12-21 | 2016-05-25 | 福清宏宝化工有限公司 | Water-based adhesive and preparation method thereof |
| CN106634686A (en) * | 2016-10-10 | 2017-05-10 | 上海金大塑胶有限公司 | Novel environment-friendly adhesive sticker material |
-
2017
- 2017-12-29 CN CN201711479320.XA patent/CN108192534A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102867459A (en) * | 2011-11-07 | 2013-01-09 | 中国印刷科学技术研究所 | Biodegradable adhesive sticker label |
| CN104263275A (en) * | 2014-09-10 | 2015-01-07 | 上海金大塑胶有限公司 | Environment-friendly self-adhesive label material |
| CN105602487A (en) * | 2015-12-21 | 2016-05-25 | 福清宏宝化工有限公司 | Water-based adhesive and preparation method thereof |
| CN106634686A (en) * | 2016-10-10 | 2017-05-10 | 上海金大塑胶有限公司 | Novel environment-friendly adhesive sticker material |
Non-Patent Citations (2)
| Title |
|---|
| 李建民等: "《工业设备粘接维修》", 31 January 2001, 化学工业出版社 * |
| 李红强: "《胶粘原理、技术与应用》", 31 January 2014, 华南理工大学出版社 * |
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Application publication date: 20180622 |
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