CN108187462A - High-efficiency deodorant and preparation method thereof - Google Patents
High-efficiency deodorant and preparation method thereof Download PDFInfo
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- CN108187462A CN108187462A CN201810166616.4A CN201810166616A CN108187462A CN 108187462 A CN108187462 A CN 108187462A CN 201810166616 A CN201810166616 A CN 201810166616A CN 108187462 A CN108187462 A CN 108187462A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/54—Nitrogen compounds
- B01D53/58—Ammonia
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/81—Solid phase processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/90—Odorous compounds not provided for in groups B01D2257/00 - B01D2257/708
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Biomedical Technology (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Emergency Medicine (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention belongs to utilize deodorant compositions to air deodorization technical field, and in particular to a kind of high-efficiency deodorant and preparation method thereof.The deodorant includes following components：Molecular sieve, nano zine oxide, antiseptic and Macrogol 600.The deodorant good deodorization effect of the present invention, and with high efficiency；It is nonirritant, non-toxic, safety and environmental protection；Have a wide range of application；Preparation method is simple and practicable, it is easy to accomplish industrialized production.
Description
Technical field
The invention belongs to using deodorant compositions to air deodorization technical field, and in particular to a kind of high-efficiency deodorant and its
Preparation method.
Background technology
The lavatory of the public arenas such as family, hospital or hotel is after a period of use, it is easy to give out foul smell, these are smelly
Gas mainly contains ammonia, hydrogen sulfide, amine and sulfuric acid substance.Exerted a gradual, corrupting influence on for a long time by this kind of odorous substance, people can be made fidgety
Uneasy, lassitude, can even cause the symptoms such as headache, insomnia, laryngitis, pneumonia when serious.In addition, often given out in lavatory
The parasitic various poisonous and harmful bacteriums of stink meeting seriously endanger the health of people.
In order to prevent with eliminate foul smell, commonly using following three kinds of deodorization modes：The first is to utilize the fragrance of fragrance will
Foul smell covers in, and this mode distributes there is no foul smell, foul smell is thoroughly eliminated or can influence health；Second is profit
With the mode of activated carbon adsorption come deodorization, the deficiency of this mode is that the adsorption capacity of activated carbon is limited, but also frequent
Displacement, then can not handle the stink substances such as sulfuric acid；The third method is disappeared with the method for duration flowing water
Except stink, this mode deodorizing effect is bad, and wastes a large amount of water resource.
Patent document such as Publication No. CN1043264A discloses a kind of deodorant for toilet (odour adsorbent), main ingredient
For activated carbon, silica, calcium oxide alundum (Al2O3), magnesia, fungicide and aromatic hydrocarbon organic matter etc., to lavatory, public
Different stenches and various odor gas in place particularly can adsorb ammonia, so as to reach deodorant (odour adsorbent) purification ring
The purpose in border.The patent document of Publication No. CN1064620A discloses a kind of deodorant for toilet, is by disinfectant boric acid, anti-corrosion
One kind that four kinds of substance mixtures such as agent borax, surfactant sodium dodecyl base benzene sulfonic acid sodium salt and washing assisant sodium tripolyphosphate form
Powder soluble easily in water, suitable for various types lavatory, the lavatory of particularly anhydrous flushing.Publication No. CN1076369A's
Patent document discloses a kind of deodorant for toilet, containing frerrous chloride, ferrous sulfate, maleic acid and fragrance, adds in 10 times
It is used after clear water dilution.
Although the prior art achieves certain progress in terms of deodorization, there is also deficiencies, are mainly shown as：It is main
To carry out deodorization using absorption method and masking method, effect is not strong, and effect cannot be lasting, is only applicable to the relatively low situation of odor concentration；
Water mixing or moisture is generated when in use, so as to generate some substances unfavorable to human body, make after deodorization that there was dampness in the air, circulation is not
Freely, and irritant smell, equally it is unfavorable for human body respiration, and bring certain sense of discomfort.
Invention content
In view of this, the purpose of the present invention is to provide a kind of deodorant, the deodorant good deodorization effect, action times
It is long, the higher situation of odor concentration can be suitable for, safety and environmental protection has no irritating odor, and will not generate the object unfavorable to human body
Matter.
Unless otherwise indicated, number of the present invention is mass fraction.
To achieve the above object, the technical scheme is that：
Deodorant, including following components：Molecular sieve, nano zine oxide, antiseptic and polyethylene glycol -600.
Further, the antiseptic is the 1-2 kinds in carbendazim and boric acid.
Further, in terms of mass parts, proportion relation is：30-40 parts of molecular sieves, 4-10 parts of nano zine oxides, 3-7 parts of antibacterials
Agent and 10-15 parts of polyethylene glycol -600.
Further, following components is further included：Fumaric acid or and/or citric acid and/or essence.
Further, in terms of mass parts, proportion relation is：30-40 parts of molecular sieves, 4-10 parts of nano zine oxides, 3-7 parts of antibacterials
Agent and 10-15 parts of polyethylene glycol -600, fumaric acid are no more than 10 parts no more than 20 parts, citric acid no more than 35 parts, essence.
Further, in terms of mass parts, proportion relation is：30-40 parts of molecular sieves, 4-10 parts of nano zine oxides, 3-7 parts of antibacterials
5-10 parts of agent and 10-15 parts of polyethylene glycol -600,10-20 parts of fumaric acid and/or 25-35 parts of citric acid and/or essence.
The deodorant good deodorization effect, long action time can be suitable for the higher situation of odor concentration, can effectively kill
Bacterium, safety and environmental protection will not generate the substance unfavorable to human body.
Inventor also found, the preparation method complex process of prior art deodorant, and cost is higher.
The present invention also aims to protect the preparation method of the deodorant, include the following steps：
A. molecular sieve and nano zine oxide are uniformly mixed；
B. mixture obtained by step A is uniformly mixed with fumaric acid and/or citric acid；
C. antiseptic is distributed in polyethylene glycol -600, then the mixture with deionized water is mixed again, obtains liquid
Body mixture；
D. will liquid mixture obtained by mixture obtained by step B and step C mix after stir, pelletize, then dry to get
The deodorant.
This method is simple and practicable, it is easy to accomplish industrialized production, it is at low cost.
Further, the drying refers to dry 1-3h at 100-150 DEG C.
The beneficial effects of the present invention are：
The deodorant good deodorization effect of the present invention, can handle high concentration odorous substance, deodorization speed is fast；Reaction 8 hours,
It to the deodorizing rate of ammonia up to 87%-91%, reacts 24 hours, to the deodorizing rate of ammonia up to 97%-99%.
The deodorant of the present invention is nonirritant, non-toxic, safety and environmental protection.
The deodorant of the present invention has a wide range of application, and in addition to for toilet deodorization, can be also used for deodorant for refregerator and human body removes
It is smelly.
The preparation method of the deodorant of the present invention is simple and practicable, it is easy to accomplish industrialized production.
Specific embodiment
Illustrated embodiment is to preferably be illustrated to present disclosure, but is not that present disclosure only limits
In illustrated embodiment.So those skilled in the art carry out nonessential change according to foregoing invention content to embodiment
Into and adjustment, still fall within protection scope of the present invention.
Embodiment 1
A kind of deodorant is made of the raw material of following parts by weight：25 parts of β-molecular sieves, 15 parts of 13X types molecular sieves, 5 parts
Nano zine oxide, 5 parts of carbendazim, 35 parts of citric acids, 12 parts of PEG-600 and 8 part of flavoring rose essences.
The preparation method of the deodorant is：
A. 25 parts of β-molecular sieves and 15 parts of 13X types molecular sieves are dried into preservation at 120 DEG C；
B. dry mix machine will be sent by β-molecular sieve of drying and processing, 13X types molecular sieve and 5 parts of nano zine oxides to stir
5min is mixed, obtains mixed dry material；
C. mixed dry material obtained by step B and 35 parts of citric acids are sent into dry mix machine stirring 10min, obtain mixed material
A；
D. 5 parts of carbendazim and 8 parts of flavoring rose essences are distributed under ultrasound condition in 12 parts of PEG-600, then this is mixed
Object is mixed with 100 parts of deionized waters, obtains liquid mixture B；
E. by after mixed material A and liquid mixture B uniform stirrings, graininess is made with comminutor, in 100 DEG C of drying
3h is to get the deodorant.
Embodiment 2
A kind of deodorant is made of the raw material of following parts by weight：15 parts of Y type molecular sieves, 5 parts of 13X types molecular sieves, 10 parts
5A molecular sieves, 7 parts of nano zine oxides, 5 parts of boric acid, 30 parts of citric acids, 15 parts of fumaric acid, 13 parts of PEG-600 and 8 part of jasmine perfume (or spice)
Essence.
The preparation method of the deodorant is：
A. 15 parts of Y type molecular sieves, 5 parts of 13X types molecular sieves and 10 parts of 5A molecular sieves are dried into preservation at 120 DEG C；
B. it will be sent by the Y type molecular sieve of drying and processing, 13X types molecular sieve, 5A molecular sieves and 7 parts of nano zine oxides dry
Formula blender stirs 5min, obtains mixed dry material；
C. mixed dry material obtained by step B and 30 parts of citric acids and 15 parts of fumaric acid are sent into dry mix machine stirring 10min,
Obtain mixed material A；
D. 5 parts of boric acid and 8 parts of cream jasmin frances are distributed under ultrasound condition in 13 parts of PEG-600, then by the mixture
It is mixed with 100 parts of deionized waters, obtains liquid mixture B；
E. by after mixed material A and liquid mixture B uniform stirrings, graininess is made with comminutor, in 120 DEG C of drying
2h is to get the deodorant.
Embodiment 3
A kind of deodorant is made of the raw material of following parts by weight：10 parts of ZSM-5 molecular sieves, 10 parts of MCM-22 molecular sieves,
5 parts of 13X types molecular sieves, 5 parts of 5A molecular sieves, 5 parts of nano zine oxides, 1 part of carbendazim, 4 parts of boric acid, 25 parts of citric acids, 15 parts of richnesses
Horse acid, 13 parts of PEG-600 and 8 part of lemon extracts.
The preparation method of the deodorant is：
A. by 10 parts of ZSM-5 molecular sieves, 10 parts of MCM-22 molecular sieves, 5 parts of 13X types molecular sieves and 5 parts of 5A molecular sieves 120
It dries and preserves at DEG C；
It B. will be by the ZSM-5 molecular sieve of drying and processing, MCM-22 molecular sieves, 13X types molecular sieve, 5A molecular sieves and 5 parts
Nano zine oxide is sent into dry mix machine stirring 10min, obtains mixed dry material；
C. mixed dry material obtained by step B and 25 parts of citric acids and 15 parts of fumaric acid are sent into dry mix machine stirring 10min,
Obtain mixed material A；
D. 4 parts of boric acid, 1 part of carbendazim and 8 parts of lemon extracts are distributed under ultrasound condition in 13 parts of PEG-600, then
The mixture with 100 parts of deionized waters is mixed, obtains liquid mixture B；
E. by after mixed material A and liquid mixture B uniform stirrings, graininess is made with comminutor, in 150 DEG C of drying
1h is to get the deodorant.
Performance test
The deodorizing effect verification to ammonia is carried out to deodorant made from embodiment 1-3, the results are shown in Table 1；
Deodorizing effect test method to ammonia is：2 10ml colorimetric cylinders are taken, are separately added into the ammonia spirit of 100mg/kg
1g deodorant is fitted into beanbag by 1ml, clogs colorimetric nozzle, while setting is not added with the blank control group of deodorant, respectively at
Remaining ammonia content in colorimetric cylinder is measured after 8 hours and 24 hours, and calculates deodorizing rate；
Meanwhile 2 10ml colorimetric cylinders are taken, the ammonia spirit 1ml of 1000mg/kg is separately added into, 1g deodorant is packed into small
In cloth bag, colorimetric nozzle is clogged, while setting is not added with the blank control group of deodorant, is measured behind 8 hours and 24 hours
Remaining ammonia content in colorimetric cylinder, and calculate deodorizing rate.
1 deodorizing effect of table
As shown in Table 1, after reacting 8 hours, deodorant of the invention is to the deodorizing rate of ammonia up to 87%-91%, reaction 24
After hour, deodorant of the invention is to the deodorizing rate of ammonia up to 97%-99%.
Thus it proves, deodorant good deodorization effect of the invention, high concentration odorous substance can be handled, and with efficient
Property.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in each embodiment can also be properly combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (8)
1. deodorant, which is characterized in that including following components：Molecular sieve, nano zine oxide, antiseptic and polyethylene glycol -600.
2. deodorant according to claim 1, which is characterized in that the antiseptic is the 1-2 kinds in carbendazim and boric acid.
3. deodorant according to claim 1 or 2, which is characterized in that in terms of mass parts, proportion relation is：30-40 parts points
Sub- sieve, 4-10 parts of nano zine oxides, 3-7 parts of antiseptics and 10-15 parts of polyethylene glycol -600.
4. according to the deodorant described in claim 1,2 or 3, which is characterized in that further include following components：Fumaric acid or and/or
Citric acid and/or essence.
5. deodorant according to claim 4, which is characterized in that in terms of mass parts, proportion relation is：30-40 parts of molecules
Sieve, 4-10 parts of nano zine oxides, 3-7 parts of antiseptics and 10-15 parts of polyethylene glycol -600, fumaric acid are no more than 20 parts, citric acid
It is no more than 10 parts no more than 35 parts, essence.
6. deodorant according to claim 5, which is characterized in that in terms of mass parts, proportion relation is：30-40 parts of molecules
Sieve, 4-10 parts of nano zine oxides, 3-7 parts of antiseptics and 10-15 parts of polyethylene glycol -600,10-20 parts of fumaric acid and/or citric acid
25-35 parts and/or 5-10 parts of essence.
7. the preparation method of any one of the claim 1-6 deodorant, which is characterized in that include the following steps：
A. molecular sieve and nano zine oxide are uniformly mixed；
B. mixture obtained by step A is uniformly mixed with fumaric acid and/or citric acid；
C. antiseptic is distributed in polyethylene glycol -600, then the mixture with deionized water is mixed again, liquid is obtained and mixes
Close object；
D. it is stirred after liquid mixture obtained by mixture obtained by step B and step C is mixed, pelletizes, then dry to get described
Deodorant.
8. preparation method according to claim 7, which is characterized in that the drying refers to dry 1- at 100-150 DEG C
3h。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810166616.4A CN108187462A (en) | 2018-02-26 | 2018-02-26 | High-efficiency deodorant and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810166616.4A CN108187462A (en) | 2018-02-26 | 2018-02-26 | High-efficiency deodorant and preparation method thereof |
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| CN108187462A true CN108187462A (en) | 2018-06-22 |
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| CN201810166616.4A Pending CN108187462A (en) | 2018-02-26 | 2018-02-26 | High-efficiency deodorant and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112827471A (en) * | 2020-12-29 | 2021-05-25 | 南京凯创微锌环境技术有限公司 | Preparation method of deodorant for sheep farm |
| CN113797377A (en) * | 2021-10-09 | 2021-12-17 | 绍兴道普新材料科技有限公司 | Cucurbituril air purifying agent |
| CN113908680A (en) * | 2021-09-01 | 2022-01-11 | 郑州轻工业大学 | Deodorant for organic solid waste aerobic fermentation treatment and preparation method thereof |
| CN114409961A (en) * | 2021-12-25 | 2022-04-29 | 昆山禾振瑞新复合材料有限公司 | High-performance compound deodorant and preparation method thereof |
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| CN105343918A (en) * | 2015-12-08 | 2016-02-24 | 深圳市世家丽科技发展有限公司 | Deodorant containing shell powder |
| CN106221398A (en) * | 2016-07-29 | 2016-12-14 | 蒋文兰 | Molecular sieve photocatalytic spray liquid can be cleaned |
| CN107320757A (en) * | 2017-06-22 | 2017-11-07 | 南京汉旗新材料科技有限公司 | A kind of deodorant based on the utilization of resources |
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2018
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| CN101698111A (en) * | 2009-11-09 | 2010-04-28 | 陈罘杲 | In-shoe environment purifying material |
| CN105343918A (en) * | 2015-12-08 | 2016-02-24 | 深圳市世家丽科技发展有限公司 | Deodorant containing shell powder |
| CN106221398A (en) * | 2016-07-29 | 2016-12-14 | 蒋文兰 | Molecular sieve photocatalytic spray liquid can be cleaned |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112827471A (en) * | 2020-12-29 | 2021-05-25 | 南京凯创微锌环境技术有限公司 | Preparation method of deodorant for sheep farm |
| CN112827471B (en) * | 2020-12-29 | 2023-10-31 | 南京凯创微锌环境技术有限公司 | Preparation method of deodorant for sheep farm |
| CN113908680A (en) * | 2021-09-01 | 2022-01-11 | 郑州轻工业大学 | Deodorant for organic solid waste aerobic fermentation treatment and preparation method thereof |
| CN113797377A (en) * | 2021-10-09 | 2021-12-17 | 绍兴道普新材料科技有限公司 | Cucurbituril air purifying agent |
| CN114409961A (en) * | 2021-12-25 | 2022-04-29 | 昆山禾振瑞新复合材料有限公司 | High-performance compound deodorant and preparation method thereof |
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Application publication date: 20180622 |