CN108181958A - A kind of constant temperature and moisture test device and method suitable for tobacco thermophysical property measurement - Google Patents

A kind of constant temperature and moisture test device and method suitable for tobacco thermophysical property measurement Download PDF

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Publication number
CN108181958A
CN108181958A CN201810023550.3A CN201810023550A CN108181958A CN 108181958 A CN108181958 A CN 108181958A CN 201810023550 A CN201810023550 A CN 201810023550A CN 108181958 A CN108181958 A CN 108181958A
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CN
China
Prior art keywords
temperature
constant temperature
tobacco
constant
humidity
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810023550.3A
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Chinese (zh)
Inventor
鲁端峰
孙淼
张明建
王乐
张柯
邓楠
马亚萍
申玉军
金跃平
李斌
刘勇
张龙
李志刚
姚旭
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hefei Institutes of Physical Science of CAS
Zhengzhou Tobacco Research Institute of CNTC
Original Assignee
Hefei Institutes of Physical Science of CAS
Zhengzhou Tobacco Research Institute of CNTC
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Filing date
Publication date
Application filed by Hefei Institutes of Physical Science of CAS, Zhengzhou Tobacco Research Institute of CNTC filed Critical Hefei Institutes of Physical Science of CAS
Priority to CN201810023550.3A priority Critical patent/CN108181958A/en
Publication of CN108181958A publication Critical patent/CN108181958A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05DSYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
    • G05D27/00Simultaneous control of variables covered by two or more of main groups G05D1/00 - G05D25/00
    • G05D27/02Simultaneous control of variables covered by two or more of main groups G05D1/00 - G05D25/00 characterised by the use of electric means
    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05BCONTROL OR REGULATING SYSTEMS IN GENERAL; FUNCTIONAL ELEMENTS OF SUCH SYSTEMS; MONITORING OR TESTING ARRANGEMENTS FOR SUCH SYSTEMS OR ELEMENTS
    • G05B11/00Automatic controllers
    • G05B11/01Automatic controllers electric
    • G05B11/36Automatic controllers electric with provision for obtaining particular characteristics, e.g. proportional, integral, differential
    • G05B11/42Automatic controllers electric with provision for obtaining particular characteristics, e.g. proportional, integral, differential for obtaining a characteristic which is both proportional and time-dependent, e.g. P.I., P.I.D.

Abstract

A kind of constant temperature and moisture test device and method suitable for tobacco thermophysical property measurement, it is characterised in that:Including sample bin, be the constant temperature water bath system that constant temperature is provided outside sample bin, be gas circuit constant temperature and humidity system and data collecting system, control system and computer that constant temperature and humidity gas is provided in sample bin;0 100 DEG C of circulator bath, the compressed air of arbitrary proportion mixing and the mixed gas of saturated steam can be selected in the present invention, to ensure that the tobacco sample in sample bin has uniform temperature and humidity.And recirculated water and the parameters such as mixed gas temperature and flow can be adjusted respectively, the temperature of effective control loop water and the humiture of mixed gas, adjustable range is broad, has many advantages, such as that temperature and humidity control is accurate reliable, easy to operate.The device adapts to a variety of test parameters, provides reliable and stable experiment porch for less than 100 DEG C tobacco thermophysical property measurements, achievees the purpose that effectively to control sample humiture, improve the accuracy and reliability of thermophysical property measurement.

Description

A kind of constant temperature and moisture test device and method suitable for tobacco thermophysical property measurement
Technical field
The present invention relates to tobacco thermophysical property measurement fields, and in particular to a kind of constant temperature for being adapted to tobacco thermophysical property measurement is permanent Wet test device and method.
Background technology
Tobacco is a kind of thermal sensitivity biological material, and under temperature match curing conditions, tobacco heat physical state easily changes, and Tobacco thermophysical property measurement requirement test sample is in stable condition.Thermophysical property measurement temperature and humidity control device phase under previous tobacco temperature match curing conditions To simple, temperature and humidity control is inaccurate, and therefore, a set of effective constant temperature and humidity device of research and design has tobacco thermophysical property measurement Important meaning.
Temperature and humidity is two important parameters during tobacco thermophysical property measurement, and whether Temperature and Humidity Control is accurate directly Influence the validity and reliability of tobacco thermophysical property measurement result.During the temperature of tobacco system tends to be uniform, moisture It can migrate, tobacco moisture can be caused to be unevenly distributed in this way, it is unreliable so as to cause tobacco thermophysical property measurement result.
The thermal physical property parameter of tobacco designs and develops smoke machine equipment and hot-working process control parameter has the function of directiveness, And temperature and humidity is two important parameters during tobacco thermophysical property measurement, so, humiture is accurately controlled to tobacco heat Physical measurement is most important.But previous tobacco thermophysical property measurement temperature and humidity control device is relatively easy, it is difficult to avoid temperature not , the problems such as water translocation, accurately and reliably thermal physical property parameter is hardly resulted under temperature match curing conditions.
Invention content
For tobacco thermophysical property measurement present situation and the above-mentioned deficiency of the prior art, the object of the present invention is to provide one kind to be applicable in In the constant temperature and moisture test device of tobacco thermophysical property measurement, which is adapted to different ermal physics states, can be tobacco alternating temperature Under the conditions of thermophysical property measurement test platform is provided so that temperature and humidity is uniform in test sample, improve tobacco thermophysical property measurement Accuracy and reliability.
The purpose of the present invention is achieved through the following technical solutions:
A kind of constant temperature and moisture test device suitable for tobacco thermophysical property measurement, including sample bin, to provide perseverance outside sample bin The constant temperature water bath system of temperature, the gas circuit constant temperature and humidity system to provide constant temperature and humidity gas in sample bin and data acquisition system System, control system and computer;The constant temperature water bath system includes constant temperature circulating water pump, constant water bath box and respective cycle pipe Road, sample bin are arranged in constant water bath box;The gas circuit constant temperature and humidity system includes constant temperature water tank, is arranged in constant temperature water tank Heating rod, bubble dish, gas mixing chamber and saturated vapor chamber, be respectively equipped on gas mixing chamber and connected with saturated vapor chamber Saturated vapor entrance and the dry air entrance that is connected with over dry air air source, the gas outlet of gas mixing chamber passes through pipeline It is connected with sample bin, heat exchanger is equipped on the dry air air inlet pipeline of gas mixing chamber;The data collecting system includes setting The import and export air-flow Temperature Humidity Sensor on sample bin is put, is accordingly arranged on constant temperature water bath system, gas circuit constant temperature and humidity system In temperature sensor and data collecting card form;The control system includes the dry air being located on dry air air inlet pipeline Flow controller, the saturated vapor flow controller being located on bubble dish air inlet pipeline, for controlling the PID of constant temperature water tank water temperature Temperature controller and relay;The data collecting system and control system are connected with computer.
In the present invention, the quantity of sample bin is two, is arranged in constant water bath box, permanent with gas circuit in sample bin Constant temperature and humidity system connectivity is both provided with import and export air-flow Temperature Humidity Sensor on two sample bins.
The temperature sensing being arranged in constant temperature water bath system, gas circuit constant temperature and humidity system include be located on sample bin into, Exit flow Temperature Humidity Sensor, the temperature sensor being located on constant water bath box, the water tank temperature being located on constant temperature water tank pass Sensor and saturated vapor sensor and gas mixing chamber temperature sensor.
In the present invention, the control mode of control system is controlled using closed loop, i.e., constant temperature water tank uses PID Self-tuning Systems Constant-temperature control method, by the temperature value that feeds back constant temperature water tank temperature sensor measurement compared with setting value, control relay Whether the break-make and then control heating rod of device work.
Heat preserving and insulating material is coated on each pipeline of the experimental rig.
Using above-mentioned experimental rig carry out sample constant temperature and moisture test method, be by respectively to constant temperature water tank water temperature, Gas flow temperature, humidity and flow parameter in water bath water temperature, mixing chamber control effectively so that water bath water temperature and into The mixed airflow humiture for entering sample bin keeps constant value, so as to ensure the tobacco sample in sample bin itself moisture content and temperature It keeps constant, improves the accuracy of tobacco thermophysical property measurement.
Tobacco thermophysical property measurement constant temperature and moisture test device using the above structure, feature are:
1) constant temperature circulating water pump has heating and temperature controlling function, and the pipeline being connect with water bath is cladded with thermal insulation material, a constant temperature The water of degree establishes closed circulation by constant temperature circulating water pump, ensures that sample bin surrounding maintains the temperature of setting, temperature adjusts model It is 0~100 DEG C to enclose, temperature temperature-controlled precision ± 0.2 DEG C.
2) bubble dish generates bubble and reaches constant temperature water tank top into saturated vapor, and saturated vapor is pressed with heated dry air Setting ratio is sufficiently mixed, and mixed proportion is in the range of 0~100%, humid control precision ± 0.5%.
3) mixed gas of certain humiture is constantly passed through in sample bin, after a certain period of time, tobacco sample in sample bin Dynamic equilibrium is desorbed in water adsorption, at this point, tobacco sample has uniform temperature and humidity, reaches tobacco thermophysical property measurement Condition.
Advantages of the present invention is as follows:In temperature control aspect, heating water bath is carried out to sample bin using constant temperature circulating water pump, And be aided with and carry out heated at constant temperature to being passed through sample bin mixed gas, accurate temperature controlling, temperature control range 0~100 can be carried out to sample bin DEG C, temperature-controlled precision ± 0.2 DEG C;In terms of humid control, tobacco sample is passed through using saturated vapor and the mixing of dry air arbitrary proportion, The mode that tobacco sample is in adsorption/desorption dynamic equilibrium is made to keep constant sample moisture content, avoids moisture during alternating temperature The influence to tobacco thermophysical property measurement is migrated, controls wet range 0~100%, adjustable range is wide, controls wet precision ± 0.5%.
Description of the drawings
Fig. 1 is the constant temperature and moisture test apparatus structure schematic diagram for tobacco thermophysical property measurement of the present invention.
In Fig. 1:1- constant temperature water tanks, 1.1- constant temperature water tank temperature sensors;1.2- mixing chamber temperature sensors, 1.3- saturations Steam temperature sensor;2- water baths, 2.1- water bath temperature sensors;3- sample bins;3.1- sample bin inlet air flows are warm and humid Spend sensor;3.2- sample bin exit flow Temperature Humidity Sensors;4- saturated vapor chambers, 5- mixing chambers;6- heat exchangers;It is 7.1- full With steam flow controller;7.2- dry air flow controllers;8- heating rods;9- bubble dishes;10-PID temperature controllers;11- relays Device;12- data collecting cards;13- constant temperature circulating water pumps;14- serial servers;15- computers.
In Fig. 1:1.1- constant temperature water tank;1.2- water bath;2- sample bins;2.1- sample bin inlet air flow temperature and humidity sensings Device;2.2- sample bin exit flow Temperature Humidity Sensors;3- bath temperature sensors;4.1- water tank temperature sensors;It is 4.2- mixed Close chamber temperature sensor, 4.3- saturated-steam temperature sensors;5- mixing chambers;6- heat exchangers;7.1- saturated vapors flow controls Device;7.2- dry air flow controllers;8- heating rods;9- bubble dishes;10-PID temperature controllers;11- relays;12- data acquire Card;13- constant temperature circulating water pumps;14- serial servers;15- computers.
Specific embodiment
The present invention is described further below in conjunction with attached drawing:
As shown in Figure 1:A kind of constant temperature and moisture test device for tobacco thermophysical property measurement, including sample bin 3, for outside sample bin Portion provides the constant temperature water bath system of constant temperature, the gas circuit constant temperature and humidity system to provide constant temperature and humidity gas in sample bin and number According to acquisition system, control system and computer;The constant temperature water bath system include constant temperature circulating water pump 12, constant water bath box 2 and Respective cycle pipeline, sample bin 3 are arranged in constant water bath box 2;The gas circuit constant temperature and humidity system includes constant temperature water tank 1, if Heating rod 7, bubble dish 8, gas mixing chamber 5 and saturated vapor chamber 4 in constant temperature water tank are put, is distinguished on gas mixing chamber 5 It is mixed equipped with the saturated vapor entrance connected with saturated vapor chamber 4 and the dry air entrance connected with over dry air air source, gas The gas outlet for closing chamber 4 is connected by pipeline with sample bin 3, and heat exchanger is equipped on the dry air air inlet pipeline of gas mixing chamber 4 6;The data collecting system includes the import and export air-flow Temperature Humidity Sensor 3.1,3.2 being arranged on sample bin 3, accordingly sets The temperature sensor and data collecting card 12 put in constant temperature water bath system, gas circuit constant temperature and humidity system are formed;The control System includes the dry air flow controller 7.2 being located on dry air air inlet pipeline, the saturation being located on bubble dish air inlet pipeline Steam flow controller 7.1, for controlling the PID temperature controllers 10 of 1 water temperature of constant temperature water tank and relay 11;The data acquisition system System and control system are connected with computer 15.
In the present invention, the quantity of sample bin 3 is two, is arranged in constant water bath box 2, in sample bin and gas circuit Constant temperature and humidity system connects, and import and export air-flow Temperature Humidity Sensor 3.1,3.2 is both provided on two sample bins.
The temperature sensing being arranged in constant temperature water bath system, gas circuit constant temperature and humidity system include be located on sample bin into, Exit flow Temperature Humidity Sensor 3.1,3.2, the temperature sensor 2.1 being located on constant water bath box, is located on constant temperature water tank Water tank temperature sensor 1.1 and saturated-steam temperature sensor 1.3 and gas mixing chamber temperature sensor 1.2.
Specific works step and control process are as follows:
As shown in Figure 1, the constant water to set temperature is sent into water bath 2 by constant temperature circulating water pump 13, to keep sample bin 3 four Zhou Hengwen, while detect whether water temperature in water bath 2 reaches setting value by bath temperature sensor 2.1;Added by heating rod 8 Water in hot constant temperature water tank 1, while wherein water temperature is measured, and temperature data is sent into PID temperature controls by water tank temperature sensor 1.1 Instrument 10 is compared with setting value, is controlled whether heating rod 8 heats by relay 11 according to comparing result, is made constant temperature water tank 1 Middle water temperature is kept constant;Compressed air require is controlled by saturated vapor flow controller 7.1 all the way, is led to through respective line Enter bubble dish 9 and generate micro-bubble in water, so as to generate the saturated vapor under the water temperature condition, saturated-steam temperature is by saturation Steam temperature sensor 4.3 is detected, and saturated vapor is subsequently entered in mixing chamber 5;Dry air flow is by dry air flow control Device 7.2 processed controls, and dry air enters heat exchanger 6 through respective line and carries out heat exchange with water in constant temperature water tank 1.1, makes its temperature It is heated to identical with water temperature, subsequently enters the wet sky for being mixed into certain humiture in mixing chamber 5 by setting ratio with saturated vapor Gas, humid air temperature is detected by mixing chamber temperature sensor 1.2 in mixing chamber;Saturated vapor and compressed air are after mixing The gaseous mixture of formation enters through respective line in sample bin 3, and 3 inlet air flow temperature of sample bin is by sample bin inlet air flow humiture Sensor 3.1 is detected, and 3 exit flow temperature of sample bin is measured by sample bin exit flow Temperature Humidity Sensor 3.2.
By being carried out respectively to parameters such as constant temperature water tank water temperature, water bath water temperature, mixed airflow temperature, humidity and flows Effectively control so that water bath water temperature and the mixed airflow humiture into sample keep constant value, so as to ensure tobacco sample Itself moisture content is kept constant with temperature, improves the accuracy of tobacco thermophysical property measurement.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe The personage for knowing this technology all can carry out modifications and changes under the spirit and scope without prejudice to the present invention to above-described embodiment.Cause This, those of ordinary skill in the art is complete without departing from disclosed spirit and institute under technological thought such as Into all equivalent modifications or change, should by the present invention claim be covered.

Claims (6)

1. a kind of constant temperature and moisture test device suitable for tobacco thermophysical property measurement, it is characterised in that:Including sample bin, be sample There is provided outside storehouse the constant temperature water bath system of constant temperature, the gas circuit constant temperature and humidity system to provide constant temperature and humidity gas in sample bin, with And data collecting system, control system and computer;The constant temperature water bath system include constant temperature circulating water pump, constant water bath box and Respective cycle pipeline, sample bin are arranged in constant water bath box;The gas circuit constant temperature and humidity system includes constant temperature water tank, is arranged on Heating rod, bubble dish, gas mixing chamber and saturated vapor chamber in constant temperature water tank, are respectively equipped on gas mixing chamber and saturation The saturated vapor entrance of vapor chamber connection and the dry air entrance connected with over dry air air source, the outlet of gas mixing chamber Mouth is connected by pipeline with sample bin, and heat exchanger is equipped on the dry air air inlet pipeline of gas mixing chamber;The data acquisition System includes the import and export air-flow Temperature Humidity Sensor being arranged on sample bin, and it is permanent to be accordingly arranged on constant temperature water bath system, gas circuit Temperature sensor and data collecting card in constant temperature and humidity system are formed;The control system includes being located at dry air air inlet pipeline On dry air flow controller, the saturated vapor flow controller being located on bubble dish air inlet pipeline, for controlling thermostatted water The PID temperature controllers and relay of case water temperature;The data collecting system and control system are connected with computer.
2. the constant temperature and moisture test device according to claim 1 suitable for tobacco thermophysical property measurement, it is characterised in that:Sample The quantity in product storehouse is two, is arranged in constant water bath box, is connected in sample bin with gas circuit constant temperature and humidity system, in difference Import and export air-flow Temperature Humidity Sensor is both provided on product storehouse.
3. the constant temperature and moisture test device according to claim 1 suitable for tobacco thermophysical property measurement, it is characterised in that:If It puts the temperature sensing in constant temperature water bath system, gas circuit constant temperature and humidity system and includes the import and export air-flow temperature being located on sample bin Humidity sensor, the temperature sensor being located on constant water bath box, the water tank temperature sensor being located on constant temperature water tank and full With vapor sensor and gas mixing chamber temperature sensor.
4. the constant temperature and moisture test device according to claim 1 suitable for tobacco thermophysical property measurement, it is characterised in that:It should Heat preserving and insulating material is coated on each pipeline of experimental rig.
5. the constant temperature and moisture test device according to claim 1 suitable for tobacco thermophysical property measurement, it is characterised in that:Institute State temperature control ranging from 0-100 DEG C of the constant water bath box to sample bin.
6. a kind of method for the constant temperature and moisture test that tobacco thermophysical property measurement is carried out using claim 1 described device, feature It is:By respectively to gas flow temperature, humidity and the flow parameter in constant temperature water tank water temperature, water bath water temperature, mixing chamber into Row effectively control so that water bath water temperature and the mixed airflow humiture into sample bin keep constant value, so as to ensure sample Tobacco sample itself moisture content in storehouse is kept constant with temperature, improves the accuracy of tobacco thermophysical property measurement.
CN201810023550.3A 2018-01-10 2018-01-10 A kind of constant temperature and moisture test device and method suitable for tobacco thermophysical property measurement Pending CN108181958A (en)

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CN201810023550.3A CN108181958A (en) 2018-01-10 2018-01-10 A kind of constant temperature and moisture test device and method suitable for tobacco thermophysical property measurement

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CN201810023550.3A CN108181958A (en) 2018-01-10 2018-01-10 A kind of constant temperature and moisture test device and method suitable for tobacco thermophysical property measurement

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111399568A (en) * 2020-02-29 2020-07-10 天津大学 Multi-closed-loop temperature and humidity control system for mechanical testing of micro-cavity environment
CN113966855A (en) * 2021-11-24 2022-01-25 河南中烟工业有限责任公司 Co-heating type tobacco sample preparation device with fixed moisture content and preparation method

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111399568A (en) * 2020-02-29 2020-07-10 天津大学 Multi-closed-loop temperature and humidity control system for mechanical testing of micro-cavity environment
CN111399568B (en) * 2020-02-29 2024-03-29 天津大学 Multi-closed-loop temperature and humidity control system for mechanical testing of micro-cavity environment
CN113966855A (en) * 2021-11-24 2022-01-25 河南中烟工业有限责任公司 Co-heating type tobacco sample preparation device with fixed moisture content and preparation method

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Application publication date: 20180619